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Abstract
A new design for a diverter and weighing tank system has been developed. Experiments have been carried out on a prototype. Diverter wings
are set as partitions along the diameter of a half-cylinder tube. The rotation axis is at the center of the half cylinder and runs parallel to liquid jets
flowing vertically downward from several independent nozzles. This design contributes to small diverter timing error, compact design, small wet
area, a simple and robust mechanism, easy implementation of the ISO4185 test, and easy adjustment of diverter trigger timing. After adjustment
of start and stop signal timings, the estimated standard uncertainty caused by diverter timing error is reduced within a negligible small value
(0.0019% or less) over a wide range of flow rates at any nozzle position. The weighing tank system has been improved by some refined devices.
A single movement of the weighing platform can prevent escaping vapor, enable connection of an air tube, provide protection against impact, and
provide a fail-safe against overflow. It is confirmed that the liquid flow calibration facility using the present system achieves accurate measurement,
easy operation, wide flow range, high throughput, low cost, small weighing tank, easy maintenance, and safety.
c 2006 Elsevier Ltd. All rights reserved.
Keywords: Diverter; Weighing tank system; Double wing; Liquid flowmeter; Calibration
maximum flow rate, because the contribution of the diverter to be negligibly small. Some demonstrations have been carried
timing error increases as the collection time decreases. out on the prototype in order to confirm that the new system has
ISO4185 [8] recommends adjustment of the trigger timing the features demanded.
on the basis of the diverter error time obtained from estimation
tests. In the traditional diverter, the correct timing exists at only 2. Development of rotating double-wing diverter
one symmetric point against a liquid jet velocity profile [9,10].
Confirmation and adjustment of the error should be performed 2.1. Diverter timing error
under all calibration conditions, because the liquid jet velocity
profile is dependent on the flow rate and the shape of the nozzle. On the basis of the static gravimetric method, the standard
However, estimating the error under all calibration conditions is mass flow rate q is given by Eq. (1).
very difficult, resulting in significant uncertainty derived from m1 − m0
the diverter timing error. q= (1)
tC (1 − ρA /ρW )
Traditionally, several techniques for reducing the diverter tC = tTRUE − t. (2)
error have commonly been used. A larger collection tank
has been adopted to obtain a longer collection time. Trigger Here, m 0 is initial weight, m 1 is weight after collection, ρ A
actuation has been set to be as symmetric as possible. The and ρ L denote the density of air and liquid, respectively, and tC
diverting wing has been made to move at high speed to reduce is the time interval between the starting and stopping signals.
the transit time of the liquid jet, resulting in smaller diverter The diversion causes a timing error in the measurement of
timing error. However, splashes can occur when the speed is collection time. The collection time tC may include the diverter
too fast. timing error t. This timing error influences the calibration
Various new attempts have been made to reduce this error. results systematically, and cannot be reduced by repeating
At PTB, the nozzle and the feeding pipe have been specially calibration. The diverter system is thus a key component in
designed by computational fluid dynmics (CFD) simulations achieving a highly accurate liquid flow rate standard.
to achieve a symmetrical velocity profile at the liquid jet [11]. Fig. 1 shows typical time profiles of the flow rate directed
Furthermore, a new method for estimating timing error by using to the weighing tank. Ideally, the diverter should change the
an angular encoder and storage device was proposed to enable flow direction in a moment of time. But that is impossible
easy adjustment of the trigger position [12]. in practice. Some descriptions of the flow rate, qIN , into the
Recently, NMIJ developed a double-wing diverter [13] weighing tank are shown in the transient flow rate profiles in
and succeeded in minimizing the timing error. A similar Fig. 1. The tTRUE value is the time equivalent to the collection
unidirectional motion diverter was also designed by NIST time assuming the diverter is ideal. In the case of a conventional
[14,15]. This new system has two diverter wings which, at single-wing diverter (SW Diverter), the ideal trigger timing
the start and end of measurement, are made to move in the may move when the velocity profile of a liquid jet, which is
same direction at a constant speed across the liquid jet. After discharged from the nozzle, changes. Using this diverter, the
appropriate adjustment, the double-wing diverter maintains a flow rate profile becomes symmetric, as shown in Fig. 1(a)
small diverter timing error for any given flow rate and any because the single wing moves across the path of the liquid
given nozzle condition. This system is already used in the jet in opposite directions at the start and end of measurement.
primary standard facility for NMIJ [6]. Uncertainty analysis Thus the collection time should be measured at an exact timing
has confirmed that the contribution of the adjusted diverter condition (S1 = S2 and S3 = S4) in order to obtain the ideal
timing error is negligible compared with other sources of error collection time tTRUE [9,10]. If the trigger timing does not
[16]. However, the double-wing diverter has a problem in the satisfy the exact condition, the timing should be adjusted to the
implementation of the estimation test under ISO4185. Details exact timing, which exists at only one point. When the flow rate
of the problem and its solutions are discussed in the subsequent profile changes because of a different flow rate or a different
sections. nozzle width, the true timing tTRUE can be of different period,
In the near future, NMIJ plans to extend the facility’s range such as in Fig. 1(b). In the case of Fig. 1(b), the collection time
to smaller flow rates by providing another calibration line. tC contains the diverter timing error t, because the timing
Therefore, the authors have developed an improved double- described by the dotted line does not satisfy the condition
wing diverter and an advanced weighing tank system to resolve (S1 = S2 and S3 = S4). Commonly, it is said that the timing
the problems mentioned above in the construction of the small error should be less than 10 ms at a condition of maximum flow
test line. The new design of this system aims to satisfy several rate. Otherwise, the collection time needs to be longer than 100
demands: accurate measurement, easy operation, a wide range s to make the contribution of the timing error to the calibration
of flow rate, high throughput, low cost, a small weighing tank, uncertainty less than 0.01%. Therefore, a diverter system needs
easy maintenance, and safety. a large weighing tank or it limits its maximum flow rate.
In the present paper, the design of the diverter and weighing In view of this problem, the double-wing diverter (DW
tank systems is proposed. The diverter timing error was Diverter) was developed by Shimada et al. [13,17]. The new
estimated using a small prototype in a water flow circuit in order system has two diverter wings which, at the start and end of
to compare the features of the new diverter system with the measurement, are made to move in the same direction at a
previous system, and to confirm that the error time was reduced constant speed across the liquid jet, as shown in Fig. 2. In
R. Doihara et al. / Flow Measurement and Instrumentation 17 (2006) 141–152 143
flow rates, as long as the profile remains stable from the start
to the end of the diversion. The value of diverter timing is a
function of the difference between the distance of the wings
L wing and the distance of the sensors L sensors when the moving
speed is constant. The condition (S1 = S3 and S2 = S4,
thus tC = tTRUE ) can exist for any timing as long as L wing =
L sensors, and the moving speed is constant. See the reference
article [17] for the detailed theory of the double wing method.
The condition (S1 = S3 and S2 = S4) is maintained at any flow
rate profile after adjustment. Therefore, once the diverter has
been adjusted appropriately, adjustment of the trigger timing
is unnecessary for any given flow rate and any given nozzle
position.
However, the double-wing diverter described above has
practical difficulties in the implementation of the ISO4185 test,
because the two wings are moved in the same direction.
in many calibration facilities for large flow rates, the duration can drop directly into the weighing tank. The diverter is rotated
is insufficient because of economical or physical limitations. by a servo motor via a center shaft linked to a timing belt. Two
In many calibration facilities, the error caused by the diverter photosensors and a disk with a slit are used as a trigger signal
has often been the main source of uncertainty. This error also generator for starting and stopping the timer, and these are set
constitutes one reason to limit the maximum flow rate with at the top of the rotating shaft.
reference to the volume of the weighing tank. Before collection, the half cylinder is set in the bypass
Even if a diverter is designed on the principle of the double- position to locate the bypass side under the nozzle. In this paper,
wing method, some tests for estimating diverter timing error this angular position is defined as 0◦ . To start collection, the
must be conducted for adjustment of the timing. In the previous cylinder is rotated 180◦ (to the collection position). On the way
DW diverter shown in Fig. 2, the end position is different from to the collection position, at 90◦ , one of the diverter wings cuts
the start position because the wings travel linearly in the same the liquid jet. At that moment, one of the photosensors detects
direction. When the wings must return to the start position the slit of the disk and sends the start trigger signal to the
for the next diversion, the liquid jet drops into the weighing timer. While the cylinder is in the collection position, the liquid
tank because the wings pass under the liquid jet. In the test jet falls into the weighing tank. When the tank has filled, the
under ISO4185, this mechanism leads to a problem in practical cylinder again rotates 180◦ in the same direction (to 360◦ ) in
operation. order to stop collection. The other diverter wing cuts the liquid
There are some solutions to prevent this unnecessary inflow. jet at 270◦, and the other photosensor sends the stop trigger
One method is to install an additional diverter at the duct signal to the timer. The sensors are fixed on a precision traverse
between the main diverter and the weighing tank. But some stage so that the sensor position can be adjusted on the basis of
liquid that is not intended to drop into the weighing tank the estimated diverter timing error.
may fall and wet the wall of the collection side. This error In contrast to the previous diverter, the new design offers
mechanism can become large in the case of a small oil facility, many advantages: the wet area can be minimized; the diverter
because the wet liquid on the wall becomes significant relative wings do not have to return, because the end position is the
to the small resolution of the weighing scale. A large wet same as the start position; the wet area of the collection side
area also lengthens the waiting time for the liquid to run is completely separated from the bypass side; the ISO4185
down completely. In the case of oil, the wet area should be test can be run consecutively without any waiting time; usual
made as small as possible, since the waiting time is apt to calibration can be carried out accurately; and the mechanism of
increase drastically because of high viscosity. Determining a this rotating motion is simple and robust. However, tests should
method for checking for leaks presents another problem. Using be carried out in order to confirm that the rotating motion of the
this additional device only for the estimation test will reduce diverter poses no problem.
accuracy in usual calibration; in addition, ISO4185 tests are
seldom carried out. 3. Improvement of weighing tank system
Another method is to set a plastic bag between the diverter
wings in order to prevent the unnecessary inflow. However, this In many cases, weighing tank systems have an open section
involves setting the bag by hand at each diversion. In an oil at the inlet, through which vapor might escape from the
facility, especially, this operation is terribly hard and unsafe. collected mass. A weighing tank is often linked by electric
wires to detect the liquid level, and by air tubes to actuate the
2.3. Design of the rotating double-wing diverter drain valve. These can be sources of error. Especially in the case
of a weighing tank with a small scale, even if the tension caused
Using a new design, we have achieved small diverter timing by those connections is small, these errors could exert a greater
error, compact design, small wet area, a simple and robust influence on measurement than the resolution of the scale.
mechanism, easy implementation of an ISO4185 test, and easy The weighing tank that we have used includes devices to
adjustment of diverter trigger timing. This diverter system is measure the mass of collected liquid accurately. The weighing
based on the concept of symmetric diversion by two wings that tank in the present system has no open section from which
move across the liquid jet in the same direction at constant vapor and mist can escape into the atmosphere, except for
speed at both the start and end of measurement. In the present a short time during weight measurement. Fig. 4 shows the
design, the wings are rotated, whereas in the previous double- sequence of operation of the weighing system. The weighing
wing method they are moved linearly. tank is placed on a lift-platform which is elevated by air
Fig. 3 illustrates the design of the diverter with two rotating actuators. The tank is lifted from the scale and pushed in tightly
wings. The diverter wings are set as partitions along the against the bottom of the diverter box, in order to protect
diameter of a half-cylinder tube. The axis of rotation is at the the scale against sudden impact by the jet and to prevent the
center of the cylinder and runs parallel to the liquid jets that flow escape of vapor. Although the air inside the tank flows from the
vertically downward. One side of the diverter has a rectification weighing tank to the diverter box as the tank is filled with liquid,
surface that resembles a half cone with a closed bottom (Bypass the air inside the box has already been saturated with mist or
side). When this side comes under the nozzle, the liquid flow vapor. Therefore, diffusion and evaporation hardly progress.
is led into a bypass line. The other side (Collection side) is a Even in the event of unexpected overflow due to malfunction
semicircle shape with an open bottom, such that the liquid jet of the diverter, the liquid will flow to the bypass line through
R. Doihara et al. / Flow Measurement and Instrumentation 17 (2006) 141–152 145
the diverter box. This tight sealing at the inlet functions as a after a sufficient interval after the time the float passes by the
fail-safe mechanism. sensor.
The weighing tank is placed on the scale in a completely The system also features automatic connection of an air tube
free state during weighing, because no electric wires or air for the drain valve. When the tank is pushed up, the connection
tubes are connected to the weighing tank. In order to avoid any
is established, allowing the valve to be operated by the air
mechanical connection to the tank, the liquid level is detected
signal. When the tank is placed on the scale, the connection is
by optical sensors and a float inside a transparent tube. The
completely separated. These devices are especially adaptable
automatic operating system can discriminate the liquid level of
the weighing tank by detecting the float with the optical sensor. and useful in a hydrocarbon flow facility. In such a facility,
When the optical sensor that is set at the desired full level mark oil vapor ejection to the atmosphere is unfavorable in view of
detects the float, the diverter is rotated. If an optical sensor measurement accuracy and the environment of the room. The
set at the very top of the tank detects the float, the system is air connection is safe in a hazardous area. Of course, in the case
immediately shut down to ensure safety in an emergency. An of an oil facility, the necessary ground wire to be connected
optical sensor set at the lowest position closes the drain valve must be as flexible as possible.
146 R. Doihara et al. / Flow Measurement and Instrumentation 17 (2006) 141–152
Table 1
Average of the diverter timing error t and its standard deviation σt
The standard deviation σt was 0.4 ms. These values are
summarized in Table 1.
The results of the single wing method suggest that the
diverter timing error is somewhat dependent on flow rate. The
flow rate dependency of the timing error was 1.5 ms at the
maximum difference among averaged values on each flow rate.
This value was less than the value that was expected. But it
Fig. 7. Estimated diverter timing error before and after adjustment for single
and double wings. depends on the liquid jet condition, which is namely the nozzle
ability. This value might be small, because the nozzles consist
investigate the influence of the flow rate profile and the nozzle of a plural number of circular pipes that have relatively small
position, two nozzle positions were tested: a straight position diameter. The important point is that the DW diverter has no
(A) and an oblique position (B), as shown in Fig. 6. In practical flow rate dependency, although the SW diverter can be affected
calibration, the valves of the larger nozzles are closed as the by flow rate. Especially in the case of this multi-nozzle system,
flow rate becomes small. In these experiments, all four valves a combination of open nozzles will change to keep the flow
were always open. velocity high. The center position of the liquid jet is easily
The results of the estimation test of the diverter timing moved, because these nozzles are not set exactly aligned along
error are shown in Fig. 7. Nozzle position A was used in this the straight line. Therefore, we discuss how the RDW diverter
experiment. First, the photosensor for the start signal was set is able to maintain the smallest diverter timing error versus
at 90◦ . The diverter timing error was measured using only one different liquid jet conditions.
wing in order to simulate a single-wing diverter. The averaged
diverter timing error for the single wing was about 7.5 ms, 5.1.2. Performance at different nozzle positions
because the nozzles are not set exactly aligned with the 90◦ Diverted flow rates were measured versus the angle of the
line (Fig. 6). Second, from the time of error and the angular diverter wing as follows. The diverter wing enters the region
velocity of the wing, the adjustment angle of the photosensor of the liquid jet and is stopped at an arbitrary angle. During
was calculated, corresponding to −1.4◦. After the photosensor a constant time (30 s), a portion of the liquid jet flows into
position was adjusted to near 88.6◦, the estimation tests were the weighing tank. The flow rates are then calculated from the
again carried out using the single-wing method. Next, with the weight of liquid and the time. The angles are set from 80◦ to
position of the photosensor maintained near 88.6◦, the other 130◦ in increments of 0.5◦ .
photosensor was set at 270◦. Then the diverter timing error Fig. 8 shows the measurement result of the diverted flow rate
was measured by the double-wing method. The average error (1500 kg/h) versus diverter wing angle. The flow rate pattern
time and correction angle for the double wing were −2.1 ms for position A is relatively symmetric. The pattern for position
and −0.8◦ , respectively. Finally, after the other sensor position B, however, is quite bumpy and asymmetric. In the case of
was adjusted to 269.2◦, estimation of the timing error was the single-wing diverter, the diverter timing error theoretically
again carried out with two wings. After adjustment of the becomes zero [9,10] under the conditions of S1 = S2 and S3 =
sensors, the diverter timing error fell within 1 ms for the double- S4, as illustrated in Fig. 8. The angle that satisfies S1 = S2
wing method regardless of flow rate. The averaged value of was calculated from the flow rate data under the premise that
the diverter timing error after adjustment t was −0.1 ms. the velocity of rotation is constant. The calculated angle for the
148 R. Doihara et al. / Flow Measurement and Instrumentation 17 (2006) 141–152
Fig. 8. Diverted flow rate versus position of the diverter wing. Fig. 10. Adjustment of diverter timing error cased by wing with reduced
splashing.
position A is 88.8◦, which is close to the adjusted angle in the 5.3. Demonstration of rapid calibration
single-wing method. The angle for position B was 95.6◦.
As a result of calibration, we can obtain the K -factor of
Fig. 9 shows the results for position B. The averaged value
a flowmeter under calibration. If the diverter timing error is
of the double-wing method was −0.4 ms. The RDW diverter
insufficiently small compared with the collection time, the
has succeeded in keeping small timing error. Although the jet
K -factor is greatly affected as the collection time decreases. In
condition was changed remarkably, the results confirm that,
a calibration facility using a flying start and stop method, the
in the case of the double-wing method, the diverter timing
K -factor is calculated from the pulse frequency of the
error is not dependent on the flow profile. A conspicuous
flowmeter and the measured standard mass flow rate:
difference from the single-wing method is observed. The value
of the diverter timing error at 1500 kg/h is −39.8 ms, which fp
K = (4)
corresponds to an angle of 95.8◦ for the sensor position. q
Obtaining such close values using different methods indicates where K is the K -factor, and f p is the pulse frequency of the
the high reliability of these experiments. flowmeter. The affected K -factor resulting from the diverter
According to these experiments, it is confirmed that timing error is derived from Eqs. (1), (2) and (4):
the rotation motion of the double-wing and multi-nozzle
fp (1 − ρA /ρW )
system does not cause problems with calibration. Therefore KD = = fp (tTRUE − t)
these systems have the following advantages: they can q m1 − m0
maintain accuracy using the double-wing method, allow t ∼ t
= K TRUE 1 − = TRUE
K 1 −
easy implementation of ISO4185 test, operate with a simple tTRUE tC
mechanism at low cost, and prevent the persistence of bubbles. (5)
R. Doihara et al. / Flow Measurement and Instrumentation 17 (2006) 141–152 149
Based on Eqs. (7), (8) and (14), the relative combined standard
uncertainty in collection time is obtained in Eq. (15):
u(tC )
tC
2
2
1 × 10−6 2 2 1.9 × 10−4
= + 1.3 × 10−5 + 1.0 × 10−5 +
tC tC
3.6 × 10−8
= 2.6 × 10−10 + . (15)
tC2
When the collection time tC is quite short, for instance 10 s, where K V is the affected K -factor of the test meter, and qV
the contribution of diverter timing error becomes just 0.0019% is the evaporation flow rate. When qV << q, Eq. (17) is
at any nozzle condition, which is a comparable value to the approximated as Eq. (18):
uncertainty in the timer itself (0.0016%). Normally, the diverter
timing error is negligible in the case of the double-wing diverter fp 1 qV
KV = · ≈ K TRUE 1 + . (18)
combined with a multi-nozzle system. Therefore, the RDW q (1 − qV /q) q
diverter enables calibration at very high flow rates relative to
Thus the calibrated K -factor increases with increasing
the weighing tank capacity.
evaporation flow rate qV . It is obvious that the effect is
larger at low flow rates from the proportionality coefficient of
5.4. Effect of the lift-up closure mechanism of the tank lid
1/q. In order to evaluate the evaporation effect, calibrations
In order to investigate the effectiveness of the lift-up at low flow rates (20 kg/h) were carried out for the three
mechanism which seals the inlet of the weighing tank, the conditions described in the previous section. The test meter was
weight is measured after the weighing tank is filled. Three replaced by the small-size Coriolis flowmeter (max flow rate:
conditions are examined. The first condition is with the tank 83 kg/h). Only one nozzle (4 mm) was used to maintain the
raised and tightly sealed. The second condition is with the walls flow velocity of the liquid jet. In Fig. 13, the K -factors are
of the diverter box removed to allow vapor to diffuse through plotted assuming that the evaporation flow rates were the same
the collection side duct of the diverter. The third condition is as the results of Section 5.4. As predicted by Eq. (18), the K -
with the tank lowered to allow vapor to escape from the inlet of factor is overestimated for the condition in which the tank was
the tank into the atmosphere directly. in the lowered position. The least squares fit indicates that the
Fig. 12 shows the weight loss from the filled weighing tank unaffected K -factor should be 1000.6 P/kg. This result is close
with time. In the third condition, in which the inlet remained to the K -factor for the condition in which the tank is raised and
open, the collected mass was lost at a rate of about 0.13 g/min sealed tightly. Therefore, it is confirmed that the tight sealing
because of the evaporation and diffusion of vapor. In the second tank system effectively functions at a low flow rate.
condition, the loss rate became relatively small, because the The standard uncertainty in the contribution from liquid
duct out of which the vapor could diffuse was narrow compared vapor escape (m) is estimated as below:
with the third condition. The first condition demonstrates that m1 − m0
the tight seal of the weighing tank and the closed diverter box m = qV · tC = qV · (19)
q
succeeded in preventing evaporation loss. Therefore, even if the u(m) u(qV )
weighing tank is filled at a low flow rate, thereby requiring a ≈ . (20)
m1 − m0 q
long time, the evaporation effect will be negligible, as long as
the lift platform is in the raised position. Assuming that the evaporation flow rate qV is 0.004 g/min
from the data of Fig. 12, the relative standard uncertainty
5.5. Test calibration at low flow rate caused by evaporation is given as
In this section, the effect of evaporation on the calibration u(qV ) 0.004 3.8 × 10−8
= √ = . (21)
factor is discussed. A calibrated K -factor of the test meter is q 60 × 1000 × 3 × q q
affected by the flow rate of evaporation: Even at long calibration time (over one hour), the standard
fp uncertainty in evaporation is reduced to 0.0007% by using this
KV = (17) lift-up closure mechanism. If the tank is in the lowered position,
q − qV
R. Doihara et al. / Flow Measurement and Instrumentation 17 (2006) 141–152 151
6. Conclusions
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