102L Spring 2021

16.2 Raw data unk trial

1
2
OBSERVATIONS 3
white crystal powder
not difficult to dissolve T1 burette (mL) titrant added delta v
0.7 0.0
1.1 0.4 0.4
1.5 0.8 0.4
2.0 1.3 0.5
2.1 1.4 0.1
2.3 1.6 0.2
2.4 1.7 0.1
unknown: EN08I 2.5 1.8 0.1
2.6 1.9 0.1
2.8 2.1 0.2
2.9 2.2 0.1
3.1 2.4 0.2
3.4 2.7 0.3
3.5 2.8 0.1
3.7 3.0 0.2
4.0 3.3 0.3
4.3 3.6 0.3
4.7 4.0 0.4
5.2 4.5 0.5
5.7 5.0 0.5
5.9 5.2 0.2
6.3 5.6 0.4
6.4 5.7 0.1
6.5 5.8 0.1
6.6 5.9 0.1
7.0 6.3 0.4
7.3 6.6 0.3
7.4 6.7 0.1
7.6 6.9 0.2
7.8 7.1 0.2
7.9 7.2 0.1
8.0 7.3 0.1
8.4 7.7 0.4
8.6 7.9 0.2
8.8 8.1 0.2
9.0 8.3 0.2
9.5 8.8 0.5
initial mass final mass
14.354 14.192
14.192 14.045
14.045 13.854

T1 pH delta pH T2 burette (mL) titrant added delta v T2 pH

3.98 0.0 0.0 3.94
4.11 0.13 0.5 0.5 0.5 4.16
4.22 0.11 1.0 1.0 0.5 4.34
4.46 0.24 1.5 1.5 0.5 4.52
4.51 0.05 2.2 2.2 0.7 4.73
4.54 0.03 3.0 3.0 0.8 4.92
4.57 0.03 3.2 3.2 0.2 4.98
4.61 0.04 3.5 3.5 0.3 5.06
4.65 0.04 4.0 4.0 0.5 5.16
4.68 0.03 4.5 4.5 0.5 5.28
4.73 0.05 5.0 5.0 0.5 5.41
4.79 0.06 5.5 5.5 0.5 5.56
4.82 0.03 6.0 6.0 0.5 5.79
4.85 0.03 6.5 6.5 0.5 6.00
4.90 0.05 7.0 7.0 0.5 6.43
4.95 0.05 7.2 7.2 0.2 6.76
5.03 0.08 7.5 7.5 0.3 10.10
5.10 0.07 8.0 8.0 0.5 10.77
5.22 0.12 8.5 8.5 0.5 11.01
5.37 0.15
5.40 0.03
5.53 0.13
5.59 0.06
5.64 0.05
5.67 0.03
5.76 0.09
5.91 0.15
5.95 0.04
6.07 0.12
6.27 0.20
6.46 0.19
6.78 0.32
9.52 2.74
10.41 0.89
10.66 0.25
10.84 0.18
11.06 0.22
delta pH T3 burette (mL) titrant added delta v T3 pH delta pH
8.5 0.0 3.96
0.22 9.0 0.5 0.5 4.17 0.21
0.18 9.5 1.0 0.5 4.34 0.17
0.18 10.0 1.5 0.5 4.48 0.14
0.21 11.0 2.5 1.0 4.71 0.23
0.19 12.0 3.5 1.0 4.93 0.22
0.06 13.0 4.5 1.0 5.10 0.17
0.08 15.0 6.5 2.0 5.49 0.39
0.10 17.0 8.5 2.0 6.34 0.85
0.12 18.0 9.5 1.0 10.67 4.33
0.13 20.0 11.5 2.0 11.43 0.76
0.15
0.23
0.21
0.43
0.33
3.34
0.67
0.24
T1
v of titrant Titrant 1 v of titrant Titrant 2 v of titrant Titrant 3
0.0 0.0 0.0
0.4 0.3 0.5 0.4 0.5 0.42
0.8 0.3 1.0 0.4 1.0 0.34
1.3 0.5 1.5 0.4 1.5 0.28
1.4 0.5 2.2 0.3 2.5 0.23
1.6 0.2 3.0 0.2 3.5 0.22
1.7 0.3 3.2 0.3 4.5 0.17
1.8 0.4 3.5 0.3 6.5 0.195
1.9 0.4 4.0 0.2 8.5 0.425
2.1 0.1 4.5 0.2 9.5 4.33
2.2 0.5 5.0 0.3 11.5 0.38
2.4 0.3 5.5 0.3
2.7 0.1 6.0 0.5
2.8 0.3 6.5 0.4
3.0 0.3 7.0 0.9
3.3 0.2 7.2 1.7
3.6 0.3 7.5 11.1
4.0 0.2 8.0 1.3
4.5 0.2 8.5 0.5
5.0 0.3
5.2 0.2
5.6 0.3
5.7 0.6
5.8 0.5
5.9 0.3
6.3 0.2
6.6 0.5
6.7 0.4
6.9 0.6
7.1 1.0
7.2 1.9
7.3 3.2
7.7 6.9
7.9 4.5
8.1 1.2
8.3 0.9
8.8 0.4
 First Derivative Chart for the Titration Curve
12

10

8
Delta pH/ Delta Volume

0
0.0 2.0 4.0 6.0 8.0 10.0

Volume of Titrant Added

Titrant 1 Titrant 2 Titrant 3

he Titration Curve

8.0 10.0 12.0 14.0

ant Added

2 Titrant 3
102L Spring 2021
16.2 Raw data unk trial initial mass final mass
1 14.162 14
2 14 13.853
OBSERVATIONS 3 13.853 13.667
white crystal powder
easily soluble in water T1 burette (mL) T1 pH T2 burette (mL) T2 pH
0.60 3.97 0.0 3.94
1.00 4.12 0.5 4.16
1.40 4.24 1.0 4.34
1.90 4.48 1.5 4.52
2.00 4.50 2.0 4.70
2.20 4.52 3.0 4.92
2.30 4.56 3.2 4.98
unknown: 05WAJ 2.60 4.68 3.5 5.06
2.80 4.73 4.0 5.16
3.00 4.79 4.5 5.28
3.35 4.82 5.0 5.41
3.55 4.85 6.0 5.79
3.75 4.90 6.5 6.00
4.00 4.95 7.0 6.43
4.30 5.03 7.2 6.76
4.65 5.10 7.5 10.10
5.20 5.24 8.0 10.77
5.70 5.37 8.5 11.01
5.50 5.40
6.25 5.53
6.40 5.59
6.50 5.64
6.55 5.67
7.00 5.76
7.30 5.91
7.35 5.99
7.60 6.07
7.80 6.27
7.85 6.47
8.00 6.77
8.30 9.55
8.45 10.41
8.75 10.66
9.05 10.84
9.70 11.06
T3 burette (mL) T3 pH
0.0 3.96
0.5 4.17
1.0 4.34
1.5 4.48
3.0 4.71
3.0 4.93
4.5 5.10
6.5 5.49
8.5 6.34
9.5 10.67
11.5 11.43
102L Spring 2021
16.2 Raw data unk trial initial mass final mass
1 15.122 14.971
2 14.971 14.82
3 14.82 14.624

T1 burette (mL) T1 pH
OBSERVATIONS 0 6.42
colorless 0.5 6.43
did not require stirring or heat 1 6.44
1.5 6.45
unknown: 09QSO 1.78 6.5
1.98 6.51
2.1 6.53
2.5 6.59
2.81 6.61
3.22 6.69
3.74 6.72
3.99 6.75
4.21 6.8
5.11 6.82
5.74 6.99
6.01 7.01
6.5 7.03
7.5 7.1
8 7.2
8.5 7.31
9.01 7.33
9.1 7.45
9.2 7.52
9.3 7.59
9.4 7.64
9.5 7.78
9.6 7.82
9.8 7.94
10 8.01
10.1 8.12
10.2 8.2
10.3 8.32
10.4 8.7
10.5 9.6
10.6 10.15
 10.8 10.3
11 10.5
11.25 10.73
11.5 10.88
12 10.9
13 10.95
T2 burette (mL) T2 pH T3 burette (mL) T3 pH
0 6.43 0 6.41
1 6.44 1.6 6.53
2 6.52 2.5 6.6
3 6.68 3.4 6.7
3.7 6.71 5 6.8
4 6.79 6 6.9
4.5 6.81 7 7.01
5 6.81 8 7.1
5.5 6.87 9 7.2
5.8 6.88 9.5 7.23
6.2 7.01 10 7.32
7 7.08 10.5 7.44
7.8 7.12 10.7 7.5
8 7.21 11 7.52
8.1 7.23 11.3 7.62
8.3 7.25 11.5 7.78
9 7.35 12 8.3
9.4 7.67 12.2 8.45
9.7 7.83 12.3 8.61
9.8 7.96 12.5 9.52
9.9 7.99 12.8 10.3
10 8.02 13 11
10.1 8.1 13.5 11.5
10.2 8.15
10.25 8.23
10.3 8.32
10.4 8.8
10.9 9.89
11 10.37
12 10.89
102L Spring 2021
16.2 Raw data
unk trial initial mass final mass
1 17.135 16.979
OBSERVATIONS 2 16.979 16.785
white crystal powder 3 16.785 16.623
not difficult to dissolve

T1 burette (mL) T1 pH T2 burette (mL) T2 pH

0 1.78 0 1.77
0.5 1.79 1 1.79
1 1.8 2 1.83
unknown: 05QNT 1.5 1.81 3 1.84
2 1.82 4 1.85
2.5 1.83 5 1.91
3 1.84 6 2.14
3.5 1.85 7.6 2.16
4 1.86 8.5 2.2
4.5 1.87 10.4 2.25
5 1.88 13.5 2.35
5.5 1.89 14.8 2.59
6 1.9 17 2.78
6.5 1.91 18.3 3.1
7 1.92 18.4 3.5
7.5 1.93 18.5 3.54
8 1.96 18.6 3.56
8.5 2.12 18.7 3.58
9 2.28 18.8 3.64
9.5 2.3 18.9 3.72
10 2.5 19 3.77
10.5 2.52 19.1 3.85
11 2.54 19.25 3.89
11.5 2.55 19.4 3.96
12 2.6 19.5 4.01
12.5 2.64 19.9 4.08
13 2.71 20 4.1
13.5 2.86 20.1 4.12
14 2.98 20.2 4.18
14.5 3.22 20.3 4.2
15 3.5 20.4 4.23
15.5 4.1 20.5 4.24
16 4.22 20.6 4.38
16.5 4.23 21 4.46
 17 4.43 21.5 4.59
17.5 4.78 21.9 4.69
18 4.91 22.5 4.82
18.5 5.19 23 4.99
19 5.29 24 5.12
20 5.43 25 5.53
20.8 5.58 26 5.76
21.5 5.69 27 5.82
22 5.88 28 5.91
22.5 5.9 29 6
23 5.92 30 6.02
23.5 5.95 31.5 6.09
24 5.98 33 6.18
25 6.05 33.5 6.23
26 6.09 34 6.31
27 6.12 35 6.42
28 6.23 35.2 6.43
29 6.35 35.4 6.44
30 6.45 35.6 6.45
31 7.12 35.8 6.52
33 7.91 36 6.69
33.3 8.3 36.2 6.76
33.5 8.5 36.4 6.87
33.6 9 36.6 6.91
33.7 9.9 37 7.01
34 10 37.3 7.14
35 10.1 37.6 7.27
38 7.56
38.3 8.01
38.9 9.3
39.3 9.4
40 9.9
41 9.97
42 9.98
43 10
44 10.1
T3 burette (mL) T3 pH
0 1.8
2 1.82
4 1.86
6 1.91
8 1.94
10 1.99
12 2.6
14.9 3.25
16 3.88
16.5 3.96
17 4.54
17.5 4.65
18 4.62
18.2 4.64
18.4 4.75
18.6 4.8
19 4.86
19.5 5.03
20 5.34
21 5.59
22 5.81
23 5.9
24 5.96
25 6.02
26 6.14
27 6.28
28 6.33
29 6.4
30 6.45
33 8.2
33.2 8.56
33.4 9.19
33.6 9.21
33.8 9.52
 34 9.92
34.2 9.96
34.5 10
34.8 10.02
35 10.09
102L Spring 2021
16.2 Raw data
unk trial initial mass final mass
1 15.222 15.075
OBSERVATIONS 2 15.075 14.893
white crystal powder 3 14.893 14.681
not difficult to dissolve

T1 burette (mL) T1 pH T2 burette (mL)

0 2.01 0
unknown: 01VMV 2 2.56 2
4 3.39 4
6 3.69 6
6.2 3.88 7
6.5 4.02 7.5
7 4.18 7.6
7.4 4.53 7.65
7.7 6 7.75
8 8.72 7.8
8.1 9.53 7.85
8.2 10.04 7.9
8.5 10.21 7.95
8.8 10.59 8
9 11 8.05
8.1
8.15
8.2
8.25
8.3
8.35
8.4
8.8
9.3
9.8
9.85
9.9
10
10.1
10.2
10.3
10.4
10.5
10.6
10.7
 10.8
10.95
T2 pH T3 burette (mL) T3 pH
2.01 0 2.03
2.58 2.2 2.62
3.41 4 3.45
3.68 5.2 3.46
3.77 6.4 3.47
3.8 8.2 3.92
3.81 9.3 3.97
3.82 10 3.99
3.83 10.5 4.01
3.84 11 4.25
3.85 11.5 4.6
3.86 12 4.99
3.87 12.1 5.01
3.93 12.2 5.21
3.932 12.3 5.46
3.94 12.4 5.69
3.942 12.5 5.89
3.95 12.6 6.01
3.96 12.7 6.32
3.97 12.8 6.56
3.98 12.9 6.72
4.01 13 7.01
4.21 13.2 7.14
4.32 13.4 7.22
4.88 13.6 8.01
5.14 13.8 8.33
5.88 14 8.97
6.42 14.1 9.34
6.64 14.2 9.45
7.42 14.3 10.01
8.1 14.5 10.34
8.23
9.2
9.65
10
10.65
11
102L Spring 2021
16.2 Raw data unk trial initial mass
1 16.413
2 16.197
3 15.993
OBSERVATIONS
white crystal powder
needed to warm to dissolve in water and swirl a good bit.
T1 burette (mL) T1 pH
unknown: 08LDR 0 3.99
1 4.16
2 4.31
2.6 4.62
3.25 4.71
4.3 5.24
5.2 5.36
7 5.69
8.65 5.81
10 6.03
10.35 6.49
11.55 10.12
12 10.99
12.5 11.32
13 11.6
14 11.69
15 11.81
final mass
16.197
15.993
15.784

T2 burette (mL) T2 pH T3 burette (mL) T3 pH

0 3.98 0 3.99
1 4.16 1 4.12
2.3 4.44 3 4.43
3.6 4.85 4.1 5
4.2 5.23 5.5 5.53
5.75 5.46 7 5.78
6.8 5.65 8.35 5.89
8.1 5.79 9.8 6.32
9.4 5.8 10.1 6.89
9.5 5.82 10.2 7.55
9.6 5.99 10.3 7.69
10 6.01 10.5 9.01
10.2 6.34 10.8 10.34
10.3 6.48 11.4 11.03
10.4 6.57 11.6 11.21
11 7.04 12.5 11.63
11.3 7.65 14 11.94
11.4 9.04
11.6 10.43
12.1 11.5
12.6 11.7
14 11.79
102L Spring 2021
16.2 Raw data unk trial
1
2
3

OBSERVATIONS
grainy colorless solid
did not dissolve in water at room temperature
needed to heat and stir

unknown: VL09M
initial mass final mass
16.211 16.055
16.055 15.897
15.897 15.734

T1 burette (mL) T1 pH T2 burette (mL) T2 pH T3 burette (mL) T3 pH

0 4.31 0 4.24 0 4.25
2 4.33 1.5 4.32 2 4.28
4 4.37 2 4.35 4 4.29
6 4.54 3 4.36 4.5 4.39
7 4.59 4 4.4 5.1 4.47
7.1 4.6 4.2 4.43 5.2 4.53
7.2 4.65 4.4 4.47 5.3 4.6
7.3 4.7 4.5 4.53 5.4 4.63
7.4 4.73 5 4.56 5.5 4.7
7.5 4.74 5.1 4.61 6 4.71
7.6 4.75 5.2 4.63 7 4.72
7.7 4.76 5.3 4.68 8 4.77
7.8 4.77 5.5 4.71 9 5.48
7.9 4.78 6 4.73 10.1 6.12
8 4.8 6.5 4.74 10.2 6.34
8.1 4.81 7 4.75 10.3 6.81
8.2 4.82 7.5 4.77 10.4 6.84
8.3 4.83 8 4.83 10.5 6.99
8.4 4.84 8.5 4.93 10.6 7.21
8.5 4.93 9 5.45 10.7 7.39
8.6 4.99 9.5 5.88 10.8 7.44
8.7 5.02 10 6.01 11 7.65
8.8 5.05 10.5 6.88 12 8.55
8.9 5.24 11 7.44 13 8.9
9 5.37 12 8.35
9.2 5.4 13 8.87
9.3 5.48 14 9.55
9.4 5.69
9.5 5.78
10 5.98
11 7.12
12 8.21
13 8.9
14 9.34
14.5 10
102L Spring 2021 unk trial
16.2 Raw data 1
2
3

OBSERVATIONS
grainy white solid
did not dissolve in water at room temperature
heat was needed
stirring helped to solubilizing

unknown: 240FM
initial mass final mass
14.123 13.968
13.968 13.81
13.81 13.648

T1 burette (mL) T1 pH T2 burette (mL) T2 pH T3 burette (mL) T3 pH

1 4.31 0 4.24 0 4.25
3 4.33 1.5 4.32 2 4.28
5 4.37 2 4.35 4 4.29
7 4.54 3 4.36 4.5 4.39
8 4.59 4 4.4 5.1 4.47
8.1 4.6 4.2 4.43 5.2 4.53
8.2 4.65 4.4 4.47 5.3 4.6
8.3 4.7 4.5 4.53 5.4 4.63
8.4 4.73 5 4.56 5.5 4.7
8.5 4.74 5.1 4.61 6 4.71
8.6 4.75 5.2 4.63 7 4.72
8.7 4.76 5.3 4.68 8 4.77
8.8 4.77 5.5 4.71 9 5.48
8.9 4.78 6 4.73 10.1 6.12
9 4.8 6.5 4.74 10.2 6.34
9.1 4.81 7 4.75 10.3 6.81
9.2 4.82 7.5 4.77 10.4 6.84
9.3 4.83 8 4.83 10.5 6.99
9.4 4.84 8.5 4.93 10.6 7.21
9.5 4.93 9 5.45 10.7 7.39
9.6 4.99 9.5 5.88 10.8 7.44
9.7 5.02 10 6.01 11 7.65
9.8 5.05 10.5 6.88 12.5 8.55
9.9 5.24 11 7.44 13 8.9
10 5.37 11.95 8.35
10.2 5.4 12.75 8.87
10.3 5.48 13.5 9.55
10.4 5.69
10.5 5.78
11 5.98
12 7.12
13 8.21
14 8.9
15 9.34
15.5 10
102L Spring 2021
16.2 Raw data unk trial initial mass final mass
1 15.122 14.971
2 14.971 14.82
3 14.82 14.624

T1 burette (mL) T1 pH
OBSERVATIONS 0 6.42
colorless 0.5 6.43
did not require stirring or heat 1 6.44
1.5 6.45
unknown: 14MBP 1.78 6.5
1.98 6.51
2.1 6.53
2.5 6.59
2.81 6.61
3.22 6.69
3.74 6.72
3.99 6.75
4.21 6.8
5.11 6.82
5.74 6.99
6.01 7.01
6.5 7.03
7.5 7.1
8 7.2
8.5 7.31
9.01 7.33
9.1 7.45
9.2 7.52
9.3 7.59
9.4 7.64
9.5 7.78
9.6 7.82
9.8 7.94
10 8.01
10.1 8.12
10.2 8.2
10.3 8.32
10.4 8.7
10.5 9.6
10.6 10.15
 10.8 10.3
11 10.5
11.25 10.73
11.5 10.88
12 10.9
13 10.95
T2 burette (mL) T2 pH T3 burette (mL) T3 pH
0 6.43 0 6.41
1 6.44 1.6 6.53
2 6.52 2.5 6.6
3 6.68 3.4 6.7
3.7 6.71 5 6.8
4 6.79 6 6.9
4.5 6.81 7 7.01
5 6.81 8 7.1
5.5 6.87 9 7.2
5.8 6.88 9.5 7.23
6.2 7.01 10 7.32
7 7.08 10.5 7.44
7.8 7.12 10.7 7.5
8 7.21 11 7.52
8.1 7.23 11.3 7.62
8.3 7.25 11.5 7.78
9 7.35 12 8.3
9.4 7.67 12.2 8.45
9.7 7.83 12.3 8.61
9.8 7.96 12.5 9.52
9.9 7.99 12.8 10.3
10 8.02 13 11
10.1 8.1 13.5 11.5
10.2 8.15
10.25 8.23
10.3 8.32
10.4 8.8
10.9 9.89
11 10.37
12 10.89
102L Spring 2021
16.2 Raw data unk trial
1
unknow eno08i 2
3

OBSERVATIONS
grainy white crystals
particles didn't stick
acid unknown dissolved very quickly and needed no stirring
unknown: Z06MJ
initial mass final mass
13.421 13.25
13.25 12.904
12.904 12.741

T1 burette (mL) T1 pH T2 burette (mL) T2 pH T3 burette (mL)

0 1.21 0 1.21 0
1 1.21 1 1.21 1.6
1.5 1.21 2 1.21 3.7
2.3 1.22 3 1.22 6
3 1.22 3.7 1.24 9
3.5 1.23 4 1.24 13
4 1.24 5 1.26 14
4.5 1.25 6 1.29 15
4.7 1.25 7 1.31 18
4.9 1.26 8 1.31 21
5.1 1.27 8.5 1.32 23
5.3 1.29 10 1.33 25
5.6 1.3 12 1.36 27
5.9 1.3 13 1.42 29
6.3 1.31 13.5 1.45 30
6.8 1.32 15 1.68 32
7.3 1.33 17 1.71
8.1 1.33 19 1.86
8.9 1.34 21 1.99
9.6 1.34 21.5 2.43
10.2 1.34 22 2.89
10.5 1.35 22.5 4.13
10.8 1.4 23 4.57
11 1.4 27 5.14
11.3 1.42 29 5.55
11.9 1.46 30 6.15
12 1.48
12.1 1.48
13.1 1.55
13.3 1.66
17 1.74
18 1.93
19 2.01
21.5 2.43
 22 2.67
22.1 3.24
22.4 3.99
22.7 4.12
23 4.34
23.1 4.36
23.2 4.4
23.3 4.54
23.4 4.67
23.5 4.88
23.6 5.23
23.9 5.33
25 5.88
25.5 6.54
T3 pH
1.21
1.22
1.23
1.31
1.32
1.43
1.44
1.44
1.64
1.99
4.53
4.57
5.16
5.56
5.64
5.65