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Int J Adv Manuf Technol (2016) 87:647–656

DOI 10.1007/s00170-016-8466-y

ORIGINAL ARTICLE

A study on the residual stress during selective laser melting (SLM)


of metallic powder
Yang Liu 1 & Yongqiang Yang 1 & Di Wang 1

Received: 26 August 2015 / Accepted: 1 February 2016 / Published online: 27 February 2016
# Springer-Verlag London 2016

Abstract The complex thermal history of the parts 1 Introduction


manufactured by selective laser melting (SLM) leads to
complex residual stress, having a significant impact on Selective laser melting (SLM) is an emerging manufacturing
the quality of SLM part. The origin of residual stress technique, which is capable of manufacturing parts with prop-
was investigated in terms of temperature gradient mecha- erties of metallurgical bonds, relatively high densities, high
nism. Then, stresses along the height and horizontal direc- dimensional accuracies, and favorable mechanical properties.
tions were measured by X-ray diffraction, and effects of Successive layers of metallic powder are melted and solidified
processing parameters on the stress distribution were stud- on top of each other, thereby generating complex three-
ied. Results showed that residual stress distribution and dimensional parts [1]. Despite its numerous advantages,
evolution along the height direction are affected by the SLM still has many shortcomings in its processing compared
subsequent thermal cycling (STC) significantly. In the hor- to the conventional manufacturing technologies [2]. Due
izontal direction, higher energy input and longer track to the locally concentrated energy input, the temperature
length induce larger residual stress. The stress parallel to gradient mechanism and consequent plastification lead
the scanning direction is much larger than that perpendicular to residual stress and deformation [3]. On one hand,
to the scanning direction, and the peak values of residual stress the dimensional and shape accuracies and mechanical strength
always occurs at the onset of scanning tracks. Based on this of the parts are affected. On the other hand, residual stress
study, corresponding measures can be taken to reduce the contributes to crack formation and disconnection of parts from
residual stress or avoid stress concentration, thereby im- the base plate [4].
proving the process stability of SLM. Some researchers studied residual stress by experimental
approaches, which included the crack compliance method
(CCM) [4, 5], hole drilling [6, 7], neutron diffraction [8, 9],
Keywords Selective laser melting . Residual stress . and X-ray diffraction [10, 11] methods. However, the CCM fails
Subsequent thermal cycling . X-ray diffraction . Temperature to measure the stress on the surface of the part. In contrast to this,
gradient . Warps the neutron diffraction and X-ray diffraction methods fail to
measure the stresses within the parts, whereas the hole drilling
method requires large dimensional sizes and smooth surfaces to
be effective. Other researchers established theoretical models to
predict the residual stress and deformation [4, 12, 13], or built a
finite element model to study the stress field [7, 14–16], using
* Yongqiang Yang
experimental values to verify their models. Moreover, qualita-
meyqyang@scut.edu.cn tive and semi-quantitative analyses were carried out by measur-
ing deformation rather than stress on structures, such as cantile-
ver or bridge-shaped specimens [17, 18]. The previous studies
1
School of Mechanical and Automotive Engineering, South China were successful in revealing the stress characteristics along the
University of Technology, Guangzhou, China 510640 height direction to a certain extent.
648 Int J Adv Manuf Technol (2016) 87:647–656

Technology. The machine used a ytterbium fiber laser with a


maximum power of 200 W with a continuous wavelength of
1090 nm. Based on the direction of a dual-axis mirror posi-
tioning system and a galvanometer optical scanner, the laser
beam could move along the X- and Y-axes. The focus of the
laser spot was about 70 μm through a F-theta lens with a focal
length of 163 mm. Figure 1 shows the schematic diagram of
the principle of operation of the DiMetal-100 equipment, and
its main technical parameters are presented in Table 1. The
metal powder used in this study was gas-atomized 316L stain-
less steel spherical powder [1, 22], as shown in Fig. 2. The
particle size distributions were d10 = 22.5 μm, d50 = 39.02 μm,
Fig. 1 Schematic diagram of SLM fabricating equipment and d80 = 56.04 μm; the average particle size was 42.83 μm,
and the relative density was 4.02 g/cm3. The mechanical prop-
erties included a tensile strength of 485 MPa, yield strength of
During SLM, successive layers of metallic powder are 170 MPa, elongation of 30 %, Young’s modulus of 196 GPa,
melted and solidified on top of each other, generating a com- and Poisson’s ratio of 0.294. The chemical composition of the
plex three-dimensional part. When a new layer of powder is powdered material is shown in Table 2.
irradiated with the laser beam, part of the heat is absorbed and
the rest of it conducts through to the underlying layers, thereby 2.2 Production of samples by SLM
affecting the temperature and distribution of stress. This ther-
mal process is called subsequent thermal cycling (STC). As shown in Fig. 3a, the test samples for height direction were
Moreover, the shrinkage of the newly added layers during marked as samples 1, 2, and 3. Each sample had a fixed width
the cooling process gives rise to additional tensile stress in and thickness of 30 mm × 1 mm, and heights were 12, 16, and
the underlying layers [19]. This state is related to the accumu- 20 mm, respectively. The processing parameters are shown in
lation of heat and stress during the SLM process [20, 21]. Table 3. To avoid any influence of wire cutting on the stress
In the present study, the origin of residual stress in terms of field of samples, bases were manufactured and subsequently
temperature gradient mechanism was firstly studied. Then, the subjected to a stress relief heat treatment consisting of two
distribution of stress along height direction and horizontal hours at 450 °C and furnace cooling. Then, samples were
direction was measured by means of X-ray diffraction, and manufactured on the bases, and the part along with the base
the effects of energy input and scanning track length on stress was cut from the base plate as a whole. The measuring points
distribution were investigated. Lastly, optimized support were arranged along the height direction of samples (Y direc-
structures were used to inhibit warps and cracks, caused by tion). The points on sample 1 were marked as A1, B1, and C1;
the residual stress. points on sample 2 were marked as A2, B2, C2, and D2; and
points on sample 3 were marked as A3, B3, C3, D3, and E3.
To investigate the stress distribution in SLM parts, the sam-
ples were manufactured as shown in Fig. 3b. The measuring
2 Experimental conditions and methods points were labeled as m_n, where m represents the sample
number, and m = 1, 2, 3, 4, 5, 6; n represents the measuring
2.1 Equipment and materials point, and n = A, B, C, D, E, F, G. The samples 1, 2, and
3 were used to study the influence of scanning track
The experiments were carried out using a SLM machine length on the residual stress field. Samples 3, 4, and 5
DiMetal-100 developed by South China University of were manufactured with different scanning speeds, which

Table 1 Main technical parameters of the DiMetal-100

Item Value Item Value

Wavelength 1090 nm Focus length 163 mm


Max laser power 200 W Building envelop 100 × 100 × 120 mm
Beam coefficient M2 ≤1.1 Scanning speed 30-2000 mm/s
Focus beam size 70 μm Layer thickness 20-50 μm
Int J Adv Manuf Technol (2016) 87:647–656 649

Fig. 2 SEM image of 500 mesh 316L stainless steel powder

were used to study the influence of energy input (ψ = P/v)


on the residual stress field. Sample 6 was divided into
three segments, and then each short segment was scanned,
which was used to study the influence of sector-wise scan-
ning strategy on the stress field. The interval between
adjacent measuring points was 6 mm, and the distance
between the point and the edge was 3 mm.

2.3 Measure methods Fig. 3 CAD models for experiments of residual stress distribution. a
Along height direction. b Along horizontal direction

The test samples were studied using a Quanta 200 scanning


electron microscope (SEM). X-ray diffraction (XRD) patterns
material and generates an extremely large temperature gradi-
were obtained and residual stresses were measured on a D8-
ent of over 108 K/s [24, 25], which causes high residual stress
ADVANCE X-ray diffractometer (Bruker AXS GmbH,
within the SLM parts [4]. Figure 5a shows the temperature
Germany). The XRD patterns of the samples were obtained
distribution in the height direction. Tm and Tp represent the
under the following conditions: 2θ range from 10 to 90°, scan-
melting point and plastic point of material, respectively,
ning speed 1°/min with increments of 0.02°, and Cu-Kα radi-
whereas, Tn represents the ambient temperature. It can be di-
ation. The residual stresses were measured three times and the
vided into three regions according to their thermal states:
average of the three readings was recorded. Prior to the mea-
melted zone (region І), heat-affected zone (region II), and
surements, all the samples were electrolytically polished in
non-affected zone (region III) [24, 26].
saturated sodium chloride solution (NaCl) for 1 min to remove
The SLM process can be subdivided into heating and
any oxides on the surfaces. The surface roughnesses complied
cooling processes. During heating, the laser beam irradiates
with the requirements of the Chinese National Standard GB/T
at a specific point, then the temperature of region II falls be-
7704–2008 [23].
tween the range of Tn and Tp, the material expands but is
restricted by region III. This consequently induces tensile
stress in region III and compressive stress in region II. Since
3 Effects of the temperature gradient on SLM the temperature of region І exceeds Tp, it is converted into a
process complete plastic state and therefore no residual stress is pro-
duced, as illustrated at stage 1 in Fig. 4b.
3.1 Effect on the residual stress During cooling, the laser beam moves away from the spe-
cific point and the temperature immediately decreases. When
In SLM, a high-power laser locally melts successive layers of
powder, after which the heat conducts to the surrounding Table 3 Process parameters for manufacturing of testing samples

Table 2 Chemical compositions (wt %) of 316L stainless steel Items Power/W Speed/ Hatch/mm Thickness/ Scanning strategy
(mm/s) mm
Element C Cr Ni Mo Si Mn O Fe
Value 200 400 0.08 0.04 X-Y inter layer
Mass fraction (%) 0.03 17.53 12.06 2.16 0.86 0.38 0.13 Bal stagger
650 Int J Adv Manuf Technol (2016) 87:647–656

Fig. 4 Temperature and residual


stress distribution in height
direction during SLM. a
Temperature. b Residual stress

the temperature of region І is lower than Tp, the material When a high energy laser irradiates the molten pool, the tem-
changes from the former complete plastic state into an incom- perature gradient between the bottom of the molten pool and
plete plastic state and the volume shrinkage is restricted by the surface provides a driving force for the growth of the grain.
region II. Thus, tensile stress is produced in region І and com- However, the solidification rate can reach values as high as
pressive stress in region II increases, as shown at stage 2 in 108 K/s when the laser beam moves out of the molten pool
Fig. 4b. [24, 25]; thus, the crystal development of austenite is signifi-
As the temperature drops continuously, region І shrinks cantly restricted due to insufficient time for the grain growth
further, but is still restricted by region II. This causes tensile [24, 27].
stress in region І and compressive stress in region II to further In SLM, a subsequent layer is deposited on the underlying
increase, and compressive stress is extended to region III, as layer, the temperature in the underlying layers has already
illustrated at stage 3 in Fig. 4b. decreased to a lower level, which leads to a non-
synchronous heating and cooling process between the ad-
3.2 Effect on the microstructure jacent layers. This so called thermal boundary effect
makes a discrepant of microstructures in the adjacent
Figure 5a shows a macro crack with a maximum length of layers. However, heat in the subsequent layer conducts
about 500 μm on the unpolished side surface, whereas through to the underlying layers, which changes the
Fig. 5b shows a micro crack with a maximum length about cooling and solidification processes as well as the micro-
30 μm on the polished side surface. This is because under the structural evolution, as shown in Fig. 6b–d.
action of a moving high energy laser, the melting and solidi-
fication processes are completed in a considerably short peri-
od of time, which induce a high temperature gradient and a 4 Results and discussion
high stress, as a result of which, cracks tend to be formed in
order to release the thermal stress [22]. 4.1 Residual stress distribution along the height direction
The microstructure of SLM 316L part is shown in Fig. 6.
Figure 6a shows that the sizes of most of the grains are less The residual stress along the height direction is shown in
than 1 μm, which can be attributed to the complete melting Fig. 7. It shows that residual stresses within SLM 316L
and high heating and cooling rates during the SLM process. parts are of lower magnitude and the range is between

Fig. 5 Cracks on the SLM part. a


Macro cracks. b Micro cracks
Int J Adv Manuf Technol (2016) 87:647–656 651

Fig. 6 Microstructures of the


SLM 316L part

−90 and 120 MPa. Stresses in the underlying layers are maximum σy of 73, 61, and 114 MPa. This is because
compressive, the maximum σ x are −41, −54, and the underlying layers near the base plate, the temperatures
−64 MPa, and the maximum σ y are −33, −68, and of which decrease initially and then the shrinkage of the
−88 MPa, respectively, which occur in the centers of newly added layers causes the underlying layers to be
parts. Peak values of tensile stresses are found in the top compressed, thereby producing compressive stresses in
layers with maximum σ x of 44, 31, and 54 MPa and the underlying layers [28]. With the increasing number

Fig. 7 Residual stresses along


height direction in the three
samples
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4.2 Residual stress distribution along the horizontal


direction

4.2.1 Effect of the energy input

The lengths of sample 3, 4, and 5 were 18 mm, and the


fixed processing parameters were laser power 200 W, lay-
er thickness 0.035 mm, hatching space 0.08 mm, and the
scanning strategy Z-type X-direction (Fig. 3b). The scan-
ning speeds were 400, 200, and 800 mm/s, respectively,
and the total number of layers was 50. Here, stress in the
X direction was referred to as σx, and stress in the Z
Fig. 8 Comparisons of residual stresses between the three samples direction as σz.
Curves in Fig. 9 show the residual stresses under dif-
ferent energy inputs. Consistent with the previous study,
of layers, heat accumulates in the formed layers, which residual stresses on the top surfaces are tensile. This is
reduces the temperature gradient in the part. Hence, the because the shrinkage of top layers is restricted by the
compressive stress shows a trend that decreases from the underlying layers. According to the formula: ψ = P/v, the
bottom to the top, which then converts into tensile stress energy input of sample 4 is twice that of sample 3 and
in the top layers. four times that of sample 5. Correspondingly, the sample
The comparisons of residual stresses of the three 4 shows the greatest residual stress, and it is followed by
samples are shown in Fig. 8. It can be seen that when sample 3 and sample 5 possesses the least stress. This
a new layer is added on the previously scanned layers, indicates that the more the energy input, the greater the
compressive stress within the underlying layers in- residual stress produced. This factor can be attributed to
creases and tensile stress within the top layers converts larger energy inputs leading to a larger melting pool and a
into compressive stress. This variation can be explained accompanying larger volume shrinkage of molten pool
by considering sample 2 as an example. During the after solidification, which in turn leads to larger residual
manufacturing of D2, the regions A2 and B2 are heated stress within the parts.
to a higher temperature, but do not exceed the plastic A comparison of the curves in Fig. 9a, b, highlights
point (Tp), whereas the region C2 is heated to a tem- that σx is far greater than σz. Taking the sample 3 as an
perature exceeding the Tp due to STC. Hence, the ten- example, the range of σx is between 110 and 145 MPa,
sile stress in region C2 is released. Expansions of re- whereas the range of σz is between 30 and 55 MPa. This
gions A2 and B2 are only restricted by the underlying is because in high-speed scanning by laser beam, the
layers (including the base plate), so compressive stresses heat-affected zone (HAZ) and the molten pool form an
within regions A2 and B2 increase. During the cooling elongated shape along the direction of X axis (along the
period, the shrinkage of region D2 is restricted by the scanning direction) [10]. The temperature gradient along
underlying layers (including regions A2, B2, and C2). the X direction is far greater than that along the Z direc-
Hence, compressive stresses within regions A2 and B2 tion (perpendicular to scanning direction). In SLM pro-
increase continuously, compressive stress is produced in cess, a larger temperature gradient leads to larger residual
region C2, and tensile stress in region D2. stress.

Fig. 9 Residual stresses versus


different energy inputs
Int J Adv Manuf Technol (2016) 87:647–656 653

Fig. 10 Residual stresses versus


different scanning track lengths

4.2.2 Effect of the scanning track length rapidly at the onset of tracks, and subsequently oscillates to a
small degree. This is because the molten pool is surrounded by
Samples 1, 2, and 3 were used to investigate the influence of non-melted powder at the onset of tracks, which possesses
scanning track length. The lengths were 44, 32, and 18 mm, lower thermal conductivity than that of the corresponding sol-
respectively, as shown in Fig. 3b. The laser power was 200 W, id material [30]. Heat in the molten pool is not easily trans-
scanning speed was 400 mm/s, layer thickness was 0.035 mm, mitted to the surrounding materials. Hence, a larger tempera-
hatching space was 0.08 mm, the scanning strategy was Z- ture gradient is produced in scanning tracks, which induces
type X-direction, and the total number of layers was 50. greater residual stress at the onset of tracks. As the laser beam
Curves in Fig. 10 show the distribution of residual moves forwards, the heat in the scanning tracks is diverted,
stress for different scanning track lengths. The longer and then the temperature gradient decreases and tends to grad-
the scanning track, the larger the residual stress. This ually bring about dynamic balance, and consequently the re-
trend is consistent with the finite element analysis (FEA) con- sidual stress decreases.
ducted by Matsumoto et al. [29]. An explanation for this is that
when the laser irradiates the powder bed and forms melting 4.2.3 Effect of sector scanning strategy
tracks, the tracks mainly shrink along the scanning direction.
When the scanning tracks are excessively long, the shrink- The above analysis illustrates that residual stresses mainly
age compensation is insufficient, which induces a larger occur along the scanning direction, and are the main causes
residual stress. In addition, the range of σx is between of warp in SLM parts. Finite element analyses [29, 31]
80 and 200 MPa, and the range of σz is between 30 showed that the degree of warping in SLM parts is propor-
and 90 MPa (except point 1_A). Hence, σx is much larger tional to the scanning tracks, hence implying that the residual
than σz. stresses in SLM parts can be significantly reduced if only the
The peak values of σx and σz occur at the onset of scanning length of the scanning track is shortened. As shown in Fig. 11,
tracks, and then decrease along the scanning direction; how- the length of sample 6 is equal to sample 1, but it was divided
ever, the trends are different. In the first half of the scanning into three segments. Each segment was scanned by scanning
track, the decrease in σx is minimal, and then in the second strategy of Z-type X-direction. The results show that sector
half the decrease is dramatic. On the contrary, σz decreases scanning can reduce residual stresses in SLM parts effectively;

Fig. 11 Residual stresses versus


different scanning strategies
654 Int J Adv Manuf Technol (2016) 87:647–656

Fig. 12 Schematic diagram of


warp

the average decrease of σx reaches 22 %, whereas the average producing elastic compressive strains. When yield strength of
decrease of σz reaches 17 %. However, it is evident that sector the material is reached, the top layers become plastically com-
scanning has a greater impact on σx. At the measuring points pressed. During the cooling and shrinking period, the plasti-
of 1_A, 1_B, 1_C, 1_D, and 1_E, the σx decreases by more cally compressed upper layers become shorter than the bottom
than 50 MPa. This is because a short track length leads to a layers with the development of a bending angle (θ), towards
minimal cooling time between adjacent tracks [19], thereby the laser beam [19], as shown in Fig. 12. In this case, stable
resulting in a smaller temperature gradient, along the X support structures not only prevent the deformation of part
direction. caused by the material’s shrinkage, but also maintain the
manufacturing stability during the SLM process [20, 32]. As
shown in Fig. 13, the main parameters of support structure are
4.3 Measures for preventing warps and cracks tooth base interval, tooth base length, tooth top length, tooth
height, and hatching. The larger the tooth base interval +
Residual stress contributes to the crack formation or discon- length, top length or the smaller the hatching, the larger the
nection of parts from the base plate, therefore taking measures strength between support structure and part, the lesser is the
to reduce the residual stress in SLM part is necessary. probability of warping [33, 34].
Annealing treatment is a conventional and long established Three parts with same high aspect ratio (the length is
method to reduce stress in metallic parts, which are normally 60 mm, the section dimensions are 6 × 6 mm) were presented
used in welding, casting, forging, etc. Zhang et al. [28] used in Table 4. Part І was added uniform support structure, in
annealing treatment to reduce the residual stresses in Ti6Al4V which the hatching was 2 mm, tooth base interval + length
alloys manufactured by laser engineering net shaping (LENS). was 2 mm, and tooth top length was 0.3 mm. In part II, the
The results showed that the average stress could be reduced by hatching was 1 mm at the two ends, and 2 mm in the central
72 %. Although annealing treatment can effectively reduce region, the tooth base interval + length was 2 mm, and tooth
residual stress after manufacturing, it cannot prevent top length was 0.3 mm. Part III was added uniform support
warping and cracking caused by thermal stress during the structure, in which the hatching was 2 mm, tooth base inter-
SLM process. It is therefore necessary to try out other val + length was 2 mm, and tooth top length was 1 mm. The
methods to resolve these issues. processing parameters were laser power of 150 W, scanning
When a new layer is produced, the expansions of the heated speed of 400 mm/s, layer thickness of 35 μm, scanning space
top layers are restricted by the surrounding material, thereby of 80 μm, scanning strategy was X-Y inter-layer stagger. The
results were shown in Fig. 14, the part І warped at two ends,
whereas parts II and III were manufactured successfully. This
is because support structures with smaller hatching and larger
top length not only constrain warping at both ends of the parts,
but can also conduct heat from the top layers to the base plate,
thereby reducing the temperature gradient in the SLM parts.

5 Conclusions

In this paper, the residual stress during SLM process was


investigated. The effects of temperature gradient on the resid-
Fig. 13 Parameters of the support structure ual stress and microstructure characteristics were studied
Int J Adv Manuf Technol (2016) 87:647–656 655

Table 4 Three types of support structure

No. Support parameters


Aspect
ite Interval Tooth Tooth top
ratio Hatching
m + length height length

Part
10 2 mm 1 mm
I

Part
10 2 mm 1 mm
II

Part
10 2 mm 1 mm
III

Laser power: 150 W, scanning speed: 400 mm/s


Process
Layer thickness: 35 µm, scanning space: 80 µm
parameters
Scanning strategy: X-Y inter-layer stagger

theoretically. Stresses along height and horizontal directions layers on the previously scanned layers, the tensile stress
were measured by X-ray diffraction, the influences of subse- converts into compressive, and the compressive stress is
quent thermal cycling, energy input and scanning track length enhanced due to subsequent thermal cycling.
were investigated, and several conclusions can be drawn, (2) Residual stress parallel to the scanning direction is
which are as follows: much larger than that perpendicular to the scanning
direction. Lower energy input and shorter line length
(1) Compressive stress occurs at the bottom and tensile induce smaller residual stress in SLM parts.
stress at the top of SLM part, but with addition of new Therefore, sector scanning strategy, which reduces

Fig. 14 SLM manufactured parts


with large aspect ratio
656 Int J Adv Manuf Technol (2016) 87:647–656

the scanning track length, can reduce residual stress 15. Zhao HH, Zhang GJ, Yin ZQ, Wu L (2012) Three-dimensional
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