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Rapid Prototyping Journal

Residual stresses in selective laser sintering and selective laser melting


Peter Mercelis Jean-Pierre Kruth
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Peter Mercelis Jean-Pierre Kruth, (2006),"Residual stresses in selective laser sintering and selective laser melting", Rapid
Prototyping Journal, Vol. 12 Iss 5 pp. 254 - 265
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J-P. Kruth, P. Mercelis, J. Van Vaerenbergh, L. Froyen, M. Rombouts, (2005),"Binding mechanisms in selective laser sintering
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J.P. Kruth, X. Wang, T. Laoui, L. Froyen, (2003),"Lasers and materials in selective laser sintering", Assembly Automation, Vol.
23 Iss 4 pp. 357-371 http://dx.doi.org/10.1108/01445150310698652
Ben Vandenbroucke, Jean-Pierre Kruth, (2007),"Selective laser melting of biocompatible metals for rapid manufacturing of
medical parts", Rapid Prototyping Journal, Vol. 13 Iss 4 pp. 196-203 http://dx.doi.org/10.1108/13552540710776142

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Residual stresses in selective laser sintering
and selective laser melting
Peter Mercelis and Jean-Pierre Kruth
Division PMA, Department of Mechanical Engineering, University of Leuven, Leuven, Belgium

Abstract
Purpose – This paper presents an investigation into residual stresses in selective laser sintering (SLS) and selective laser melting (SLM), aiming at a
better understanding of this phenomenon.
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Design/methodology/approach – First, the origin of residual stresses is explored and a simple theoretical model is developed to predict residual
stress distributions. Next, experimental methods are used to measure the residual stress profiles in a set of test samples produced with different process
parameters.
Findings – Residual stresses are found to be very large in SLM parts. In general, the residual stress profile consists of two zones of large tensile
stresses at the top and bottom of the part, and a large zone of intermediate compressive stress in between. The most important parameters determining
the magnitude and shape of the residual stress profiles are the material properties, the sample and substrate height, the laser scanning strategy and the
heating conditions.
Research limitations/implications – All experiments were conducted on parts produced from stainless steel powder (316L) and quantitative results
cannot be simply extrapolated to other materials. However, most qualitative results can still be generalized.
Originality/value – This paper can serve as an aid in understanding the importance of residual stresses in SLS/SLM and other additive manufacturing
processes involving a localized heat input. Some of the conclusions can be used to avoid problems associated with residual stresses.

Keywords Sintering, Lasers, Stress (materials)

Paper type Research paper

Introduction parameters on the residual stress can be concluded. Finally,


some guidelines are presented to reduce the residual stress in
Selective laser sintering (SLS) and selective laser melting SLS and SLM.
(SLM) are two production technologies offering great The difference between SLS and SLM concerns the
advantages and opportunities compared to traditional binding mechanism that occurs between the powder particles
material removal techniques (Kruth et al., 2003, 2004). (Kruth et al., 2004). In SLS, either a combination of a low
However, the residual stresses that arise in the parts being melting binder and high melting structural material is used -
produced impose some serious limitations to the practical use, called liquid phase sintering (LPS) or the powder particles are
since they introduce part deformations and/or micro cracks. just partially molten. In case of LPS, a post treatment is
Moreover, large residual stresses can limit the load resistance of generally necessary to enhance the mechanical properties and
the parts compared to a stress free state. to increase the part’s density. In SLM, the powder particles
In the field of Laser Engineered Net Shaping, a lot of effort are fully molten. Since the border between SLS and SLM is
has been done to measure, predict and control residual rather vague, the stress inducing mechanisms are explained
stresses (Vasinonta et al., 2000; Aggarangsi and Beuth, 2003). generally for the case of SLM. In the case of partial melting
Whereas researchers mainly focussed on the stresses in the without infiltration, the same stress inducing mechanisms will
growth-direction at the substrate-part connection, the current occur. On the other hand, in the case of the LPS mechanism,
research will focus on the stresses perpendicular to the build the furnace cycle that is used to infiltrate the parts, will result
direction, and their variation along the build direction. in stress relaxation, so the resulting parts can be expected to
In order to investigate the residual stresses, the origin of the
be stress free.
stresses is firstly explained. Next, a simple theoretical model is
presented to predict the basic residual stress distribution.
Using an experimental procedure, residual stress profiles are The origin of residual stresses
then measured in a set of test samples having different kinds
Residual stresses are stresses that remain inside a material, when
of process parameters. Thus, the effect of the process
it has reached equilibrium with its environment. Residual stresses
are generally classified according to the scale at which they occur
The current issue and full text archive of this journal is available at (Withers and Bhadeshia, 2001). This investigation includes only
www.emeraldinsight.com/1355-2546.htm

This research was funded by the IAP project P5-08 of the Belgian Federal
Science Policy and the GOA/2002/06 project from KU Leuven.
Rapid Prototyping Journal
12/5 (2006) 254– 265 Received: 1 January 2006
q Emerald Group Publishing Limited [ISSN 1355-2546] Revised: 1 March 2006
[DOI 10.1108/13552540610707013] Accepted: 23 June 2006

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Residual stresses in selective laser sintering and selective laser melting Rapid Prototyping Journal
Peter Mercelis and Jean-Pierre Kruth Volume 12 · Number 5 · 2006 · 254 –265

type I residual stresses, which vary over large distances, namely thus introducing tensile stress in the added top layer and
the dimensions of the part. These macro stresses can result in compressive stress below.
large deformations of the part. Type II and type III residual
stresses, which occur due to different phases in the material and
due to dislocations at atomic scale, are not considered in this Simplified theoretical model
study, since they are of less importance for the material’s To get an idea of the residual stress profiles that would be
strength. Moreover, the measurement resolution of most test found in SLM samples, a simplified theoretical model was
methods is not small enough to measure type II and type III developed. Assume that a part is being built on top of a base
residual stresses. plate with height hb. The part that was built so far has height
Residual stresses are not always disadvantageous, e.g. glass hp and the layer thickness is t (Figure 2). This simple
plates are many times rapidly cooled to introduce compressive theoretical model assumes that:
stress in the surface area of the plate, thus increasing the .
the base plate and the part being built are at room
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overall loading resistance and preventing crack growth at temperature;


the surface. However, in most cases, residual stresses are .
the upper layer induces stress due to its shrinkage (aDT);
unwanted, since they result in deformations from the tensile stress is equal to the material’s yield strength s
the intended shape. Moreover, tensile pre-stress adds to the (since a strain of aDT would result in a stress much larger
stresses caused by external loading, thus reducing the strength than the material’s yield strength);
of the parts and favoring propagation of cracks from the .
the stress sxx is independent of the y coordinate, i.e. the
surface. variation of the normal stress across the part’s width is
Each production process introduces some amount of neglected;
residual stress (Withers and Bhadeshia, 2001). However, the .
the general beam theory is valid; and
amount of residual stress that is introduced varies a lot among .
no external forces are applied to the combination part-
different production processes. Laser based processes (laser base plate.
welding, SLM, etc.) are known to introduce large amounts of
residual stress, due to the large thermal gradients which are At each moment, the equilibria of force equation (1) and
inherently present in the processes. In case of laser bending, moment equation (2) need to be obeyed, since there are no
these stresses are, e.g. used to deform sheet metal plates to a external forces acting on the system:
desired shape. Two mechanisms can be distinguished which Z
cause residual stresses. sxx ðzÞdz ¼ 0 ð1Þ
The first mechanism introducing residual stress is called the Z
temperature gradient mechanism (TGM, Figure 1). It results sxx ðzÞzdz ¼ 0 ð2Þ
from the large thermal gradients that occur around the laser
spot. The TGM mechanism is commonly used for laser
bending of sheets along straight lines. Owing to the rapid Owing to the continuity of the deformation at the border
heating of the upper surface by the laser beam and the rather between the base plate, following strain profile is assumed
slow heat conduction, a steep temperature gradient develops. over the combination base plate-part:
The material strength simultaneously reduces due to the e xx ðzÞ ¼ az þ b ð3Þ
temperature rise. Since the expansion of the heated top layer
is restricted by the underlying material, elastic compressive Owing to the different stiffness of the base plate and the part
strains are induced. When the material’s yield strength is material, this deformation results in different stress levels; the
reached, the top layer will be plastically compressed. In stress profile reveals a jump at the border between the base
absence of mechanical constraints, a counter bending away plate and the part. Suppose that m represents the ratio of base
from the laser beam would be perceived. During cooling the plate stiffness to the part’s stiffness:
plastically compressed upper layers start shrinking and a E base
m¼ ð4Þ
bending angle towards the laser beam develops. This E part
mechanism is also present in SLS and SLM, where the
underlying layers inhibit the expansion of the heated top Using this assumption, the equilibrium conditions can be
layers. It is important to notice that this mechanism does not rewritten as:
require the material to be molten. Figure 2 Simplified theoretical model of the SLM process
A second mechanism that induces residual stresses is the
cool-down phase of the molten top layers (in SLM). The
latter tend to shrink due to the thermal contraction. This
deformation is again inhibited by the underlying material,

Figure 1 TGM inducing residual stress

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Residual stresses in selective laser sintering and selective laser melting Rapid Prototyping Journal
Peter Mercelis and Jean-Pierre Kruth Volume 12 · Number 5 · 2006 · 254 –265

Z hb Z hb þhp Z hb þhp þt
Figure 3 Residual stress in the part and the base plate
mðazþbÞdzþ ðazþbÞdzþ sdz ¼ 0 ð5Þ
0 hb hb þhp
Z hb Z hb þhp Z hb þhp þt
mðazþbÞzdzþ ðazþbÞzdzþ szdz ¼ 0 ð6Þ
0 hb hb þhp

From equations (5) and (6), the coefficients a and b can be


derived:
ð2mhb hp þ mhb hp t þ h2p þ hp t þ mh2b Þ
a ¼ 26st ð7Þ
ð4mh3b hp þ h4p þ m2 h4b þ 6mh2b h2s þ 4mhb h3p Þ
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ð2mh3b þ 6hp mh2b þ 3mh2b t þ 6hb h2p þ 6hb hp t þ 2h3p þ 3h2p tÞ


b ¼ st
ð4mh3b hp þ h4p þ m2 h4b þ 6mh2b h2s þ 4mhb h3p Þ
ð8Þ

Equations (5) and (6) assume that the part and the base plate
are equally wide. Usually the base plate is wider than the part.
Including the widths of the part and the base plate in the
equations would result in a different m factor: m ¼ Ebasewbase/
Influence of number of layers, base plate geometry and
Epartwpart. The influence of a wider base plate can thus be
material properties
simulated by increasing the E modulus of the base plate.
Number of layers
After the production, the parts produced are generally
Figure 5 shows the influence of the number of layers on the
removed from the base plate. To simulate this, a relaxation
residual stress profile. Before part removal, the stress in the part
stress must be added to the stress profile calculated in the
equals the yield strength at the top. However, when the number
part. This relaxation stress has a linear profile (z 0 ¼ z-hb,
of layers keeps increasing, compressive stresses occur at the
Figure 2):
bottom of the part. It can also be seen that the stresses in
srelaxation ðz0 Þ ¼ cz0 þ d ð9Þ the base plate become very large, so plastic deformation of the
base plate could occur. However, this behaviour is not included
The constant part of the relaxation stress corresponds to a
in the model. After part removal, a more or less symmetrical
uniform shrinkage of the part that is being removed from the
stress profile remains in the part. At the top and bottom of the
base plate. The linear part results in a curvature of the part.
part, tensile residual stress remains, with a zone of compressive
The coefficients c and d can be determined by recalculating
stress in between. The tensile residual stress is somewhat larger
the equilibrium conditions for the produced part (with hc the
at the bottom than at the top surface.
height of the part in the new coordinate system X, Y, Z0 ): Figure 6 shows the influence of the number of layers on the
Rh Rh
22 0c z0 sðz0 Þdz0 þ hc 0c sðz0 Þdz0 relaxation stresses. It can be seen that the constant part,
c ¼ 26 ð10Þ which relates to the shrinkage in X direction, is reduced by
h3c
adding more layers, while the linear part is increased.
R hc 0 0
R hc 0 0 0
0 sðz Þdz 2 3hc 0 z sðz Þdz
However, one should not conclude that this would increase
d ¼ 2hc ð11Þ the part’s bending deformation, since the surface moment of
h2c
inertia increases with the number of layers (according to h3).

Base plate geometry


Theoretical residual stress profiles Since the model assumes that the general beam bending theory
When a layer is added to the base plate, it induces a is valid, the width of the base plate can be combined with its E
compressive stress in the upper part of the base plate and a modulus to represent the stiffness. The base plate height,
tensile stress in the lower part. When successive layers are however, must be treated separately. Figure 7 shows the
added on top, each layer induces a certain stress profile in the influence of the base plate height on the stress profiles.
base plate, but also in the underlying solidified layers, thus According to this simple theoretical model, the height of the
reducing the initial tensile stress present in these layers. base plate has a clear influence on the residual stress
Figure 3 shows the resulting stress profile in the part and distribution. Before part removal, a higher height results in a
baseplate, after 50 layers (properties: base plate lower stress level in the base plate itself and a more uniform
thickness ¼ 20 mm, E base ¼ 210 GPa, Epart ¼ 110 GPa, stress level in the part. This means that a thick base plate results
t ¼ 50 mm, s ¼ 300 MPa). It can be seen that the stress at in a smaller deformation due to part removal, compared to a
the last added layer equals the yield stress of the material. thin base plate. Since almost all stress is released by a uniform
When the part is removed from the base plate, the stress state shrinkage, only little residual stress remains in the part after
in the part is drastically changed; due to the relaxation, the removal. Figure 8 shows the influence of the base plate height on
resulting stress in the part will be much lower. The constant part the relaxation stress components.
of the relaxation stress corresponds to the shrinkage of the part,
whereas the linear part of the relaxation stress corresponds to Material properties
the bending deformation. Figure 4 shows the relaxation Figure 9 shows the influence of the material’s yield strength
principle and the resulting stress in the part. on the residual stress being developed. The higher the yield

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Residual stresses in selective laser sintering and selective laser melting Rapid Prototyping Journal
Peter Mercelis and Jean-Pierre Kruth Volume 12 · Number 5 · 2006 · 254 –265

Figure 4 Relaxation of the residual stress and resulting stress in the part
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Figure 5 Influence of the number of layers on the residual stress profile

Figure 6 Influence of the number of layers on the relaxation stress strength, the higher the stresses being developed. The stresses
after part removal are also larger.

Conclusions
.
Stress profiles before removal consist of a large zone
of tensile stress at the upper zone of the part being built. The
maximum stress is reached at the surface of the part (equal to
the yield stress). The stress reduces with decreasing Z
values. The lower part of the base plate is under tensile
stress, the upper part is under compressive stress.
.
Part removal drastically reduces the residual stresses
which are present in the part; the residual stress relaxes by
a uniform shrinkage and a bending deformation. The
residual stress after removal consists of a zone of tensile
stress at the upper and lower zone of the part and a
compressive stress zone in between. The stresses after part
removal are much smaller than before part removal.

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Residual stresses in selective laser sintering and selective laser melting Rapid Prototyping Journal
Peter Mercelis and Jean-Pierre Kruth Volume 12 · Number 5 · 2006 · 254 –265

Figure 7 Influence of the base plate height on the residual stress profile
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Figure 8 Influence of the base plate height on the relaxation stress components

Figure 9 Influence of the materials yield strength on the residual stress profile

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Residual stresses in selective laser sintering and selective laser melting Rapid Prototyping Journal
Peter Mercelis and Jean-Pierre Kruth Volume 12 · Number 5 · 2006 · 254 –265

.
The more layers are added, the larger the final residual X
n
stress will be. The shrinkage along the X axis will reduce e xx ðzÞ ¼ Aj C j ðzÞ ¼ ½C {A} ð13Þ
when the amount of layers increases. j¼1
. The thicker the base plate, the smaller the resulting
From equation (13), the coefficients Aj can be calculated
residual stresses will be (for a fixed part thickness). A very
using a least-squares fitting algorithm:
thick base plate results in a large shrinkage in X direction,
while the bending deformation becomes smaller. A thin
base plate height results in high residual stresses in the {A} ¼ ð½C T ½C Þ21 ½C T {e measured } ð14Þ
part and in a high bending deformation.
.
The higher the yield strength of the added material, the Substitution of the coefficients [A ] in equation (12) results in
higher the resulting residual stresses. the residual stress profile.
Figure 11 shows the compliance functions that were
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Experimental measurement of residual stress: the calculated for the selected top face and back face strain
gauge positions.
Crack compliance method
In practise, the strains are measured at two locations, while
In order to measure the residual stresses in the parts, a novel the parts are being cut by wire-EDM. Figure 12 shows the
experimental model is used, based on measurement of the practical setup.
part’s deformation when the stresses are relieved. The method
is called the “Crack Compliance Method” (CCM) (Prime,
1999; Nowell et al., 2000). Compared with “traditional” test Experimental results
methods like X-ray diffraction or hole drilling, this method
has the advantage that trough-thickness measurements can be Test of the CCM method
performed in a simple and cheap way (Schindler, 2000). The In order to evaluate the suitability of the Crack compliance
method will be shortly explained first, without discussing method to do residual stress tests on SLM samples, and to
the mathematical implementation in detail. check the FEM model being used, some initial experiments
Figure 10 shows a sample in which an unknown residual stress were performed on samples with a know residual stress
distribution sxx(z) is present. This stress distribution is distribution.
supposed to be independent from the Y coordinate. One or A first tests performs a stress measurement on an
more strain gauges are connected to the sample’s surface at aluminium sample that was heated up to 2008C for 1 h and
known positions. Next, the part is cut in subsequent small steps cooled in air, to remove all residual stresses. Figure 13 shows
using wire electric discharge machining (EDM). After each the stress distribution that was calculated from the strain
cutting step, the strain is measured at each strain gauge position. measurements. As it can be seen, the stress level of 0 MPa lies
Suppose that the unknown stress distribution can be written within the two sigma uncertainty bound (95 per cent
as a series expansion of functions Pj (z). confidence limit) at most points.
Using a four point bending setup some test samples were
X
n produced, having a known stress distribution. The four point
sxx ðzÞ ¼ Aj P j ðzÞ ¼ ½P {A} ð12Þ bending test ensures a constant bending moment between the
j¼1
two middle contact points. The samples were bent until
The set of basic functions Pj (z) can be polynomials, Fourier plastic deformation occurs at the upper and lower zones of the
series, etc. Legendre polynomials are generally chosen, since parts. After removing the force, a new equilibrium is formed,
these polynomials (from order 2 on) automatically obey the that can be calculated from the recorded force values and the
equilibrium conditions of force and moment. For each basic yield strength. Figure 14 shows the calculated stress profile for
function Pj (z) we can now calculate the strain profiles that one of the test samples. The stress distribution that is
would be measured at the strain gauge locations, if this basic calculated this way, assumes that the samples are bent
function was the actual residual stress profile. These according to the general beam bending theory. It also assumes
calculations are generally performed using a finite element a perfect elastic-plastic behaviour of the material, with a clear
method[1]. The calculated strains, belonging to each of the yield strength; in reality the real stress profile could be slightly
basic functions, are referred to as “compliances” Cj (di). Using different, but the general tendencies are assumed to be
the superposition principle, the total strain due to the sum of correct.
all the basic functions can be written as: Figure 15 shows the stress profile that is calculated from the
measured strains. It can be seen that the calculated stress
Figure 10 Schematic representation of test sample distribution matches the “known” stress profile rather well.
However, at some points large deviations occur.
Figure 16 shows the calculated stress distribution for a
second test sample. In this case, the deviations are much
larger. This is due to the steepness of the “real” stress profile,
which cannot be fit accurately with the set of Legendre
polynomials that is being used. This is shown in Figure 17
which shows the optimal fit of the “real” stress profile using
the Legendre polynomials up to order 7. In order to fit these
sharp peaks accurately, higher order polynomials are
necessary. When sharp peaks are expected in a residual
stress profile, the Legendre polynomials are therefore not the

259
Residual stresses in selective laser sintering and selective laser melting Rapid Prototyping Journal
Peter Mercelis and Jean-Pierre Kruth Volume 12 · Number 5 · 2006 · 254 –265

Figure 11 Top face (left) and back face (right) compliance functions for 2nd-9th order Legendre polynomials
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Figure 12 Practical setup of the CCM method Description of test samples


Table I summarizes the most important test parameters of the
test samples that were all built on a concept laser M3 linear
machine. All test samples were produced from a standard
stainless steel powder (grade 316L). The parts were built on
top of a 15 mm thick stainless steel substrate plate.

Influence of the exposure strategy


The exposure strategy of the laser beam highly influences the
thermal gradients which occur in the parts being produced.
To test the influence of the exposure strategy on the residual
stresses, a set of test samples was made using different
scanning strategies. Figure 18 shows the different exposure
strategies that were used.
The “line Y” part is scanned along the Y axis and is thus
also referred to as “short track” scanning, while the “line X”
part will be named “long track” scanning. To test the
Figure 13 Calculated stress distribution in a stress free Al test sample influence of the sector scanning, two different sector sizes
were used: 5 by 5 mm and 10 by 10 mm. The position of the
islands is shifted in X and Y direction between successive
layers. The sector scanned parts discussed in this paragraph
are all scanned according to a certain patented pattern, which
minimizes the thermal influence of previous scanned sectors
on the next scanned sector. The influence of the sector
scanning order is investigated in the next paragraph.
Figure 19 shows the stress distributions that were measured
for the exposure strategies. Some important conclusions can
be derived:
.
all stress profiles correspond to the general tendency of a
small zone with high tensile stresses at the top of the part,
followed by broad zone of compressive stress and again a
small zone of tensile residual stress;
.
there is a clear difference between “short track” scanning
and “long track” scanning: scanning along the Y direction
results in the largest values for sxx, while scanning along
the X direction results in the smallest sxx values;
.
division of the part surface in smaller sectors yields an
ideal ones and other types of basic functions are favorable. intermediate stress level; the top layer stress lies between
However, from the theoretical model there is no reason to the stress resulting from “long” and “short” scanning of
expect sharp peaks in the residual stress profiles, thus the the whole part surface; and
Legendre polynomials with their inherent force and moment .
there is no significant difference in the resulting stress
equilibrium were used. profile between 5 and 10 mm sector size.

260
Residual stresses in selective laser sintering and selective laser melting Rapid Prototyping Journal
Peter Mercelis and Jean-Pierre Kruth Volume 12 · Number 5 · 2006 · 254 –265

Figure 14 Calculated stress distribution in bent test sample 1 Figure 17 Optimal fit of the real stress profile of test sample 2 using
Legendre polynomials up to order 7
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Figure 15 Calculated and measured stress distribution in bent test Table I Parameters used for the production of all test samples
sample 1
Length 50 mm
Width 10 mm
Height 10.5 mm
Laser power 100 W
Scanning speed 400 mm/s
Scan spacing 140 mm
Layer thickness 30 mm

Figure 18 Different exposure strategies

Figure 16 Calculated and measured stress distribution in bent test


sample 2 Figure 19 Measured stress distributions for different exposure strategies

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Residual stresses in selective laser sintering and selective laser melting Rapid Prototyping Journal
Peter Mercelis and Jean-Pierre Kruth Volume 12 · Number 5 · 2006 · 254 –265

A possible explanation for the reduction of the maximal Figure 21 Measured stress distributions for different sector exposure
stress level in case of sector scanning, is the fact that the orders
stress at the borders of each individual sector -that has no
neighbouring sectors yet -is zero, since no material exhibits
its contraction at the sector borders (Figure 20). When
more sectors are added, neighbouring sectors are connected
and the stress level also rises at the sector borders.
However, the overall stress level will be still be lower than
the maximum stress level in case of simple line scanning in
the perpendicular direction.

Influence of the sector scanning order


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Knowing that a subdivision of the part surface can reduce the


largest tensile stresses that occur in the upper layers of the
parts, the question remains how to expose these sectors.
There are number of ways to do so. Three different exposure
orders were tested in the investigation, all with the same sector
size (3-3 mm):
1 scanning of the sectors along the width of the part;
2 scanning the sectors along the length of the part; and
3 scanning the sectors in a randomized order, minimizing
by increasing the scan speed accordingly. Each of the parts was
the mutual thermal influence of the different sectors.
scanned with a “short track” exposure strategy, as well for the
Since the exposure order of the sector influences the thermal normal scanning as the post scanning step. Figure 22 shows the
gradients that occur, it also affects the level of residual stress measured stress distributions for the 50 and 100 per cent post
in the parts. Figure 21 shows the difference between the two scanning levels, compared to the case without post scanning. It
first exposure orders. It can be seen that scanning the sectors can clearly be seen that the 50 per cent post scanning level
along the width of the part yields a larger sxx value at the top reduces the tensile stress in the upper zone of the part (from
of the part, than scanning along the part’s length. This is no 120 ^ 7 to 84 ^ 11 MPa). Scanning each layer twice with the
surprise, since the exposure order along the part width normal scanning parameters (100 per cent) does not reduce the
corresponds to the “short track” scanning strategy, if the residual stresses inside the part; the already solidified layer is
sector size goes to zero. The stress level in case of the simply remelted partially and the same residual stress
randomized scanning order was comparable to the stress level distribution remains. The stress reducing effect of heating the
when scanning along the length of the part (red curve in underlying layers could result in a reduction of stress levels, but
Figure 21), however, a bad top face strain reading resulted in it is cancelled out by the TGM mechanism that introduces new
a high uncertainty border. stress inside the part.

Post scanning of the produced parts X-ray diffraction experiments


To simulate a stress reducing heat treatment, post scanning of The Crack compliance method that was used in the
the part surface was investigated. After the normal exposure of experiments, offered the possibility to measure the residual
each layer, the same layer was exposed again with the laser, at a stress trough the thickness of the test samples, unlike more
lower energy level. Four parts were tested, with a post scanning traditional XRD and hole drilling stress measurement
energy of 10, 33, 50 and 100 per cent of the normal layer energy, methods. Alas, the Crack compliance method fails to
measure the stress at the part surface very accurately,
Figure 20 Sector scanning mechanism leading zero normal stress the
first sector borders Figure 22 Measured stress distributions for different post-scanning
parameters

262
Residual stresses in selective laser sintering and selective laser melting Rapid Prototyping Journal
Peter Mercelis and Jean-Pierre Kruth Volume 12 · Number 5 · 2006 · 254 –265

because of several reasons, some of which were already Figure 24 XRD result with stress free dummy sample
mentioned before:
.
The first useful data point is the strain value recorded at
the first cut depth. Therefore, the stress at the part surface
is already an extrapolation of the calculated stress profile.
.
The first few stress readings are rather small (less than
5 mm strain), and the uncertainty on these readings is
therefore relatively large, resulting in a large stress
uncertainty near the upper surface.
.
The top face strain readings are very sensitive to the exact
distance between the gauge and the edge of the cut. A
slight positioning error of the top face gauge results in a
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large variation in the top face strains, causing erroneous


results near the surface.
To cope with the large uncertainty of the stress readings near
the surface, additional XRD tests were performed on several
SLM samples. Due so practical size limitations, the SLM
samples tested with the Crack compliance method, could not
be tested using XRD, so a different set of test samples was in the etching step and a zero stress value is measured indeed
produced. in X and Y direction.
The X-ray diffraction stress measurements were performed Owing to the removal of the upper layer, the stress values
on a Siemens D500 diffractometer. The diffraction peak of that are measured are not any more the values at the upper
the 316L stainless steel material at a 2u angle of 1478 was used layer of the SLM part. However, the total removed thickness
to measure the peak shift. of about 120 mm is small enough compared to the total height
of the XRD test samples (10.5 mm) to consider them as the
Sample preparation
top layer stress values.
A first X-ray diffraction experiment on a untreated SLM
The influence of the base plate removal step is shown in
sample, resulted in a stress level of 12 ^ 7 MPa. This
Figure 25. The sample that was tested was exposed with a
unrealistically low value was caused by the roughness of the
top surface. Since the X-rays penetrate the material only to a random sector exposure. Thus, the stresses are equally large
depth of about 30 mm, large roughness values prohibit a in X and Y direction. The same sample was then cut from its
correct stress measurement. base plate and was measured again. It is clear that the base
To cope with this problem, an EDM finishing cut was used plate removal yields a large reduction of the stress levels.
to remove the peaks from the surface. However, the EDM The influence of the number of layers was investigated by
operation itself introduces large tensile stresses in a ^ 40 mm testing a series of three samples, having a height of 2.5, 5 and
thick zone below the surface (Kruth and Bleys, 2000), which 10 mm, respectively. The base plate was removed with all
deteriorates the measurement result. Therefore, the thermally samples. All three samples were scanned without dividing the
influenced layer from the EDM operation was removed by surface in sectors, to check the influence of the scanning
chemically etching a small top layer from the samples[2]. direction on the residual stresses. Figure 26 shows the axis
Figure 23 shows the sample preparation steps schematically. orientation and the exposure strategy that was used. From
Figure 24 shows the results of three different XRD Figure 27 it can clearly be seen that the sample height has a
measurement on a stress free dummy sample that was used large influence on the residual stress level, as expected from
to check the influence of the sample preparation steps. the theoretical model. Furthermore, Figure 27 shows the
The first XRD measurement indicates a low but non-zero influence of the scanning direction on the residual stresses;
stress value in X direction (the Y direction was not
measured). The non-zero value was probably caused by the Figure 25 Influence of base plate removal
presence of a small oxide layer resulting from the heat
treatment. Next, the dummy sample was cut with wire-EDM
on a finishing regime. The second XRD measurement reveals
very large stress values X and Y direction. There is no
significant difference between the direction of the cut and the
direction of the wire. The third XRD measurement indicates
the stress values after the etching step. It is clear that the small
thermally influence layer of the EDM process is removed

Figure 23 XRD sample preparation steps

263
Residual stresses in selective laser sintering and selective laser melting Rapid Prototyping Journal
Peter Mercelis and Jean-Pierre Kruth Volume 12 · Number 5 · 2006 · 254 –265

Figure 26 Exposure strategy and axis orientation Figure 28 Influence of base plate heating
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Figure 27 Influence of the sample height

parameters, which appeared to contain a rather high


degree of porosity. This resulted in stress values much
lower than in the case of full density, since the stress
equals zero at each porosity border. The XRD samples
from Figures 27 and 28 were build with optimized
scanning parameters, yielding nearly 100 per cent density
and having much higher stress values.

Conclusions
This paper presented a theoretical and experimental
investigation on residual stresses in SLS and SLM. A simple
theoretical model could predict the basic shape of the
residual stress profile of a basic rectangular geometry. Two
experimental methods -the Crack Compliance Method and
the stresses perpendicular to the scanning direction are
an X-ray diffraction method -were used to validate the
significantly larger than the stresses along the scanning
theoretical predictions and to find a qualitative and
direction. This result corresponds to the Crack compliance
quantitative estimation of the residual stresses.
experiments.
From the theoretical model and the experiments, some
Since residual stresses arise from temperature gradients,
heating up the build platform can reduce the stress levels important conclusions can be derived:
.
A distinction should be made between parts that remain
present in the parts (Over, 2003),(Vasinonta et al., 2000). To
validate this assumption the build platform was heated up to connected to their base plate and parts that are removed
2008C. Figure 28 shows the effect of the raised based plate afterwards. In general, parts that stay connected to the
temperature. It is clear that the stresses are reduced by the baseplate contain very high stress levels, in the range of
base plate heating. However, the stress reduction is rather the material’s yield strength. Parts that are removed from
poor. It can be expected that a higher base plate heating the base plate, contain much lower stress levels, but they
temperature will result in a greater stress reduction. Like suffer from deformation during part removal.
Figure 27, Figure 28 also clearly indicates the influence of the
.
The basic residual stress distribution in the Z direction for
scanning direction. a part removed from its base plate, consists of a zone of
In general, there is a good qualitative agreement between tensile stresses just below the upper surface, followed by a
the theoretical model, the Crack compliance experiments and large zone of compressive stress, to end again with a
the XRD tests. However, a quantitative comparison is not tensile stress zone at the bottom. The magnitude of the
easy, because of several reasons: stresses depends amongst others on the part height and
.
The theoretical model calculates the stresses resulting the stiffness and height of the base plate.
from the shrinkage of the added molten layers. It does not . The exposure strategy that is being used to fuse the
include the TGM, which induces extra residual stresses. powder layers, has a large influence on the residual stress
.
The sample geometry of the Crack compliance test levels being developed. In general, the stresses are larger
samples and the XRD samples was different, due to perpendicular to the scan direction than along the scan
practical reasons. direction. A subdivision of the surface in smaller parts
.
The Crack compliance test samples and the first batch of results in a lower maximum stress value and in equally
XRD test samples, used non optimized scanning large stresses in X and Y direction.

264
Residual stresses in selective laser sintering and selective laser melting Rapid Prototyping Journal
Peter Mercelis and Jean-Pierre Kruth Volume 12 · Number 5 · 2006 · 254 –265

.
It is possible to reduce the stress level by applying a heat Schindler, H. (2000), “Residuals stress measurements in
treatment using the laser source. However, no drastic cracked components: capabilities and limitations of the
reductions could be obtained in this investigation. cut compliance method”, Materials Science Forum,
.
Heating of the substrate plate results in a reduction of the Vol. 347-349, pp. 150-5.
residual stress level, since temperature gradients are Vasinonta, A., Beuth, J. and Griffith, M. (2000), “Process
reduced. maps for controlling residual stress and melt pool size in
laser-based sff processes”, Proceedings of the Solid Freeform
Notes Fabrication Symposium, pp. 200-8.
1. The calculations were performed using the Abaqus FEM Withers, P. and Bhadeshia, H. (2001), “Residual stress,
package. part 2 -nature and origin”, Materials Science and Technology,
2. A mixture of HCl and HNO3 was used to remove a top Vol. 17, pp. 366-75.
layer of ^ 80 mm thickness from the top surface.
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References About the authors


Aggarangsi, P. and Beuth, J. (2003), “Melt pool size and Peter Mercelis obtained a MSc degree in Mechanical
stress control for laser-based deposition near a free edge”, Engineering -Mechatronics at the University of Leuven and is
Proceedings of the Solid Freeform Fabrication Symposium, currently working as a PhD candidate at the department of
pp. 196-207. Mechanical Engineering at the University of Leuven. He is
Kruth, J. and Bleys, P. (2000), “Measuring residual stress part of the research group on production processes. His
caused by wire EDM of tool steel”, International Journal of research focuses mainly on process monitoring and control in
Electrical Machining, Vol. 5, pp. 23-8. Selective Laser Sintering and Selective Laser Melting of metal
Kruth, J., Froyen, L., Rombouts, M., van Vaerenbergh, J. and powders. Peter Mercelis is the corresponding author and can
Mercelis, P. (2003), “New ferro powder for selective laser be contacted at: peter.mercelis@mech.kuleuven.ac.be; web
sintering of dense parts”, Annals of the CIRP, pp. 139-42. site: http://people.mech.kuleuven.ac.be/ , pmerceli/
Kruth, J., Mercelis, P., Froyen, L. and Rombouts, M. (2004),
Jean-Pierre Kruth is Full Professor at the University of
“Binding mechanisms in selective laser sintering and
Leuven, (KU Leuven), Belgium, where he is responsible for
selective laser melting”, Proceedings of the Solid Freeform
Fabrication Symposium, pp. 44-59. Production Engineering. His main research activities are:
Nowell, D., Hills, D. and Tochilin, S. (2000), “Use of the CAD/CAM/CAPP, production processes, metal cutting, non-
crack compliance method for the measurement of residual traditional machining (EDM, laser machining, . . .), Rapid
stress”, Proceedings of the 6th International Conference on Prototyping and Manufacturing, dimensional metrology,
Residual Stresses, Vol. 2, pp. 845-52. quality control, reverse engineering. He is Active Member of
Over, C. (2003), “Generative Fertigung von Bauteilen aus CIRP, Fellow of SME, Honorary member Romanian Society
Werkzeugstahl X38CrMoV5-1 und Titan TiAl6V4 mit of Mech. Eng., Member BSMEE, Member IMEKO/
Selective Laser Melting”, PhD thesis, RWTH Aachen. BEMEKO, Member K.VIV and founding board member of
Prime, M. (1999), “Residual stress measurement by seccessive the companies MATERIALISE N.V. (1997), METRIS N.V.,
extension of a slot: the crack compliance method”, Applied MIH N.V. Email: jean-pierre.kruth@mech.kuleuven.be;
Machanics Reviews, Vol. 52 No. 2, pp. 75-96. website: www.mech.kuleuven.be/pma/

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