Professional Documents
Culture Documents
The investigation of the influence of laser re-melting on density, surface quality and microstructure of
selective laser melting parts
Evren Yasa Jan Deckers Jean-Pierre Kruth
Article information:
To cite this document:
Evren Yasa Jan Deckers Jean-Pierre Kruth, (2011),"The investigation of the influence of laser re-melting on density, surface
quality and microstructure of selective laser melting parts", Rapid Prototyping Journal, Vol. 17 Iss 5 pp. 312 - 327
Permanent link to this document:
http://dx.doi.org/10.1108/13552541111156450
Downloaded on: 04 March 2015, At: 05:01 (PT)
References: this document contains references to 27 other documents.
To copy this document: permissions@emeraldinsight.com
The fulltext of this document has been downloaded 1103 times since 2011*
Users who downloaded this article also downloaded:
Downloaded by Universite Laval At 05:01 04 March 2015 (PT)
J-P. Kruth, P. Mercelis, J. Van Vaerenbergh, L. Froyen, M. Rombouts, (2005),"Binding mechanisms in selective laser sintering
and selective laser melting", Rapid Prototyping Journal, Vol. 11 Iss 1 pp. 26-36 http://dx.doi.org/10.1108/13552540510573365
Peter Mercelis, Jean-Pierre Kruth, (2006),"Residual stresses in selective laser sintering and selective laser melting", Rapid
Prototyping Journal, Vol. 12 Iss 5 pp. 254-265 http://dx.doi.org/10.1108/13552540610707013
Ben Vandenbroucke, Jean-Pierre Kruth, (2007),"Selective laser melting of biocompatible metals for rapid manufacturing of
medical parts", Rapid Prototyping Journal, Vol. 13 Iss 4 pp. 196-203 http://dx.doi.org/10.1108/13552540710776142
Access to this document was granted through an Emerald subscription provided by 331053 []
For Authors
If you would like to write for this, or any other Emerald publication, then please use our Emerald for Authors service
information about how to choose which publication to write for and submission guidelines are available for all. Please visit
www.emeraldinsight.com/authors for more information.
About Emerald www.emeraldinsight.com
Emerald is a global publisher linking research and practice to the benefit of society. The company manages a portfolio of
more than 290 journals and over 2,350 books and book series volumes, as well as providing an extensive range of online
products and additional customer resources and services.
Emerald is both COUNTER 4 and TRANSFER compliant. The organization is a partner of the Committee on Publication Ethics
(COPE) and also works with Portico and the LOCKSS initiative for digital archive preservation.
Abstract
Purpose – Selective laser melting (SLM) is a powder metallurgical (PM) additive manufacturing process whereby a three-dimensional part is built in a
layer-wise manner. During the process, a high intensity laser beam selectively scans a powder bed according to the computer-aided design data of the
part to be produced and the powder metal particles are completely molten. The process is capable of producing near full density (,98-99 per cent
relative density) and functional metallic parts with a high geometrical freedom. However, insufficient surface quality of produced parts is one of the
important limitations of the process. The purpose of this study is to apply laser re-melting using a continuous wave laser during SLM production of
316L stainless steel and Ti6Al4V parts to overcome this limitation.
Design/methodology/approach – After each layer is fully molten, the same slice data are used to re-expose the layer for laser re-melting. In this
manner, laser re-melting does not only improve the surface quality on the top surfaces, but also has the potential to change the microstructure and to
improve the obtained density. The influence of laser re-melting on the surface quality, density and microstructure is studied varying the operating
Downloaded by Universite Laval At 05:01 04 March 2015 (PT)
parameters for re-melting such as scan speed, laser power and scan spacing.
Findings – It is concluded that laser re-melting is a promising method to enhance the density and surface quality of SLM parts at a cost of longer
production times. Laser re-melting improves the density to almost 100 per cent whereas 90 per cent enhancement is achieved in the surface quality of
SLM parts after laser re-melting. The microhardness is improved in the laser re-molten zone if sufficiently high-energy densities are provided, probably
due to a fine-cell size encountered in the microstructure.
Originality/value – There has been extensive research in the field of laser surface modification techniques, e.g. laser polishing, laser hardening and
laser surface melting, applied to bulk materials produced by conventional manufacturing processes. However, those studies only relate to laser
enhancement of surface or sub-surface properties of parts produced using bulk material. They do not aim at enhancement of core material properties,
nor surface enhancement of (rough) surfaces produced in a PM way by SLM. This study is carried out to cover the gap and analyze the advantages of
laser re-melting in the field of additive manufacturing.
Keywords Surface roughness, Solid freeform fabrication, Rapid manufacturing, Layered manufacturing, Surface texture, Metallurgy
312
Influence of laser re-melting on density, surface quality and microstructure Rapid Prototyping Journal
Evren Yasa, Jan Deckers and Jean-Pierre Kruth Volume 17 · Number 5 · 2011 · 312 –327
Figure 1 Produced parts by SLM However, those studies only relate to laser enhancement of
surface or sub-surface properties (up to a depth range of
hundreds of microns (Ukar et al., 2010)) of parts produced using
bulk material. They do not aim enhancement of core material
properties, nor surface enhancement of (rough) surfaces
produced in a powder metallurgical (PM) way by SLM.
On the other hand, it is possible to modify the material
properties throughout the depth of products by applying laser
re-melting during additive manufacturing after the generation
of each layer. In SLM, laser melting refers to melting of
powder particles to generate a 2D layer by selectively scanning
the laser beam over the powder bed. Therefore, the term “laser
re-melting” is used to refer to a second pass of the laser beam
for different purposes such as further material densification,
surface quality and microstructural enhancement of SLM
parts. In the field of additive manufacturing, not enough work
has been dedicated to laser re-melting except the studies
reported in (Morgan et al., 2002; Lamikiz et al., 2007).
Lamikiz et al. (2007) applies laser re-melting only on outer
surfaces of selectively laser sintered parts and deals with
Figure 2 Operating principle of SLM process surface quality improvement, whereas Morgan et al. (2002)
Downloaded by Universite Laval At 05:01 04 March 2015 (PT)
Laser uses laser re-melting after each layer to release any entrapped
gas and to create a smooth surface finish to each layer.
Mirror scanner
Thus, the influence of laser re-melting is not thoroughly
XY deflection explored yet in additive manufacturing in terms of different
f-θ lens improvement aspects, although laser surface modification of
Roll bulk materials has been studied extensively by some
Overflow researchers.
N2 atmosphere
Therefore, in this study, the potential of laser re-melting to
enhance the density and the core or surface quality of SLM
parts is investigated. The effect of changing process
Y parameters is studied with respect to density, surface
roughness, microstructures and microhardness obtained by
laser re-melting after each layer or after LSR. This research is
X
carried out to cover the gap and analyze the advantages of
Feed container Z axis laser re-melting in the field of additive manufacturing.
Build cylinder
2. Experimental procedure
the same slice is scanned again before putting a new layer of In this study, two types of commonly used metal powders
powder. This solution, named as laser re-melting, definitely were used:, i.e. AISI 316L stainless steel and Ti6Al4V. The
increases the production time, but on the other hand, it can experiments with stainless steel were carried out on a Concept
be the ultimate solution for applications where a density of Laser M3 Linear machine which employs an Nd:YAG laser
98 per cent is not sufficient. However, laser re-melting can also with a wavelength of 1,064 nm. The laser can be operated in
be applied only to the top layers if it is only aimed to enhance the either Q-switched or continuous modes. In this work, laser
surface quality and/or roughness. In this case, it is named as laser re-melting was conducted in the continuous mode (i.e. the
surface re-melting (LSR) and the production time is not same mode as used for SLM) whereby the maximum laser
significantly affected. output power was approximately 100 W. It is possible to
There has been extensive research in the field of laser surface adjust the laser spot diameter, F21/e to 53 and 133 mm (F99%,
modification techniques, e.g. laser polishing, laser hardening and respectively, 80 and 200 mm) by using an aperture, which also
laser surface melting, applied to bulk materials produced by changes the power. Ti6Al4V powder was processed on an
conventional manufacturing processes. Laser surface in-house developed LM machine at K.U.Leuven. The LM
modification can be applied to reduce surface roughness machine employs an Yb:YAG fibre laser with a wavelength of
(Wissenbach et al., 2006; Henari and Blau, 1995; Nicolas et al., 1,085 nm and can only be operated in continuous mode.
1997; Triantafyllidis et al., 2005; Lamikiz et al., 2007; Ramos- The maximum laser output power is about 300 W and the
Grez and Bourell, 2004), or to improve other surface material standard beam diameter F21/e is 50 mm.
properties such as surface microhardness (Kac and Kusinski, The surface roughness of the top surfaces was measured by
2004; Xianqing et al., 2007; Pinto et al., 2003), friction and wear a surface profilometer (Taylor Hobson Form Talysurf 120L).
behavior (Zhang et al., 2008; Felgueroso et al., 2008), corrosion In this paper, the surface quality of the parts was mostly
resistance (Tang et al., 2004; Xu et al., 2006; Guozhi et al., 2007), expressed by the arithmetic mean surface roughness (Ra),
wettability (Hao and Lawrence, 2006; Lawrence and Li, 2001; measured without a filter. The total height of the roughness
Triantafyllidis et al., 2005; Roemer et al., 2009) and sub-surface profile (Rt) and the surface roughness depth (Rz) were also
microstructural properties (Grabowski et al., 2006). measured and follow the same trend as Ra.
313
Influence of laser re-melting on density, surface quality and microstructure Rapid Prototyping Journal
Evren Yasa, Jan Deckers and Jean-Pierre Kruth Volume 17 · Number 5 · 2011 · 312 –327
In this study, micro-Vickers hardness measurements were of 200 mm was utilized together with a bi-directional scan
done instead of macro- or nano-Vickers hardness strategy with long scan vectors. With a spot size of 200 mm, a
measurements. By not using a macro hardness tester pump current of 39 A corresponds to a laser power of 105 W,
(HB, HRc, HRb), the measurements could be done relatively whereas a pump current of 35 A corresponds to 85 W. The
close to each other, making it possible to investigate the change scan spacing factor (a1) together with the spot size (dspot)
of hardness of the SLM parts with depth. By not using the determines the scan spacing distance (s) between two
Vickers nano-indenter, the measurements gave a more global consecutive scan lines (s ¼ a1 £ dspot). In order to enhance
overview of the surrounding hardness. The measurements were the density in the laser re-melting experiments, the scan
done by a Leitz/Durimet Vickers microhardness tester. For one speed was changed in the range of 50-200 mm/s, whereas a
hardness measurement, a load of 1.94 N was applied for 30 s. scan spacing factor was varied between 5 and 20 per cent
The resulting pyramidal indentation, whose dimensions are (a1 ¼ 0.05-0.2). The effect of the laser power was
related to the Vicker Pyramid Number [HV], was visualized on investigated in the ranges of 85-105 W as well as two
a computer screen via a charge-coupled device camera and different numbers of re-melting scans (1 or 3). All tested
manually measured by encasing it with a box. Eight hardness parameters are given in the table in Figure 4.
measurements were done to calculate a mean hardness value. Figure 5 shows an optical microscope image of the cross-
Confidence intervals were also calculated, using a confidence section of a part machined by SLM without any re-melting.
level of 95 per cent. To investigate the change of hardness of The black spots throughout the part are pores that were
the cross-section of one part as a function of depth, eight created during the SLM process. They are homogeneously
hardness measurements were done at three different depths distributed and can be formed due to several reasons such as
as shown in Figure 3. decrease in the solubility of the dissolved elements in the melt
The microstructure of the parts made by SLM and pool during cooling and solidification and evaporation of
Downloaded by Universite Laval At 05:01 04 March 2015 (PT)
subjected to laser re-melting was characterized with an optical elements with a high vapor pressure (Rombouts, 2006).
microscope and a scanning electron microscope (SEM) using Besides, those melting and solidification phenomena, high-
secondary electrons. Before making pictures with the SEM, surface roughness can also cause low density: high-roughness
the parts were polished, etched and covered with a nano-layer peaks and valleys that are formed after each layer can prevent
of carbon. the coater depositing a new homogenous powder layer.
Moreover, the laser energy may be not enough to melt the
3. Experimental results and discussion new layer completely since the thickness of the powder in
some regions will be higher because of the high-surface
This section discusses the density (Section 3.1) and surface roughness. Morgan et al. has already found that a rough
quality (Section 3.2) improvements obtained after laser surface causes the entrapment of gas upon deposition of a new
re-melting experiments. Resulting hardness (Section 3.3) powder layer. When the new layer is being scanned, the gas is
and microstructural changes (Section 3.4) are also reported. superheated and expands rapidly removing the liquid metal
above it, thus creating a pore (Rombouts, 2006).
3.1 Density improvement
The densities (or porosity) of the samples produced with no
SLM of the stainless steel powder was always carried out
re-melting (standard SLM parameters) and of samples
with the standard parameters optimized for maximum
obtained by applying different laser re-melting parameters
density on the Concept Laser M3 Linear machine (island
after each SLM layer, were observed with an optical
scanning with a scan speed 380 mm/s, a laser power 105 W, a
microscope. First, the micrographs were converted to black
scan spacing 125 mm and F99% spot size of 200 mm). After
and white images using a constant threshold value. Then,
SLM of each layer, the same slice was scanned with
the ratio of the number of black pixels to the total number of
re-melting parameters, which were changed for each test
pixels was calculated giving the porosity. For every set
specimen. In this work, the influence of laser re-melting
of parameters, at least three pictures taken at different
parameters such as scan spacing, scan speed, number of
locations of the cross-section were observed. The average
re-melting scans or laser power was investigated while others
porosities measured in this way are shown in Figure 4,
(spot size and scan strategy) were kept constant throughout
together with a confidence interval of 95 per cent.
this set of laser re-melting experiments. A F99% spot size
Within the range applied in this study, higher re-melting
scan speed (200 mm/s) in combination with low laser power
Figure 3 Hardness measurements (85 or 35 A) exhibits very-low-porosity values as shown in
tests from 1 to 4. Applying the re-melting three times
instead of 1 did not significantly change the porosity in this
low-energy input range (tests 2 and 3). As the energy input
was increased by decreasing the scan spacing and increasing
the number of re-melting scans at the same time (test 5),
a significant rise in the porosity occurred.
Figure 4 shows that all parameter sets applying laser
re-melting improves the density when compared to test case
with no re-melting (see the last bar). The average porosity of
parts with no re-melting is about 0.77 per cent, whereas the
densest re-melted part obtained with the second parameter set
has a porosity of 0.032 per cent which is almost 25 times less.
The optical microscope pictures of some parameter sets are
shown in Figures 6 and 7. The laser re-melting parameters for
314
Influence of laser re-melting on density, surface quality and microstructure Rapid Prototyping Journal
Evren Yasa, Jan Deckers and Jean-Pierre Kruth Volume 17 · Number 5 · 2011 · 312 –327
Scan Scan
Diode # of re-
Test # speed spacing
current [A] melting
[mm/s] (a1)*
1 200 35 0.1 1
2 200 35 0.1 3
3 200 35 0.2 3
4 200 35 0.05 1
5 200 35 0.05 3
6 200 35 0.2 1
7 200 39 0.1 3
8 200 38 0.1 3
9 200 37 0.1 3
10 200 39 0.1 1
11 200 38 0.1 1
12 200 37 0.1 1
13 100 35 0.1 1
14 75 35 0.1 1
15 50 35 0.1 1
2 3 4 5 6 7 8 9 10 11 12 13 14 SLM 16 SLM only - no re-melting
* Scan spacing = scan spacing factor (a1) × spot size
Downloaded by Universite Laval At 05:01 04 March 2015 (PT)
315
Influence of laser re-melting on density, surface quality and microstructure Rapid Prototyping Journal
Evren Yasa, Jan Deckers and Jean-Pierre Kruth Volume 17 · Number 5 · 2011 · 312 –327
Figure 6 Optical microscopy images of the laser re-melted parts with Figure 7 Optical microscopy images of the laser re-melted parts with
different parameters (porosity , 0.06 per cent) different parameters (porosity . 0.13 per cent)
1 0.052% 5 0.252%
200 µm 200 µm
35 A, 200 mm/s, a1 = 0.1, 1 layer 35 A, 200 mm/s, a1 = 0.05, 3 layers
2 0.032% 7 0.136%
200 µm 200 µm
35 A, 200 mm/s, a1 = 0.1, 3 layers 35 A, 200 mm/s, a1 = 0.1, 3 layers
3 0.043% 14 0.205%
Downloaded by Universite Laval At 05:01 04 March 2015 (PT)
200 µm
200 µm 35 A, 200 mm/s, a1 = 0.1, 1 layer
35 A, 200 mm/s, a1 = 0.2, 3 layers
8 0.151%
6 0.036%
200 µm
200 µm 37 A, 200 mm/s, a1 = 0.1, 3 layers
35 A, 200 mm/s, a1 = 0.2, 1 layer
316
Influence of laser re-melting on density, surface quality and microstructure Rapid Prototyping Journal
Evren Yasa, Jan Deckers and Jean-Pierre Kruth Volume 17 · Number 5 · 2011 · 312 –327
Porosity (%)
0.8 0.8
0.4 0.4
0 0
50 75 100 200 SLM with no 0.05 0.1 0.2 SLM with no
laser re-melting laser re-melting
Scan speed (mm/s) Scan spacing factor a1
(a) (b)
200 mm/s, a1= 0.1, onere-melting scan, big aperture
1.2 1.2
85 W, 200 mm/s, a1 = 0.1
85 W, 200 mm/s, a1 = 0.05
105 W, 200mm/s, a1 = 0.1
0.8
Porosity (%)
0.8
Porosity (%)
Downloaded by Universite Laval At 05:01 04 March 2015 (PT)
0.4 0.4
0 0
1 3
SLM with no laser re- 85 95 100 105 SLM with no
melting laser re-melting
Number of re-melting scans
Laser power (W)
(c)
Notes: (a) Scan speed; (b) scan spacing; (c) number of re-melting scans; (d) laser power (d)
Figure 9 Roughness results of ten layers of LSR for a scan spacing of a scan speed of 225 mm/s (Figure 13(a)). Each of these last
0.1 £ spot size 20 layers was then exposed to laser re-melting with scan
vectors perpendicular to the scan vectors of the melting. For
Scan spacing factor (a1) = 0.1 for laser re-melting each part, a different combination of scan speed and laser
16 power was used for re-melting the 20 last layers, as shown in
50 mm/s Figure 11(a). The following scan speeds were used: 20, 80,
200 mm/s 320, 1,280 and 5,120 mm/s. Each of these scan speeds was
12
400 mm/s used in combination with the following laser power values: 16,
600 mm/s 32, 64, 128 and 256 W. On each part, three linear roughness
Ra [µm]
317
Influence of laser re-melting on density, surface quality and microstructure Rapid Prototyping Journal
Evren Yasa, Jan Deckers and Jean-Pierre Kruth Volume 17 · Number 5 · 2011 · 312 –327
200 µm 200 µm
Building axis Building axis
(a) (b)
Notes: (a) SLM-only part; (b) Laser re-melted part with 200 mm/s and 98W exhibiting a very smooth surface
Figure 11 Average roughness, Ra, of the Ti6Al4V experiments with the standard deviations expressed in micrometers regarding (a) first set of tests;
(b) second set of tests
Ra (µm) Ra (µm)
Downloaded by Universite Laval At 05:01 04 March 2015 (PT)
256 6.9 (2.1) 4.2 (1.2) 4.3 (0.7) 6.4 (1.7) 17.3 (3.6) 256 6.8 (1.1) 7.3 (2.7) 2.9 (0.3) 5.1 (1.1)
128 5.9 (3.8) 5.7 (0.8) 3.6 (1.1) 6.6 (0.6) 14.6 (1.2) 181 6.7 (1.4) 5.6 (1.7) 3.7 (0.6) 4.7 (1.0)
P (W)
P (W)
64 17.6 (9.7) 7.6 (2.7) 6.8 (0.8) 12.3 (0.7) 14.0 (0.8) 128 4.2 (0.4) 4.7 (1.5) 4.8 (1.6) 6.1 (1.6)
32 9.7 (1.3) 13.7 (2.2) 14.3 (1.3) 14.5 (1.7) 12.6 (0.9) 91 4.1 (0.5) 5.1 (0.6) 5.8 (0.7) 5.7 (0.3) 7.8 (0.6)
16 13.8 (3.1) 16.5 (3.0) 16.9 (1.7) 14.7 (2.0) 12.3 (1.4) 64 4.9 (0.5) 5.1 (0.7) 6.1 (0.4) 7.0 (1.7) 11.5 (2.8)
three reference parts were made with the standard SLM edges and high-scan speeds (high productivity). The darker
parameters (i.e. 40 W and 225 mm/s for the last 20 layers) the shading in Figure 11(b), the more preferable the
and not re-melted. The cross-section of one of these reference re-melting parameters.
parts is shown in Figure 13(a). The results are shown in To sum up, the smoothness of SLM parts could be greatly
Figures 11(b) and 12(b). There is a significant improvement improved by re-melting the outer surface. The best results
in the roughness values when laser re-melting is applied either were obtained with relatively high-energy settings (high-laser
with high-scan speed (640 mm/s) and high-laser power power, small-scan spacing, medium-scan speed, possibly
(256 W) or medium scan speed (320 mm/s) and medium several re-melting scans). This adds to the production time,
laser power (128 W). yet to a limited extend since only the outer layer has to be
The flatness of the top surface was, however, affected by the re-melted in this case.
occurrence of edges that arise when the re-melted material is 3.2.3 Edge-effect
partially pushed to the contours of the part by the laser beam The possible reasons for the edge effect, also accompanying
(Figure 13(b)). These edges, referred to as the “edge-effect” SLM, are discussed further in (Yasa et al., 2009). In that
by the authors, sometimes also occur in pure SLM parts, study, different process parameters and scanning strategies
but are generally larger if the parts are re-melted with were used to understand and combat the elevated edges
a relatively low-scan speed and high-laser power. To find in SLM. As a result, the reason of elevated edges is given
the power and scan speed that optimizes the given re-melting as follows: during the SLM process, the first scan line of the
process, an assessment between surface roughness and the layer that is being scanned (part’s border) is surrounded
size of the edges is necessary. The combinations of scan power at both sides with powder particles with very low-thermal
and scan speed that gave the lowest roughness values with conductivity. Owing to the change of shape of the melt pool in
acceptable edges is considered to lie in a diagonal band most cases, more powder particles are dragged to the melt
as marked on Figure 11(b). The most preferable zone of this volume thereby increasing the size of melt pool as well as
diagonal band is the one with low-roughness values, low affecting the solidification rate of the melt. In addition,
318
Influence of laser re-melting on density, surface quality and microstructure Rapid Prototyping Journal
Evren Yasa, Jan Deckers and Jean-Pierre Kruth Volume 17 · Number 5 · 2011 · 312 –327
Figure 12 Average roughness plots of the Ti6Al4V experiments shown due to powder particles being dragged to the melt pool since
in Figure 11 no powder material is involved in laser-re-melting. If the
energy intensities are high enough, evaporation of material
25 occurs. However, the laser energy intensity is not high enough
20 mm/s
at the sides due to insufficient overlapping of successive scan
20 80 mm/s
tracks. As the material inside the contours starts to evaporate,
320 mm/s
the melted material is expelled towards the sides creating
Ra (um)
15 1,280 mm/s
5,120 mm/s an elevated edge. The cross-sectional view of an LSR sample
10 SLM with no LSR is shown in Figure 13(c). If the provided energy intensity in
LSR is not high enough for evaporation, only the melted
5 material being pushed in the sides and backward of scanning
direction causes the edges.
0
0 100 200 300
Laser power (W) 3.3 Microhardness
(a) The results of microhardness measurements for stainless steel
parts were shown in Figure 14 for different sets of scan speed
25 and laser power values. The measurements were taken on the
80 mm/s cross-section of the parts having a normal vector perpendicular
20 160 mm/s to the building axis at three different depths (Figure 3). One
320 mm/s
line of measurements was conducted close to the top surface at
Ra (um)
15 640 mm/s
a depth of approximately 100 mm, whereas the others were
1,280 mm/s
Downloaded by Universite Laval At 05:01 04 March 2015 (PT)
319
Influence of laser re-melting on density, surface quality and microstructure Rapid Prototyping Journal
Evren Yasa, Jan Deckers and Jean-Pierre Kruth Volume 17 · Number 5 · 2011 · 312 –327
300 300
31 A – 50 mm/s 31 A – 400 mm/s
35 A – 50 mm/s 35 A – 400 mm/s
275 39 A – 50 mm/s 275 39 A – 400 mm/s
Only SLM Only SLM
250 250
225 225
200 200
Top Middle Bottom Top Middle Bottom
(a) (b)
300
31 A – 800 mm/s
35 A – 800 mm/s
39 A – 800 mm/s
275 Only SLM
Downloaded by Universite Laval At 05:01 04 March 2015 (PT)
250
225
200
Top Middle Bottom
(c)
Notes: (a) With low scan speed (50 mm/s); (b) with medium scan speed (400 mm/s); (c) with high scan
speed (800 mm/s)
Figure 15 Top surface of an SLM part with no laser re-melting (polished and etched) with an optical microscope
µm
which was in good agreement with the scan spacing and spot size onto the other tracks surrounding it. Figure 16 also shows that
values used during the experiments. In Figure 16, the cross- during SLM a fully melted pool with a depth of about 80-90 mm
sections of the melted scan tracks are visible showing that the was formed which was significantly greater than the layer
stainless steel powder particles were completely fused together thickness (30 mm).
within melted and solidified zones having curved edges. The SEM is also used for the analysis of smaller microstructural
laser tracks overlapped so that each melted track was bonded features. Figure 17 shows the SEM image of the cross-section
320
Influence of laser re-melting on density, surface quality and microstructure Rapid Prototyping Journal
Evren Yasa, Jan Deckers and Jean-Pierre Kruth Volume 17 · Number 5 · 2011 · 312 –327
Figure 16 Cross-section of an SLM part with no laser re-melting (polished and etched) with an optical microscope
200 µm
Building axis
Downloaded by Universite Laval At 05:01 04 March 2015 (PT)
Figure 17 SEM image of the cross-section of an SLM part with no laser re-melting
of an SLM part with no re-melting. A fine cellular/dendritic 38 A (,100 W), a spot size of 200 mm, a scan spacing of
structure exists, formed as a result of rapid solidification due 20 mm and three times laser re-melting. The contour and its
to very high-cooling rates encountered in SLM. However, it is connection with the core of the part is clearly distinguishable.
not homogenously visible throughout the cross-section of In the contour zone, the cross-sections of the melted scan
SLM parts. This microstructure is also encountered in laser tracks are visible having curved edges. The lamellar structure
welding of steels (Rombouts, 2006). Figure 17 also shows inside the part shows a smaller thickness than an SLM layer.
spherical pores with different sizes formed during the SLM The thickness of visible layers in the optical microscopy
process. The bigger hole is filled with epoxy particles during picture of this part was found to be around 20 mm whereas in
grinding of the embedded sample surfaces in the preparation SLM one layer thickness was chosen to be 30 mm. This
stage before etching with an etchant called V2A-Beize distance between horizontal lines depends on the process
(200 ml distilled water, 200 ml HCl (32 per cent), 20 ml parameters of laser re-melting. For comparison, the optical
HNO3 (65 per cent) and 0.6 ml Vogels Sparbeize) at 808C. micrographs of laser re-melted parts with various process
3.4.1 Laser re-melting after each layer parameters are shown in Figure 19 together with an SLM part
Figure 18 shows one of the samples treated with laser with no laser re-melting. The figure reveals that a higher
re-melting after each SLM layer with the following number of scans in laser re-melting leads to a significantly
parameters: a scan speed of 200 mm/s, a diode current of finer lamellar structure.
321
Influence of laser re-melting on density, surface quality and microstructure Rapid Prototyping Journal
Evren Yasa, Jan Deckers and Jean-Pierre Kruth Volume 17 · Number 5 · 2011 · 312 –327
Figure 18 Cross-section of a part with laser re-melting after each layer showing the contour scanning
Downloaded by Universite Laval At 05:01 04 March 2015 (PT)
100 µm
Building
direction
Figure 19 Cross-sectional views of parts with different laser re-melting parameters applied after each layer together with an SLM part
with no re-melting
200 µm
322
Influence of laser re-melting on density, surface quality and microstructure Rapid Prototyping Journal
Evren Yasa, Jan Deckers and Jean-Pierre Kruth Volume 17 · Number 5 · 2011 · 312 –327
When laser re-melting is applied, the layers are apparently seen a re-melted zone was formed where the scan tracks of LSR
with borders of dark lines, whereas the layers are not were clearly seen. The thickness of this zone highly depended
distinguishable in SLM parts with no laser re-melting whereby on the selected parameters, especially, the scan speed and
only the borders of the melted scan tracks are visible (Figure 16). laser power. As the scan speed was decreased or laser power
The layers in laser re-melting are actually visible as horizontal was increased, the re-melted depth became significantly
dark lines due to very low scan spacing (5-10 per cent). The higher. The scan spacing changed the overlap between
cross-section of multiple scan tracks that overlap significantly successive tracks, but the depth stayed almost constant as
appear as a line instead of curved melt lines which is also shown evident from Figure 21, where two micrographs from two
in Figure 10. In Figure 19, the cross-sectional view of the part samples re-melted exactly with same parameters, except the
which was re-melted with a scan spacing factor of 20 per cent scan spacing, are shown. Another important observation from
depicts less visible horizontal bands compared to the parts with a the micrographs of LSR parts was the densification of the
scan spacing of 5 or 10 per cent. Owing to the reason that laser re-melted zone where a full density was achieved, in other
re-melting efficiently improves the density of SLM parts by words, no pore was encountered.
removing pores formed between neighbouring melt pools in the The cellular/dendritic structure was also visible throughout
borders (see arrows in Figure 20), lamellar structures are desired the re-melted zone. The cell-size was finer in parts with LSR
for improved density leading to better mechanical properties than the one of the parts with no laser re-melting. It was
and avoiding unexpected failures of SLM parts. SEM images equiaxed and homogenously visible throughout the re-melted
of two parts exposed to laser re-melting with different zone. The SEM images of a sample part are shown in
parameters shown in Figure 21 clearly show the lamellar Figure 22, where the overlapping laser tracks in the re-melted
structure where no irregular pore is present. zone are clearly visualized with a cellular/dendritic
3.4.2 Laser surface re-melting (LSR) microstructure with a cell size smaller than 1 mm.
Downloaded by Universite Laval At 05:01 04 March 2015 (PT)
Some examples of SLM parts with LSR are shown in To sum up, laser re-melting often refined the
Figures 20 and 21 with the parameters used for LSR. microstructure. LSR also assisted in elimination of pores in
When the last layer was subjected to multiple laser re-melting, the outer part surface (Figures 23 and 24).
Figure 20 SEM image of an SLM part without laser re-melting showing pores between the melt pools
20 µm
Figure 21 SEM images of two SLM part with laser re-melting at different parameters showing almost full density
10 mm 10 mm
(a) (b)
Notes: (a) 35 A, 200 mm/s, a1 = 0.1, 1 scan; (b) 38 A, 200 mm/s, a1 = 0.1, 3 scans
323
Influence of laser re-melting on density, surface quality and microstructure Rapid Prototyping Journal
Evren Yasa, Jan Deckers and Jean-Pierre Kruth Volume 17 · Number 5 · 2011 · 312 –327
Re-molten zone
200 µm
Building axis
Downloaded by Universite Laval At 05:01 04 March 2015 (PT)
200 µm
Building axis
324
Influence of laser re-melting on density, surface quality and microstructure Rapid Prototyping Journal
Evren Yasa, Jan Deckers and Jean-Pierre Kruth Volume 17 · Number 5 · 2011 · 312 –327
200 µm
Building axis
Downloaded by Universite Laval At 05:01 04 March 2015 (PT)
200 µm
Building axis
Figure 24 SEM pictures of the LSR part with 200 mm/s, 39 A (105 W), a1 ¼ 0.1 and ten layers
(a) (b)
Notes: (a) Low magnification; (b) high magnification
325
Influence of laser re-melting on density, surface quality and microstructure Rapid Prototyping Journal
Evren Yasa, Jan Deckers and Jean-Pierre Kruth Volume 17 · Number 5 · 2011 · 312 –327
Additionally, laser re-melting is an easy method to improve International Solid Freeform Fabrication Symposium, Austin,
the surface quality significantly (more than 90 per cent) TX, USA, pp. 321-32.
without removing the parts from the SLM machine and any Kruth, J.-P., Froyen, L., van Vaerenbergh, J., Mercelis, P.,
fixation errors when applied on top surfaces after the parts are Rombouts, M. and Lauwers, B. (2004), “Selective laser
completely built by SLM. It can also be easily applied on the melting of iron-based powder”, Journal of Materials
inclined or curved surfaces after the surrounding powder is Processing Technology, Vol. 149 Nos 1-3, pp. 616-22.
blown away around the parts. With a few-basic software Lamikiz, A., Sanchez, J.A., Lopez de Lacalle, L.N. and
changes to allow the movement of the building platform to Arana, J.L. (2007), “Laser polishing of parts built up by
keep the laser beam in focus, it can be applied automatically. selective laser sintering”, Machine Tools and Manufacture,
For surface quality enhancement, the production time is not Vol. 47 Nos 12/13, pp. 2040-50.
necessarily affected since the laser re-melting is applied only Lawrence, J. and Li, L. (2001), “A laser based technique for
on the outer surfaces of the SLM parts. Surface quality the coating of mild steel with a vitreous enamel”, Surface
enhancement by laser re-melting also leads to a fully dense and Coatings Technology, Vol. 140, pp. 238-43.
shell around the part. Since surface porosity is known to affect Morgan, R.H., Papworth, A.J., Sutcliffe, C., Fox, P. and
both the stress distribution and deformation of subsurface O’Neill, W. (2002), “High density net shape components
layers leading to subsurface crack formation and propagation, by direct laser re-melting of single phase powders”, Journal
fully dense shell is especially important for applications of Materials Science, Vol. 37, pp. 3093-100.
requiring high-wear resistance. Not only wear, but also other Nicolas, G., Autric, M., Marine, W. and Shafeev, G.A.
surface properties, such as thermal and electrical conductivity (1997), “Laser induced surface modifications on ZrO
are highly dependent on the surface porosity. ceramics”, Applied Surface Science, Vols. 109/110,
The laser re-melting experiments applied on AISI 316L pp. 289-92.
parts also showed that microhardness was improved in the Pinto, M.A., Cheung, N., Ierardi, M.C.F. and Garcia, A.
laser re-melted zone if sufficiently high-energy densities were (2003), “Microstructural and hardness investigation of an
provided, probably due to a fine-cell size encountered in the aluminum-copper alloy processed by laser surface melting”,
microstructure. Materials Characterization, Vol. 50 Nos 2/3, pp. 249-53.
Ramos-Grez, J.A. and Bourell, D.L. (2004), “Reducing
surface roughness of metallic freeform-fabricated parts
References using non-tactile finishing methods”, International Journal
Braga, F.J.C., Marques, R.F.C., Filho, E.A. and of Materials and Product Technology, Vol. 21 No. 4,
Guastaldi, A.C. (2007), “Surface modification of Ti dental pp. 297-316.
implants by Nd:YVO4 laser irradiation”, Applied Surface Roemer, G.R.B.E., Huis in’t Veld, A.J., Meijer, J. and
Science, Vol. 253, pp. 9203-8. Groenendijk, M.N.W. (2009), “On the formation of laser
Das, S. (2003), “Physical aspects of process control in induced self-organizing nanostructures”, CIRP Annals –
selective laser sintering of metals”, Advanced Engineering Manufacturing Technology, Vol. 58, pp. 201-4.
Materials, Vol. 5 No. 10, pp. 701-11. Rombouts, M. (2006), “Selective laser sintering/melting of
Felgueroso, D., Vijande, R., Cuetos, J.M., Tucho, R. and iron-based powders”, PhD thesis, Katholieke Univesiteit
Hernandez, A. (2008), “Parallel laser melted tracks: effects Leuven, Leuven.
on the wear behaviour of plasma-sprayed Ni-based Tang, C.H., Cheng, F.T. and Man, H.C. (2004),
coatings”, Wear, Vol. 264, pp. 247-63. “Improvement in cavitation erosion resistance of a copper
Grabowski, A., Formanek, B., Sozanska, M. and Nowak, M. based propeller alloy by laser surface melting”, Surface and
(2006), “Laser re-melting of Al-Fe-TiO3 composite powder Coatings Technolog, Vol. 182 Nos 2/3, pp. 300-7.
326
Influence of laser re-melting on density, surface quality and microstructure Rapid Prototyping Journal
Evren Yasa, Jan Deckers and Jean-Pierre Kruth Volume 17 · Number 5 · 2011 · 312 –327
Taylor, C.M. (2004), “Direct laser sintering of stainless steel: composite by laser surface re-melting”, Applied Surface
thermal experiments and numerical modeling”, PhD thesis, Science, Vol. 253 No. 9, pp. 4409-14.
School of Mechanical Engineering, University of Leeds, Xu, W.L., Yue, T.M., Man, H.C. and Chan, C.P. (2006),
Leeds. “Laser surface melting of aluminium alloy 6013 for
Triantafyllidis, D., Li, L. and Stott, F.H. (2005), “The effects improving pitting corrosion fatigue resistance”, Surface
of laser-induced modification of surface roughness and Coatings Technology, Vol. 200 Nos 16/17, pp. 5077-86.
of Al2O3-based ceramics on fluid contact angle”, Yasa, E., Deckers, J., Craeghs, T., Badrossamay, M. and
Materials Science & Engineering A, Vol. 390, pp. 271-7. Kruth, J.P. (2009), “Investigation on occurrence of elevated
Ukar, E., Lamikiz, A., Lopez de Lacalle, L.N., del Pozo, D. edges in selective laser melting”, International Solid Freeform
Fabrication Symposium, Austin, TX, USA, pp. 673-85.
and Arana, J.L. (2010), “Laser polishing of tool steel with
Zhang, Y., Chen, J., Lei, W. and Xv, R. (2008), “Effect of
CO2 laser and high-power diode laser”, International
laser surface melting on friction and wear behaviour of
Journal of Machine Tools & Manufacture, Vol. 50 No. 1,
AM50 magnesium alloy”, Surface and Coatings Technology,
pp. 115-25. Vol. 202, pp. 3175-9.
Wissenbach, K., Willenborg, E. and Pirch, N. (2006),
“Method for smoothing and polishing by treating them
with energetic radiation”, US patent 2006/0081573.
Corresponding author
Xianqing, Y., Chengjun, Z., Xuefeng, S., Manping, H. and Evren Yasa can be contacted at: evren.yasa@mech.kuleuven.
Jianguo, M. (2007), “Microstructure evolution of WC/steel be
Downloaded by Universite Laval At 05:01 04 March 2015 (PT)
327
This article has been cited by:
1. Eberhard Abele, Hanns A. Stoffregen, Michael Kniepkamp, Sebastian Lang, Manfred Hampe. 2015. Selective laser melting for
manufacturing of thin-walled porous elements. Journal of Materials Processing Technology 215, 114-122. [CrossRef]
2. Donghua Dai, Dongdong Gu. 2015. Tailoring surface quality through mass and momentum transfer modeling using a volume
of fluid method in selective laser melting of TiC/AlSi10Mg powder. International Journal of Machine Tools and Manufacture
88, 95-107. [CrossRef]
3. I. Yadroitsev, P. Krakhmalev, I. Yadroitsava. 2014. Hierarchical design principles of selective laser melting for high quality metallic
objects. Additive Manufacturing . [CrossRef]
4. Chandrika Kamath, Bassem El-dasher, Gilbert F. Gallegos, Wayne E. King, Aaron Sisto. 2014. Density of additively-
manufactured, 316L SS parts using laser powder-bed fusion at powers up to 400 W. The International Journal of Advanced
Manufacturing Technology 74, 65-78. [CrossRef]
5. P. Li, Z. Wang, N. Petrinic, C.R. Siviour. 2014. Deformation behaviour of stainless steel microlattice structures by selective laser
melting. Materials Science and Engineering: A 614, 116-121. [CrossRef]
6. Evgueni V. Bordatchev, Abdullah M. K. Hafiz, O. Remus Tutunea-Fatan. 2014. Performance of laser polishing in finishing of
metallic surfaces. The International Journal of Advanced Manufacturing Technology 73:1-4, 35-52. [CrossRef]
7. X.J. Wang, L.C. Zhang, M.H. Fang, T.B. Sercombe. 2014. The effect of atmosphere on the structure and properties of a selective
laser melted Al–12Si alloy. Materials Science and Engineering: A 597, 370-375. [CrossRef]
Downloaded by Universite Laval At 05:01 04 March 2015 (PT)
8. H. K. Rafi, N. V. Karthik, Haijun Gong, Thomas L. Starr, Brent E. Stucker. 2013. Microstructures and Mechanical Properties
of Ti6Al4V Parts Fabricated by Selective Laser Melting and Electron Beam Melting. Journal of Materials Engineering and
Performance 22:12, 3872-3883. [CrossRef]
9. Joakim Karlsson, Anders Snis, Håkan Engqvist, Jukka Lausmaa. 2013. Characterization and comparison of materials produced
by Electron Beam Melting (EBM) of two different Ti–6Al–4V powder fractions. Journal of Materials Processing Technology 213,
2109-2118. [CrossRef]
10. H. Khalid Rafi, Thomas L. Starr, Brent E. Stucker. 2013. A comparison of the tensile, fatigue, and fracture behavior of Ti–
6Al–4V and 15-5 PH stainless steel parts made by selective laser melting. The International Journal of Advanced Manufacturing
Technology 69:5-8, 1299-1309. [CrossRef]
11. S. Dadbakhsh, L. Hao. 2012. Effect of Al alloys on selective laser melting behaviour and microstructure of in situ formed particle
reinforced composites. Journal of Alloys and Compounds 541, 328-334. [CrossRef]
12. Bey Vrancken, Lore Thijs, Jean-Pierre Kruth, Jan Van Humbeeck. 2012. Heat treatment of Ti6Al4V produced by Selective
Laser Melting: Microstructure and mechanical properties. Journal of Alloys and Compounds 541, 177-185. [CrossRef]
13. Jan Deckers, Jean-Pierre Kruth, Khuram Shahzad, Jef Vleugels. 2012. Density improvement of alumina parts produced through
selective laser sintering of alumina-polyamide composite powder. CIRP Annals - Manufacturing Technology 61:1, 211-214.
[CrossRef]