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Atomic and Nuclear Physics

Electron Spin Resonance
The equipment for this topic set provides
the basis for the investigations of the
microphysical quantities of the electron.
With the resonance method used, the dif-
ference in energy between two spins can
be measured directly. For this a paramag-
netic substance (e.g. DPPH = diphenyl-
pikryl-hydrazyl) is placed between a pair of
Helmholtz coils (constant field with 50 Hz
Títulos relacionados
range 15 to 150 MHz). The r.f. coil is part of
a high quality parallel resonance circuit. In
the resonant case the sample absorbs
r.f.energy, thus changing the AC resistance
(damping) of the oscillatory circuit. By trig-
gering the two-channel oscilloscope with the
modulation signal of the magnetic field it is
possible to simultaneously display the cur-
ves for field modulation and ESR absorption
The resonance frequencies f at different
field strengths B are directly indicated on a
digital frequency counter, built-in to the
ESR unit. From the f-B  graph the gyro-
magnetic ratio (g -factor) can be deter-
mined for the particular electron spin
system.


modulation) and an r.f. coil (frequency (see fig. below).

Markem_Imaje_45 Sound Holes MIT 12 AD_GT3L_Man- 10.1.1.619.9544 22120e Cellule Ningbo 211640385-Erbe-
HW EN 12-07… Ant Electronics… VIO300S-Servic…

Determination of the g factor

Topics
 – Resonance absorption of an r.f. tuned
circuit
 – Electron spin resonance (resonant
frequency as a function of magnetic field
strength, determination of the g -factor)

Equipment list:
1 ESR basic unit 514 550
1 ESR control unit 514 570
1 Pair of Helmholtz coils 555 06 0
2 Multimeters M 2012 531 560
1 Two-channel oscilloscope 575 211
3 Saddle bases 300 110
1 Insulated stand rod 590 130
2 Screened cables BNC, 4 mm 575 2 40
3 Conn. leads, 25 cm 501 230
Resonance frequency f as a function of magnetic Oscilloscope display 5 Conn. leads, 50 cm 501 280
resonant field strength B 

428 B

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Atomic and Nuclear Physics

514 55 ESR basic unit
For experiments on electron spin resonance
in conjunction with the ESR control unit
(514 57) or the ESR adapter (51456).
 Power supply: 12 V; 175 mA
 Frequency range of each coil:
approx. 13 to 30 MHz,
approx. 30 to 75 MHz,
approx. 75 to 130 MHz
 Voltage at RF coil:
approx. 6 Vpp (with respect to earth) at 13 MHz
and max. amplitude setting
 ESR signal:
approx. 1 to 6 V (frequency dependent)
 Frequency divider: 1000 : 1
 Frequency response for digital counter: TTL
 Resonance meter current (DC):
approx. 100 µA
 Frequency range of the passive
resonant circuit: 10 to 50 MHz
 Dimensions of the probe head:
13 cm x 7 cm 4 cm
 Stand length: 18.5 cm
 Weight: approx. 0.7 kg

Scope of delivery: 
1 ESR probe head (variable high-frequency
transmitter, frequency divider and low-
frequency signal amplifier)
3 Plug-in coils for different frequency
514 57 514 55 on 300 11
ranges
1 Measuring cable, for employing the unit
as a resonance meter
1 Passive electric resonant circuit for inves- Está leyendo una previsualización
tigating the dependence of the resonant
frequency on the magnetic field
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51456 tu prueba GRATUITA de 30 días 55506

514 57 ESR control unit
Power supply unit for the RF transmitter of
the ESR basic unit (514 55) and the pair of
Helmholtz coils (555 06) for experiments on
electron spin resonance; integrated high-fre-
quency counter with digital display and
phase shifter between the oscilloscope-
compatible output voltages, which are
proportional to the RF amplitude or the coil
current.
 Power supply for magnetic field:
0 to 10 V DC,
0 to 5 V AC, continuously adjustable
Current: max 3 A (no overload protection)
 Adjustable phase difference: 0 to 90°
 Frequency display: 4 decades (MHz)
 Connection:
115/230 V, 50/60 Hz, via mains cable
514 56 ESR adapter
For connection of the ESR basic unit
(514 55) to other power supply units with
4 mm sockets and meters with BNC
sockets; required when the ESR control unit
(514 57) is not used.
A built-in frequency output allows high fre-
quency measurements with conventional
counters (e.g. 575 40 or 575 45).
 Output: 5-pole multiple socket for ESR basic unit
 Signal output: BNC socket
 Frequency output: BNC socket
 Connection: + 1 2 V/0 V/–12 V, via 4 mm sockets
 Dimensions: 9.5 cm x 7.5 cm x 2.5 cm
Additionally required: 
DC power supply
0 to 15 V........................................ 521 45
     
55506 Pair of Helmholtz coils
The pair of coils are used to produce a
homogeneous magnetic field of variable
strength in which the deflection of electrons
within tubes 555 07–17 can be shown and
investigated, also used with the apparatus
for electron spin resonance (514 55). For
use with stand (555 05).
 Number of turns per coil: 320
 Max. continuous current: 1.5 A (U = 10 V)
 Max. short-time current: 2 A (U = 15 V)
 Average diameter: 13.5 cm
 Stand rod: 14.5 cm x 8 mm dia.
 Connection two 4-mm sockets on each coil

 Fuses:
Variable extra low voltage
for 230 V: T 0.8 B
for 115 V; T 1.6 D transformer S.................................... 521 35
 Dimensions: 30 cm x 21 cm x 23 cm Counter P ..........................................57545
 Weight: approx. 6.2 kg Stopclock...........................................313 07

428 C

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