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Automated Cleveland Open Cup Flash Point Tester

Model aco-8/aco-8 as

Instruction Manual
Rev.2.26 200221

IMPORTANT:
*This Manual contains important technical information
as well as safety information.
*Read this Manual thoroughly before use, and store in
a safe place for future reference.
TANAKA SCIENTIFIC LIMITED

FOREWORD
Thank you for purchasing the Automated Flash Point Tester Model aco-8 from Tanaka Scientific
Limited.
This instruction manual provides necessary information for using the aco-8.
Read this manual thoroughly before use and ensure that you have understood its contents.
This manual employs the following precautionary notation. For your safety, ensure that you
understand these precautions and heed them at all times.

! WARNING:・・・・・・・・・・
Warnings indicate a significant risk of death or serious physical
injury if the information is ignored.
! CAUTION:・・・・・・・・・・
Cautions indicate a significant risk of physical injury or property
damage if the information is ignored.

USES
! Warning: Use the product only to measure flash point and fire point as
prescribed under ISO 2592/IP36 “Determination of flash and
fire points - Cleveland open cup method”, ASTM D92
“Standard Test Method for Flash and Fire Points by Cleveland
Open Cup Tester”.

This instrument has automated test processes corresponding


to those prescribed in ISO 2592/IP36 “Determination of flash
and fire points - Cleveland open cup method”, ASTM D92
“Standard Test Method for Flash and Fire Points by Cleveland
Open Cup Tester” for the purpose of obtaining flash and fire
points only. This product is not to be used for any other
purpose.

1
ABOUT THIS INSTRUCTION MANUAL
 This manual is intended for all operators of the aco-8.
 The reader is assumed to have sufficient knowledge of ISO/IP and ASTM procedures and
standards as well as knowledge of the correct handling procedures for hazardous materials.

 The content this manual is subject to change without notice due to enhancements to the
performance and functionality of the instrument.

 If this manual is lost or damaged, contact Tanaka Scientific Limited or an authorized distributor
for a replacement copy.

 The contents of this manual have been thoroughly reviewed. If any pages are missing, out of
order, or the manual contains spelling, grammatical or descriptive errors, please contact Tanaka
Scientific Limited or an authorized distributor.

BEFORE USE
 Before using this instrument, ensure that you have read this manual thoroughly and have
understood all of the content. If you have any questions, be sure to contact Tanaka Scientific
Limited or an authorized distributor

 Keep this manual in a safe, easily accessible place.

 This product is to be used for its intended purpose only. Adhere strictly to all procedures given in
this manual.

 Ensure that you understand and abide by all warnings and cautions given in this manual.

2
WARNINGS AND CAUTIONS FOR SAFE USE
Failure to follow all of the warnings and cautions listed below may result in damage to the instrument
and/or serious personal injury. Tanaka Scientific Limited will not assume any responsibility for faults
or accidents arising from failure to adhere to these instructions.

Installation Environment
! Warning: The instrument must be installed to the place where there is
ventilation.
Flammable harmful vapor and toxic gas are generated by a
sample heating, an operator will be in danger of harmful gas
poisoning if ventilation is insufficient.
When testing a sample which may generate toxic gas, give
protection by appropriate PPE(Person Protect Equipment).
! Warning: The instrument must be installed on a flat, sturdy surface to
prevent the instrument from falling over.
Do not leave combustible material near the instrument.
Place fire extinguisher near the instrument to protect fire
disaster.

Gas Piping
! Caution: The gas pressure supplied to the instrument must be lower
than 9.8kPa.
Ensure that each joint of the gas hose is securely fastened to
prevent pulling out of hose by high pressure.

Electric Connection
! Warning: Observe the following instructions when handling AC power
cord and electric connections:
 Do not connect or disconnect AC power cord or electric
connections when the mains power is ON.
 Do not handle any cords or electrical connections with wet
hands.
 Be sure to use the plug to remove cord. Never use the
cord to pull a plug from an outlet.
 Do not place heavy items on cord.
3
 Do not use force to bend any cord.
 Ensure that all electric connections (plugs, sockets,
connectors, etc.) are free of dust.
 Keep cord and electrical connections free of water and
other liquids.
Failure to adhere to the above precautions may result in
electric shock, damage to the instrument, cords, and/or fire
due to overheating.
! Warning: Ensure that supply voltage meets the specifications of the
product. Do not turn the power on until all electric connections
are secured. Incorrect power supply specifications or loose
electric connections may damage the instrument and result in
electric shock and/or other electrical accidents.

! Warning: Ensure all ground wires are securely grounded.


Loose or disconnected ground wires may result in electric
shock.
Never connect ground wires to gas pipes, as this may result in
fire or an explosion.
Ground wires may be connected to one of the following:
 Ground terminal of a power outlet
 Copper bar buried 65 cm or more underground

4
Handling Precautions

! Caution: Ensure that an expected flash point is entered prior to every


test run. If an expected flash point is not entered or the value
entered is much greater than the actual flash point, the
specimen catches a fire at the first application, and then the
instrument is destroyed by fire.

! Warning: Never touch the test cup with bare hands after the test end.
The sample cup may still hot and the operator gets burned.
Use gloves and hold the test cup handle for operator’s safety.

! Warning: Never discard hot sample to a waste tank. Sample in the


waste tank may blow up.

Operational Precautions
! Warning: Never touch around test cup during testing. An operator gets
burned.
! Warning: Never run the tester unattended. The specimen may catch a
fire and blaze up by some sort of cause. It is essential that at
least one-trained personnel be present in the test room.
! Warning: If the instrument makes any abnormal noises or exhibits any
abnormal behavior, stop operation immediately, turn the
power off at the mains, and contact Tanaka Scientific Limited
or an authorized distributor.

Consumables, Accessories and Replacement Parts


! Caution: Use only Tanaka Scientific Limited genuine consumables,
parts and accessories or such parts as recommended by
Tanaka Scientific Limited.

5
Repairs, Alterations and Maintenance
! Warning: Do not make any modifications or alterations to the instrument
without the approval of Tanaka Scientific Limited.

! Warning: Do not attempt to repair the instrument yourself. In the event


that the instrument exhibits any abnormal behavior
whatsoever, contact Tanaka Scientific Limited or an
authorized distributor.

! Warning: Only Tanaka Scientific Limited service personnel or


authorized representatives are to repair or maintain the
instrument.

6
CONTENTS
FOREWORD .................................................................................................................... 1
USES ............................................................................................................................... 1
ABOUT THIS INSTRUCTION MANUAL .......................................................................... 2
BEFORE USE .................................................................................................................. 2
WARNINGS AND CAUTIONS FOR SAFE USE .............................................................. 3
CONTENTS ..................................................................................................................... 7
1. Section Names and Function .................................................................................. 9
2. Installation ............................................................................................................ 12
2.1 Installation Site .......................................................................................................................12
 An area subject to rapid changes in ambient temperature ....................................................12
2.2 Install Thermal Insulator .........................................................................................................13
2.3 Gas Piping ..............................................................................................................................13
2.4 Electric Connections ...............................................................................................................14
3. Daily Check .......................................................................................................... 16
4. Test Preparation ................................................................................................... 19
4.1 Power ON ...............................................................................................................................19
4.2 Setting of Expected Flash Point .............................................................................................20
4.3 Entry of Sample ID and Operator Name (NEW) ....................................................................21
4.4 Selecting of Test Method ........................................................................................................22
4.5 Entering Sample Information ..................................................................................................26
4.6 Preparation of Test Cup and sample .....................................................................................27
5. Test Sequence...................................................................................................... 28
5.1 Test Start ................................................................................................................................28
5.2 Test Sequence .......................................................................................................................30
5.3 Flash Detection.......................................................................................................................30
5.4 Fire Point Detection ................................................................................................................34
5.5 Flash Point Detection By manual detection ...........................................................................35
5.6 Test End .................................................................................................................................36
6. Test Parameter Setting ......................................................................................... 37
7. Data Storage......................................................................................................... 39
8. Maintenance ......................................................................................................... 40
8.1 Temperature Correction.............................................................................................................41
8.2 Date and Time Setting .............................................................................................................41
8.3 Barometric Pressure Correction ............................................................................................42
8.4 RS-232C Settings .....................................................................................................................42
8.5 USB Settings ............................................................................................................................47
8.6 Password Settings ...................................................................................................................48
8.7 Calibration Ticket (NEW) .........................................................................................................49
7
9. User Custom Method ............................................................................................ 50
10. Equipment Information .......................................................................................... 51
11. In Case of Abnormal Operation or Trouble ........................................................... 52
12. Periodic Inspection, Adjustment and After Sales Service ..................................... 54
12.1 Periodic Inspection ................................................................................................................54
12.2 Adjustment ...............................................................................................................................54
13. After-sales Service................................................................................................ 54
14. Other Cautions...................................................................................................... 55
14.1 Caution when this instrument is not used for a long time ................................................55
14.2 Precaution in case of Loss of Instruction Manual .............................................................55
14.3 Caution when Transferring This Instrument.......................................................................55
14.4 Caution when Discarding This Instrument .........................................................................55
15. Specification ......................................................................................................... 56
Product Warranty

8
1. Section Names and Function

Needle Valve for


Arm Test Flame
Lift this arm up when
Adjusts test flame size
the test cup is set

Heater/Cooler Output
Dual Pilot
Indicator
Lights to ignite test
flame when test start Lights when heater is ON

Thermofuse
Detects blaze up of
specimen

Display
Fire Containment
Displays test status
and result as well as Lid Reset Knob
test parameters. Push this knob to reset
the lid to original position

MAIN Switch
Used for switching
power source to the
instrument
Emergency Switch
Fig. 1 Front-Right View
Activates fire
containment lid manually

Fire Containment Arm Handle


Lid Handle
Hold here when
Lift/Lower the arm
Activates when tester
detects fire
Test Cup Handle
Hold here when
set/remove the test cup

Flame Size Comparison


Test Flame Nozzle Bead
Swing over the test Adjust test flame size to
this bead

Panel Sheet Switch


USB Port
Operation keys are
Used for connecting to located
Keyboard or USB Flash
Memory

Fig. 2 Front-Left View

9
Temperature Sensor
Senses specimen temperature

Aco-8as only
Skimmer Shaft
Skimmer Paddle
Removes surface skin
Remove this when skimmer
is not used

Flash Detector Rings


Detects a flash by ionic current

Fig. 3 Around Test Cup

RS-232C Port
Gas Inlet
(25pin)

AC Power Inlet

Fig. 4 Rear View


10
(4)

Cleveland Open Cup


EXP FP
Sample ID 01

Operator 01
OK (5)
Method ASTM Normal
(1)

23.4 oC

C O O L A P P L M E N U start reset
Gas 2013/12/06(Fri)

Fig. 5 Panel
(2) (6) (3)

(1) Color LCD Display:


Displays test mode, specimen temperature, flash point (when blinking), expected flash point, trouble
message, etc..

(2) START Key:


Used when starting test.

(3) RESET Key:


Used when returning stand-by status. (e.g. stopping a test, stopping a cooling)

(4) Left-Right Keys:


Used when moving cursor and selecting items.

(5) Up-Down Keys:


Used when increasing/decreasing numeric figures and selecting items.

(6) OK key
Used when changed value is settled

11
2. Installation
2.1 Installation Site

OVERVOLTAGE CATEGOLY II, POLLUTION DEGREE 2, Altitude up to 2000m

! Warning: The instrument must be installed to the place where there is


ventilation.
Flammable harmful vapor and toxic gas are generated by a sample heating,
an operator will be in danger of harmful gas poisoning if
ventilation is insufficient.
When testing a sample which may generate toxic gas, give protection by
appropriate PPE(Person Protect Equipment).
! Warning: The instrument must be installed on a flat, sturdy surface to
prevent the instrument from falling over.
Do not leave combustible material near the instrument.
Place fire extinguisher near the instrument to protect fire disaster.

Install the Tester on a draft-free, level and stable table. The Tester needs to be placed at least 20cm
away from other objects.
Ambient temperature to be 10-30oC and RH to be less than 90% (no condensation)
The following locations should be avoided as the installation site:
 An area exposed to direct the sun
 An area with poor ventilation
 An area with dusty air
 An area higher than 2000m
 An area subject to rapid changes in ambient temperature

12
2.2 Install Thermal Insulator
Install thermal insulator ④ on the brass heating plate ① so that flame size comparison bead ②
and guide pin ③ passes to 2 small holes (4mmD) of the thermal insulation. There is no front/back
side for the thermal insulator.


① ④

Fig. 6 Thermal Insulator

2.3 Gas Piping

! Caution: The gas pressure supplied to the instrument must be lower


than 9.8kPa.
Ensure that each joint of the gas hose is securely fastened
to prevent pulling out of hose by high pressure.

Using the rubber hose supplied for gas, connect the gas source (LP gas or Natural gas) and the gas
inlet nipple on the rear panel of the Test Unit. Then fasten both ends with hose bands. See Fig. 4.
This tester does not have gas leak sensor. Do not use old/damaged rubber hose which has a risk of
gas leak.

13
2.4 Electric Connections

! Warning: Observe the following instructions when handling AC


power cord and electric connections:
 Do not connect or disconnect AC power cord or electric
connections when the mains power is ON.
 Do not handle any cords or electrical connections with wet
hands.
 Be sure to use the plug to remove cord. Never use the
cord to pull a plug from an outlet.
 Do not place heavy items on cord.
 Do not use force to bend any cord.
 Ensure that all electric connections (plugs, sockets,
connectors, etc.) are free of dust.
 Keep cord and electrical connections free of water and
other liquids.
Failure to adhere to the above precautions may result in
electric shock, damage to the instrument, cords, and/or fire
due to overheating.
! Warning: Ensure that supply voltage meets the specifications of the
product. Do not turn the power on until all electric connections
are secured. Incorrect power supply specifications or loose
electric connections may damage the instrument and result in
electric shock and/or other electrical accidents.

! Warning: Ensure all ground wires are securely grounded.


Loose or disconnected ground wires may result in electric
shock.
Never connect ground wires to gas pipes, as this may result in
fire or an explosion.
Ground wires may be connected to one of the following:
 Ground terminal of a power outlet
 Copper bar buried 65 cm or more underground

14
Confirm the voltage of the serial number label located right side of the instrument and your electric
source.
Plug in the AC power cord to the instrument AC inlet and then other side to an electric outlet(1). Be
sure to get grounding to prevent an accident.

Note : The power consumption of the aco-8 is 1.0kW . Be careful the total power consumption of the
outlet not exceed to the capacity of the outlet

15
3. Daily Check

Please check following matters everyday when power ON the instrument

Table 1 Checklist
Item Check that…

Appearance Each part of the instrument is undamaged


Gas Piping No damage on the gas hose
Hose band is securely fastened
Electric Connection All power cords and cables are free of damage
No gap between AC plug and outlet
ground wires are securely grounded
Each Function <Power ON the instrument>
Stand-by screen displays normally
Each key functions correctly
Expected Flash Point can be entered correctly
Emergency Switch works correctly

! Warning: If the instrument makes any abnormal noises or exhibits


any abnormal behavior, stop operation immediately, turn the
power off at the mains, and contact Tanaka Scientific Limited or
an authorized distributor.

16
About Fire Containment Lid

This unit has a fire containment lid for preventing of expanse of fire when;
① Sample catches a fire, and then thermofuse blows.
 Error message appears on the display and beeps continuously. Confirm that a fire is
extinguished and then push Emergency switch again to alarm clear, push reset to
return standby screen.
② Detects fire point
 Terminate the test, and then flash point and fire point are displayed alternately.
③ Push Emergency Switch
 The same as ①. Push Emergency switch again to alarm clear, push reset to return
standby screen.

T R O U B L E

THERMOFUSE BLOWN

Fig. 7 Thermofuse 2012/02/27 14:58

Fig. 8 Trouble Screen

Fig. 9 Emergency Switch Fig. 10 Fire Containment Lid

17
<How to reset Fire Containment Lid>
Procedure of resetting the fire containment lid is as follows.
① When the fire containment lid activates,
display shows error message as shown on left,
then buzzer beeps continuously.
T R O U B L
Or display shows flash point and fire point.

THERMOFUSE BLOWN

2012/02/27/ 14:58

Fig. 11 Error Message

② Push Emergency switch to clear alarm when


display shows “TROUBLE”.
Push reset key to return stand-by screen.

Fig. 12 Emergency Switch


③ Push the reset knob.
Note- Leave test cup on the heating plate.

Fig. 13 Reset of Fire Containment Lid

18
4. Test Preparation

4.1 Power ON
Turn the MAIN switch ON. Stand-by screen as in Fig. 14 appears on the display.

Cleveland Open Cup


EXP FP Expected Flash
Point
Sample ID 01
Sample ID
Operator 01 Test Method
Method ASTM Normal
Specimen

23.4
Temperature
/Flash Point o
C
C O O L A P P L M E N U

Ignition Source Gas 2013/12/06 (Fri)

COOL Button Ignition Source MENU Button


Application Button

Fig. 14 Stand-by Screen

Expected Flash Point: Enter expected flash point (EXP FP) here before a test start.
When MAIN switch is turned ON or reset key is pressed, the display returns to “”.
Sample ID: Displays Sample ID.
Test Method: Displays Test Method.
Specimen Temperature and Flash Point: Displays the temperature measured by Temperature
Sensor. Once flash is detected, the flash point blinks/holds this area until reset.
Color of the background of the temperature display changes:
White : When stand-by
Orange : When test is in progress
Green : When cooling
Ignition Source: Displays “Gas” only.
COOL Button: Used when cooling is performed manually.
Ignition Source Application Button: Used when ignition source is applied manually.
MENU Button: Used when go to MENU screen.

19
4.2 Setting of Expected Flash Point

! Caution: Ensure that an expected flash point is entered prior to


every test run. If an expected flash point is not entered or the
value entered is much greater than the actual flash point, the
specimen catches a fire at the first application, and then the
instrument is destroyed by fire.

The correct expected flash point entering is absolutely imperative. Enter/confirm the expected flash
point before each test. The expected flash point (EXP FP) is displayed in three-digit figure in integer.
When altering the expected flash point, press the Up-Down key to move the yellow cursor to EXP
FP and press OK key. The numeric figure change from to 000. After the cursor is moved
to numeric figures of EXP FP, move the digit with Right-Left key and increase/decrease the value
with the Up-Down keys. No numeric figures above 400 (760 in oF) can be set.

Enter approximate expected flash point even if run a test with SPE method. If expected flash point is
unknown, use SPE method and then set higher expected flash point. When selecting SPE method,
ignition source application will be done just after start a test. So, a test will be done without worry.
The other way, if entered expected flash point is too low, test will be canceled by safety over cut
function. (Expected Flash Point+ 30oC(+ 60 oF)).

20
4.3 Entry of Sample ID and Operator Name (NEW)
Sample ID can be entered up to 12 letters. The letter which can be entered is following 43 characters
in total. Each instrument is initialized to “01” prior to shipping.

Table 2 Characters
A B C D E F G H I J K L M N O

P Q R S T U V W X Y Z # + - %

/  0 1  3 4 5 6 7 8 9

(1) Move the yellow cursor to Sample ID / Operator


(2) Press OK key, then the yellow cursor moves to entry field of
Sample ID/Operator name.

(When Sample ID/Operator Name already registered)


Sample ID LUBRICANT [09]
(3) Registered Sample ID/Operator name can be selected
by Up & Down key when Yellow cursor is in large size. Large Cursor

*“01” is registered as default in the list No [01].


(When entering a letter one by one)
Sample ID 01 + - [01]
(4) Press Right-Left Key, then the cursor becomes
nas
reduced in size (small cursor).
Small Cursor
The letter can be changed per single digit.
(How to overwrite/register/delete)
Sample ID TANAKA + - [01]
(5) Select the List No of which you want to change the nas
Change letters and press OK ↓
name. Change the letter and press OK to overwrite Sample ID TANAKA + - [01]
the new name to the List No. nas
(6) Press OK key when the yellow cursor is on plus (+),
Operator TANAKA + - [01]
then the Sample ID/Operator Name is registered to nas
the next List No.
In this case, “TANAKA”is registered List No
*Operator can be registered up to 20 names. to the List No 02 by pressing OK
when the cursor in on “+”.
*Sample ID can be registered up to 10 names.
(7) Press OK key when the yellow cursor is on minus
Operator TANAKA + - [01]
(-), then the registered Sample ID/Operator Name is nas
deleted from the list.
When optional USB keyboard is installed, sample ID can be entered easily by typing keyboard.
For setting of USB port, refer to chapter 8.5 USB Settings.

21
4.4 Selecting of Test Method
The aco-8 has more than 10 kinds of test method,
Move the cursor with Up-Down key to Test Method and press ok key. After the cursor is moved to
the display of the test method, press Up-Down key to select test method.

Table 3 Test Method in Celsius

Test Method Contents

Used when a sample is CRM. A corrected flash point is


ISO CRM
rounded to the nearest 0.1 oC.
The test proceeds in accordance with ISO 2592 or ASTM
ISO Normal D92 until flash point is detected.
ASTM Normal A corrected flash point is rounded to the nearest 2 oC
(ISO) or 1oC (ASTM).
Used for measuring the approximate flash point of a
sample of unknown expected flash point.
ISO SPE
Ignition source application is carried out every 2oC from
ASTM SPE
the test start.
This is different from the ISO/ASTM Normal method.
The test proceeds in accordance with ISO 2592 or ASTM
ISO Fire D92 until fire point is detected.
ASTM Fire A corrected flash point/fire point is rounded to the nearest
2 oC (ISO) or 1oC (ASTM).
The test proceeds in accordance with ISO 2592 or ASTM
D92 until flash point is detected. The skimmer starts to
ISO Skim* work at -30.2oC below EXP.FP, and then work with
ASTM Skim* specified interval to remove surface skin of specimen
*Work on ACO-8as only during a test.
A corrected flash point is rounded to the nearest 2 oC
(ISO) or 1oC (ASTM).
For interval setting, Refer to Chapter 6 Parameter Setting

22
The test proceeds in accordance with ISO 2592 or ASTM
ISO Manual
D92 until flash point is detected by manual detection.
ASTM Manual
A corrected flash point is rounded to the nearest 2 oC
“For visual detection
(ISO) or 1oC (ASTM).

The test proceeds in accordance with ISO 2592 or ASTM


D92 until flash point is detected by manual detection. The
ISO Skim+Man* skimmer starts to work at -30.2oC below EXP.FP, and then
ASTM Skim+Man* work with specified interval to remove surface skin of
*Work on ACO-8as only specimen during a test.
A corrected flash point is rounded to the nearest 2 oC
(ISO) or 1oC (ASTM).
For interval setting, Refer to Chapter 6 Parameter Setting
User can make arbitrary setting for heating rate,
Custom application interval etc. Refer to chapter 9 User Custom
Mode

23
Table 4 Test Method in Fahrenheit

Test Method Contents

Used when a sample is CRM. A corrected flash point is


ISO CRM
rounded to the nearest 2 oF.
The test proceeds in accordance with ISO 2592 or ASTM
ISO Normal D92 until flash point is detected.
ASTM Normal A corrected flash point is rounded to the nearest 2 oF
(ISO&ASTM).
Used for measuring the approximate flash point of a
sample of unknown expected flash point.
ISO SPE
Ignition source application starts at the first (EXP.FP-5x)
ASTM SPE
point after the start. (x=Integer)
This is different from the ISO/ASTM Normal method.
The test proceeds in accordance with ISO 2592 or ASTM
ISO Fire D92 until fire point is detected.
ASTM Fire A corrected flash point/fire point is rounded to the nearest
2 oF (ISO&ASTM).
The test proceeds in accordance with ISO 2592 or ASTM
D92 until flash point is detected. The skimmer starts to
ISO Skim* work at -30.2oC(-60oF) below EXP.FP, and then work with
ASTM Skim* specified interval to remove surface skin of specimen
*Work on ACO-8as only during a test.
A corrected flash point is rounded to the nearest to 2 oF
(ISO&ASTM).
For interval setting, Refer to Chapter 6 Parameter Setting

The test proceeds in accordance with ISO 2592 or ASTM


ISO Manual
D92 until fire point is detected by manual detection.
ASTM Manual
A corrected flash point/fire point is rounded to the nearest
“For visual detection
2 oF (ISO&ASTM).

24
The test proceeds in accordance with ISO 2592 or ASTM
D92 until flash point is detected by manual detection. The
ISO Skim+Man* skimmer starts to work at -30.2oC(-60oF) below EXP.FP,
ASTM Skim+Man* and then work with specified interval to remove surface
*Work on ACO-8as only skin of specimen during a test.
A corrected flash point is rounded to the nearest to 2 oF
(ISO&ASTM).
For interval setting, Refer to Chapter 6 Parameter Setting
User can make arbitrary setting for heating rate,
Custom application interval etc. Refer to chapter 9 User Custom
Mode

In case the temperature at which the first test flame application is made is above the fire point of the
specimen, there is a danger: the specimen catches a fire to blaze up.
So as to prevent such a danger in advance, for testing a sample of unknown flash point, use the SPE
method. Be sure to arrange at least one proper person in your test room, lab, etc., when testing, to
cope with possible accidents.

※ Test Sequence of ISO SPE, ASTM SPE in Fahrenheit


Entered EXP.FP → 203 oF
Start Specimen Temp → 70 oF
First Application Temp → 73 oF (Application Interval 5 oF)
Over Cut Temp → 263 oF (Entered EXP.FP + 60 oF)

25
4.5 Entering Sample Information
Bundle Expected Flash Point, Operator Name and Test Method to Sample No.

(1) Move the cursor to MENU by


MENU B a c k
Up-Down key or Right-Left key
at Stand-by screen.
S t o r e D a t a
(2) Press OK key to display the
S a m p l e I n f o MENU.
M a i n t e n a n c e (3) Move the cursor to Sample Info by
U s e r C u s t o m Up-Down key.
E q u i p m e n t I n f o

Sample Information B a c k
(4) Press OK key, the Sample

OFF Information will be displayed on


Bundle
the screen.
(5) Move the cursor to Bundle, and
then press OK.

Sample Information
B a c k
(6) If you select ON by UP-Down key,

Bundle ON the left display will appear and


then you can resister Expected
Set Sample No. [01]
Flash Point, Sample ID, Operator
Exp. FP 000 Name and Test Method.

Sample ID TEST-SAMPLE Refer to 4.2~4.4 for the entry.

Operator TANAKA
*Sample No. can be registered up
Method ASTM Nomal
to 20.

26
4.6 Preparation of Test Cup and sample

(1) Wash the test cup with the cleaning solvent to remove any test specimen or traces of gum or
residue remaining from a previous test. When the upper side of cup’s flange is covered with
carbon deposit, the flash detector cannot operate normally. Also when conductive material
adheres to the insulator of electrode ring (outer ring), bad insulation can cause mis-detection of
flash. Therefore, keep the parts cleanly.
(2) When testing samples of very viscous materials and containing dissolved or free water, follow
Sampling section of ISO 2592/ASTM D92.
(3) Fill the test cup with the test specimen to the filling mark inside of the test cup.
(4) Push up the arm handle and place the test cup on the center of the heater.
(5) Lower the arm gently until stopper is touching the flange of the cup.

Fig. 15 Test Cup Handle Position (Left: Correct, Right: Wrong)

Now you have completed the preparation for the test.

27
5. Test Sequence
5.1 Test Start

! Warning: Never touch around test cup during testing. An operator


gets burned.
! Warning: Never run the tester unattended. The specimen may catch
a fire and blaze up by some sort of cause. It is essential that at
least one-trained personnel be present in the test room.
! Warning: If the instrument makes any abnormal noises or exhibits
any abnormal behavior, stop operation immediately, turn the
power off at the mains, and contact Tanaka Scientific Limited or
an authorized distributor.

Open the main gas cock, and then press the start key to start a test. The background of the
temperature display turns orange as the Run condition. See Fig. 16.
(If press the start key without entering expected flash point, display shows “INVALID EFP”. Press
reset key to return Stand-By Screen)
The expected flash point(4) is displayed for 5 seconds on the temperature display. The dual pilot
turns on, specimen heating starts(5) .

Cleveland Open Cup

EXP FP
Sample ID 01

Operator 01

Method ASTM Normal

23.4 oC

C O O L A P P L M E N U

Gas 2013/12/06 (Frin)

Fig. 16 Run Screen

28
Note(4): Expected Flash Point can be changed even during the test. After changing expected flash
point in accordance with Section 4.2, re-press the start key. Also in this case, the newly set expected
flash point appears in the center of the display for 5 seconds.
Note(5) Heater output can be confirmed by Heater Output Indicator.
Lighting: 100% full power
Extinction: 0% (no heat)
Blink: interlevel
In most cases, heater output varies and then this indicator blinks.

Test flame is ignited by dual pilots automatically. The time until auto ignition will be seconds
(continuous run) to minutes (first run)(6). Do not leave the instrument until ignition is confirmed.
Adjust the test flame to 4mm in diameter (the flame size comparison bead size) by needle valve.

Note(6): The first run after the gas piping (installation or transfer of the instrument), there is full of air in
the gas hose. Lift the windscreen and then open the needle valve for test flame fully to get out air
from the hose. Be careful that the big flame comes out from the nozzle when ignites. After this, turn
the needle valve clockwise to adjust the flame size. Besides, flame grows big slowly because the
portion of the gas increases with the same flow rate till air can be removed completely. Please take
care valve operation diligently for the first run.

The test proceeds automatically hereafter.

29
5.2 Test Sequence
After the test starts, the specimen temperature rises at a rate of 14 to 17 oC /min(25 to 30 oF /min).
When the temperature reaches 56 oC (100 oF) below the expected flash point, the heating rate is
decreased so that the rate of temperature increase during the last 28 oC (50 oF) before the expected
flash point is 5 to 6 oC(9 to 11 oF). When the temperature of the test specimen is 28 oC(50 oF) below
the expected flash point, the test flame begins to apply. After that, the application operation is
repeated at each 2 oC(5 oF).
Note: heating rate might be unstable in particular kind of sample like asphalt.

5.3 Flash Detection


When a flash is detected, the Flash Point is displayed on the screen as Fig. 17, and then starts
blink(7).
At the same time buzzer beeps intermittently for 8 seconds. Furthermore, the solenoid valve for gas
is closed, the test flame goes out and dual pilot goes off, and the stove section starts cooling.
(background of temperature display turns green).
When “ASTM Fire” or “ISO Fire” Method is selected, aco-8 suspends a test 1 minute. During this
suspend, push start key again to continue fire point test, otherwise aco-8 terminates a test and then
starts cooling. Please do not leave the aco-8 until fire point is detected. Fire point test is dangerous.

Cleveland Open Cup

EXP FP
Sample ID 01

Operator 01

Method ASTM Normal

Corrected Flash Point

224.0 C o

C O O L A P P L M E N U

Gas 2013/12/06 (Fri)


Fig. 17 Flashed in Good Condition

Note(7): The blinking flash point on the screen is held until reset key or start key is pressed. Once
reset key or start key is pressed, temperature display returns to present specimen temperature.

30
The Flash Point (8) blinking on the screen is corrected by barometric pressure and rounded, not
observed.
The test result is automatically stored in the memory. To view the stored data, refer to chapter 0.
Data Storage.

Note(7)(8):The calculation of the flash point is done by following procedure.


(1) Calculate the corrected flash point, Tc, using the following equation
TC = To + 0.025(1013 - P)
where
To: the observed flash point, in oC
P :the barometric pressure (hPa) measured by built-in barometric pressure
sensor
(2) Round Tc to the nearest 1.0 oC(ASTM) or 2.0 oC (ISO) or 0.1 oC(ISO CRM)
(2.0 oF) (2.0 oF) (2.0 oF)
For example, the flash is detected at 222 oC. And then measured barometric pressure is 970hPa, the
corrected flash point will be “223.075” by above equation, then to be “223” by rounded to the nearest
1.0 oC(ASTM), then to be “224” by rounded to the nearest 2.0 oC(ISO).

When measured barometric pressure is between 974 and 1052hPa, observed flash point and the
flash point will be the same value.

31
< When a flash is detected at first application of the ignition source >
When a flash is detected at the first ignition source application, the test is terminated. In this case,
screen shows “INVALID: flashed on 1st appl” under the flash point display as Fig. 18. Do a test again
with fresh sample and lower EXP FP. If flash is not observed, the test is continued as follows.

Cleveland Open Cup

EXP FP
Sample ID 01

Operator 01
Method ASTM Normal

Corrected Flash Point

194.0 oC

C O O :Lflashed on
INVALID A 1P stP appl
L M E N U

Gas 2013/12/06 (Fri)

Fig. 18 Flashed on 1st application

32
< When a flash is detected at out of limit >
When a flash point is detected at a temperature which is less than 18 oC (32 oF) above the
temperature of the first application of the ignition source, INVALID and its detail appear under the
flash point. See Fig. 19.

Cleveland Open Cup

EXP FP
Sample ID 01
Operator 01
Method ASTM Normal

Corrected Flash Point

210.0 C o

o
INVALID
C O O: Lflashed @ A< P18
P LC aft 1stM appl
E N U

Gas 2013/12/06 (Fri)

Fig. 19 Flash is detected out of limit

33
< If a flash has not been detected when the safety cut temperature is reached >
This instrument has a function to prevent overheat called “safety cut temperature”. The safety cut
temperature is set at EXP FP+30 oC (+60 oF)or upper limit of the test method.
If a flash has not been detected when the safety cut temperature is reached, terminate the test
forcibly.
(Solenoid valve for gas is closed, the test flame goes out and dual pilot goes off, and the heater
section starts cooling down)
The buzzer beeps intermittently for 8 seconds again.
The following screen is an example of the safety cut temperature termination.

T R O U B L E

Flash Point >


252 oC
2012/02/27 14:35

Fig. 20 Safety Overcut Screen

5.4 Fire Point Detection


When “ASTM Fire” or “ISO Fire” Method is selected, and then operator push start key again after
detectiong flash point, aco-8 continue a test until fire point.
※Please note that there is no automatic transition from the flash point test to the fire point test.
Once flash point is detected the buzzer sounds intermittently for 1 min, please push start key again
within 1 min to continue a fire point test.
When aco-8 detects continuous specimen burning for 5 seconds, test is terminated, fire containment
lid activates to extinguish a fire, and then display shows fire point and flash point alternately.
In the fire method, aco-8 does not move to cooling cycle automatically for safety reason.
Operator has to confirm the fire is extinguished completely, and then reset fire containment lid to the
original position, then move the cursor to COOL by Up-Down key or Right-Left key, and then press
the OK key to start cooling.

34
5.5 Flash Point Detection By manual detection
First of all the flash point detection principle of aco-8 is considered as a flash when there is
conduction between two large and small flash detection rings (usually insulated).
This means that if there is conduction between the rings other than the flame at the time of flash
point, it will be detected. Therefore, If the sample expands excessively due to heating and touches
the rings, or if bubble is generated from the sample and touches the rings, false detection may occur.
In such cases, please use the following manual detection mode.
When “ASTM Manual” or “ISO Manual” or “ASTM Skim+Man” or “ISO Skim+Man” Method is
selected, aco-8 ignores the first detection even if detected by foam or sample expansion, and then
operator push start key again after ignoring the first detection, aco-8 continue a test until flash point
detection.However, even if the initial sample expansion or bubble contact to rings can be detected
automatically, there is no way to determine which is the true flash point, so the flash point detection is
a visual check by operatiors.
Once the first detection by sample expansion or bubble is detected the buzzer sounds intermittently
for 1 min, please push start key again within 1 min to continue a test.
After that, automatic detection is not possible, so flash point detection is a manual operation by visual
check. Do not leave until you see the flash point or test end. After visually checking the flash point
please press the START key immediately. Pressing the START key is regarded as a flash point
detection and the flash point result is displayed.
In these method, aco-8 does not move to cooling cycle automatically for safety reason.
Operators move the cursor to COOL by Up-Down key or Right-Left key, and then press the OK key
to start cooling.

35
5.6 Test End

! Warning: Never touch the test cup with bare hands after the test
end. The sample cup may still hot and the operator gets burned.
Use gloves and hold the test cup handle for operator’s safety.

! Warning: Never discard hot sample to a waste tank. Sample in the


waste tank may blow up.
! Warning: Never discard hot sample to a waste tank. Sample in the
waste tank may blow up.

The cooling stop automatically (the green background on the temperature display turns white) in 10
minutes (9). When further cooling is required, move the cursor to COOL by Up-Down key or Right-
Left key, and then press the OK key. Cooling is available for another 10 minutes (9).
Cooling cycle can be canceled by pressing the reset key.

The temperature display (flash point) is held until the reset key is pressed.

Note(9): Cooling time is adjustable. For changing cooling time, refer to chapter 6. Test Parameter
Setting.

One cycle of a test is completed at this moment and you can start the next test.
Press reset key first, and then return to section 4.2 Setting of Expected Flash Point when the next
test is available. If not press reset key, and then press start key, display shows INVALID EFP.
Turn the MAIN switch of the instrument off and close the main gas cock when today’s work is
finished.

36
6. Test Parameter Setting
When test parameter needs to be changed from factory setting, please change them by following
procedure.
(1) To change test parameters, move
MENU the cursor to MENU (turns yellow) in
B a c k
the stand-by screen by Up-Down

S t o r e D a t a key, and then press the OK key.


(2) After change the screen, move the
M a i n t e n a n c e
cursor to Maintenance by Up-Down
U s e r C u s t o m
key, and then press the OK key.
E q u i p m e n t I n f o

Fig. 21 MENU Screen


(3) Press OK when the cursor is on
Maintenance B a c k calibration.

C a l i b r a t i o n
D a t e & T i m e S e t t i n g
R S - 2 3 2 C s e t t i n g s
U S B s e t t i n g s
P a s s w o r d s e t t i n g s

(4) Press OK when the cursor is on Test


Calibration B a c k Parameter.

T e s t P a r a m e t e r
T e m p c o r r e c t i o n
B a r o c o r r e c t i o n
S a m p l e 0 – S p a n
B a t h 0 – S p a n
P r i n t C a l T i c k e t

37
Test Parameter (5) After the cursor is moved to the
B a c k
numeric figures of each item, move
the digit with Right-Left key and

T e m p u n i t o
C increase/decrease the value with the
Up-Down keys.
I n i t
保存データ h e a t 3デー
0 %
(6) Press the OK key to fix the value.
C o o l t i m e 1 0 m i n
(7) Move the cursor to Back, and then
A p p l t e m p 2 8 oC
press OK to MENU screen, or Press
D e t s e n s S t d reset key to return stand-by screen.
S k i m i n t v l 0 2 oC

Fig. 22 Test Parameter Screen

Temperature Unit Setting: Select temperature unit oC or oF. Default setting is oC


Initial Heat Setting: Too strong an initial heat would cause hunching of temperature rise rate. Too
weak an initial heat could not reach the set rate. Please input an even number (every 2%)
Standard value of Initial Heat is as follows.

AC Source 100V 110V 115V 120V 220V 230V 240V


Standard Value 30 28 26 24 26 24 22

Cooling Time Setting: Cooling time can be change from 00min (No Cooling) to 99min.
Test Flame Application Start Temperature Setting: This value means flame application starts from
XXoC below EXP.FP. Default value is 28.
Detection Sensitivity Setting: If the sensitivity is so high as to detect a flame that could not reach a
flash point, select Low. Hight is solely for silicon oil and must not be selected for others. When testing
silicone oil, set the flash detecting sensitivity to High and use flash detector ring dedicated for silicone
(option).
Default setting is “Std”.
Skimmer Interval Setting (apply only aco-8as): Select skimmer interval time. Input even number
like 2, 4, 6…. Default setting is2 oC(4 oF) .

38
7. Data Storage
aco-8 has a data storage function. Up to 200 test data can be memorized.
After aco-8 detects a flash point, the data will be stored automatically.
The recalling procedure is as follows.

MENU B a c k (1) Move the cursor to MENU by Up-


Down key or Right-Left key.
(2) Press OK key to display the
S t o r e D a t a
MENU.
M a i n t e n a n c e
(3) Move the cursor to Store data by
U s e r C u s t o m
Up-Down key.
E q u i p m e n t I n f o

Fig. 23 MENU Screen

Storedata
B a c k (4) Press OK key, the stored data will
be displayed on the screen as Fig.
No Sample ID: Date & Time Result
24 Stored Data Screen.
000 LUBE0287 12/02/27 15:30 266.0oC
001 LUbE0286 12/02/27 14:21 258.0 oC (5) Press Down key to display next
002 FPRM4D 12/02/27 13:27 223.5 oC 10 data, press UP key to display
003 FPRM2D 12/02/27 12:30 163.2 oC previous 10 data.
004 FPRM14 12/02/27 11:26 116.1 oC
005 LUBE0285 12/02/27 10:48 165.5 oC (6) Move the cursor to Back, and then
006 AAAAAAAAAAAA 12/02/20 09:34 166.0 oC press OK to MENU screen, or
007 AAAAAAAAAAAA 12/02/20 09:00 TRBL Press reset key to return stand-by
008
009 screen.

Fig. 24 Stored Data Screen


To re-print certain data, the procedure is as follows. (Software version “8FP20” or later)
(1) Connect dedicated printer.
(2) Press Right-Left key at Stored Data Screen to turn the cursor yellow in No area.
(3) Select the data by pressing Up-Down key.
(4) Press OK to start re-print.

39
8. Maintenance
Indicated temperature correction, date and time setting, barometric pressure sensor calibration, RS-
232C settings, USB settings and password setting are done by pressing panel keys. The operation
procedure is as follows.

MENU (1) Move the cursor to MENU by Up-


B a c k
Down key or Right-Left key.
(2) Press OK key to display the
S t o r e D a t a
MENU.
M a i n t e n a n c e
(3) Move the cursor to Maintenance
U s e r C u s t o m
by Up-Down key, then press OK
E q u i p m e n t I n f o key.

Fig. 25 Menu Screen

(4) After change the screen, select


Maintenance B a c k
the item by Up-Down key, and
then press OK key.

C a l i b r a t i o n
D a t e & T i m e S e t t i n g
R S - 2 3 2 C s e t t i n g s
U S B s e t t i n g s
P a s s w o r d s e t t i n g s
Calibration B a c k

T e s t P a r a m e t e r
Fig. 26 Maintenance Screen
T e m p c o r r e c t i o n
B a r o c o r r e c t i o n
S a m p l e 0 – S p a n
B a t h 0 – S p a n
P r i n t C a l T i c k e t

40
8.1 Temperature Correction
Displayed temperature can be adjusted by inputting temperature offset values. For the detail and
procedure of temperature calibration, refer to aco-8 Maintenance Manual.
(1) Move the cursor to temperature
Temp Correction correction point by Up-Down key
B a c k
or Right-Left key.
(2) Press OK key to move the cursor
POS +0.0 0 +0.0 40 +0.0 to offset value.

80 +0.0 120 +0.0 160 +0.0 (3) Change offset value by Up-Down
保 保 保 保 保 保
key, and then press OK key.
200 +0.0 240 +0.0 280 +0.0
(4) After complete the changing,
320 +0.0 360 +0.0 400 +0.0
move the cursor to Back by Up-
Down key, then press OK key to
return the Maintenance Screen,
or press reset key to return the
Fig. 27 Temperature Correction Screen Stand-by Screen.

8.2 Date and Time Setting


Displayed date and time can be adjusted by following procedure
(1) Move the cursor to date and time
Date & Time Setting
B a c k column by Up-Down key, and
then press OK key.
(2) After the cursor is moved to
numeric figure, move the cursor
2 0 1 2 0 2 2 7 1 5 : 5 3 by Right-Left key and then
change the value by Up-Down
key.
(3) After inputting present date &
time, press OK key to set the
clock.
(4) After complete the setting, move
the cursor to Back by Up-Down
key, then press OK key to return
Fig. 28 Date and Time Setting Screen
the Maintenance Screen, or press
reset key to return the Stand-by
Screen

41
8.3 Barometric Pressure Correction
Barometric pressure sensor correction, pressure unit changing and valid/invalid of barometric
pressure correction can be done by following procedure.
(1) Move the cursor to the item by
Barometric Pressure
B a c k Up-Down key, and then press
OK key.(
(2) After the cursor is moved to the
P r e s e n t 1 0 0 1
right column, change the value by
B a r o S e t
保存データ 1保存
0 0 1
Up-Down key, and then press
B i a s S e t - 0 0 1 7 OK key.
U n i t h P a (3) After complete the changing,
B a r o C o r r O N move the cursor to Back by Up-
Down key, then press OK key to
return the Maintenance Screen,
or press reset key to return the
Fig. 29 Barometric Pressure Setting Screen
Stand-by Screen.

8.4 RS-232C Settings


When connecting aco-8 to optional printer or PC, data transfer format may be changed. The
changing procedure is as follows. Below setting is for connecting optional printer, BS-80TS.
(1) Move the cursor to the item by
RS-232C Settings
B a c k Up-Down key, and then press
OK key.
(2) After the cursor is moved to the
F o r m a t P r i n t e right column, change the value by
B a u d
保存データ R a t e 9保存
6 0 0 b p Up-Down key, and then press
D a t a B i t s 7 b i t s OK key.
P a r i t y O d d (3) After complete the changing,

S t o p B i t s 2 B i t s move the cursor to Back by Up-

L i n e F e e d C R L F Down key, then press OK key to


return the Maintenance Screen,
or press reset key to return the
Fig. 30 RS-232C Setting Screen
Stand-by Screen.
Format: Select Comm when PC (LIMS) is connected.

42
Comm 1 : Current communication format *P.39
Comm 2 : Additional communication format ( Not transferred when trouble) *P.40
8.4.1 Connection
The connection to a computer is through the 25 pin or 9 pin D-Sub type connector located at the back
of the control unit. An extreme care should be taken when making pin-to-pin connections, since the
tester is a DTE device.

8.4.2 Pin Assignment


The pin assignment is as follows:
Table 5 Pin Assignment
Pin # Signal Function Direction
1 GND (FG) Frame Ground
2 TXD (SD) Transmitting Data Tester  Computer
3 RXD (RD) Receiving Data Computer  Tester
4 RTS (RS) (Connect w/pin #5)
5 CTS (CS) (Connect w/pin #4)
6 DSR (DR) (See note-1) Computer  Tester
7 GND (SG) Signal Ground
20 DTR (ER) (See note-2) Tester  Computer

Note: When starting data communication, switch this signal line to “0” logic (3V to 12V).
This signal line turns to “0” when the tester detects a flash; then turns “1” (-12V)
when press RESET key. This signal is provided for user’s convenience.

8.4.3 Signal Voltages


Input Voltages “0”: 3V to 12V
“1”: -3V to –12V
Output Voltages “0”: 12V
“1”: -12V

43
8.4.4 Example for Connection
As an example for the connection, connection with IBM/AT compatible is as illustrated below.

Tester(25P) Computer(25P)

FG 1 1 FG
TXD 2 2 TXD
RXD 3 3 RXD
RTS 4 4 RTS
CTS 5 5 CTS
DSR 6 6 DSR
SG 7 7 SG
DTR 20 20 DTR

Tester(25P) Computer(9P)

TXD 2 2 RXD
RXD 3 3 TXD
RTS 4 4 DTR
CTS 5 5 GND
DSR 6 6 DSR
SG 7 7 RTS
DTR 20 8 CTS

44
8.4.5 Transmitted Data
The data consists of ASCII coded 39 characters. It starts with “STX” and ends with “ETX”.

(Comm 1)

STX A C O 8 0 2 CR LF 0 0 0 0 0 1 CR LF
Instrument No. (6 ltrs) Test No. (6 ltrs)

1 3 8 . 0 CR LF 1 4 0 . 0 CR LF

Flash Point (5 ltrs) EXP FP (5 ltrs)

0 1 4 . 0 CR LF ETX

No. of Applications
( 5 ltrs)

Instrument No.: The first 4 characters represent the model; last 2 the ID number.
Test No.: A six-digit number that is increased one by one as a test is executed
properly.
Flash Point: The number is a 4-digit number including 1 digit after decimal point.
In case of the following situation, this number is replaced by character
strings:
Trouble during test.
“TRBL_” (4 letters plus 1 space)
The flash point is detected during the first application.
“UNDER” (5 letters)
The actual flash point exceeded the safety cut temperature.
“OVER_” (4 letters plus 1 space)
No. of applications: The number of ignition source applications when the flash point is
detected. (If the flash point is detected at the 10th application, the value
is “010.0”.)

45
(Comm 2) NEW

46
8.5 USB Settings
When connecting a key board to aco-8, select a type of keyboard (layout, LED, ten key) by following
procedure.
(1) Move the cursor to the item by
Up-Down key, and then press
USB Settings OK key.
B a c k
(2) After the cursor is moved to the
right column, change the value by

Keyboard layout United States Up-Down key, and then press


OK key.
LED on keyboard
保存デー Without
保存デ LED
(3) After complete the changing,
Ten key keypad Without ten key
move the cursor to Back by Up-
Store parameters
Down key, then press OK key to
Load parameters Cancel return the Maintenance Screen,
Store results or press reset key to return the
Stand-by Screen.
Fig. 31 USB Setting Screen
Current parameters and test data in aco-8 can be copied to an USB memory with csv format, and
aco-8 can load saved parameters from the USB memory. The procedure is as follows.
 Store Parameters: Plug in an USB memory  Move the cursor to Store parameters  Press
OK.
After store parameters, confirm that the csv file is created in the USB memory by a PC.
 Load Parameters: Plug in an USB memory  Move the cursor to Load parameters  Press OK
 Select/Confirm file name  Press OK.
 Store Result: Plug in an USB memory  Move the cursor to Store results  Press OK.

47
8.6 Password Settings

Caution!: Once password is set, and then forgot the password, the unit cannot
recovered. Please record the password to the safe place.

aco-8 has a function to protect parameters by user own password. The procedure for setting a
password is as follows.
8.6.1 Setting Password
(1) Move the cursor to Password by
Password Settings Up-Down key, and then press
B a c k
OK key.
(2) Select “Use” by Up-Down key,
Password Not use then press OK key.
Old password
保存 ************
保存データ (3) Move the cursor to New

New Password ************ Password by Up-Down key, and


then press OK key. After the
cursor is moved to the right
column, enter password (max. 12
characters) by Up-Down key and
Right-Left key, and then press
Fig. 32 Password Setting Screen
OK key.

(4) “Password has been changed.” appears on the screen. (Use of external key board is easy)
(5) After complete the changing, move the cursor to Back by Up-Down key, then press OK key to
return the Maintenance Screen, or press reset key to return the Stand-by Screen.
After setting password, following screen appears when go to Maintenance screen.
Enter password by Up-Down key and
Enter Password Right-Left key, and then press OK
key. Maintenance screen appears by

 
this operation.

Enter password and push OK key.

Fig. 33 Password Entering Screen


48
8.6.2 Changing Password
(1) Go to Password Setting Screen.
(2) Move the cursor to Old Password by Up-Down key, and then press OK key.
(3) After the cursor is moved to the right column, enter old password by Up-Down key and Right-
Left key, and then press OK key. “Password matched.” appears on the screen.
(4) Move the cursor to New Password by Up-Down key, and then press OK key.
(5) After the cursor is moved to the right column, enter new password by Up-Down key and Right-
Left key, and then press OK key. “Password has been changed.” appears on the screen.
(6) After complete the changing, move the cursor to Back by Up-Down key, then press OK key to
return the Maintenance Screen, or press reset key to return the Stand-by Screen.

8.6.3 Clear Password


(1) Go to Password Setting Screen.
(2) Move the cursor to Password by Up-Down key, and then press OK key.
(3) Select “Not use” by Up-Down key, then press OK key.
(4) Move the cursor to Old Password by Up-Down key, and then press OK key.
(5) After the cursor is moved to the right column, enter old password by Up-Down key and Right-
Left key, and then press OK key. “Password matched.” appears on the screen.
(6) Move the cursor to Back by Up-Down key, then press OK key to return the Maintenance
Screen, or press reset key to return the Stand-by Screen.

8.7 Calibration Ticket (NEW)


Calibration Ticket

Calibration B a c k

T e s t P a r a m e t e r
T e m p c o r r e c t i o n
B a r o c o r r e c t i o n
S a m p l e 0 – S p a n
B a t h 0 – S p a n
P r i n t C a l T i c k e t

(1) Calibration Ticket is printed out by pressing OK when the cursor


is on “Print Cal Ticket”
For Sample 0-span and Bath 0-Span, please consult with Tanaka
Scientific Limited

49
9. User Custom Method
The procedure of User Custom method setting is as follows.
(1) Move the cursor to Temp Rate by
User Custom
B a c k Up-Down key, and then press
OK key.

T e m p R a t e
(2) After change the screen, Move
F l a m e A p p l i c a t i o n
the cursor to the item by Up-
Down key, and then press OK
Temp Rate key.
B a c k
(3) After the cursor is moved to the
right column, change the value
Temp Rate 1 3 . 0
by Up-Down key, and then
Temp Rate 2
保存データ 保存3 . 0 press OK key.
Change temp 0 1 0 (4) move the cursor to Back by Up-
Down key, then press OK key
to return the User Custom
Screen, or press reset key to
Flame Application
B a c k return the Stand-by Screen.

Interval 1 10 . 0
Interval 2
保存データ 保存2 . 0
Start Temp 1 0 0
Change Temp 0 8 0

Fig. 34 User Custom Method setting Screen

Temp Rate 1: Apply from test start to EXP FP- Change temp. Select from 3.0, 5.5, 10.0 and 15.5
Temp Rate 2: Apply from EXP FP- Change temp to test end. Select from 3.0, 5.5, 10.0 and 15.5
Change temp: Heating rate switching temperature. Enter XXXoC below EXP FP.
Interval 1: Apply from test start to EXP FP- Change temp. Select from 0.5, 1.0, 2.0, 5.0, and 10.0.
Interval 2: Apply from EXP FP- Change temp to test end. Select from 0.5, 1.0, 2.0, and 10.0
Start Temp: Test Flame application starting temperature. Enter XXXoC below EXP FP.
Change Temp: Test Flame application switching temperature. Enter XXXoC below EXP FP.

50
10. Equipment Information
Equipment information can be seen by Equipment Information screen.
Only ID Number can be changed by user. If several aco-8 is used, set ID number 01, 02, 03…. so
that Lims system can identify the unit.
(1) Move the cursor to ID Number by
Up-Down key, and then press
Equioment Info
B a c k OK key.
(2) After the cursor is moved to the
S e r i a l N o : 3 1 0 0 1 right column, change the value by
S o f t w a r e : 8 F P 3 1 Up-Down key, and then press

M a i n P C B : 1 3 – 1 0 OK key.
(3) Move the cursor to Back by Up-
I D N u m b e r 0 0
Down key, then press OK key to
return the Maintenance Screen,
or press reset key to return the
Stand-by Screen.
Fig. 35 Equipment Information Screen

51
11. In Case of Abnormal Operation or Trouble

! Warning: Do not attempt to repair the instrument yourself. In the event


that the instrument exhibits any abnormal behavior whatsoever,
contact Tanaka Scientific Limited or an authorized distributor.
! Warning: Only Tanaka Scientific Limited service personnel or
authorized representatives are to repair or maintain the
instrument.

Self Diagnose Function


When a problem occurs on the Tester, a buzzer will sound and one of the trouble messages in
Table 6 will be shown. When one of these events occurs, all outputs will be shut off. For
troubleshooting, refer to the Maintenance Manual or consult Tanaka authorized distributor.

52
Table 6 Trouble Messages

Trouble Message on Display Buzzer


Control computer runs Beeps continuously
way
None

Temperature sensor for Beeps intermittently for


TROUBLE
sample is found eight (8) seconds
defective
SAMPLE TEMP SENSOR
Flash detector is found Beeps intermittently for
TROUBLE
defective eight (8) seconds
FLASH DETECTOR
Electric ignitor is found Beeps intermittently for
TROUBLE
defective eight (8) seconds
FILAMENT BREAK
Built-in battery has Beeps intermittently for
TROUBLE
expired eight (8) seconds
REPLACE BATTERY
Arm is not set in place Beeps intermittently for
TROUBLE
eight (8) seconds
ARM POSITION
Thermofuse is blown Beeps big sound
TROUBLE
continuously
THERMOFUSE BLOWN
Application motor is Beeps intermittently for
TROUBLE
found defective eight (8) seconds
APPL MOTOR

Abnormal behavior without trouble message


If the instrument exhibits any abnormal behavior without any trouble message, refer to the aco-8
Maintenance Manual or consult Tanaka authorized distributor.

53
12. Periodic Inspection, Adjustment and After Sales Service
12.1 Periodic Inspection
In order to maintain accurate performance of the aco-8 and to guarantee safe operation of the
instrument, periodic inspections must be performed at regular intervals. For detail, refer to the aco-8
Maintenance Manual.
Gas piping inside the instrument is made of Nylon tube; outside, Viton tube. Gas is very dangerous if
it leaks. Consult the Tanaka authorized distributor for periodical gas leakage check. THE TESTER IS
NOT EQUIPPED WITH A GAS LEAKAGE DETECTOR.

12.2 Adjustment
The aco-8 is already adjusted for common users, but further adjustment may be require for accuracy
control or customizing some parameters, like creating user custom mode, changing cooling time,
connect to a printer or PC. For detail, refer to the aco-8 Maintenance Manual.

13. After-sales Service


! Caution: Use only Tanaka Scientific Limited genuine consumables,
parts and accessories or such parts as recommended by
Tanaka Scientific Limited.
For ordering consumable items or parts or to request servicing, please contact Tanaka authorized
distributor.
Please note that spare parts that are necessary to maintain/regain the function of this instrument is
kept in inventory for a minimum of 5 years after the delivery of this instrument.
The main consumables are listed to Table 7 Main Consumables.
Please use the code# and part name with the model name “aco-8” when you place an order.

Table 7 Main Consumables


Code# Part Name
1000949 TEST CUP ASSEMBLY
1000711 THERMOFUSE, Pack of 5, with Insulation Tube.
1001020 IGNITER TOP for aco-8
1001018 TEMPERATURE SENSOR for aco-8
1005152 HEATER COIL, 100/120V 800W, for 100/120V model
1000267 HEATER COIL, 220/240V 800W, for 220/240V model
1000960 INNER DETECTOR RING
1000961 OUTER DETECTOR RING
1000964 INSULATING COLLAR for aco-8
1001027 SKIMMER PADDLE (for aco-8as only)

54
14. Other Cautions

14.1 Caution when this instrument is not used for a long time
When this instrument is not used for a long time, please pull AC power cord out of an outlet.
In addition, please put cover not to be affected by dust and moisture.

14.2 Precaution in case of Loss of Instruction Manual


The Instruction Manual is a part of this instrument. In case it is lost, please request a new copy to
Tanaka authorized distributor.
Also, it is highly recommended that the address and telephone number of Tanaka and/or its
authorized distributor be kept separately from this Manual.

14.3 Caution when Transferring This Instrument


When this instrument is transferred or sold to a third party, please inform Tanaka or its authorized
distributor. Wrong source voltage and/or AC frequency could cause damages or malfunctioning. In
case of transferring this instrument, make sure to attach this Instruction Manual.

14.4 Caution when Discarding This Instrument


This instrument does not include harmful substance; please discard this instrument according to the
local regulations.

55
15. Specification
Conforming standard: ISO 2592, ASTM D92, IP34
Measuring Range: Ambient to 400 oC(700 oF)
Test Modes: ISO CRM, ISO Normal, ISO SPE, ISO Flash & Fire, ISO Skim*, ASTM
Normal ASTM SPE, ASTM Flash & Fire, ASTM Skim*, and User Custom
*:aco-8as only
Display: 5.7 inch (117 x 88mm) color LCD with LED back light
Temperature Sensor: PT-100 in stainless steel sheath
Flash Detector: Double Ionization Rings
Heater: Nichrome Coil heater 800@115V or 800W@230V
Cooling Device: Forced air cooling by sirocco fan
Ignition Source: Gas ignition with automatic lighting
Barometric Correction: By built-in barometric pressure sensor
Safety shutdown: Automatically shuts off and the problem is reported by buzzer and display
in case:
(a) EFP+30 oC (+60 oF) or 400 o C(700 oF) is reached,
(b) Temperature sensor for sample is found defective
(c) Flash detector is found defective
(d) Thermofuse is blown (also fire containment lid activates)
(e) built-in battery is found drained out
(f) arm is not set in place
(g)control computer runs away (no display)
Dimensions & Weight: 230W x 470D x 390H(mm), approx.16kg
Operation room temp.: 10 to 35 oC (50-95 oF)
Humidity: less than 90% (No Condensation)
Altitude: less than 2000m
Overvoltage Category: II
Pollution Degree: 2
Utility: Power Supply: 100/120VAC or 220/240VAC, 50/60Hz (set at the factory), 1000W Max.
Gas Supply : LP gas or natural gas (Max. pressure<9.8kPa)
Standard Accessories:
Description Quantity
Test Cup Assembly 1pc
AC Power Cord, 2.5m (>AC200V) or 3.0m (<AC125V) 1pc
Thermofuse (pack of 5, w/insulating tube) 1pack
Gas Hose 9 x 16 x 1500mm 1pc
Gas Hose Band 2pcs

56
Instruction Manual 1pc
Optional Accessories:
1000245 Printer, BS2-80TS (with connecting cable and AC adapter)
Suggested Spares for 2 years:
1000949 Test Cup Assembly 1pc
1000711 Thermofuse (pack of 5), with Insulation Tube 1pk
1001020 Igniter Top for aco-8 5pcs
1001018 Temperature Sensor for aco-8 1pc
1005152 Heater Coil, 100/120V 800W
or 100-00-011 Heater Coil, 220/240V 800W 1pc
1000960 Inner Detector Ring 1pc
1000961 Outer Detector Ring 1pc
1000964 Insulating Collar for aco-8 2pcs
1001027 Skimmer Paddle (for aco-8as only) 5pcs

Specifications subject to change without prior notice.

57
Product Warranty
1. This product has passed a quality assurance inspection to the standards of Tanaka
Scientific Limited.
2. This product will be warranted for a period of one year from the date of delivery.
To avoid later confusion, be sure to enter the date of delivery in warranty ticket below.
3. If any faults occur due to normal use within the warranty, the product will be repaired
free of charge.
4. Be sure to notify Tanaka Scientific Limited when repairs being requested are covered
under the warranty.
5. The following faults or damage are not covered by the warranty:
▪ Any fault or damage arising from failure to adhere to all warnings and precaution as
described in the instruction manual
▪ Any fault or damage arising from misuse or carelessness
▪ Any fault or damage arising from repairs or alterations unauthorized by Tanaka
Scientific Limited
▪ Any fault or damage arising from falls or accidents during transportation after the
initial delivery
▪ Any fault or damage arising from external causes, such as fire, act of God
(earthquake, storm, or flood), environmental contamination, or power supply variations
6. All other repairs, consumables and accessories are chargeable. (Temperature Sensor,
Flash Detector, Electric Igniter, Skimmer Paddle etc.)

Product Name Automated Cleveland Open Cup Flash Point Tester

Model Name aco-8 Serial No.

Warranty
One year from the date of delivery:
Period

Manufactured and sold by: TANAKA SCIENTIFIC LIMITED


Contact: 7-10-3, Ayase, Adachi-ku, Tokyo 120-0005
Phone: +81-3-3620-1711 Fax: +81-3-3620-1713 E-mail: overseas-group@tanaka-sci.com

Distributor:

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