Quantachrome® ASiQwin™- Automated Gas Sorption Data

Acquisition and Reduction

© 1994-2012, Quantachrome Instruments
version 3.0

Analysis Report
Operator: Lab. Energi ITS Date:2020/01/15 Operator: Lab. Energi ITS Date:2020/01/16
Sample ID: EI-14 AKTIVATOR H2SO4 Filename: iq_phisy_st1_2020_01_15_13_34_16EI-14 AKTIVATOR H2SO4.qps
Sample Desc: Comment:
Sample Weight: 0.1375 g Instrument: Autosorb iQ Station 1
Approx. Outgas Time:12.7 hrs Final Outgas Temp.: 140 °C Extended info: Available
Analysis gas: Nitrogen Non-ideality: 6.58e-05 1/Torr CellType: 9mm w/o rod
Analysis Time: 3:47 hr:min Bath temp.: 77.35 K
Analysis Mode: Standard VoidVol Remeasure: off
VoidVol. Mode: He Measure Cold Zone V: 3.95662 cc Warm Zone V: 17.2389 cc
Multi-Point BET

Data Reduction Parameters Data

Thermal Transpiration: on Eff. mol. diameter (D): 3.54 Å Eff. cell stem diam. (d): 4.0000 mm
Adsorbate Nitrogen Temperature 77.350K
Molec. Wt.: 28.013 Cross Section: 16.200 Ų Liquid Density: 0.808 g/cc

Multi-Point BET Data

Relative Volume @ STP 1 / [ W((Po/P) - 1) ] Relative Volume @ STP 1 / [ W((Po/P) - 1) ]

Pressure Pressure
[P/Po] [cc/g] [P/Po] [cc/g]

5.29093e-02 -0.4353 -1.0268e+02 2.02760e-01 -1.7110 -1.1893e+02

7.80855e-02 -0.6214 -1.0906e+02 2.27684e-01 -1.9617 -1.2024e+02
1.02766e-01 -0.8204 -1.1171e+02 2.52750e-01 -2.2167 -1.2209e+02
1.27654e-01 -1.0255 -1.1417e+02 2.76851e-01 -2.1509 -1.4241e+02
1.52722e-01 -1.2485 -1.1551e+02 3.02749e-01 -2.3514 -1.4775e+02
1.77783e-01 -1.4797 -1.1692e+02

BET summary
Slope = -147.676
Intercept = -9.389e+01
Correlation coefficient, r = 0.903330
C constant= 2.573

Surface Area = 0.000 m²/g

Quantachrome® ASiQwin™- Automated Gas Sorption Data Acquisition and Reduction © 1994-2012, Quantachrome Instruments version 3.0 Report id:{539412751:20200116 124210140} Page 1 of 1