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j o u r n a l o f m a t e r i a l s p r o c e s s i n g t e c h n o l o g y 2 0 4 ( 2 0 0 8 ) 34–38

journal homepage: www.elsevier.com/locate/jmatprotec

Effect of expanded perlite aggregate on the properties of


lightweight concrete

İlker Bekir Topçu a,∗ , Burak Işıkdağ b


a Eskişehir Osmangazi University, Department of Civil Engineering, 26480 Eskişehir, Turkey
b Anadolu University, Porsuk Vocational School, 26470 Eskişehir, Turkey

a r t i c l e i n f o a b s t r a c t

Article history: Expanded perlite aggregate (EPA) is a heat and sound insulator, and lightweight material
Received 27 April 2007 which ensures economical benefits in constructions. This paper investigates the properties
Received in revised form of concrete containing EPA considering cement types (CEM II 32.5R and CEM I 42.5R), dosages
4 October 2007 (300, 350 and 400) and replacement ratios (0, 15, 30, 45 and 60). The tests were conducted on
Accepted 22 October 2007 fresh and hardened concrete. 150 mm × 150 mm × 150 mm cube, ∅150 mm × 300 mm cylinder
and 100 mm × 100 mm × 500 mm prismatic specimens were used for destructive and nonde-
structive tests at the end of 28 days. In experiments, the minimum unit weight of concrete
Keywords: mixture was 1800 kg/m3 at the dosage of 300, and compressive strengths of EPAC (expanded
Lightweight concrete perlite aggregate concrete) were obtained between 20 and 30 MPa at the replacement ratios
Expanded perlite aggregate of 30% considering cement types, thus it was proved that EPAC can be used as lightweight
Fresh and hardened properties concrete with adequate replacement ratios, despite some losses in mechanical properties.
© 2007 Elsevier B.V. All rights reserved.

1. Introduction The economical benefits of lightweight concrete are the


low-heat conductivity and unit weight (Yalgın, 1983a; Seyhan,
Perlite is obtained from pumice, which is a glassy form of rhy- 1977; Maso, 1978; Cilason and Balta, 1994; Topçu, 1999). Today,
olitic or dacitic magma. It contains 2–5% water (Mladenovic et lightweight property of concrete has been still desirable in
al., 2004). Upon rapid heating, perlite transforms into a cellu- constructional elements (Yalgın, 1983b). In most cases, high
lar material of low bulk-density. As the chemical water held buildings have been affected during earthquakes due to the
within the perlite boils (at temperatures of 900–1100 ◦ C), the higher unit weight of concrete; however, replacement of EPA
resultant steam forms bubbles within the softened rock to in concrete may be a solution for reducing damages of earth-
produce a frothy-like structure. The formation of these bub- quakes owing to lightweight property (Durmuş, 1985; Lacroix
bles allows perlite to expand up to 15–20 times of its original and Fuentes, 1980; Ergen, 1983; Balta and Cilasun, 1993). Other-
volume (Gunning, 1994). Expanded perlite aggregate (EPA) has wise, EPA bricks may be used in buildings to reduce the weight
been used in constructional elements such as brick, plaster, of walls which is mentioned in a recent study (Topçu and
pipe, wall and floor block; however has not been industrially Işıkdağ, 2007b). In most studies, EPA has been used as admix-
used in concrete yet (Çobanlı, 1993). Approximately, 4.5 billion ture in cement or directly in concrete as aggregate. In concrete,
tonnes of the total 6.6 billion tonnes of perlite reserve is EPA is used instead of fine aggregate with various replacement
located in Turkey. Besides, other reserves are located in Greece, ratios depending on required strength. In cement, perlite is
USA, Japan, Philippines, Russia, Hungary, Mexico and Italy easier to be ground than the Portland cement clinkers; there-
(Hamamcı, 1998). fore they result in less energy requirement to produce blended


Corresponding author.
E-mail addresses: ilkerbt@ogu.edu.tr (İ.B. Topçu), bisikdag@anadolu.edu.tr (B. Işıkdağ).
0924-0136/$ – see front matter © 2007 Elsevier B.V. All rights reserved.
doi:10.1016/j.jmatprotec.2007.10.052
j o u r n a l o f m a t e r i a l s p r o c e s s i n g t e c h n o l o g y 2 0 4 ( 2 0 0 8 ) 34–38 35

cements by grinding clinker and perlite together. However, weight and specific gravity of aggregates were determined
blended cements with perlite may cause strength losses at according to Turkish Standards (TS 706 EN 12620).
early ages compared to Portland cement, then the strength is
improved by pozzolanic reactions lately (Erdem et al., 2007). 2.1.4. Mixture water
The strength of EPA-based concrete is explained with the In concrete production network water was used according to
bonds between cement and perlite aggregate (Glenn et al., Turkish Standards (TS 1247).
1999).
Generally, admixtures such as silica fume and fly ash
has been used in concrete to improve mechanical properties 2.2. Experimental method
(hydration, alkali silica reaction and permeability) (Demirboğa
et al., 2001). Nonetheless, EPA is an alternative material In initial experiments, the effect of cement types were inves-
to these admixtures; however unit weight and compressive tigated according to 30% EPA ratio. EPA was used instead
strength are decreased with replacement of EPA in concrete of fine aggregate (sand) by volumetric batching considering
mixtures. As is known, the effect of EPA on concrete is volumetric expansion of perlite after wetted. In labora-
increased with increasing cure periods (Demirboğa and Gül, tory, standard cylindrical (150 mm × 300 mm) and cubic
2003). Furthermore, the natural perlite powder has a signifi- (150 mm × 150 mm × 150 mm) concrete specimens were pro-
cant pozzolanic effect and is a good active mineral admixture duced with the cements of CEM I 42.5R and CEM II 32.5R at
for concrete, it has also high-freeze–thaw resistance and fire the dosages of 300, 350 and 400, to determine mechanical
protection capability (Yu et al., 2003; Mo and Fournier, 2007). and physical properties of concrete containing EPA by con-
Moreover, EPA contains some microcrystalline quartz and has ducting fresh and hardened concrete tests on the specimens.
a matrix that is mainly composed of chalcedony, which is In secondary experiments, CEM I 42.5R was used with the
potentially susceptible for alkali silica reaction (Collins et al., dosages of 300, 350, 400 and EPA was used with the replace-
2004; Topçu and Işıkdağ, 2007a). Hence, there has been an ment ratios of 0%, 15%, 30%, 45% and 60% to determine the
increasing interest in EPA-based concrete. effects of EPA on compressive and splitting tensile strengths.
The water/cement ratio was determined as 0.5 in the mixtures.
The specific weights of sand and crushed stone were 2600
2. Experimental study and 2700 kg/m3 , respectively, and the maximum aggregate size
was 31.5 mm in concrete mixtures. During production process,
2.1. Materials the fresh concrete was mixed with a mixer, and specimens
were vibrated on vibration table. The workability of concrete
2.1.1. Expanded perlite aggregate (EPA) mixtures was also determined with slump tests. The concrete
Perlite contains 70–75% silicon dioxide and 12–16% alumina. specimens were cured in lime saturated water at 23 ± 1 ◦ C for
Other components are sodium oxide, potassium oxide, ferro 28 days, afterwards destructive and nondestructive tests were
oxide, manganese oxide, titan oxide and sulfide (Topçu and conducted on specimens (TS EN 12350, 12390). The dynamic
Işıkdağ, 2007b). The physical properties of EPA are given elasticity modulus of specimens was calculated with the for-
in Table 1. The unit weight of EPA depends on grada- mula
tion and expansion. The heat conductivity of perlite with
the unit weight of 90 kg/m3 is 0.04 W/mK at 24 ◦ C accord-
ing to Turkish Standard (TS 3681) (Topçu and Işıkdağ, V 2 n(1 + )(1 − 2)
Ed (10−6 ) =
2007b). 1−

2.1.2. Cement
( = poisson, n = unit weight (kg/m3 ) and V = pulse velocity
In experiments, CEM I 42.5R and CEM II 32.5R produced by
(m/s).
ESÇİM cement factory were used (TS EN 197-1).

2.1.3. Aggregate
Osmaneli sand and crushed stones were used as aggregate 3. Results and discussion
in concrete production. The gradations of aggregates were
prepared considering the reference curves (TS 707). The unit According to experimental results, dynamic elasticity modu-
lus, compressive and splitting tensile strengths increase with
the increase in dosage and cement quality. It is proved that
cement types and dosages inconsiderably affect workability;
Table 1 – Physical properties of expanded perlite however, as the dosage and cement quality increases, VeBe
Color White time and unit weight increase, slump decreases. The test
Melting point 1300 ◦ C results of fresh and hardened concrete specimens are given
Specific heat 0.20 kcal/kg ◦ C in Figs. 1–4, respectively. The compressive and splitting ten-
Unit weight 2.2–2.4 g/cm3 sile strengths considerably decreased with the increase in EPA
Rough density 30–190 kg/m3
ratio; however it was observed that EPAC can be still pro-
Heat conductivity 0.034–0.040 kcal/m h ◦ C
duced with the lower replacement ratios despite the losses
Sound insulating 18 db (125 Hz)
in mechanical properties.
36 j o u r n a l o f m a t e r i a l s p r o c e s s i n g t e c h n o l o g y 2 0 4 ( 2 0 0 8 ) 34–38

Fig. 1 – Unit weight and VeBe value of fresh concretes Fig. 4 – Splitting-tensile strengths of concretes containing
containing 30% EPA ratio considering cement type and 30% EPA ratio considering cement type, dosage and
dosage. specimen shape.

unit weight of concrete mixtures produced with CEM I 42.5R


at dosages of 350 and 400 increased 4.78% and 10.87%, respec-
tively compared to concrete at dosage of 300 with the same
type of cement. As is known, the specific gravity of the CEM
I 42.5R was higher than specific gravity of the CEM II 32.5R
cement, therefore the fresh unit weights of the concretes pro-
duced with CEM II 32.5R cement were consequently lower, this
decrease was obtained 2.17%, 2.23% and 3.92% for concretes
at dosages of 300, 350 and 400, respectively. In experiments,
it was observed that the minimum unit weight of concrete
specimens was 1800 kg/m3 at the dosage of 300, which was
Fig. 2 – Slump and flow of fresh concretes containing 30% adequate for a lightweight concrete. Furthermore, the mini-
EPA ratio considering cement type and dosage. mum and maximum unit weights of hardened concretes were
between 1750 and 1900 kg/m3 .

3.1.2. VeBe time


3.1. Fresh concrete tests of EPAC containing 30%
It was observed that the VeBe times of concrete mixtures
perlite ratio considering cement type
increased with the increase in dosage and were between
3.40 and 3.80 s. The VeBe time of mixtures produced with
3.1.1. Unit weight
CEM II 32.5R at dosages of 350 and 400 increased 5.88%
The unit weights of concrete mixtures were calculated
and 8.82%, respectively, compared to concrete at dosage of
between 1800 and 2040 kg/m3 . It was proved that the unit
300 with the same type of cement. Nevertheless, the VeBe
weight of fresh concrete increased as the specific gravity and
time of mixtures produced with CEM I 42.5R at dosages of
dosage of cement increased. The fresh unit weight of concrete
350 and 400 increased 5.71% and 8.57%, respectively com-
mixtures produced with CEM II 32.5R at dosages of 350 and 400
pared to concrete at dosage of 300 with the same type of
increased 4.72% and 8.89%, respectively compared to concrete
cement. The VeBe time of the fresh concrete mixtures pro-
at dosage of 300 with the same type of cement. And, the fresh
duced with CEM II 32.5R was approximately 2.73% lower than
the VeBe time of the concrete mixtures produced with CEM
I 42.5R.

3.1.3. Slump and flow


The slumps of the concrete mixtures were observed between
100 and 130 mm. The concrete mixtures with lower unit
weight had higher slump values, due to their porous struc-
ture. The slumps of concretes with CEM II 32.5R and CEM I
42.5R cements at dosage of 400 decreased 7.69% and 0.09%,
respectively compared to those at 300 dosage. Consequently,
it was observed that the slump values of the concretes with
CEM II 32.5R were higher than the slump values of the con-
Fig. 3 – Compressive strengths of concretes containing 30% cretes with CEM I 42.5R cement. Furthermore, flow test results
EPA ratio considering cement type, dosage and specimen were observed between 310 and 360 mm as demonstrated in
shape. Fig. 2.
j o u r n a l o f m a t e r i a l s p r o c e s s i n g t e c h n o l o g y 2 0 4 ( 2 0 0 8 ) 34–38 37

3.2. Destructive tests of EPAC containing 30% perlite


ratio considering cement type

The hardened concrete test results of lightweight concretes


containing EPA were examined according to figures. The con-
crete specimens were grouped as 300, 350 and 400 considering
dosages, and strengths were demonstrated in Figs. 3 and 4,
in order to make a comparison. It was observed that the
compressive and splitting-tensile strengths were considerably
low compared to conventional concrete at the same dosages,
owing to EPA. The minimum compressive and splitting-tensile
strengths were 11 and 1.7 MPa at the dosages of 300, and the
maximum values of these strengths were 26 and 2.3 MPa at
the dosages of 400, respectively, for cylindrical specimens with
different types of cements.
The compressive strengths of concretes containing 30%
EPA were calculated between 11 and 33 MPa according to Fig. 6 – Splitting tensile strengths of CEM I 42.5R concrete
dosage, cement type and shape of the specimens, and they cylindrical specimens considering cement dosage and
approximately increased 20% and 30% at the dosages of replacement ratio of EPA.
350 and 400, respectively, compared to 300 dosages. Con-
sequently, it was observed that the cylindrical compressive
strengths were 30% lower than cubic compressive strengths.
Furthermore, the splitting-tensile strengths increased with
the increase in dosage, and were observed between 0.9 and
2.3 MPa depending on specimen shape, dosage and cement.
The splitting-tensile strength increased 13% and 22% at the
dosages of 350 and 400, respectively, compared to those at 300
dosage, and splitting-tensile strength of concrete produced
with CEM II 32.5R cement was approximately 8% lower than
those with CEM I 42.5R.

3.3. Destructive tests of EPAC containing 0%, 15%, Fig. 7 – Ultrasonic pulse velocity and modulus of dynamic
30%, 45% and 60% perlite considering cement type and elasticity of concretes containing 30% EPA ratio considering
replacement ratio cement type and dosage.

The concrete specimens were produced with CEM I 42.5R at


the dosages of 300, 350 and 400 considering 0%, 15%, 30%,
45% and 60% replacement ratios to determine the effects of of 300, and the maximum values of these strengths were 37
EPA on compressive and splitting tensile strengths, as demon- and 3.5 MPa at the dosages of 400, respectively. According to
strated in Figs. 5 and 6. The minimum compressive and results, the optimum strengths for lightweight concrete were
splitting-tensile strengths were 15 and 1.5 MPa at the dosages obtained between 15% and 30% ratios at the dosage of 350 and
400. Furthermore, results have shown that higher replacement
of EPA (60%) negatively affects both compressive and split-
ting strengths of concrete specimens, but positively affects the
lightweight property.

3.4. Nondestructive tests of EPAC containing 30%


perlite ratio considering cement type

3.4.1. Ultrasonic pulse velocity and dynamic elasticity


modulus
The maximum and minimum ultrasound pulse velocities
were 2.5 and 3.2 km/s, respectively. These results were used
for calculating dynamic elasticity modulus of specimens.
The dynamic elasticity moduli of the concrete specimens
were determined between 11 and 20 GPa. It was observed
that dynamic elasticity modulus increased as the dosage
Fig. 5 – Compressive strengths of CEM I 42.5R concrete increased, as shown in Fig. 7. This increase were approxi-
cylindrical specimens considering cement dosage and mately 16% and 9% at the dosages of was 400 and 350 for
replacement ratio of EPA. cylindrical specimens, compared to 300 dosage with same
38 j o u r n a l o f m a t e r i a l s p r o c e s s i n g t e c h n o l o g y 2 0 4 ( 2 0 0 8 ) 34–38

type of cement. However, dynamic elasticity modulus of cubic of lightweight concrete. Cement Concrete Res. 33 (5),
specimens approximately increased 26% and 4.5%, at the 723–727.
dosages of 350 and 400, respectively, compared to the concrete Demirboğa, R., Örüng, İ., Gül, R., 2001. Effects of expanded perlite
aggregate and mineral admixtures on the compressive
at the dosage of 400 with same type of cement.
strength of low-density concretes. Cement Concrete Res. 31
(11), 1627–1632.
Durmuş, A., 1985. Prestressed Concrete Course Notes. Karadeniz
4. Conclusions
Technical University, Department of Civil Engineering,
Trabzon, Turkey (in Turkish).
In this study, initially 30% replacement ratio of EPA was used Erdem, T.K., Meral, Ç., Tokyay, M., Erdoğan, T.Y., 2007. Use of
to determine the effects of cement type; secondarily vari- perlite as a pozzolanic addition in producing blended
ous replacement ratios were used to determine the effects of cements. Cement Concrete Compos. 29 (1),
EPA on compressive and splitting tensile strengths for pre- 13–21.
diction of lightweight properties of concrete. According to Ergen, M., 1983. Bibliography of perlite in structure. The Scientific
and Technical Research Council of Turkey, Structural Research
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Institute, Ankara, Turkey (in Turkish).
with improving cement quality, dosage or replacement ratio
Glenn, G.M., Gray, G.M., Orts, W.J., Wood, D.W., 1999. Starch-based
of EPA. It was proved that, the more use of EPA ensures the lightweight concrete: effect of starch source, processing
less strength and better lightweight property. Furthermore, method, and aggregate geometry. Ind. Crops Prod. 9 (2),
the minimum unit weight for lightweight concrete consider- 133–144.
ing cement types was obtained with the CEM II 32.5R cement at Gunning, D.F., 1994. Perlite Market Study Report. Gunning and Mc
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Mladenovic, A., Suput, J.S., Ducman, V., Skapin, A.S., 2004.
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