UNIVERSIDAD SANTIAGO DE CALI

Project Name: cafeina

Reported by User: Breeze user (Breeze)

0,70

0,60

0,50

0,40
AU

Cafeina - 1,405
0,30

0,20

0,10

0,00

0,00 0,50 1,00 1,50 2,00 2,50 3,00 3,50 4,00 4,50 5,00
Minutes
Sample Name: STD 1 - 4 ppm; Date Acquired: 02/01/2006 03:44:38 AM COT; Vial: 1;
Injection: 1
Sample Name: STD 2 - 12 pm; Date Acquired: 02/01/2006 03:48:23 AM COT; Vial: 2;
Injection: 1
Sample Name: STD 3 -24 ppm; Date Acquired: 02/01/2006 03:51:38 AM COT; Vial: 3;
Injection: 1
Sample Name: STD 4 - 36 ppm; Date Acquired: 02/01/2006 03:54:52 AM COT; Vial: 4;
Injection: 1
Sample Name: STD 5 - 48 ppm; Date Acquired: 02/01/2006 03:58:32 AM COT; Vial: 5;
Injection: 1
Sample Name: Muestra 1 Cafe G2; Date Acquired: 02/01/2006 04:03:52 AM COT; Vial: 8;
Injection: 1
Sample Name: Muestra 2 Coca Cola G2; Date Acquired: 02/01/2006 04:09:25 AM COT; Vial:
9; Injection: 1
Sample Name: Muestra 3 Cafe M; Date Acquired: 02/01/2006 04:15:03 AM COT; Vial: 10;
Injection: 1
Sample Name: Muestra 4 Sevedol; Date Acquired: 02/01/2006 04:20:41 AM COT; Vial: 11;
Injection: 1
Sample Name: Muestra 5 Acetaminofenl; Date Acquired: 02/01/2006 04:27:38 AM COT; Vial:
12; Injection: 1

Com ponent Sum m ary For Retention Tim e

Channel: W2489 ChA
Sample
Inj. Channel Vial Cafeina
Name
1 STD 1 - 4 ppm 1 W 2489 ChA 1 1,405
2 STD 2 - 12 pm 1 W 2489 ChA 2 1,415
3 STD 3 -24 ppm 1 W 2489 ChA 3 1,406
4 STD 4 - 36 ppm 1 W 2489 ChA 4 1,403
5 STD 5 - 48 ppm 1 W 2489 ChA 5 1,407

Report Method: Component Summary with Chrom Printed: 02/01/2006

Page: 1 of 3 05:17:50 a.m. America/Bogota
UNIVERSIDAD SANTIAGO DE CALI
Project Name: cafeina
Reported by User: Breeze user (Breeze)
Com ponent Sum m ary For Retention Tim e
Channel: W2489 ChA
Sample
Inj. Channel Vial Cafeina
Name
6 Muestra 1 Cafe G2 1 W 2489 ChA 8 1,406
7 Muestra 2 Coca Cola G2 1 W 2489 ChA 9 1,411
8 Muestra 3 Cafe M 1 W 2489 ChA 10 1,412
9 Muestra 4 Sevedol 1 W 2489 ChA 11 1,407
10 Muestra 5 Acetaminofenl 1 W 2489 ChA 12 1,398
Mean 1,407
Std. Dev. 0,005
% RSD 0,3

Com ponent Sum m ary For Area

Channel: W2489 ChA
Sample
Inj. Channel Vial Cafeina
Name
1 STD 1 - 4 ppm 1 W 2489 ChA 1 109330
2 STD 2 - 12 pm 1 W 2489 ChA 2 388807
3 STD 3 -24 ppm 1 W 2489 ChA 3 587936
4 STD 4 - 36 ppm 1 W 2489 ChA 4 988605
5 STD 5 - 48 ppm 1 W 2489 ChA 5 1483738
6 Muestra 1 Cafe G2 1 W 2489 ChA 8 471879
7 Muestra 2 Coca Cola G2 1 W 2489 ChA 9 292978
8 Muestra 3 Cafe M 1 W 2489 ChA 10 72213
9 Muestra 4 Sevedol 1 W 2489 ChA 11 23433
10 Muestra 5 Acetaminofenl 1 W 2489 ChA 12 86555
Mean 450547
Std. Dev. 468976
% RSD 104,1

Com ponent Sum m ary For Am ount

Channel: W2489 ChA
Sample
Inj. Channel Vial Cafeina
Name
1 STD 1 - 4 ppm 1 W 2489 ChA 1
2 STD 2 - 12 pm 1 W 2489 ChA 2
3 STD 3 -24 ppm 1 W 2489 ChA 3
4 STD 4 - 36 ppm 1 W 2489 ChA 4

Report Method: Component Summary with Chrom Printed: 02/01/2006

Page: 2 of 3 05:17:50 a.m. America/Bogota
UNIVERSIDAD SANTIAGO DE CALI
Project Name: cafeina
Reported by User: Breeze user (Breeze)
Com ponent Sum m ary For Am ount
Channel: W2489 ChA
Sample
Inj. Channel Vial Cafeina
Name
5 STD 5 - 48 ppm 1 W 2489 ChA 5
6 Muestra 1 Cafe G2 1 W 2489 ChA 8
7 Muestra 2 Coca Cola G2 1 W 2489 ChA 9
8 Muestra 3 Cafe M 1 W 2489 ChA 10
9 Muestra 4 Sevedol 1 W 2489 ChA 11
10 Muestra 5 Acetaminofenl 1 W 2489 ChA 12
Mean
Std. Dev.
% RSD

Report Method: Component Summary with Chrom Printed: 02/01/2006

Page: 3 of 3 05:17:50 a.m. America/Bogota