GeMS No: 100463728

Revision: AL
Date: 2nd Aug 2018
METALLIC MATERIAL SPECIFICATIONS Page: 1 of 4
Title: CMS-Z28GN.0, 2-1/4 Cr-1Mo, Q&T, 90 KSI YS

1. Scope:

1.1 This specification is for 2-1/4 Cr-1Mo (ASTM A182, F 22 modified) material sizes up to 20”
in diameter.

1.2 This material meets the requirements of NACE MR0175 /ISO 15156.

2. Applicable Standards (Use latest editions)

Specification Description

ASTM A 182, F22 Forged or Rolled Alloy-Steel Pipe flanges, Forged Fittings and Valves
(modified) and Parts for High Temperature Service
ASTM A-370 Methods and Def. for Mechanical Testing of Steel Products
Petroleum and natural gas industries - Materials for use inH2S -
NACE MR0175 /
containing environments in oil and gas production- part3: Cracking-
ISO 15156
Resistant CRAs (corrosion resistant alloys) and other alloys
API 6A/

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Specification for Wellhead and Christmas Tree Equipment
ISO 10423
Recommended Practice for Completion/Workover Risers - Second
API RP17G
Edition; ISO 13628-7:2005 Adoption
Recommended Practice for Personal Qualification and Certification in
ASNT SNT TC-1A
Non-Destructive Testing
MT-16 Approved Supplier Requirement

QA-31 Control of Management Systems Records

NDE-31 Ultrasonic Examination of Wrought Metals

3. Requirements:

3.1 Material:

3.1.1 Melting Practice: The steel shall be made using fine grain practice using one of
the following methods.

3.1.1.1 Basic Oxygen Furnace followed by Vacuum Degassing (BOFVD) or Argon

Oxygen Decarburization (BOFAOD).

3.1.1.2 Electric Furnace (EF) or Electric Furnace followed by Vacuum Degassing

(EFVD) or Argon Oxygen Decarburization (EFAOD).

3.1.1.3 Vacuum Induction Melting (VIM).

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 GeMS No: 100463728
Revision: AL
Date: 2nd Aug 2018
METALLIC MATERIAL SPECIFICATIONS Page: 2 of 4
Title: CMS-Z28GN.0, 2-1/4 Cr-1Mo, Q&T, 90 KSI YS

3.2 Chemical Composition: Shall be as follows:

Element Percent
Carbon 0.10 - 0.15 Range
Manganese 0.40 - 0.80 Range
Phosphorous 0.025 Max
Sulfur 0.025 Max
Silicon 0.5 Max
Chromium 2.00 - 2.50 Range
Molybdenum 0.90 - 1.10 Range
Copper* 0.35 Max
Nickel* 0.50 Max
Vanadium* 0.05 Max

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Iron Balance

Note: *As residual elements, these need not be reported provided they comply with the
chemical requirements.

3.3 Heat Treatment:

3.3.1 Heat treating equipment qualification and calibration:

Furnaces shall be calibrated no less than once a year or when a furnace is moved,
repaired or rebuilt. The practice for qualification of heat-treating equipment shall be
one of the following:

3.3.1.1 API 6A annex for qualification of heat-treating equipment or other

equivalent internationally recognized standard.

3.3.1.2 Manufacturers’ written specifications including acceptance criteria, which

are not less stringent than the procedures identified above.

3.3.2 Temperature monitoring:

The material temperature shall be measured by use of either a contact surface

thermocouple or a heat-sink as described in API 6A, ISO 10423 or equivalent
international standard.

3.3.3 All heat treatment shall be carried out in accordance with written procedures.
Temperature, time at temperature and method of cooling must be reported for each
cycle.

3.3.4 The quench media shall be one of the following:

3.3.4.1 Oil
3.3.4.2 Polymer

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Warning: The controlled source document of this document is stored within the Product Data Management System (PDMS). Any paper
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 GeMS No: 100463728
Revision: AL
Date: 2nd Aug 2018
METALLIC MATERIAL SPECIFICATIONS Page: 3 of 4
Title: CMS-Z28GN.0, 2-1/4 Cr-1Mo, Q&T, 90 KSI YS

3.3.4.3 Interrupted water, water or other water equivalent quench

3.3.5 The temperature of the water or the quench media with cooling rate approximately
that of water shall not exceed 400C (1040F) at the start of the quench. For bath
type quenching, the temperature of water or equivalent quench media shall not
exceed 490C (1200F) at the completion of quench.

3.3.6 The temperature range for other quenching media shall meet manufacturer written
specification.

3.3.7 If the heat treatment is carried by sub-supplier, heat treater shall ensure the
compliance of mechanical properties established in section 3.4.

3.3.8 Heat Treatment Procedure:

3.3.8.1 The material shall be supplied in the quench and temper or normalized
quench and tempered condition.

3.3.8.2 Optional: Normalize at 1725-17750F (941-9680C) followed by air cool or

faster.

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3.3.8.3 Austenitize at 1675-17750F (913-9680C) followed by water or polymer
quench.

3.3.8.4 Temper at 1100-13000F (593-7040C) followed by air cool or faster.

3.4 Mechanical Properties:

After quench and temper heat treatment, a tensile test and three Charpy tests shall be
performed in accordance with ASTM A370 on each heat of material. The sample shall be
taken from mid-radius in the case of a solid bar or at the mid-wall in the case of a hollow.

Custom forgings require mechanical tests from a prolongation per API 6A. The results
shall conform to the following:

Requirement
Property
Testing Direction Value
Tensile Strength, psi (MPa), Min Transverse direction 105,000 (724)
Yield Strength, psi (MPa), Min Transverse direction 90,000 (620)
Elongation on 5D (4D), %, Min Transverse direction 16 (18)
Reduction in Area, %, Min Transverse direction 35
Hardness, BHN (HRC), Max - 237 (22)
Charpy V-Notch Average, J (Ft.Lbs), Min Transverse direction 40 (30)
@ - 29°C (-20°F) Single, J (Ft.Lbs), Min 30 (22)

3.5 NDE:

3.5.1 All NDE instructions are to be approved by a Level III Examiner. The person
performing the NDE shall be qualified in accordance with ASNT: Recommended
Practice SNT TC-1A Level II minimum. A copy of the person’s qualifications

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Warning: The controlled source document of this document is stored within the Product Data Management System (PDMS). Any paper
version of this document is uncontrolled and should be compared with the source document at time of use to ensure it is up-to-date.
 GeMS No: 100463728
Revision: AL
Date: 2nd Aug 2018
METALLIC MATERIAL SPECIFICATIONS Page: 4 of 4
Title: CMS-Z28GN.0, 2-1/4 Cr-1Mo, Q&T, 90 KSI YS

performing the NDE shall be on file at Supplier or a copy shipped with the parts.

3.5.2 Ultrasonic examination must be performed per NDE-31.

3.6 Material Quality:

The material shall be free of injurious seams, laps, or other visual imperfections, which,
due to their nature, will interfere with the use of the material in heat treating, machining,
or fabrication of suitable parts.

4. Documentation and Retention:

Supplier records involving this specification must be auditable / retrievable for a period of five (5)
years from the date that the raw materials were certified. Supplier should submit the copy of
following documents along with certification package.

4.1. Supplier should submit the copy of following documents along with certification package,
unless otherwise instructed by a Schlumberger specification.

4.2. Copy of the original mill test certificate from producing mill.

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4.3. Copy of actual chemical composition (heat analysis) of the material which lists all of the
elements specified in paragraph 3.2.

4.4. Copy of mechanical properties. Test results must meet the requirements of paragraphs 3.4.

4.5. Statement of compliance of heat treatment as per 3.3

4.6. Statement of compliance of Ultrasonic examination per section 3.5.

4.7. Statement of compliance from mill or supplier conforming compliance with this specification
(by number) and the Schlumberger Purchase order (by number and line item number).

4.8. All documentation generated by this specification shall be retained in accordance with
procedure QA-31.

5. Required Approvals: Project: MatEng

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Warning: The controlled source document of this document is stored within the Product Data Management System (PDMS). Any paper
version of this document is uncontrolled and should be compared with the source document at time of use to ensure it is up-to-date.