Professional Documents
Culture Documents
Manual
Mobile Algae Filtration - unit
(MAF-unit, 140923-00005)
SCT/1310383/DVH-FVH/dvh/15-043
October 2015
SCT/1310383/DVH-FVH/dvh/15-043
All rights, amongst which the copyright, on the materials described in this document rest with the Flemish Institute for Technological Research NV
(“VITO”), Boeretang 200, BE-2400 Mol, Register of Legal Entities VAT BE 0244.195.916.
The information provided in this document is confidential information of VITO. This document may not be reproduced or brought into circulation
without the prior written consent of VITO. Without prior permission in writing from VITO this document may not be used, in whole or in part, for the
lodging of claims, for conducting proceedings, for publicity and/or for the benefit or acquisition in a more general sense.
Summary
SUMMARY
De MAF-unit is a membrane filtration circuit of type MBR (membrane Bio Reactor). It is constructed
for India to test different membranes. The maximum membranes the test bench can contain is 3.
Therefore, 3 modules will control and measure the membranes. One module consists of a pressure
sensor, a flowmeter, a peristaltic pump (rotates right and left). This module is connected to a
membrane frame.
Mefias®-software is used for the process control, it is communicating with the compactFieldPoint-
modules van National Instruments in the electro-box.
SCT/1310383/DVH-FVH/dvh/15-043
I
Table of Contents
TABLE OF CONTENTS
Summary _______________________________________________________________________ I
CHAPTER 2 Start-up____________________________________________________________ 6
2.1. General 6
® ®
2.1.1. Microsoft Windows settings __________________________________________ 6
2.1.2. Windows® Explorer ___________________________________________________ 6
2.2. Set-up of the skid 7
2.2.1. Connection laptop to Fieldpoint _________________________________________ 7
2.2.2. Pump settings _______________________________________________________ 7
2.2.3. Installation the IPC membranes _________________________________________ 7
2.2.4. Start the influent ____________________________________________________ 8
SCT/1310383/DVH-FVH/dvh/15-043
II
Table of Contents
SCT/1310383/DVH-FVH/dvh/15-043
III
List of Tables & Figures
SCT/1310383/DVH-FVH/dvh/15-043
IV
List of Symbols
LIST OF SYMBOLS
SCT/1310383/DVH-FVH/dvh/15-043
V
CHAPTER 1 General Overview
temperature
Permeate 3
Presuure Flow measurement Pump 2
2 directions Permeate 3
measurement directions
membrane 2
membrane 1
Pressure
Flow measurement
regulator
Pressure
Flow measurement
regulator
Air
pressure
Feed pump
Pressure switch
This bioreactor is of the type submerged membrane bioreactor (MBR) containing 3 membranes
(plate). The membrane position in the reactor is very important. (see 1.3. )
SCT/1310383/DVH-FVH/dvh/15-043
1
CHAPTER 1 General Overview
1.2. P&ID
FI-1 FI-2
PU tubing 8x5,5
TT-1
R-1 R-2
4 bar 4 bar
Air
pressure
Filtratie membraan
Filtratie membraan
Filtratie membraan
PS
Algea reactor
P-4
1.3. EXPLANATION
The airflow under the membranes, is supplied in order to keep the membranes clean at the
outside, a continuous airflow of about 0,3 Nm³/h per aeration tube must be applied on the flow
indicators FI-1 and FI-2.
The algae reactor should be filled with the necessary quantity of algae influent. The level of the
algae reactor tank is controlled by the position of the level sensor (LT-1). The algae influent is
added by means of influent pump P-4. The flow rate of pump P-4 can be varied manually by turning
the potentiometer knob on the controller of pump P-4. Influent is added when the liquid level of
the reactor is below the level sensor. A delay time is implemented in order to prevent pulsation of
pump P-4. When the high level is not reached within 2 minutes, the installation stops working (this
will probably be due to lack of influent).
The flow of the permeates, caused by the permeate pumps P-1, P-2 and P-3, is measured by means
of the flow meter FIT-1, FIT-2 and FIT-3. This measurement is used to calculate the actual flux
through the membrane. Under-pressure in the permeate pipes are measured by means of the
pressure transmitters PIT-1, PIT-2 and PIT-3. These results are used for the calculation of the TMP
(transmembrane pressure).
SCT/1310383/DVH-FVH/dvh/15-043
2
CHAPTER 1 General Overview
In the algae reactor, 1 to 3 membrane IPC plates are applied. If a plate is removed, the hose should
be shut off and the plate should be replaced by a dummy plate. The purpose of this dummy plate is
to lead the air bubbles along the other membranes in order to clean them. Best is to keep the
middle plate and to replace one or both of the outer plates by a dummy depending on the
application.
The normal working procedure is for the benchmark Kubota filtration during 4 minutes and 1
minute relaxation and for the IPC membranes filtration during 4 minutes and backwash during 20
seconds (0.33 minutes) at 150 % filtration flux1 minute and 1 minute relaxation. During the
backwash phase, permeate water is sent back to the membranes, which helps to keep the
membranes clean. Therefore one must be careful that the ends of the permeate lines after the
permeate pumps are always immersed in the permeate liquid.
1.4.1. COMPONENTS
Table 1: Components A
SCT/1310383/DVH-FVH/dvh/15-043
3
CHAPTER 1 General Overview
Table 2: Components B
SCT/1310383/DVH-FVH/dvh/15-043
4
CHAPTER 1 General Overview
SCT/1310383/DVH-FVH/dvh/15-043
5
CHAPTER 2 Start-up
CHAPTER 2 START-UP
2.1. GENERAL
® ®
2.1.1. MICROSOFT WINDOWS SETTINGS
Start the computer and log on with the username “MBRP3b” and the password “IonEx2015”.
The MS Windows taskbar is set to ‘auto hide’, it appears by dragging the arrow to the bottom of
the screen.
To put data in to the settings , use the American decimal notation. (decimal dot instead of decimal
comma).
®
2.1.2. WINDOWS EXPLORER
SCT/1310383/DVH-FVH/dvh/15-043
6
CHAPTER 2 Start-up
Connect the black USB with the serial adapter cable on the computer at the USB-port which is
indicated with a yellow arrow (→, COM-port 3). Connect the other side of the USB to the serial
adapter cable with the serial cable. The other side of the serial cable is plugged to the electrical
cabinet on the front side of the installation.
Change pump settings of the 3 pumps from manual to “ANA/AUTO” setting by pressing on the
mode button.
The installation should always be used with 3 membranes as the positioning over the aeration
tubes is very important.
If it is hard to get the tubing over the column, just heat the tubing with heated air. The
polyurethane tubing has an internal diameter of 5,5mm and an external diameter of 8mm. Keep
the IPC membranes together while entering the reactor chamber (see Figure 6). It is very important
that the membranes are exactly positioned on the middle of the aeration zone.
SCT/1310383/DVH-FVH/dvh/15-043
7
CHAPTER 2 Start-up
Make sure the emergency stop is pulled out. Put the main switch on the left side of the electrical
cabinet in position I.
Fill the bioreactor with algae influent. The membranes must be completely immersed in the liquid.
Connect a compressed air supply to the inlet of the pressure switch PS-1. Regulate the pressure on
the pressure regulators R-1 and R-2 until the pressure is about 2 bar. Open the valves V-1 and V-2
until the flow indicators FI-1 and FI-2 indicate a flow of about 0,3 Nm³/h.
Place 3 permeate collection tanks. Make sure that the end of the permeate lines after the
permeate pumps are always at the bottom of the permeate collection tanks in order to avoid air
going through the lines during a backwash.
At the first start, in order to evacuate the air in all the permeate lines, one should slowly fill all the
permeate lines with water. This can best be done by selecting the program ‘deaeration’ in the tab
‘Prog’, as well as in the tabs ‘Pr. 2’ and Pr. 3’. The way to do this is explained in chapter 3.
After pressing the button, the 3 pumps will start at a low speed (10 %), and the
permeate lines will slowly fill up with water. When all the lines are filled, press the
button.
SCT/1310383/DVH-FVH/dvh/15-043
8
CHAPTER 3 Mefias®-software
CHAPTER 3 MEFIAS®-SOFTWARE
3.1. SOFTWARE
The module data for the used membranes must be loaded (see Figure 10) from which the flux can
be calculated as well as the safety parameters to protect the membrane. The desired sample
interval in seconds can be changed if needed .
Click on the button to run the program. A filename is created automatically which
contains following information (see Figure 12):
201X_XX_XX : yyyy_MM_dd (the start date);
-xx : a prefix name which can be filled in in the tab ‘Control’;
_XX(c) : the xth run on the start-up-day and (c) for the next days.
As an example one can get such a filename:
At the start-up date and time are mentioned and left of it is positioned the
actual time.
SCT/1310383/DVH-FVH/dvh/15-043
9
CHAPTER 3 Mefias®-software
SCT/1310383/DVH-FVH/dvh/15-043
10
CHAPTER 3 Mefias®-software
Since in the algae reactor 3 membranes can be inserted which can be operated separately, every
membrane must be registered as a separate module in the module data. As a result, 3 different
programs can run simultaneously. These programs must be selected via the tabs
. Both on the tab ‘Pr. 2’ as on the tab ‘Pr.3’ the module button must be switched
in the ‘On’-position if you want to work with the 3 membranes.
Fill out the name of the membranes that will be tested. This will be logged in the files. The first
module needs to be a Kubota membrane. Module 2 and 3 need a IPC membrane.
Fill out the surfaces in m² ; it is very important to calculate the TMP and the flux. The surfaces of
the membranes that are shipped with this installation are given in figure 12.
SCT/1310383/DVH-FVH/dvh/15-043
11
CHAPTER 3 Mefias®-software
When running, one can follow the actual state of the sequences in the Prog-, Pr.2- and Pr.3-TAB. In
Figure 12 the red dot on the left indicates that this is the actual
running line of the program. In the field PROGRAM LINE DATA all data of the actual line are
displayed. On the lower half of the figure it can be seen that the remaining time of the filtration is
6min10sec on a total filtration time of 8 minutes. The total amount of effluent till now has been
0.035 litres. The sample interval is 10 seconds. The permeate pump P-1 is running at 55.5% of its
maximum capacity. The flux is set at 20.00 l/hm² and the pump P-1is running forward (radio button
P1F is green).
In Figure 9 and Figure 12 it can be seen that there is one procedure line for the filtration, one
procedure line for the backwash and one procedure line for the relaxation. For the 2 other
membranes, the working procedure on the tabs ‘Pr.2’ and ‘Pr.3’ are similar as for the first
membrane on the ‘Prog’ tab.
SCT/1310383/DVH-FVH/dvh/15-043
12
CHAPTER 3 Mefias®-software
The visualisation of the parameters can be followed in the TAB Graphs (see Figure 13). Here, the
sample interval is 10 seconds and the actual number of samples taken is 230.
The selected parameters like are displayed on the graph. Selecting or deselecting a
parameter can be performed with a mouse click on the button.
The auto-scale of the X-axis and the Y-axis can be set by selecting the appropriate button
. Here, the values and the time are automatically scaled. If auto-scaling of the values
(sc.Y) is not set, there might be a risk that not all values appear on the screen. It should therefore
only be deselected to zoom in for the evaluation of a parameter. To do so, the minimum or
maximum value of the Y-axis must be selected with the mouse and the needed value must be
entered. Afterwards the appropriate button should be set back on auto-scaling.
The actual value of the parameters TMP, MTC @ 20°C and effluent flow (production) are
continuously displayed at the bottom of the screen for the 3 membranes:
. The following premise is made: since the permeate
pump sucks the liquid through the membrane plate, the TMP (and also the MTC) is negative. The
positive value is used in case the pump would push through the membrane. At start-up, the
negative value might be positive.
SCT/1310383/DVH-FVH/dvh/15-043
13
CHAPTER 3 Mefias®-software
To select the visualisation of the actual parameters again, click on and select
Real-time. The logging files can easily be imported into a spreadsheet program for
further investigation.
To bring the data to an excel sheet : drag the .txt file in to the open excel sheet.
SCT/1310383/DVH-FVH/dvh/15-043
14
CHAPTER 3 Mefias®-software
In the P&ID-TAB (see Figure 15) it can be seen which components are activated (=coloured) and all
parameters (also the non-selected in the Graphs-TAB) are continuously monitored.
In the Alarms-TAB an not only an overview of the logged alarms (e.g. no air pressure, no flow,…) is
presented, but also other actions like e.g. when high level sensor LS01 has been reached, the
program has been stopped manually, …
SCT/1310383/DVH-FVH/dvh/15-043
15
CHAPTER 3 Mefias®-software
The password “ctrl” must be used to enter the programming level. As can be seen, two TABs are
added namely TAB “Proc” (procedure) and TAB” Prog list”.
Warning: This level should be used with caution. By bad programming, parts of the
MAF-unit can be destroyed. After finishing changes to the procedure and program,
enter password “strt” to put Mefias® back in operator mode and to avoid accidental
changes of parameter settings.
While being online, a procedure can be adapted or made from scratch. For instance the flux can be
adapted, the filtration or relaxation time can be altered… Best is not to change other things.
SCT/1310383/DVH-FVH/dvh/15-043
16
CHAPTER 3 Mefias®-software
. Push the save button and keep the same name (overwrite the previous
version).
Warning: Please do not alter other things, since correct functioning of the
installation cannot be guaranteed anymore.
If one has changed the procedure name, the newly made procedure can only be implemented into
the program when it has been stopped by . The procedure can be added by pushing
the button (see Figure 9) next to the appropriate program line. If a program line has to be
deleted, use the button at the left of the considered line. Finally, save the program, if necessary
under a different name.
In this TAB an overview of the complete program is presented (see Figure 17).
By clicking the button, one can change between the programs of module 1, 2 and
3.
SCT/1310383/DVH-FVH/dvh/15-043
17
CHAPTER 3 Mefias®-software
For all the membranes there are 4 different programs available: ‘manual no alarm’, ‘deaeration’,
algae filtration’ and ‘Clear water test’
Manual no alarm: this program is intended to use only when one wants to test something,
e.g. one of the pumps. All devices are controlled manually.
Deaeration: this program has to be used at each start-up, when there is air in the permeate
lines.
Algae filtration: this is the normal program for the filtration of algae. The initial flux of the
filtration is set to 20 l/hm². Depending on the stability of the filtration, the flux can be set
to a higher or lower value. Note that when one changes the filtration flux, the backwash
flux needs to be adapted as well since the backwash flux is 150 % of the filtration flux.
Clean water test: this program is used to test the condition of the membranes before and
after an algae filtration. For every membrane, 5 cycles of filtration/relaxation (Kubota) or
filtration/backwash are performed. If the permeability of the membranes becomes too
low, the membranes need to be cleaned.
SCT/1310383/DVH-FVH/dvh/15-043
18
CHAPTER 3 Mefias®-software
SCT/1310383/DVH-FVH/dvh/15-043
19
CHAPTER 4 troubleshooting
CHAPTER 4 TROUBLESHOOTING
When the permeate collection compartment contains algae or particles the membrane is broken. It
should be replaced by a new membrane. Before adding the new membrane the good membranes
should be removed and cleaned. The permeate pipes must be cleaned with detergent and eventual
obstructions (particles) must be removed.
4.3. NO PERMEATE
If the TMP (trans membrane pressure) is too high, there is a risk of damaging the membrane. The
membrane then has to be cleaned. Take out the membrane and clean it according to the
membrane data sheet.
SCT/1310383/DVH-FVH/dvh/15-043
20
CHAPTER 5 Safety
CHAPTER 5 SAFETY
When working with the mobile algae filtration-skid the following measures should be taken into
account:
SCT/1310383/DVH-FVH/dvh/15-043
21
CHAPTER 6 Epilogue
CHAPTER 6 EPILOGUE
This manual has been written for the Mobile algae filtration unit. It remains the intellectual
property of VITO (Flemish Institute for Technological Research) and cannot be copied, passed to
neither submitted for perusal to third parties.
Mol, 2015-01-05
SCT/1310383/DVH-FVH/dvh/15-043
22