Thermal stability of Nbdoped (NdDy)(FeCoAl)B magnets (abstract)

XiaoLei Rao, YingLie Liu, Yunjin Cao, Wengui Lin, Mingying Feng, XiaoLin Dong, and Shongquan Ji

Citation: Journal of Applied Physics 69, 5534 (1991); doi: 10.1063/1.347966

View online: http://dx.doi.org/10.1063/1.347966
View Table of Contents: http://scitation.aip.org/content/aip/journal/jap/69/8?ver=pdfcov
Published by the AIP Publishing

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 The degradation of polymer-bonded M-Fe-B magnets (abstract)
Anthony M. Mazany and E. Douglas Dickens, Jr.
BFGoodrich Research and Development Center, Breckstiiile, Ohio 44I41-3289
The susceptibility of Nd-Fe-B magnet powders to oxygen and chloride ions is well known,
however, the interactions between magnet alloy powders and polymeric binders in
bonded magnets can also lead to severe irreversible losses. The losses observed for
polymer-bonded Nd-Fe-B magnets in some cases can be more substantial than the losses due
to oxidation or corrosion alone. The aging characteristics of polymer-bonded magnets
have been examined with respect to time, temperature, alloy treatment, particle size, molding
method, and polymer composition. Each sample was evaluated for magnetic properties
after thermal aging. The chemical effects of oxygen, chloride ions, and various polymers on
Nd-Fe-B alloys and the resulting changes in magnetic properties can be very different,
but all can lead to significant losses and each degradation process (oxidation, corrosion, or
polymer-alloy interactions) exhibits a different magnetic hysteresis “signature.” The
irreversible losses stemming from these processes -can be alleviated through the use of
passivating coatings.

Thermal stability of Nb-doped (Nd y)(FeCoAI)B magnets (abstract)

Xiao-Lei Rao, Ying-Lie Liu, Yun-jin Cao, Wen-gui Lin, Ming-ying Feng,
Xiao-Lin Dong, and Shong-quan Ji
San Huan Inc., Chinese Academy of Sciences, Beijing 100080, People’s RepubIic of China
To improve the poor thermal stability of NdFeB magnets, we add Dy, Co, Al, and Nb into
the magnets with nominal composition (Nde,sDyc,t) 17FebCosA11.7B7Nbx(X = 0.3-1.5
at. %). We have measured their Hci at room temperature. The data of irreversible loss (IL)
of open-circuit flux density at different temperatures are also obtained using cylinder
samples with L/D=O.7 (P=2). We have also compared the IL of the same sample with
different P. The results show that Hcj increases linearly with Nb content in average 4.8
kOe/Nb at. %. The higher the H,-- and/or the longer the sample is, the lower the absolute I

value of IL is. The IL of sample with x = 1.5 at. % and L/D = 0.7 is less than 5%
even at 150 “C. Nb effectively achieves the thermal stability of the magnets. The SEM has
been used to observe the microstructure of the surface and cross section of a typical I

sample.
I
5534 J. Appl. Phys. 69 (8), 15 April 1991 0021-8979/91/085534-01$03.00 @ 1991 American institute of Physics 5534 I

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