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BEPNESA COCA COLA

G003315 380 GPM

INSTRUMENTS AND MEMBRANE

OEM literature Index

MANUFACTURER COMPONENT
BARKSDALE H90 PRESSURE SWITCH
SIGNET 8860 DUAL CHANNEL CONDUCTIVITY/RESISTIVITY CONTROLLER
SIGNET 8850-2 CONDUCTIVITY/RESISTIVITY TRANSMITTER
SIGNET 2820 SERIES CONDUCTIVITY SENSOR
SIGNET 515/2536 ROTOR-X FLOW SENSORS
SIGNET 8750-1 PH/ORP TRANSMITTER
SIGNET 8750-2 PH/ORP TRANSMITTER
SIGNET 2714-2717 TWIST-LOCK PH AND ORP ELECTRODES
SIGNET 2720 TWIST-LOCK PH/ORP PREAMPLIFIER
PROTECT PRO-8-450-MSP PRESSURE VESSELS
HYDRANAUTICS MEMBRANE SWC 5
HYDRANAUTICS MEMBRANE ELEMENT PRECAUTIONS
HYDRANAUTICS VESSEL SHIMMING PROCEDURE
HYDRANAUTICS GENERAL STORAGE PROCEDURES
HYDRANAUTICS ELEMENT LOADING GUIDELINES
HYDRANAUTICS START-UP, SHUTDOWN, AND PRESERVATIVE FLUSHING
HYDRANAUTICS PROCEDURE FOR PRESSURE VESSEL PROBING
HYDRANAUTICS BIOCIDES FOR DISINFECTION AND STORAGE
HYDRANAUTICS PROCEDURE FOR MEASURING SDI
HYDRANAUTICS FOULANTS AND CLEANING PROCEDURES
Operating Instructions Diaphragm Seal Piston Attention: Alternating pressure - vacuum applications are not authorized in switch types
which are suitable for both vacuum and pressure applications.
Pressure Switches E1S / E1H, P1H / P1X and MSPS
Set point adjustment

1. Product description In pressure switches, a displacement of the pressure sensing element occurs with a change in pressure.
Following the displacement of the pressure sensing element operates a microswitch.
Any set point adjustment may be performed by yourselves.
The pressure switches are specifically applied for monitoring and controlling of operations using maximum
and minimum pressures. A micro switch triggers an electrical signal when minimum or maximum pressure Upon delivery of the product, the set points are likely to be found in the middle of the adjustable range.
are reached.
On request, fix set points may be adjusted by our factory. In this event, the point will be indicated on the
Application according to instructions type plate or any separate plate,i = increasing, d = decreasing
The set point is adjusted by turning the adjustment screw.
Pressure switches must only be used for applications specified in the instructions.
This means that the temperature has to be within the specified ranges, the pressure values and the Attention: For pressure switches with housing, please first remove the corresponding
electrical rating must not exceed the values specified.
Attention: This device is not designed to be used as the only safety relevant element in pressurized housing cover in order to reach the adjustment screw.
systems according PED 97/23/EC.
4. Starting operations
2. Instructions on the use of pressure switches
- Allow pressure switch to reach the desired switch pressure.
General instructions - Turn adjustment screw clockwise or counterclockwise to actuate the micro switch.
Pressure peaks and pressure shocks exceeding the maximum operating pressure are inadmissible. The
maximum operating pressure is the upper final value of the adjustable range or, if specified, the pressure Please note: Please consult the wiring diagram for the contact status at atmospheric pressure
indicated as maximum operating pressure.
Exceeding the max. operating pressure affects the performance and the life span of the product and may
damage it. Pressure switches must be mounted as vibrationless as possible. Precise adjustment of set point to actuate on increasing pressure

Attention Without special provisions/actions, pressure switches are not suitable 1. Lower system pressure to 0 bar.
for pure gas / hydrogen applications. 2. Increase pressure slowly and check if micro switch is actuated at desired switch pressure.
3. If necessary, readjust by turning the adjustment screw
Contact protection 4. Repeat step 1 - 3 until microswitch operates at desired switch pressure.
The micro switches used are normally suitable for both direct and alternating current operation. Inductive,
capacitive and lamp loads may, however, considerably reduce the life expectancy of a micro switch and, Precise adjustment of set point to actuate on decreasing pressure
under extreme circumstances, even damage the contacts. Depending on the application spark supression
and current limiting is recommended (See page 2 fig. 1 to 4). 1. Increase pressure up to a point clearly above the desired switch pressure
(at least, switch pressure plus max. hysteresis; not above max. operating pressure).
Application in hazardous locations 2. Lower pressure slowly and check if micro switch is actuated at desired switch pressure.
3. If necessary, readjust by turning the adjustment screw (see figures 1 - 7).
The pressure switches to be used in hazardous locations are principally designed for intrinsically safe 4. Repeat step 1 - 3 until microswitch operates at desired switch pressure.
circuits „i“ following the applicable regulations, and are provided with a blue plate bearing the words „For
intrinsically safe EExi application“. They must be operated with a switch amplifier (see page 2 fig. 5).
They are only for use in an approved intrinsically safe circuit. The adjustment of several set points occurs for each set point as specified above. Following the adjustment
Switches with explosion proof enclosures are to be used according to their approval. of all set points, each set point must be checked and, if necessary, be readjusted.
Approval class and identification characteristics according to type label information must be observed.
EC-Design approved types are marked with a label according to ATEX 95 (see page 2).

Operating life time 5. Maintenance

The switches are designed for an operating life time of at least 1 million cycles when used under normal The country specific test intervals for monitoring-needy plants under of the PED and ATEX guideline are to
design criteria. be observed. The pressure switch is maintenance free.
Checking the set points lies within the discretion of the user.
3. Installation

Pressure and electrical connections must be provided by professional or trained staff following the general 6. Transport anhd storage
state-of-the-art standards (See page 2 fig. 6). Installation / removal must only occur with all sources of
energy (electrical and hydraulic / pneumatic) disconnected. Severe shock and vibrations, also during transport, should be avoided. Storage should be dry and clean.

1 1
Contact Protection Wiring Code for all Types
(Contact status at atmospheric pressure)

Fig. 6
E1S / E1H
able P1H / P1X
Load

C C = brown
NC NO NC = orange
Fig. 1: Protection in case of capacitive loads NO = black
R1 Protection against starting current rushs
R2,R3 Protection against high discharge currents

MSPS

Load Load

C C = brown
NC NO NC = orange
NO = black
Fig. 3: Protection in case of continuous
current and inductive load by recovery diode
NC only available at microswitch type FF and JJ

Use in Hazardous Locations

Unprotected area EExi-area

Wiring blue
EExi-approved
Art.-Nr.: 923-0167
Index E, 01. 10. 2003
Barksdale GmbH
Specifications are subject to
Dorn-Assenheimer Strasse 27
Switch amplifier Pressure switch D-61203 Reichelsheim / Germany changes without notice.
NAMUR Temperature switch Tel.: +49 - 60 35 - 9 49-0
Fax: +49 - 60 35 - 9 49-111 and 9 49-113
Fig. 5: Operation of Barksdale pressure switches in intrinsically safe areas
e-mail: Info@Barksdale.de
Web-Site: http://www.barksdale.de

2 2
E1S - ... E1H - ... P1H - ... P1X - ... MSPS - ...
Single pressure switch with adjustable Single pressure switch with adjustable Single pressure switch with adjustable Single pressure switch with adjustable Compact single pressure switch with
switch contact, for vacuum and switch contact, for vacuum and switch contact, for vacuum and switch contact, for vacuum and adjustable switch contact via adjustment
overpressure, overpressure, adjustment scale, overpressure, overpressure, screw, for vacuum and overpressure,
adjustment scale, housing: aluminum, housing: aluminum, pressure proof
no housing, protection class IP00, protection class IP65, transparent cap, housing: aluminum, enclosed acc. to CSA u. UL, no housing, protection class IP00
Exi approved Exi approved protection class IP65, Exi approved protection class IP65

Cable gland PG 13,5


(Cable diameter 7...12 mm)
60
Cable gland 1/2“ NPT,
66,5 ±0,5
(Cable diameter 7...12 mm),
Common C NO 3 screw terminals on microswitch NO
NC
Common
C NO
133,5 Cable gland 1/2“ NPT
NC
Adjustment
screw

ø32
app. 100

74
134
132

NC (Only

102,5

102,5
ø7 microswitch
72,5

72,5
type
ø7 FF and JJ)
36,5
17,5

Pressure connection

Adjustment screw
34
max. 85

3 3
Electrical Ratings E1S / E1H

Max. Hyster. of Switch Types in bar


Micro- Special Characteristics Volt AC Ind. Loat Res. Load Volt DC Ind. Load Res. Load Notes
switch 50 Hz A A A A

DD, JJ

0,05
0,07
0,60
125 10 10 6 0,5 0,5 Small hysteresis;

Medium hysteresis;

Medium hysteresis;

bar
H Microswitch with silver contacts 250 10 10 bis High AC /

(End of Range)
480 3 3 28 low DC loads

125 10 10 12 5,0 15,0 Medium hysteresis;

High AC

High AC
M Microswitch with silver contacts 250 10 10 24 1,0 2,0 High AC and

Volt AC Ind. Load Res. Load Volt DC Ind. Load Res. Load Notes
480 3 3 250 0,25 0,4 DC loads

GH Microswitch with gold-plated contacts for 125 1 1 24 1,0 1,0 Small hysteresis

EE, FF

0,04
0,06
0,55
GM low voltage and low current DC switching 30 1 1 28 1,0 1,0 Medium hysteresis

bar
0,25
0,5
A
Silver contacts, adjustable hysteresis

--
R

Values printed bold (max. increasing pressure) = max. operating pressure


Electrical Ratings P1H / P1X

0,25

(short term) bar


0,5
A
--

Proof Press.
Micro- Special Characteristics Volt AC Ind. Load Res. Load Volt DC Ind. Load Res. Load Notes
switch 50 Hz A A A A

6,9
6,9
10,0
125 10 10 6 0,5 0,5 Small hysteresis;

125
250
H Microswitch with silver contacts 250 10 10 bis High AC /

--
480 3 3 28 low DC loads

GH Microswitch with gold-plated contacts for 125 1 1 24 1,0 1,0 Small hysteresis
low voltage and low current DC switching Medium hysteresis

15

Decreasing Pressure
Microswitch with silver contacts, 125 10 10 12 10,0 15,0 Medium hysteresis;
K, B K: with sealed plunger and stainless 250 24 5,0 6,0 High AC and

0,04... 0,3
0,10... 0,93
0,70... 6,2
steel blade 480 250 0,03 0,2 DC loads

15

Adjustable Range (bar)


Adjustable Ranges E1S / E1H

50 Hz
125
250

125
250
Press. Range Code Adjustable Range (bar) Proof Press. Max. Hyster. of Switch Types in bar (End of Range)
Overpressure Increasing Pressure Decreasing Pressure (short term) bar H, GH (bar) M, GM (bar)
15 0,04... 1 0,035... 0,9 30 / 70 0,16 0,06

Increasing Pressure
90 0,25... 6 0,210... 5,8 30 / 70 0,73 0,55

Microswitch with silver contacts

Microswitch with silver contacts


250 0,80... 17 0,70 ... 16,3 30 / 70 1,86 1,38

0,09 ... 0,35


0,18 ... 1,00
1,35 ... 6,90
500 2,00... 35 1,80 ... 33,0 30 / 70 -- 1,93

Special Characteristics
Vacuum
VAC -0,07... -1 -0,02... -0,98 -1 / +2 -- 0,06

Adjustable Ranges MSPS


Electrical Ratings MSPS
Adjustable Ranges P1H / P1X
Press. Range Code Adjustable Range (bar) Proof Press. Max. Hyster. of Switch Types in bar (End of Range)

Press. Range Code


Increasing Pressure Decreasing Pressure (short term) bar B (bar) H, GH (bar) K (bar)
30 0,1 ... 2,1 0,04... 2,0 137 0,14 0,07 0,17
85 0,3 ... 6,0 0,2 ... 5,5 137 0,48 0,17 0,58

100
5
15
EE, FF

DD, JJ
switch
Micro-
340 0,7 ... 24,0 0,4 ... 22,5 137 1,52 0,42 1,83
600 2,0 ... 42,0 1,8 ... 41,0 137 2,07 1,17 2,42

Values printed bold (max. increasing pressure) = max. operating pressure

4 4
8860 Dual Channel Conductivity/Resistivity Controller English

*3-8860.090*
3-8860.090 Rev. E 3/06 English

C1 23.45 µS
CAUTION! C2 8.72 µS
Signet
• Remove power to unit before wiring input and output connections. Relay 1
Conductivity/Resistivity
Transmitter
Relay 2

• Follow instructions carefully to avoid personal injury.


• This product should only be used for the purposes and in the manner described in this manual. ENTER

Installation
1. Punch out panel and de-burr edges. Recommended clearance on all sides between instruments is 1 inch.
2. Place gasket on instrument, and install in panel.
3. Slide mounting bracket over back of instrument until quick-clips snap into latches on side of instrument.
4. Connect wires to terminals.
5. To remove, secure instrument temporarily with tape from front or grip from rear of instrument. DO NOT RELEASE. Press
quick-clips outward and remove.
6. If cleaning is necessary, wipe the front of the unit with a damp cloth.
7. The live contacts on the back of this unit must be covered to avoid accidental shock hazard.
gasket on
front side
96mm (3.8 in.) of panel
panel

Panel Cutout terminals


96 mm 92 x 92 mm mounting
(3.8 in.) Optional bracket
(+ 0.8, - 0 mm) AY 4

Rear Cover REL


AY 2
REL
AY 3
REL

AY 1

3.6 x 3.6 in.


REL
COM ER
N/O
N/C POW
COM
N/O
N/C L
COM

(+0.031, -0 in.)
N/O
N/C N
COM
N/O

OPEN COLL 3
N/C

- OPEN COLL 4

SGNL 2
TEMP 2
OUTPUT OPTION

ISO GND
SHLD
SGNL 1
COLL 3,4

TEMP 1
ISO GND
RELAY 3,4

OPEN

SHLD
56 mm
quick-clip
102 mm (2.2 in.)
(4.0 in.)

Specifications • Max loop impedance:


General 150 Ω @ 12 V, 450 Ω @ 18 V, 750 Ω @ 24 V
Compatible electrodes: Signet 2819 to 2823 • Update rate: ~100 mS
Standard or Certified • Accuracy: ±0.03 mA @ 25°C, 24 VDC
Conductivity/Resistivity Sensors Open-collector outputs (2 available, optically isolated):
Enclosure: • 50 mA sink or source, 30 VDC max. pull-up voltage
• Rating: NEMA 4X/IP65 front (NEMA 4X Rear cover available) • Programmable for:
• Case: PBT • High or Low setpoint with adjustable hysteresis
• Panel case gasket: Neoprene • Pulse operation (max. rate: 400 pulses/min)
• Window: Polyurethane-coated polycarbonate • USP standards
• Keypad: Sealed 4-key silicone rubber • Time delay: 0 to 6400 s.
• Weight: 8860-AC: 1.28 lb/0.58 kg 8860: 1.2 lb/0.55 kg Relay outputs (up to 4 SPDT relays available )
Display (Alphanumeric 2 x 16 LCD) : • Maximum resistive load: 5 A @ 250 VAC, 5 A @ 30 VDC
• Contrast: User selected, 5 levels • Isolation between open contacts: 500 V minimum
• Update rate: 1.5 seconds • Programmable for:
Sensor input range: • High or Low setpoint with adjustable hysteresis
• Conductivity: 0.01 µS/cm to 400 000 µS/cm • Pulse operation (max. rate: 400 pulses/min)
• Resistivity: 10 KΩ•cm to 100 MΩ•cm • USP standards
• TDS: 0.023 to 200 000 PPM nominal (adjustable µS/PPM) • Time delay: 0 to 6400 s
• Temperature:
-25 to 120°C (-13 to 248°F) PT 1000; 25ºC = 1096Ω Environmental
Accuracy: • Ambient operating temperature: -10 to 55°C (14 to 131°F)
• Conductivity/Resistivity: ± 2% of reading • Storage temperature: -15 to 80°C (5 to 176°F)
• Temperature: ± 0.5ºC (0 to 100ºC) • Relative humidity: 0 to 95%, non-condensing
• Maximum altitude: 2000 m (6562 ft)
Electrical • Insulation category: II
Power requirements: • Pollution degree: 2
3-8860-AC: 100 to 240 VAC ± 10% , 50-60 Hz, 20VA or
11 to 24 VDC ±10%, regulated, 0.5 A max Standards and Approvals
3-8860: 11 to 24 VDC ±10%, regulated, 0.5 A max • CE, UL listed
Three 4 to 20 mA Outputs: • Immunity: EN50082-2
• Passive, isolated, fully adjustable and reversible • Emissions: EN55011 Class B
4 to 20 mA outputs are independently source selectable • Manufactured under ISO 9001, ISO 14001
Electrical Connections
Caution: Failure to fully open terminal jaws before removing wire may permanently damage instrument.
This product must be provided with a means to disconnect all current carrying conductors connected to the main AC line, or,
as part of the building installation.

Wiring Procedure
1. Remove 0.35- 0.47 in. (9-12 mm) of insulation from wire end.
2. Press the orange terminal lever downward with a small screwdriver to open terminal jaws.
3. Insert exposed (non-insulated) wire end in terminal hole until it bottoms out.
4. Release orange terminal lever to secure wire in place. Gently pull on each wire to ensure a good connection.

Wiring Removal Procedure


1. Press the orange terminal lever downward with a small screwdriver to open terminal jaws.

Wiring Tips:
• Do not route sensor cable in conduit containing AC power wiring - electrical noise may interfere
with sensor signal.
• Routing sensor cabling in grounded metal conduit may prevent moisture damage, electrical
noise, and mechanical damage.
• Seal cable entry points to prevent moisture damage.
• Do not insert two wires into a single terminal. If necessary, splice the wires together before Caution:
inserting into the terminal. Electrical shock hazard exists!

Never connect live AC lines to the
instrument.

RELAY 1 RELAY 2 RELAY 3 RELAY 4 Always connect a ground wire to
the ground terminal when using
AC power.

N/C N/O COM N/C N/O COM N/C N/O COM N/C N/O COM *
POWER
OPEN COLL 3

+ OPEN COLL 3
+ OPEN COLL 4
- OPEN COLL 4

LOOP 3
LOOP 1

LOOP 3
LOOP 2

LOOP 2
LOOP 1

L L
N N 100 - 240V ~
+

+
+
-

-
-
-

50-60Hz, 20VA

- - 11 - 24V
+ + 0.5 A
3-8860.610A 4/00
OUTPUT OPTION

ÜL LISTED
E171559
RELAY 3,4

COLL 3,4
OPEN

LR92369
ISO GND

ISO GND
TEMP 1

SGNL 1

TEMP 2

SGNL 2
SHLD

SHLD

4 to 20 mA loop Outputs
The current loops in the 8860 are passive circuits.
12-24 VDC must be provided from an external source.
A single loop is illustrated for clarity.
Output Option Switch
• In OPEN COLLECTOR position, relays 3 and 4 are open 8860 4 to 20 mA outputs
collector outputs as shown.
Loop 1

Loop 2

Loop 3

• In RELAY 3, 4 position, relays 3 and 4 are dry contact relays


identical to relays 1 and 2.
• The menu references in the 8860 display will not change.
Outputs 3 and 4 will be identified as "Relay" regardless of
switch setting. - + - + - +

PLC or Recorder
Outputs
Internal open-collector +
output circuit -
Channel 1
4-20 mA in - +
Power
Supply
+ Channel 2 + - 12-24 VDC
- 4-20 mA in
-
+ Channel 3 +
4-20 mA in -

2 8860 Dual Channel Conductivity/Resistivity Controller


Sensor Input Connections
Cooling Tower Deionization Regen. Chemicals
• The 8860 will accept two independent sensor input signals. UPW @ 25°C USP
Bottled
Water
Waste Waters Alkali Cleaners, Acids/Bases

The two sensors may be of different cell constant values.


• Do not route sensor cable in any conduit containing AC power Brackish Sea Water
Rinse 3-2823 (Salinity) (20.0 Cell)
wiring - electrical noise may interfere with the signal. Water
3-2822, 3-2842 (10.0 Cell)
• Cable shield MUST be maintained through cable splice.
3-2821, 3-2841 (1.0 Cell)
• Use three conductor shielded cable for cable extensions up
3-2820, 3-2840 ( 0.10 Cell)
to 30 m (100 ft) max. for measurements below 10 MΩ (above
0.10 µS). 3-2819, 3-2839 (0.01 Cell)

• Maximum cable length for resistivity measurements above 0.010mS 0.054mS 1mS 10mS 100mS 200mS 1,000mS 10,000mS 100,000mS 400,000mS
10 MΩ is 25 ft, and solution temperatures must be between 100 MΩ 18.3 MΩ 1MΩ 100KΩ 10KΩ 50,000mS 200,000mS

20°C and 100°C.


ISO GND

TEMP 1

SGNL 1

ISO GND

TEMP 2

SGNL 2
SHLD

SHLD
RED SILVER (SHLD)
WHITE BLACK
BLACK WHITE
SILVER (SHLD) RED

Relay and Open Collector Functions


The 8860 is equipped with 4 SPDT relays that can be configured • Pulse Operation
for High alarm, Low alarm, Proportional pulse or USP operation. The output emits a 100 mS pulse at a rate defined by the
Source, Pulse Range and Max PlsRate settings, and by the
• Low: Output triggers when process variable is less than process condition. The maximum pulse rate is 400 pulses per
setpoint. minute.

• High: Output triggers when process variable is higher than Example: As the process falls below 10 µS the output will
setpoint. start pulsing in relation to the process value, the max pulse
endpoint and the programmed pulses/min. Pulse rate
• Off: Disables output pulse. will increase as the process approaches the programmed
endpoint.

Process

The Pulse Rate determines what the


Hysteresis maximum rate will be. The 8860 maximum
capability is 400 pulses per minute.
Low Setpoint 100 pulses Re
la
y/
O
10 pen
0
Time Pu Col
lse lec
10 uS = 0 pulses/min. s/ tor
Pulse rate

m P
Relay energized in ls
7.5 uS = 50 pulses/min. > Ra
te
Relay relaxed 5 uS = 100 pulses/min. :
0 pulses
Process
µS ----->
5 Relay 1 Rng: uS 10
High Setpoint 10.00 --> 5.00 >

RANGE defines where the pulsing starts


Hysteresis and where it reaches the maximum rate.

Time

8860 Dual Channel Conductivity/Resistivity Controller 3


VIEW menu
• During normal operation, the ProcessPro displays the VIEW menu.
• When using the CALIBRATE or OPTIONS menus, the ProcessPro will return to the VIEW
menu if no activity occurs for 10 minutes. C1 23.45 µS
• To select the item you want displayed, press the UP or DOWN arrow keys. The items C2 8.72 µS
will scroll in a continuous loop. Changing the display selection does not interrupt system Signet
Conductivity/Resistivity
operations. Relay 1
Transmitter
Relay 2

• No keycode is necessary to change display selection.


• Output settings cannot be edited from the VIEW menu.
ENTER

View Menu
Display Description

C1 1000.00 µS/cm Monitor C1 Conductivity and C2 Conductivity simultaneously. This is the


C2 30.00 µS/cm permanent display when Channel 2 is ON.

C1 1000.00 µS/cm Monitor Channel 1 Conductivity and Channel 1 Temperature. This is the
25.0 º C permanent display when Channel 2 is OFF.

The VIEW displays below are temporary. The permanent display will return after 10 minutes

C2 30.00 µS/cm Monitor Channel 2 Conductivity and Channel 2 Temperature. This view is
25.0 ºC available only when Channel 2 is ON.

Reject C1 → C2 Monitor Percent Reject, Difference, or Ratio


97.00 (Channel 1 to Channel 2 or Channel 2 to Channel 1)

Loop 1 12.03 mA Monitor Loop 1 and Loop 2 current output simultaneously.


Loop 2 5.69 mA

Loop 3 13.7 mA Monitor Loop 3 and status of Relays 3 and 4 (Open Collector 3 and 4).
R3 ON R4 PLS

Last Cal Monitor date for scheduled maintenance or date of last calibration.
06-30-01

4 8860 Dual Channel Conductivity/Resistivity Controller


ProcessPro Editing Procedure:
Step 1. Press and hold ENTER key:
• 2 seconds to select the CALIBRATE menu.
• 5 seconds to select the OPTIONS menu.
Step 2. The Key Code is UP-UP-UP-DOWN keys in sequence.
• After entering the Key Code, the display will show the first item in the selected menu.
Step 3. Scroll menu with UP or DOWN arrow keys.
Step 4. Press RIGHT ARROW key to select menu item to be edited.
• The first display element will begin flashing.
Step 5. Press UP or DOWN keys to edit the flashing element.
• RIGHT ARROW key advances the flashing element.
Step 6. Press ENTER key to save the new setting and return to Step 3.

Notes on Step 1: Notes on Step 2:


• The View Menu is normally displayed. If no key is pressed for 5 minutes while display is showing "Enter
• The CALIBRATE and OPTIONS menus require a KEY CODE. Key Code", the display will return to the VIEW menu.

CALIBRATE: ----
Press & Enter Key Code
hold for ENTER

access: CALIBRATE: *---


Enter Key Code
CALIBRATE: **--
VIEW Enter Key Code
2s 5s CALIBRATE: ***-
CALIBRATE Enter Key Code

OPTIONS Chan 1 Cell: First item in CALI-


Standard > BRATE menu

Notes on Steps 3 and 4:


• Refer to pages 6 and 7 for complete listing of menu items and their use.
Chan 1 Cell:
• From the Step 3 display, pressing the UP and DOWN keys simultaneously will Standard >
return the display to the VIEW menu.
• If no key is pressed for 10 minutes, display will also return to the VIEW menu.
Step 3

Step 3: Finished Editing? Relay 1 Setpnt:


Press the UP and DOWN keys simultaneously after Step 4
20.00 us >
saving the last setting to return to normal operation.

Notes on Steps 5 and 6:


Relay1 Setpnt:
• All output functions remain active during editing. 20.00 uS
• Only the flashing element can be edited.
Relay1 Setpnt:
• RIGHT ARROW key advances the flashing element in a continuous loop. 10.00 uS Step 5
• Edited value is effective immediately after pressing ENTER key.
• If no key is pressed for 10 minutes unit will restore the last saved value and return to step 3.
• Step 6 (pressing ENTER key) always returns you to Step 3. Relay1 Setpnt:
• Repeat steps 3-6 until all editing is completed. 10.00 uS

Relay Setpnt:
Step 5: Made an Error? 9
1 .00 uS
ENTER

Press the UP and DOWN keys simultaneously Step 6


while any element is flashing. This will recall the Relay1 Setpnt:
last saved value of the item being edited and Saving
return you to Step 3. Relay1 Setpnt:
19.00 uS >

8860 Dual Channel Conductivity/Resistivity Controller 5


Calibrate Menu
Display
Description
(Factory settings shown)
Chan 1 Cell: Select CUSTOM only if you are connecting a certified conductivity sensor. Select
Standard > STANDARD for all non-certified sensors.

Chan 1 Cell: For STANDARD sensors: Select the nominal cell constant: 0.01, 0.1, 1.0, 10.0 or 20.0.
1.0 >

Cell: Custom For CUSTOM sensors: Enter the precise cell constant from the certificate provided with your
1.0000 > sensor, or from the information label on the sensor.

Chan 1 Set: Adjust the temperature of the system based on an accurate external reference.
Temperature >

Chan 1 Set: This single-point wet calibration procedure requires a test solution of known value.
Conductivity > Enter all zeroes here to restore TEMPERATURE and CONDUCTIVITY to factory calibration.

Chan 1 Units: Select the units of measure: µS/cm, mS/cm, kΩ•cm, MΩ•cm, PPB, PPM
uS/cm >

Chan 1 TDS: If the Units selection is PPM or PPB, set the ratio of µS to Total Dissolved Solids. The factory
2.0000 uS/PPM > preset value is 2 µS per 1 PPM of TDS. (Always µS/PPM, even if units is PPB).
See page 10 for additional information.

Function: Select a functional relationship between C1 and C 2: • Ratio is (C1:C2) or (C2:C1)


Reject C1 → C2 > • Percent Reject is 100%(1-C2/C1) or 100%(1-C1/C2) • Difference is (C1-C2) or (C2-C1)

Loop 1 Source: Select the measured value or calculated FUNCTION you want Loop 1 to represent:
Chan 1 Cond > Chan 1 Cond, Chan 2 Cond, Chan 1 Temp, Chan 2 Temp, or Function

Loop 1 Range: uS Set the minimum (4 mA =) and maximum (20 mA =) range for Loop 1.
0.0000 → 100.000 > Make sure that the values are consistent with the units of the source.

Relay 1 Mode: Select operating mode for Relay 1: OFF, LOW, HIGH, USP or PULSE.
Low > For USP mode: • Relay 1 SOURCE must be Cond 1 or Cond 2
• Temp Comp (Options menu) must be set to None

Relay 1 Source: Select the INPUT SIGNAL (or FUNCTION) monitored by Relay 1:
Chan 1 Cond > • Cond 1 • Cond 2 • Temp 1 • Temp 2 • Function

Relay 1 Setpnt: Set Relay 1 activation point. The maximum value acceptable is 999999.
10.0000 uS > USP setpoints are high alarms, where the setpoint is a percentage below the USP limit.

Relay 1 Hys: Relay 1 will be deactivated at setpoint ± Hysteresis (depending on High or Low selection).
0.5000 uS > When the relay Mode is USP (defined as a HIGH alarm), Hysteresis is displayed in µS.

Relay 1 Delay: Set up to 6400 seconds delay time for relay response.
10.0 secs > Relay 1 will be activated only if the source value exceeds the setpoint for this time period.

If Relay 1 is PULSE mode, set the start and end point of the conductivity range and also set
Relay 1 Rng: uS the maximum pulse rate. (The maximum PULSE rate setting is 400 pulses per minute.)
10.0000 → 40.0000 >
The combined Relay 1 Range and Pulse rate settings shown here indicate:
Relay 1 PlsRate: "Start pulsing when the conductivity value is 10 µS and increase the pulse rate up to the
120 Pulses/Min > maximum of 120 pulses per minute when the conductivity value reaches 40 µS"

Last CAL: Use this "notepad" to record important dates, such as annual recertification or scheduled
06-30-01 > maintenance.

• All changes in this menu become effective when saved, except the "Set Cond" and "Set Temp" settings.
• All outputs affected by a change in the "Set Cond" and "Set Temp" settings are frozen until you exit the Calibrate menu.

6 8860 Dual Channel Conductivity/Resistivity Controller


USP Limits When the
USP (United States Pharmacopoeia) has defined a set of conduc- The USP limit
tivity values (limits) to be used for pharmaceutical water moni- temperature
toring. This standard requires non-temperature compensated (µS) is:
range is:
conductivity measurement be used to warn if the conductance
approaches the USP limit. The limits vary according to the tem- 0 to < 5ºC 0.6
perature of the sample.
The 8860 has the USP limits stored in memory. It will automati- 5 to < 10ºC 0.8
cally determine the proper USP limit based on the measured 10 to < 15ºC 0.9
temperature.
15 to < 20ºC 1
Using the USP function 20 to < 25ºC 1.1
In the 8860, USP setpoints are defined as a percentage below
the USP limit, so a USP alarm is always a HIGH alarm. The 8860 25 to < 30ºC 1.3
can be set to warn you if the conductivity approaches within a set 30 to < 35ºC 1.4
percentage of the USP limit.
35 to < 40ºC 1.5
The following settings and conditions are required for a USP 40 to < 45ºC 1.7
relay function:
1. In the CALIBRATE menu: 50 to < 55ºC 1.8
• RELAY MODE must be set to USP. 55 to < 60ºC 2.1
• RELAY SOURCE must be Chan 1 or Chan 2 Cond.
• SOURCE UNITS must be set to µS. 60 to < 65ºC 2.2
2. In the OPTIONS menu: 65 to < 70ºC 2.4
• The TC Mode of the USP channel must be set to None.
70 to < 75ºC 2.5
(Service tip: If a relay is constantly on when it should be off, 75 to < 80ºC 2.7
check the relay settings listed above.)
80 to < 85ºC 2.7
Example:
85 to < 90ºC 2.7
• The USP setpoint is 40%.
• The water temperature is 19ºC, so the USP limit is 1.0 µS. 90 to < 95ºC 2.7
• The relay will be activated when the conductivity value reaches
0.6 µS, or 40% below the 1.0 USP limit.
95 to < 100ºC 2.9
• If the water temperature drifts to more than 20ºC, the 8860 will 100 to < 105ºC 3.1
automatically adjust the USP limit to 1.1.
• The relay will now be activated when the conductivity value
reaches 40% below 1.1 µS, or 0.66 µS.

8860 Dual Channel Conductivity/Resistivity Controller 7


Options Menu
Display
Description
(Factory settings shown)

Contrast: Adjust the LCD contrast for best viewing. A setting of 1 is lower contrast, 5 is higher. In
general, select lower contrast if the display is in warmer ambient surroundings.
3 >

Temp Display: Select ºC or ºF.

ºC >

Channel 2: Turn CH 2 OFF if not in use. This will remove all menu functions related to CH 2.

On >

Power: Select 50 Hz or 60 Hz electrical noise suppression, according to the AC power used in your
area. Select the proper setting for all applications, whether AC or DC powered.
60 Hz >

Chan 1 TC Mode: Set the method for temperature compensation to NONE, LINEAR or PURE WATER. You
must select NONE for USP systems. Select LINEAR for applications where the water is
Linear > less than 5 MΩ (or greater than 0.2 µS). Select PURE WATER for applications where the
water is greater than 5 MΩ (or less than 0.2 µS).

Chan 1 TC Slope: For LINEAR or PURE WATER temperature compensation, select a % per ºC slope.
Maximum slope setting is 9.99 % per ºC. If Temp Comp setting is NONE, this item will not
0.00 % > be displayed.

Averaging: OFF provides the most instantaneous response to process changes. Select LOW (4 sec)
or HIGH (8 sec) averaging if your process experiences frequent or extreme fluctuations.
Off >

Chan 1 Decimal: Set the decimal to the best resolution for your application. The display will automatically
scale up to this restriction. Select *****., ****.*, ***.** **.*** or *.****
*.**** >

Loop 1 Adjust: Adjust the minimum and maximum current output. The display value represents the precise
current output. Adjustment limits:
4.00 mA > • 3.80 mA < 4.00 mA > 5.00 mA
• 19.00 mA < 20.00 mA > 21.00 mA
Loop 1 Adjust: Use this setting to match the system output to any external device.
20.00 mA > These settings repeat for Loop 2 and Loop 3.

Relay 3 Active: Select active HIGH or active LOW operation for relay 3
Recommended: Use active LOW if OUTPUT OPTION switch is set for OPEN
High > COLLECTOR operation.
Active HIGH: Power is applied to relay coil when process value reaches SETPOINT.
Active LOW: Power is removed from relay coil when process value reaches SETPOINT.

Test Loop 1: Press UP and DOWN keys to manually change Loop 1output current.
Limits are 3.6 mA to 21.00 mA. Hold UP or DOWN keys to scroll the output value.
>

Test Relay 1: Press UP and DOWN keys to manually toggle the relay state.
>
Notes:
Channel settings will repeat when Channel 2 is enabled.
Loop settings will repeat for Loop 2 and Loop 3.
Check setting for related values when making changes (for example, if temp is set for ºC with a temp alarm at 25ºC, and you change
the temp to ºF, be sure to change the alarm setpoint to 77ºF.)
Relay settings will repeat for Relays 2, 3 and 4 (except "Relay Active" selection; applies to Relay 3 and 4 only.)

8 8860 Dual Channel Conductivity/Resistivity Controller


Calibration Procedure
The 8860 has been electronically calibrated at the factory.
• Procedure A verifies the accuracy and linearity of the 8860 by simulating temperature and conductivity values with precision (±0.1%)
fixed resistors.

• Procedure B is a wet calibration. This procedure uses the sensor input and NIST traceable test solutions.

A) Accuracy Verification with Precision Resistors (Electronic Calibration):


1. Simulate the Temperature
The temperature input to the 8860 is a PT-1000 thermistor, where 1000 Ohms (Ω) is equal to 0ºC and a change of 3.84 Ω equals a
1ºC change. (1000 Ω = 0ºC, 1003.84 Ω= 1.0ºC, 1007.68 Ω = 2.0ºC...................1096 Ω = 25ºC)

• Connect a resistor (1000 Ω to 1096 Ω ) between "Temp" and "Iso. Gnd" terminals.
• Set Temp; Adjust the temperature to exact value based on the measured resistance. (See Editing Procedure, Calibrate menu).
• To verify the 8860 temperature linearity, connect a second resistor value to the terminals.
• If the 8860 does not display the correct value, service is required. ( ± 0.5ºC)

2. Simulate the Conductivity


You may calculate the exact Resistance needed to simulate a specific conductivity value , or you may calculate the exact Conductivity
based on a resistor value:

Resistance = Cell constant e.g. 0.1 Cell = 5,000 Ω or 5 KΩ


conductivity (Siemens*) 0.000020 (Siemens*)

Conductivity = Sensor cell e.g. 0.1 Cell = 0.000001 Siemens*


Simulation resistance (Ω) 100,000 (Ω) or 1µS/cm

(*1 µS = 1 X 10-6 Siemens or 0.000001 Siemens)

• Connect the conductivity resistor between the "Sgnl 1 " and "Iso Gnd" (or Sgnl 2 and Iso Gnd) terminals.
• Set Cond: Adjust the conductivity value based on the resistor value. (See Editing Procedure and Calibrate menu).
• Verify the linearity of the 8860 by connecting a second Conductivity resistor of a different value.
• If the 8860 does not display the correct value (± 2% of reading), service is required.

B) Wet Calibration with NIST Traceable Solutions:


When using NIST traceable standards, review the temperature information provided with the test solution. Prevent contamination of the
test solution. The sensor must be at the temperature specified on the test solution label.

• Remove the sensor from the system. Rinse the sensor in a small amount of test solution.
• Place the sensor into the test solution.
• Place a reference thermometer into the same solution.
• Allow sufficient time for the temperature to stabilize.
• Set Temp: Adjust the temperature value based on the reference thermometer. (See Editing Procedure.)
• Set Cond: Adjust the conductivity value based on the test solution value. (See Editing Procedure.)
• Verify the linearity of the 8860 by placing the sensor into a second test solution of a different value.
• If the 8860 does not display the correct value (Temperature ± 0.5ºC, Conductivity ± 2% of reading), service is required.

8860 Dual Channel Conductivity/Resistivity Controller 9


Temperature Effects Calculating a Linear Temperature Coefficient
Conductivity measurement is highly dependent on temperature.
The basic rule is that higher temperatures result in greater 1. Set TC Mode to NONE (see OPTIONS menu, page 8).
conductance (less resistance). 2. Heat a sample solution close to the maximum process
Temperature effects are expressed as the percentage of temperature. Place sensor in the sample solution and
conductivity change (in µS) per °C. The conductivity value is allow several minutes for stabilization. Record the 8860
generally referenced to 25ºC. The 8860 has three temperature temperature and conductivity values in the spaces provided:
compensation options:
Displayed temperature: T1 = _______ °C
None
USP standards for pharmaceutical waters require that the Displayed conductivity: C1 = _______ µS
measurement be made without temperature compensation. USP
limits are discussed on page 7.
3. Cool the sample solution close to the minimum process
temperature. Place sensor in the sample solution allowing
Pure Water (Standard Compensation) several minutes for stabilization. Record displayed
This selection is used for measurements of very clean water,
temperature and conductivity values in the spaces provided:
less than 0.2 µS. Temperature effects are not linear in this
range, so the temperature coefficient is not easily determined.
Displayed temperature: T2 = _______ °C
This selection is recommended for all Resistivity applications
measuring from 5 MΩ to 18MΩ. This selection conforms to ASTM
Displayed conductivity: C2 = _______ µS
standard D1125 and D5391.
(A 10% change in conductivity between steps 2 and 3 is
Linear recommended.)
This selection allows you to calculate a custom temperature
compensation value for Conductivity measurements in the range 4. Substitute recorded readings (steps 2 and 3) into the following
of 0.2 µS and greater (Resistivity applications measuring less formula:
than 5 MΩ). The procedure is outlined in the section on the right.
TC Slope = 100 x (C1 - C2)
(C2 x (T1 - 25)) - (C1 x (T2 - 25))

Example: A sample solution has a conductivity of 205 µS @


48°C. After cooling the solution, the conductivity was measured
at 150 µS @ 23°C. (C1 = 205, T1 = 48, C2 = 150, T2 = 23)

The TC is calculated as follows:

TC Slope = 100 x (205 - 150) =5500 = 1.42%/°C


(150 x (48 - 25)) - (205 x (23 - 25)) 3860

TDS Factor
Some industries need to display a conductivity value as Total
Dissolved Solids (TDS), measured in units of parts per million
(PPM) or parts per billion (PPB).
• 1 PPM is equivalent to 1 mg per liter.
• 1 PPB is equivalent to 1 µg per liter.
• The 8860 calculates PPM or PPB by dividing the µS value
by a TDS Factor that you define. TDS factors can vary
widely, ranging from 1.50 to 2.50 µS per PPM. Methods
for establishing a TDS factor are beyond the scope of this
manual.
• The 8860 will accept TDS factor values from 0.01 to 99999.9
µS per PPM.
(factory preset = 2.00 µS per PPM)
NOTE: The 8860 TDS factor must be set in PPM.
TDS Factor = Conductivity (µS) ÷Total dissolved solids (PPM)
PPM = Solution conductivity (µS) ÷ TDS Factor

Example:
• Solution conductivity = 150 µS
• TDS = 80 PPM
• TDS Factor = 150 µS ÷ 80 PPM = 1.88 µS per
PPM

10 8860 Dual Channel Conductivity/Resistivity Controller


Troubleshooting
Display Condition Possible Causes Suggested Solutions

"- - - -" Display is over range. This may be a Check sensor for correct range.
normal condition if your process operates Check Decimal setting in OPTIONS menu.
at/near the limits of the sensor range. Check Calibrate menu settings for incompatible
SOURCE and RANGE values.

"Value Must be 100 or less" The menu item being set is a percentage Select a value from 0 to 100.
value and must be less than 100.

"Value must be more than 0" The menu item being set cannot be zero Select a value greater than zero.
or a negative value.

"Value must be 400 or less" The Pulse Rate for Relay and Open Select a pulse rate less than 400
Collector outputs cannot be greater than
400 pulses per minute.

"Reset to Factory Calibration" A value of "0" is being set into This will remove any user calibration from the
".. Set: Conductivity" menu item. "..Set Conductivity" and "..Set Temperature"
items in the Calibrate menu.

"Too Much Error The calibration offset entered is Check calibration procedure for accuracy.
CHECK SENSOR" beyond the allowable tolerances of the Check sensor for proper operation.
instrument. Check any cable extensions for poor splices or
termination.

Technical Note
If a Current Loop is locked at 3.6 mA, the problem is related to the temperature circuit:
This occurs only if the 8860 detects a resistance from the temperature sensor that is less than 250Ω or greater than 2800Ω.
• Check the sensor wiring for open/short or poor connections on white (TEMP IN) and black (ISO GND)wires.
• The PT1000 temperature device in the sensor is defective.
• The transmitter is defective.

8860 Dual Channel Conductivity/Resistivity Controller 11


Ordering Information
Mfr. Part No Code Description
3-8860 159 000 677 Conductivity/Resistivity Controller, DC
3-8860-AC 159 000 678 Conductivity/Resistivity Controller, AC

Accessories
Mfr. Part No Code Description
3-8050.395 159 000 186 NEMA 4X Rear Cover
3-9000.392 159 000 368 Liquid-tight Connector Kit for rear cover (includes 3 connectors)
3-8050.392 159 000 640 Model 200 Retrofit Adapter
3-5000.399 198 840 224 5x5 inch Adapter Plate for Signet retrofit
3-0000.596 159 000 641 Heavy Duty Wall Mount Bracket
3-5000.598 198 840 225 Surface Mount Bracket
3-8050.396 159 000 617 RC Filter Kit (for relay use)
3-2830 159 000 628 Conductivity Certification Tool
7300-7524 159 000 687 Power Supply, 7.5W 24 V
7300-1524 159 000 688 Power Supply, 15W 24 V
7300-3024 159 000 689 Power Supply, 30W 24 V
7300-5024 159 000 690 Power Supply, 50W 24 V
7300-1024 159 000 691 Power Supply, 100W 24 V

Conductivity/Resistivity Electrodes
Mfr. Part No. Code Description
3-2819-1 198 844 010 Conductivity/Resistivity (CR) Cell, 0.01, SS
3-2820-1 198 844 000 Conductivity Cell, 0.1, SS
3-2821-1 198 844 001 Conductivity Cell, 1.0, SS
3-2822-1 198 844 002 Conductivity Cell, 10, SS
3-2823-1 198 844 003 Conductivity Cell, 20, SS
3-2819-S1 159 000 085 CR Sanitary, 0.01, SS, 1 to 1 1/2 in.
3-2819-S1C 159 000 087 CR Sanitary, 0.01, SS, 1 to 1 1/2 in., Certified
3-2819-S2 159 000 086 CR Sanitary, 0.01, SS, 2 in.
3-2819-S2C 159 000 088 CR Sanitary, 0.01, SS, 2 in., Certified
3-2819-T1 159 000 081 CR Sanitary, 0.01, Titanium, 1 to 1 1/2 in.
3-2819-T1C 159 000 083 CR Sanitary, 0.01, Titanium, 1 to 1 1/2 in., Certified
3-2819-T2 159 000 082 CR Sanitary, 0.01, Titanium, 2 in.
3-2819-T2C 159 000 084 CR Sanitary, 0.01, Titanium, 2 in., Certified
3-2820-S1 159 000 089 CR Sanitary, 0.1, SS, 1 to 1 1/2 in.
3-2820-S1C 159 000 091 CR Sanitary, 0.1, SS, 1 to 1 1/2 in., Certified
3-2820-S2 159 000 090 CR Sanitary, 0.1, SS, 2 in.
3-2820-S2C 159 000 092 CR Sanitary, 0.1, SS, 2 in., Certified
3-2820-T1 159 000 624 CR Sanitary, 0.1, Titanium, 1 to 1 1/2 in.
3-2820-T2 159 000 625 CR Sanitary, 0.1, Titanium, 2 in.
3-2821-S1 159 000 093 CR Sanitary, 1.0, SS, 1 to 1 1/2 in.
3-2821-S1C 159 000 095 CR Sanitary, 1.0, SS, 1 to 1 1/2 in., Certified
3-2821-S2 159 000 094 CR Sanitary, 1.0, SS, 2 in.
3-2821-S2C 159 000 096 CR Sanitary, 1.0, SS, 2 in., Certified
3-2821-T1 159 000 626 CR Sanitary, 1.0, Titanium, 1 to 1 1/2 in.
3-2821-T2 159 000 627 CR Sanitary, 1.0, Titanium, 2 in.
3-2839-1 159 000 921 Conductivity Cell, 0.01, 15 ft cable, NPT
3-2839-1D 159 000 923 Conductivity Cell, 0.01, 15 ft cable, ISO
3-2840-1 159 000 786 Conductivity Cell, 0.1, 15 ft cable, NPT
3-2840-1D 159 000 788 Conductivity Cell, 0.1, 15 ft cable, ISO
3-2841-1 159 000 790 Conductivity Cell, 1.0, 15 ft cable, NPT
3-2841-1D 159 000 792 Conductivity Cell, 1.0, 15 ft cable, ISO
3-2842-1 159 000 794 Conductivity Cell, 10.0, 15 ft cable, NPT
3-2842-1D 159 000796 Conductivity Cell, 10.0, 15 ft cable, ISO

NOTE: Alternate wetted materials and lengths are available through special order.
Cable length extensions to 100 ft. (30 m) are available through special order.

George Fischer Signet, Inc., 3401 Aerojet Avenue, El Monte, CA 91731-2882 U.S.A. • Tel. (626) 571-2770 • Fax (626) 573-2057
For Worldwide Sales and Service, visit our website: www.gfsignet.com • Or call (in the U.S.): (800) 854-4090

3-8860.090 Rev. E 3/06 English © George Fischer Signet, Inc. 1999 Printed in U.S.A. on Recycled Paper
8850-2 Conductivity/Resistivity Transmitter English

*3-8850.090-2*
3-8850.090-2 Rev.H 8/06 English

CAUTION! Contents 62.50 uS/cm


• Remove power to unit before wiring 1. Installation 25.0 C
Signet

input and output connections. 2. Specifications Conductivity/Resistivity


Transmitter

• Follow instructions carefully to avoid 3. Electrical Connections


ENTER

personal injury. 4. Menu Functions

1. Installation
ProcessPro transmitters are available in two styles: panel mount and field mount. The panel mount is supplied with the necessary
hardware to install the transmitter. This manual includes complete panel mounting instructions.
Field mounting requires a separate mounting kit. The 3-8050 Universal kit enables the transmitter to be installed virtually
anywhere. Detailed instructions for field installation options are included with the 3-8050 Universal kit.

1.1 Panel Installation


1. The panel mount transmitter is designed for installation using a 1/4 DIN Punch. For manual panel cutout, an adhesive
template is provided as an installation guide. Recommended clearance on all sides between instruments is 1 inch.
2. Place gasket on instrument, and install in panel.
3. Slide mounting bracket over back of instrument until quick-clips snap into latches on side of instrument.
4. To remove, secure instrument temporarily with tape from front or grip from rear of instrument. DO NOT RELEASE.
Press quick-clips outward and remove.

Optional 82 mm
96 mm Rear 92 mm 8050 8052 96 mm
(3.8 in.) (3.6 in.) (3.23 in.) (3.8 in.)
Cover

96 mm 56 mm 42 mm 64 mm 42 mm 65 mm
(3.8 in.) 41 mm (2.2 in.) (1.7 in.) (2.5 in.)
(1.6 in.) (1.7 in.) (2.5 in.)
97 mm
(3.8 in.) 106 mm (4.2 in.) 107 mm (4.2 in.)
FRONT VIEW
SIDE VIEW SIDE VIEW SIDE VIEW
Field Mount &
Panel Mount Panel Mount Field Mount w/ Field Mount w/
8050 Universal base 8052 Integral kit

2. Specifications 4 to 20 mA Outputs:
General • Passive, isolated, fully adjustable and reversible 4 to 20 mA
Compatible electrodes: outputs are independently source selectable for conductivity or
Signet 3-28XX-1 Standard and Certified (NIST) Series temperature.
Conductivity/Resistivity Electrodes • Max loop impedance: 50 Ω max. @ 12 V
Accuracy: ±2% of reading 325 Ω max. @ 18 V
Enclosure: 600 Ω max. @ 24 V
• Rating: NEMA 4X/IP65 front • Update rate: 200 ms
• Case: PBT • Accuracy: ±0.03 mA @ 25°C, 24 V
• Panel case gasket: Neoprene Relay outputs (2 sets mechanical SPDT contacts):
• Window: Polyurethane coated polycarbonate • Maximum voltage rating:
• Keypad: Sealed 4-key silicone rubber 5 A @ 30 VDC, or 5 A @ 250 VAC, resistive load
• Weight: Approx. 325g (12 oz.) • Hi or Lo programmable with adjustable hysteresis
Display: • Pulse programmable (maximum 400 pulses/minute)
• Type: Alphanumeric 2 x 16 LCD Environmental
• Contrast: User selected, 5 levels • Operating temperature: -10 to 70°C (14 to 158°F)
• Update rate: 1.8 s • Storage temperature: -15 to 80°C (5 to 176°F)
• Relative humidity: 0 to 95%, non-condensing
Electrical • Maximum altitude: 2000 m (6562 ft)
Power: 12 to 24 VDC ±10%, regulated, 290 mA max. • Insulation category: II
Sensor input range: • Pollution degree: 2
• Conductivity: 0.01 µS/cm to 400 000 µS/cm Standards and Approvals
• Resistivity: 10 KΩ•cm to 100 MΩ•cm • CE, UL listed
• TDS: 0.023 to 200 000 PPM nominal (adjustable µS/PPM) • Immunity: EN50082-2
• Temperature: PT 1000, -25 to 120°C (-13 to 248°F) • Emissions: EN55011 Class B
Measurements above 10 MΩ (below 0.1 µS) must be • Manufactured under ISO 9001 and ISO 14001
performed in solution temperatures from 20°C to 100°C.
U.S.A. Patent # 5,708,363
3. Electrical Connections
Caution: Failure to fully open terminal jaws before removing wire may permanently damage instrument.

Wiring Procedure
1. Remove 0.5 - 0.625 in. (13-16 mm) of insulation from wire end. 2
2. Press the orange terminal lever downward with a small screwdriver to open terminal jaws. 1
3. Insert exposed (non-insulated) wire end in terminal hole until it bottoms out.
4. Release orange terminal lever to secure wire in place. Gently pull on each wire to ensure a good connection.

Wiring Removal Procedure


1. Press the orange terminal lever downward with a small screwdriver to open terminal jaws.
2. When fully open, remove wire from terminal.

Wiring Tips:
• Do not route sensor cable in conduit containing AC power wiring. Electrical noise may interfere with sensor signal.
• Routing sensor cable in grounded metal conduit will help prevent electrical noise and mechanical damage.
• Seal cable entry points to prevent moisture damage.
• Only one wire should be inserted into a terminal. Splice double wires outside the terminal.

Terminals 3 and 4: Loop Power Terminals 11-14: Sensor input


12-24 VDC ±10% system power 11 is conductivity input
and current loop output. 12 is temperature input
Max. loop impedance: 13 is the isolated signal ground
50 Ω max. @ 12 V 14 is the sensor earth ground
325 Ω max. @ 18 V
600 Ω max. @ 24 V

Relay 2
10 (NO)
Relay 2
9 (COM)
System Pwr Relay 2 Sensr Gnd
4 Loop - 8 (NC) 14 (SHIELD)
System Pwr Relay 1 Iso. Gnd
3 Loop + 7 (NO) 13 (BLACK)
AUX Relay 1 Temp. IN
2 Power - 6 (COM) 12 (WHITE)
AUX Relay 1 Signal IN
1 Power + 5 (NC) 11 (RED)

Terminals 1-2: Auxiliary power Terminals 5-10: Relay Outputs


Provides DC power to measurement circuit. • Two SPDT mechanical relays, programmable as:
Required for all 8850 systems • High or Low setpoint with adjustable hysteresis.
• Proportional Pulse (400 pulses per minute maximum).
• May be disabled (Off) if not used.

3.1 Sensor Input Connections

14
Shield (Sensor Gnd) 62.50 uS/cm
25.0 C ≤30 m (100 ft.)
Black (Iso Gnd)
Signet
Conductivity/Resistivity
Transmitter

13
White (Temp In) ENTER

12
Red (Signal In)
11
Terminals Cable length is limited to 7.5 m (25 ft.)
where the operating range is above 10MΩ.
Signet 28XX-1
Standard and Certified Cells

2 8850-2 Conductivity/Resistivity Transmitter


Select the sensor with the range that best straddles your Cooling Tower Deionization Regen. Chemicals
Bottled Waste Waters Alkali Cleaners, Acids/Bases
application requirements. UPW @ 25°C USP Water
• 2819-1, 2839-1 (0.01 cell): 0.01 to 100 µS
Brackish Sea Water
(10 kΩ to 100 MΩ) Rinse 3-2823 (Salinity) (20.0 Cell)
Use the 2819-1 or the 2839-1 for all resistivity requirements Water
3-2822, 3-2842 (10.0 Cell)

3-2821, 3-2841 (1.0 Cell)


• 2820-1, 2840-1 (0.1 cell): 1 to 1000 µS
3-2820, 3-2840 ( 0.10 Cell)
• 2821-1, 2841-1 (1.0 cell): 10 to 10,000 µS
3-2819, 3-2839 (0.01 Cell)
• 2822-1, 2842-1 (10.0 cell): 100 to 200,000 µS
• 2823-1 (20.0 cell): 200 to 400,000 µS 0.010mS 0.054mS 1mS 10mS 100mS 200mS 1,000mS 10,000mS 100,000mS 400,000mS
100 MΩ 18.3 MΩ 1MΩ 100KΩ 10KΩ 50,000mS 200,000mS

3.2 System Power/Loop Connections

Stand-alone application, no current loop used


Transmitter
Terminals
System Pwr Loop - 4 - Power
Supply
System Pwr Loop + 3 + 12-24 VDC
AUX Power - 2
AUX Power + 1

Connection to a PLC/Recorder, separate supply Connection to a PLC with built-in power supply

PLC or Recorder
Transmitter
Transmitter
+ Loop Input Terminals
PLC Terminals
Terminals
- 4-20 mA
System Pwr Loop - 4
System Pwr Loop - 4 + Loop Input
4-20 mA
System Pwr Loop + System Pwr Loop + 3 -
3
AUX Power -
AUX Power - 2 - Power 2 - Power
Supply
AUX Power + 1 +
Supply AUX Power + 1 + 12-24 VDC
12-24 VDC
Internal
AUX power required for all 8850 systems PLC Connection

Example: Two transmitters connected to PLC/Recorder with separate power supply

PLC or Recorder

+ Channel 1
- 4-20 mA in

- Channel 2
Transmitter 1 Transmitter 2
Terminals + 4-20 mA in
Terminals

System Pwr Loop - 4 4 System Pwr Loop -


System Pwr Loop + 3 3 System Pwr Loop +
AUX Power - 2 2 AUX Power -
AUX Power + 1 1 AUX Power +

- Power
Supply
+ 12-24 VDC

8850-2 Conductivity/Resistivity Transmitter 3


3.3 Relay Output • Proportional Pulsing
The relays can be used as a switch that responds when the The relay will generate a 100 mS pulse at the rate defined by
process value moves above or below a setpoint, or to generate a settings in the CALIBRATE menu.
pulse at a rate proportional to the process value.
In the example below:
• Low: • The output will be 0 pulses/min. when value is less than 5.
Relay triggers when process is less than the setpoint. • The output will be 50 pulses/min. when value is 7.5.
The relay will relax when the process moves above the setpoint • The output will be 100 when value is greater than 10.
plus the hysteresis value.
The starting point, endpoint and maximum pulse rate are select-
• High: able in the CALIBRATE menu.
Relay triggers when process is greater than the setpoint.
The relay will relax when the process moves below the setpoint
plus the hysteresis value.

Process
100 pulses

in. :
s/m te
lse Ra
Pu ut
0 tp
Hysteresis

10 Ou

Pulse rate
to lay
Re
Low Setpoint

0
Time
0 pulses
Relay energized
5 10
Relay relaxed Starting point endpoint
Process

High Setpoint

Hysteresis

Time

VIEW menu
• During normal operation, ProcessPro displays the VIEW menu.
• When editing the CALIBRATE or OPTIONS menus, ProcessPro will return to the VIEW menu if no activity
62.50 uS/cm
occurs for 10 minutes. 25.0 C
• To select a VIEW display, press the UP or DOWN keys. The selections will scroll in a continuous loop. Signet
Conductivity/Resistivity
Transmitter
• Changing the VIEW display does not interrupt system operations.
• No key code is necessary to change display selection. ENTER

• Output settings cannot be edited from the VIEW menu.

View Menu
Display Description

1234.5 µS Monitor the Conductivity and temperature values from the sensor.
+67.89 ºC This is the permanent display.

The VIEW displays below are temporary. The permanent display will return after 10 minutes

Loop Output: Monitor the Loop Current output.


13.75 mA

Last CAL: Check the Last Calibration date.


04-20-07

4 8850-2 Conductivity/Resistivity Transmitter


ProcessPro Editing Procedure:
Step 1. Press and hold ENTER key:
• 2 seconds to select the CALIBRATE menu.
• 5 seconds to select the OPTIONS menu.
Step 2. The Key Code is UP-UP-UP-DOWN keys in sequence.
• After entering the Key Code, the display will show the first item in the selected menu.
Step 3. Scroll menu with UP or DOWN arrow keys.
Step 4. Press RIGHT ARROW key to select menu item to be edited.
• The first display element will begin flashing.
Step 5. Press UP or DOWN keys to edit the flashing element.
• RIGHT ARROW key advances the flashing element.
Step 6. Press ENTER key to save the new setting and return to Step 3.

Notes on Step 1: Notes on Step 2:


• The View Menu is normally displayed. If no key is pressed for 5 minutes while display is showing "Enter
• The CALIBRATE and OPTIONS menus require a KEY CODE. Key Code", the display will return to the VIEW menu.

CALIBRATE: ----
Press & Enter Key Code
hold for ENTER

access: CALIBRATE: *---


Enter Key Code
CALIBRATE: **--
VIEW Enter Key Code
2s 5s CALIBRATE: ***-
CALIBRATE Enter Key Code

OPTIONS Cell Constant: First item in CALI-


Standard > BRATE menu

Notes on Steps 3 and 4:


• Refer to pages 6 and 7 for complete listing of menu items and their use.
Cell Constant:
• From the Step 3 display, pressing the UP and DOWN keys simultaneously will Standard >
return the display to the VIEW menu.
• If no key is pressed for 10 minutes, display will also return to the VIEW menu.
Step 3

Step 3: Finished Editing? Relay1 Setpnt:


Press the UP and DOWN keys simultaneously after Step 4
20.0 uS >
saving the last setting to return to normal operation.

Notes on Steps 5 and 6:


Relay1 Setpnt:
• All output functions remain active during editing. 20.00 uS
• Only the flashing element can be edited.
Relay1 Setpnt:
• RIGHT ARROW key advances the flashing element in a continuous loop. 10.00 uS Step 5
• Edited value is effective immediately after pressing ENTER key.
• If no key is pressed for 10 minutes unit will restore the last saved value and return to step 3.
• Step 6 (pressing ENTER key) always returns you to Step 3. Relay1 Setpnt:
• Repeat steps 3-6 until all editing is completed. 10.00 uS

Relay1 Setpnt:
Step 5: Made an Error? 9
1 .00 uS
ENTER

Press the UP and DOWN keys simultaneously Step 6


while any element is flashing. This will recall the Relay1 Setpnt:
last saved value of the item being edited and Saving
return you to Step 3. Relay1 Setpnt:
19.00 uS >

8850-2 Conductivity/Resistivity Transmitter 5


Calibrate Menu
Display
Description
(Factory settings shown)
Cell Constant: Select CUSTOM only if you are connecting a certified conductivity sensor. Select
STANDARD for all other systems.
Standard >

Cell: Standard For STANDARD sensors: Select from these options: 0.01, 0.1, 1.0, 10.0 or 20.0.
1 >

Cell: Custom For CUSTOM sensors: Enter the precise cell constant from the certificate provided with
your sensor, or from the information label on the sensor.
1.0000 >

Cond Units: Select from these options: µS/cm, mS/cm, ký•cm, Mý•cm, PPB
µS >

PPM Factor: If the Units selection is PPM, set the ratio of Total Dissolved Solids to µS. The maximum
allowable is 3 µS = 1 PPM. The TDS factor can only be set in PPM.
2.00 >

Set: Adjust the temperature of the system based on an accurate external reference.
Temperature >

Set: For use with STANDARD sensors: Perform this single-point wet calibration for most
accurate results. Not required for CUSTOM sensors except for periodic system accuracy
Conductivity > confirmation. Enter all zeroes to restore factory calibration to TEMP and COND settings.

Loop Source: Select the input (Conductivity or Temperature) source to be associated with the current loop
output:
Cond >

Loop Range: µS Select the minimum and maximum values for the current loop output.
Be sure to modify this setting if you change the Cond. Units.
0.0000 → 100.000 >

Relay1 Source: Select the source (Conductivity or Temperature) for this relay output:
Cond >

Relay1 Mode: Select the mode of operation for the relay.


Options available are High, Low or proportional Pulse.
Low > The relay may be disabled (Off) if not in use.

Relay1 Setpnt: In Low or High Mode, the relay will be activated when the process reaches this value. Be
sure to modify this setting if you change the Cond. Units.
10.0000 µS >

Relay1 Hys: µS The relay will be deactivated at Setpoint ± Hysteresis, depending on High or Low Setpoint
selection.
0.5000 >

Relay1 Rng: µS In Pulse mode, set the process values where the proportional pulse will start and where it
will reach the maximum rate. Be sure to modify this setting if you change the Cond. Units.
10.0000 → 40.0000 >

Relay1 PlsRate: In Pulse mode, set the maximum rate for the proportional Pulse. The 8850 will accept any
value from 0 to 400.
120 Pulses/Min >

Last CAL: Use this “note pad” to record important dates, such as annual recertification or scheduled
maintenance.
04-20-07 >

6 8850-2 Conductivity/Resistivity Transmitter


Options Menu
Display
Description
(Factory settings shown)
Contrast: Adjust the LCD contrast for best viewing. A setting of 1 is lower contrast, 5 is higher. In
general, select lower contrast if the display is in warmer ambient surroundings.
3 >

Cond Decimal: Set the decimal to the best resolution for your application. The display will automatically
scale up to this restriction. Select *****., ****.*, ***.** **.*** or *.****
****.* >

Averaging: OFF provides the most instantaneous response to process changes. Select LOW (4 sec)
or HIGH (8 sec) averaging if your process experiences frequent or extreme fluctuations.
Off >

Loop Adjust: Adjust the minimum and maximum current output. The display value represents the
4.00 mA > precise current output. Adjustment limits:
• 3.80 mA < 4.00 mA > 5.00 mA
Loop Adjust: • 19.00 mA < 20.00 mA > 21.00 mA
Use this setting to match the system output to any external device.
20.00 mA >

Temp Display: Select ºC or ºF.


ºC >

Temperature Set the percent change in Conductivity caused by a 1ºC change in temperature. May be
from 0.00 to 10.00.
Comp %: 2.00 >

Test Loop: Press UP and DOWN keys to manually order any output current value from 3.8 mA to
21.00 mA to test the output loop.
>

Test Relay1: Press UP and DOWN keys to manually toggle the relay state.

>

8850-2 Conductivity/Resistivity Transmitter 7


Calibration Procedure
This instrument has been electronically calibrated at the factory.
• Procedure A verifies the accuracy and linearity of the instrument by simulating temperature and conductivity values with precision
(±0.1%) fixed resistors.
• Procedure B is a wet calibration. This procedure uses the sensor input and NIST traceable test solutions. When done correctly,
this procedure offers the most accurate system calibration.

A) Accuracy Verification with Precision Resistors (Electronic Calibration):


1. Simulate the Temperature
The temperature input to the 8850 is a PT-1000 thermistor, where 1000 Ohms (Ω) is equal to 0ºC and a change of 3.84 Ω equals a
1ºC change. (1000 Ω = 0ºC, 1003.84 Ω = 1.0ºC, 1007.68 Ω = 2.0ºC...................1096 Ω = 25ºC)

• Connect a resistor (1000 Ω to 1096 Ω ) between "Temp IN" and "Iso. Gnd" terminals.
• Set Temp; Adjust the temperature to exact value based on the measured resistance. (see Editing Procedure, Calibrate menu).
• To verify the temperature linearity, connect a second resistor value to the terminals.
• If the instrument does not display the correct value, service is required. ( ± 0.5ºC)

2. Simulate the Conductivity


You may calculate the exact Resistance needed to simulate a specific conductivity value , or you may calculate the exact Conductivity
based on a resistor value:

Resistance = Cell constant e.g. 0.1 Cell = 5,000 Ω or 5 KΩ


conductivity (Siemens*) 0.000020 (Siemens*)

Conductivity = Sensor cell e.g. 0.1 Cell = 0.000001 Siemens*


Simulation resistance (Ω) 100,000 (Ω) or 1µS/cm

(*1 µS = 1 X 10-6 Siemens or 0.000001 Siemens)

• Connect the conductivity resistor between the "Signal IN " and "Iso Gnd" terminals. Iso. Gnd
13 (BLACK)
• Set Cond: Adjust the conductivity value based on the resistor value. (see Editing
Temp. IN
Procedure and Calibrate menu). 12 (WHITE)
TC resistor
• Verify the linearity of the instrument by connecting a second resistor of a different value. Signal IN
• If the instrument does not display the correct value (± 2% of reading), service is required.
11 (RED)
Simulation resistor

B) Wet Calibration with NIST Traceable Solutions:


When using NIST traceable standards, review the temperature information provided with the test solution. Prevent contamination of the
test solution. The sensor must be at the temperature specified on the test solution label.

• Remove the sensor from the system. Rinse the sensor in a small amount of test solution.
• Place the sensor into the test solution.
• Place a reference thermometer into the same solution.
• Allow sufficient time for the temperature to stabilize.
• Set Temp: Adjust the temperature value based on the reference thermometer. (see Editing Procedure.)
• Set Cond: Adjust the conductivity value based on the test solution value. (see Editing Procedure.)
• Verify the linearity by placing the sensor into a second test solution of a different value.
• If the instrument does not display the correct value (Temperature ± 0.5ºC, Conductivity ± 2% of reading), service is required.

8 8850-2 Conductivity/Resistivity Transmitter


Temperature Coefficient
Conductivity measurement is highly dependent on temperature. Temperature dependence is expressed as the relative change per °C,
commonly known as percent/°C change from 25°C, or slope of the solution.

Slopes can vary significantly depending on process solution type. The factory default temperature compensation factor is 2.00%/°C.
Process solutions may require adjustment for maximum accuracy. To determine the optimum temperature compensation factor for a
process:

1. Disable the 8850 temperature compensation % factor by entering 0.00.

2. Heat the sample solution close to the maximum process temperature. Place sensor in the sample solution allowing several
minutes for stabilization. Access the VIEW menu and record the displayed temperature and conductivity values in the spaces
provided:

Displayed temperature: T1 = _______ °C


Displayed conductivity: C1 = _______ µS

Do not use this procedure for solutions from 0.055 µS to 0.1 µS (10 MΩ to 18 MΩ). An internal pure water curve is used for
these ranges. The factory default setting of 2.00% per °C should be used.

3. Cool the sample solution close to the minimum process temperature. Place sensor in the sample solution allowing several
minutes for stabilization. Record displayed temperature and conductivity values in the spaces provided:

Displayed temperature: T2 = _______ °C


Displayed conductivity: C2 = _______ µS

(A 10% change in conductivity between steps 2 and 3 is recommended.)

4. Substitute recorded readings (steps 2 and 3) into the following formula:

TC Slope = 100 x (C1 - C2)


(C2 x (T1 - 25)) - (C1 x (T2 - 25))

Example: A sample solution has a conductivity of 205 µS @ 48°C. After cooling the solution, the conductivity was measured at
150 µS @ 23°C. (C1 = 205, T1 = 48, C2 = 150, T2 = 23)
The TC is calculated as follows:

TC Slope = 100 x (205 - 150) = 5500 = 1.42%/°C


(150 x (48 - 25)) - (205 x (23 - 25)) 3860

Parts Per Million (PPM) Factor


This feature is only applicable when PPM display units are selected. The programmable PPM Factor is adjustable from 0.01 to
3.00 (factory default = 2.00).

Determine the best PPM Factor for a process solution by calculating the solution's conductivity (µS) and the percent of total
dissolved solids (PPM).

PPM Factor = Solution conductivity (µS/cm)


Total dissolved solids (PPM)

TDS (PPM) = Solution conductivity (µS/cm)


PPM Factor

Example: • Solution conductivity = 400 µS/cm

• TDS = 200 PPM (mg/L)

PPM Factor = 400 µS/cm = 2.00


200 PPM

8850-2 Conductivity/Resistivity Transmitter 9


Troubleshooting
Display Condition Possible Causes Suggested Solutions

Display is over range. This may be a • Check sensor for correct range.
"- - - -" normal condition if your process operates • Check Decimal setting in OPTIONS menu.
at/near the limits of the sensor range. • Check Calibrate menu settings for incompatible
SOURCE and RANGE values.

Value Must be less The PPM factor must be a value from Set a PPM value less than 3.
than 3 0.00 to 3.00

Value must be greater than 0 Custom cell constant cannot be set to 0 Set cell constant to a value greater than 0

"Value must be Pulse Rate cannot be greater than 400 set a pulse rate value less than 400
400 or less"

Display erratic, shows "0" or Aux Power not connected Wire 8850 according to diagram (Section 3.1)
"------" intermittently

"Too much Error • Defective or dirty/coated sensor • Clean or replace sensor


Check Sensor" • Wiring error • Check and correct wiring
• Fluid conductivity too low
• Defective temp element • Replace sensor

Technical notes
If a Current Loop is locked at 3.6 mA, the problem is related to the temperature circuit:
This occurs only if the 8850 detects a resistance from the temperature sensor that is less than 250Ω or greater than 2800Ω.
• Check the sensor wiring for open/short or poor connections on white (TEMP IN) and black (ISO GND)wires.
• The PT1000 temperature device in the sensor is defective.
• The transmitter is defective.

Auxiliary Power (terminals 1 and 2) must ALWAYS be connected for the 8850 to operate.

10 8850-2 Conductivity/Resistivity Transmitter


Notes

8850-2 Conductivity/Resistivity Transmitter 11


Ordering Information
Mfr. Part No Code Description
3-8850-2 159 000 230 Conductivity/Resistivity transmitter Field mount with relays
3-8850-2P 159 000 231 Conductivity/Resistivity transmitter Panel mount with relays

Parts and Accessories


Mfr. Part No Code Description
3-8050 159 000 184 Universal mounting kit
3-8050.395 159 000 186 Splashproof rear cover
3-8050.396 159 000 617 RC Filter kit (for relay use)
3-8052 159 000 188 3/4” Integral mounting kit
3-8052-1 159 000 755 3/4" NPT mount junction box
3-0000.596 159 000 641 Heavy duty wall mount bracket
3-8050.392 159 000 640 Model 200 retrofit adapter
3-5000.598 198 840 225 Surface mount bracket
3-5000.399 198 840 224 5 x 5 inch adapter plate for Signet retrofit
3-9000.392 159 000 368 Liquid-tight connector kit, 3 sets, 1/2 in. NPT
3-9000.392-1 159 000 839 Liquid-tight connector kit, 1 set, 1/2 in. NPT
3-9000.392-2 159 000 841 Liquid-tight connector kit, 1 set, PG 13.5
7300-7524 159 000 687 24 VDC Power Supply 7.5 W, 300mA
7300-1524 159 000 688 24 VDC Power Supply 15 W, 600mA
7300-3024 159 000 689 24 VDC Power Supply 30 W, 1.3 A
7300-5024 159 000 690 24 VDC Power Supply 50 W, 2.1 A
7300-1024 159 000 691 24 VDC Power Supply 100 W, 4.2 A
Conductivity/Resistivity Electrodes
Mfr. Part No. Code Description
3-2819-1 198 844 010 Conductivity/Resistivity (CR) Cell, 0.01, SS
3-2820-1 198 844 000 Conductivity Cell, 0.1, SS
3-2821-1 198 844 001 Conductivity Cell, 1.0, SS
3-2822-1 198 844 002 Conductivity Cell, 10, SS
3-2823-1 198 844 003 Conductivity Cell, 20, SS
3-2819-S1 159 000 085 CR Sanitary, 0.01, SS, 1 to 1 1/2 in.
3-2819-S1C 159 000 087 CR Sanitary, 0.01, SS, 1 to 1 1/2 in., Certified
3-2819-S2 159 000 086 CR Sanitary, 0.01, SS, 2 in.
3-2819-S2C 159 000 088 CR Sanitary, 0.01, SS, 2 in., Certified
3-2819-T1 159 000 081 CR Sanitary, 0.01, Titanium, 1 to 1 1/2 in.
3-2819-T1C 159 000 083 CR Sanitary, 0.01, Titanium, 1 to 1 1/2 in., Certified
3-2819-T2 159 000 082 CR Sanitary, 0.01, Titanium, 2 in.
3-2819-T2C 159 000 084 CR Sanitary, 0.01, Titanium, 2 in., Certified
3-2820-S1 159 000 089 CR Sanitary, 0.1, SS, 1 to 1 1/2 in.
3-2820-S1C 159 000 091 CR Sanitary, 0.1, SS, 1 to 1 1/2 in., Certified
3-2820-S2 159 000 090 CR Sanitary, 0.1, SS, 2 in.
3-2820-S2C 159 000 092 CR Sanitary, 0.1, SS, 2 in., Certified
3-2820-T1 159 000 624 CR Sanitary, 0.1, Titanium, 1 to 1 1/2 in.
3-2820-T2 159 000 625 CR Sanitary, 0.1, Titanium, 2 in.
3-2821-S1 159 000 093 CR Sanitary, 1.0, SS, 1 to 1 1/2 in.
3-2821-S1C 159 000 095 CR Sanitary, 1.0, SS, 1 to 1 1/2 in., Certified
3-2821-S2 159 000 094 CR Sanitary, 1.0, SS, 2 in.
3-2821-S2C 159 000 096 CR Sanitary, 1.0, SS, 2 in., Certified
3-2821-T1 159 000 626 CR Sanitary, 1.0, Titanium, 1 to 1 1/2 in.
3-2821-T2 159 000 627 CR Sanitary, 1.0, Titanium, 2 in.
3-2839-1 159 000 921 Conductivity Cell, 0.01, 15 ft cable, NPT
3-2839-1D 159 000 923 Conductivity Cell, 0.01, 15 ft cable, ISO
3-2840-1 159 000 786 Conductivity Cell, 0.1, 15 ft cable, NPT
3-2840-1D 159 000 788 Conductivity Cell, 0.1, 15 ft cable, ISO
3-2841-1 159 000 790 Conductivity Cell, 1.0, 15 ft cable, NPT
3-2841-1D 159 000 792 Conductivity Cell, 1.0, 15 ft cable, ISO
3-2842-1 159 000 794 Conductivity Cell, 10.0, 15 ft cable, NPT
3-2842-1D 159 000796 Conductivity Cell, 10.0, 15 ft cable, ISO
NOTE: Alternate wetted materials and lengths are available through special order.
Cable length extensions to 100 ft. (30 m) are available through special order.

George Fischer Signet, Inc., 3401 Aerojet Avenue, El Monte, CA 91731-2882 U.S.A. • Tel. (626) 571-2770 • Fax (626) 573-2057
For Worldwide Sales and Service, visit our website: www.gfsignet.com • Or call (in the U.S.): (800) 854-4090

3-8850.090-2 Rev. H 8/06 English © George Fischer Signet, Inc. 2001 Printed in U.S.A. on recycled paper
Signet 2820 Series Conductivity Sensor Instruction Manual English

*3-2820.090*
3-2820.090-1 Rev. K 11/04 English

Warning! SAFETY INSTRUCTIONS FOR IN-LINE ELECTRODE INSTALLATION


1. Do not remove from pressurized lines.
2. Do not exceed maximum temperature/pressure specifications.
3. Wear safety goggles or face shield during installation/service.
4. Do not alter product construction.
5. Disconnect instrument power before wiring this sensor.
Failure to follow safety instructions may result in severe personal injury!

1. Wiring
Signet 5800CR Signet 9050CR
RLY3 RLY4 ANL2 SERIAL CH2 CH1
C NO C NO R+ R- Tx GND Rx S2 T2 S1 T1 SG

SILVER (SHLD)
BLACK
WHITE
1 2 3 4 5 6 7 8 9 10 11 12 13 14
RED RED
CH 2 WHITE
BLACK
SILVER (SHLD)
Iso. Gnd
Temp. IN
Signal IN

Shld

RED
WHITE
BLACK
CH 1 SILVER (SHLD)

• Use three conductor shielded cable for cable extensions up to 30 m (100 ft) max.
• Shield must be maintained through cable splice.
• Disable power to instrument before connecting this sensor.

2. Recommended Position 3. 2819/2820/2821 In-line Installation

In-line Submersible

Standard Mark hole Hole up 3/4 in. NPT


fitting kit position
Customer
supplied
pipe tee/
reducer
2821-1 Sealant
O-ring
Hand tighten only!

Optional Mark hole Hole up 1/2 in. NPT


OR fitting kit position
Customer
supplied
pipe tee/
Sealant reducer
Use caution to avoid air bubble O-ring
or sediment trapping inside the
electrode cavity.
Hand tighten only!
4. 2822 In-line Installation 5. 2823 In-Line Installation Customer
supplied
3/4 in. NPT pipe tee/
Mark hole position Hole up reducer

Customer
supplied
pipe tee/
Sealant reducer
Sealant
Install behind
hole ONLY!

1-1/4 turns past finger tight

6. 2819/2820/2821 Submersible Installation 7. 2822 Submersible Installation

1 2 1 2

Sealant Customer supplied


Customer pipe
supplied pipe Optional
submersion Sealant
fitting kit
Sealant #3-2820.390
Customer supplied
Sealant coupling
Customer
3/4 in. NPT
supplied
O-ring coupling
1-1/4 turns
Hand 3/4 in. 1/2 in. past finger
tighten NPT NPT tight
only!

Standard Optional Standard Optional


fitting kit fitting kit fitting kit fitting kit

8. 2823 Submersible Installation

1 2

Customer supplied
pipe

Sealant
Fill with
3 to 4 in.
of sealant
Customer supplied
coupling

3/4 in. NPT

1-1/4 turns
past finger
Sealant tight

Attach 3/4 in. watertight pipe to the top of the sensor. Secure
the threaded connection to prevent any leakage. For additional
defense against possible accumulation of condensation at the
back seal area of the sensor, fill the lower 3-4 inches (75-100
mm) of conduit or extension pipe with a flexible sealant such as
silicone.

2 Signet 2820 Series Conductivity Sensor Instruction Manual


9. Specifications
Alternate wetted materials and overall lengths are available through special order. Cable length extensions to 100 ft. (30 m) are available
through special order. For resistivity measurements above 10 MΩ and/or below 20°C, maximum cable length is 25 ft. (7.6 m).

2819-1/2820-1/2821-1
• 2819-1 cell: 0.01
15 ft/4.6 m cable (std.)
2819-1 range: 0.010 to 100 µS (10 kΩ to 100 MΩ)
• 2820-1 cell: 0.1
2820-1 range: 1 to 1000 µS Reversible
• 2821-1 cell: 1.0 fitting assy.
6 in./ for submersion
2821-1 range: 10 to 10,000 µS 152 mm mounting

Temperature compensation: PT1000


Wetted materials: 3/4 in. NPT

• O-rings: EPR 4.2 in./


• Insulator material: PTFE 107 mm

• Electrodes: 316 stainless steel 2820-1 2821-1


Standard fitting: Polypropylene sensor tip sensor tip

• Max. pressure: 6.9 bar (100 psi) 2 in./


• Max. temperature: 100°C (212°F) 50 mm
0.8 in./
Optional fitting: 316 stainless steel (1/2 in. NPT) 21 mm 0.3 in./
• Max. pressure: 13.8 bar (200 psi) 8 mm
• Max. temperature: 120°C (248°F) 2819-1 0.5 in./
Quality Standard: CE 13 mm

2819-S1/2820-S1/2821-S1/2819-T1/2820-T1/2821-T1
2.0 in./
• 2819-X1 cell: 0.01 50 mm
2819-X1 range: 0.010 to 100 µS (10 kΩ to 100 MΩ)
• 2820-X1 cell: 0.1 15 ft/4.6 m cable (std.)
2820-X1 range: 1 to 1000 µS
• 2821-X1 cell: 1.0
2821-X1 range: 10 to 10,000 µS

Sanitary fitting size: 1 and 11/2 in.


Temperature compensation: PT1000 6.0 in./
152 mm
Wetted materials:
• O-rings: EPR 5.0 in./
• Insulator material: PTFE 126 mm
2820-X1 2821-X1
• Electrodes: 316 stainless steel or titanium sensor tip sensor tip
Sanitary fitting: 316 stainless steel or titanium
Max. pressure: 6.9 bar (100 psi) 2.0 in./
50 mm
Max. temperature: 120°C (248°F) 0.8 in./
21 mm 0.3 in./
Quality Standard: CE 8 mm

2819-X1 0.5 in./


13 mm

2819-S2/2820-S2/2821-S2/2819-T2/2820-T2/2821-T2 2.5 in./


64 mm
• 2819-X2 cell: 0.01
2819-X2 range: 0.010 to 100 µS (10 kΩ to 100 MΩ)
• 2820-X2 cell: 0.1 15 ft/4.6 m cable (std.)
2820-X2 range: 1 to 1000 µS
• 2821-X2 cell: 1.0
2821-X2 range: 10 to 10,000 µS

Sanitary fitting size: 2 in.


6.0 in./
Temperature compensation: PT1000 152 mm
Wetted materials:
• O-rings: EPR 5.0 in./
• Insulator material: PTFE 126 mm
2820-X2 2821-X2
• Electrodes: 316 stainless steel or titanium sensor tip sensor tip

Sanitary fitting: 316 stainless steel or titanium 2.0 in./


Max. pressure: 6.9 bar (100 psi) 50 mm
0.8 in./
Max. temperature: 120°C (248°F) 21 mm 0.3 in./
8 mm
Quality Standard: CE
2819-X2 0.5 in./
13 mm
Signet 2820 Series Conductivity Sensor Instruction Manual 3
2822-1 15 ft/4.6 m
Cell: 10.0 cable (std.)
3/4 in. NPT
Range: 100 to 200,000 µS

Temperature compensation: PT1000


5.8 in./
147 mm
Wetted materials: Optional 316 SS
• O-rings: EPR submersion fitting
kit #3-2820.390
• Insulator material: CPVC
3/4 in. NPT
• Electrodes: 316 stainless steel
Standard fitting: 316 stainless steel
Max. pressure: 6.9 bar (100 psi) 3.4 in./
86 mm
Max. temperature: 95°C (203°F)
Quality Standard: CE

0.75 in. 19 mm

2823-1
Cell: 20.0 15 ft./4.6 m
cable (standard)
Range: 200 to 400,000 µS
8.0 in./
Temperature compensation: PT1000 203 mm

Wetted materials: Reversible


• O-rings: EPR fitting assy
• Insulator material: PTFE for submersion
mounting
• Electrodes: 316 stainless steel
3/4 in. NPT
Fitting: 316 stainless steel
Max. pressure: 6.9 bar (100 psi)
Max. temperature: 150°C (302°F)
Quality Standard: CE 3.5 in./
89 mm

0.75 in. 19 mm

10. Maintenance Sensor tip Sensor tip


(end view) (side view)
Any coatings on electrodes will cause readings to drift or show
poor response. Clean metallic surfaces with a mild detergent and
a non-abrasive brush or cotton swab.
Electrode Insulator
8-32
A B

Cotton swab
2823-1 Sensor Tip Removal Procedure:
C
Clean electrode
Electrode Clean metal body

Insulator

Sensor tip
(side view)

11. Accessories

Part No. Description


3-2820.392 Optional 1/2" 316 SS Fitting
3-2820.390 Optional 3/4" 316 SS Fitting

George Fischer Signet, Inc. 3401 Aerojet Avenue, El Monte, CA 91731-2882 U.S.A. • Tel. (626) 571-2770 • Fax (626) 573-2057
For Worldwide Sales and Service, visit our website: www.gfsignet.com • Or call (in the U.S.): (800) 854-4090

3-2820.090-1 Rev. K 11/04 English © George Fischer Signet, Inc. 2003 Printed in U.S.A. on recycled paper
Signet 515/2536 Rotor-X Flow Sensors English
Instructions for all versions of: 515/8510-xx and 2536/8512-xx
*3-0515.090*
3-0515.090 E 8/04 English

SAFETY INSTRUCTIONS
1. Depressurize and vent system prior to installation or removal.
2. Confirm chemical compatibility before use.
3. Do not exceed maximum temperature/pressure specifications.
4. Wear safety goggles or faceshield during installation/service.
5. Do not alter product construction.

1. Specifications
2536 Sensor
General Data Signal:
Flow Rate Range: 515: 0.3 to 6 m/s (1 to 20 ft/s) Frequency: 49 Hz per m/s nominal (15 Hz per ft/s nominal)
2536: 0.1 to 6 m/s (0.3 to 20 ft/s) Supply voltage: 3.5 to 24 VDC regulated
Pipe Size Range: DN15 to DN1000 (½ in. to 12 in.) Supply current: <1.5 mA @ 3.3 to 6 VDC
Linearity: ±1% of full range <20 mA @ 6 to 24 VDC
Repeatability: ±0.5% full range Output Type: Open collector transistor, sinking
Cable Length: 7.6 m (25 ft) standard Output current: 10 mA max.
515: 60 m (200 ft.) maximum
2536: 305 m (1000 ft) maximum Fluid Conditions
Cable Type: 2-conductor twisted pair w/shield (22 AWG) Rotor-X Sensor Pressure/Temperature Ratings:
Minimum Reynolds Number Required: 4500
Cap Material: Glass Filled Polypropylene Polypropylene Body:
515: Red • 12.5 bar (180 psi) max. @ 20 °C (68 °F)
2536: Blue • 515: 1.7 bar (25 psi) max. @ 90 °C (194 °F)
Wetted Materials: • 2536: 1.7 bar (25 psi) max. @ 85 °C (185 °F)
• Sensor Body: Glass filled Polypropylene (black) or PVDF
(natural) PVDF Body:
• O-Rings: FPM (Std) or EPDM or FFKM • 14 bar (200 psi) max @ 20 °C (68 °F)
• Pin: Titanium or Hastelloy-C or PVDF; other • 515: 1.7 bar (25 psi) max @ 100 °C (212 °F)
material options available • 2536: 1.7 bar (25 psi) max @ 85 °C (185 °F)
• Rotor: Black PVDF or natural PVDF; optional Tefzel® bar psi
with or w/o Fluoraloy B® sleeve 14 200
Shipping Weight: -X0 0.454 kg (1 lb)
-X1 0.476 kg (1.04 lbs) 11 160
51

51
5/

-X2 0.680 kg (1.50 lbs) 5/


85

85
10

-X3 0.794 kg (1.75 lbs) 8 120 10


-X

-X
-X4 0.850 kg (1.87 lbs)
X

X
-P

-P
-X5 1.0 kg (2.20 lbs)
oly

6 80
VD
pr

3519 1.3 kg (2.86 lbs)


F
op
yle

515 Sensor 3 40
ne

Signal:
Frequency: 19.7 Hz per m/s nominal (6 Hz per ft/s)
Amplitude: 3.3 V p/p per m/s nominal (1 V p/p per ft/s) °F 0 40 80 120 160 200 240
Source Impedance: 8 kΩ °C -18 4 27 49 71 93 115

Dimensions
8510-XX/8512-XX bar psi
515/2536 Sensor Integral Sensor 14 200
shown with Transmitter
Standard and Integral Adapter Kit 11 160
25

7.6 m/25 ft.


25

cable (sold separately)


36

36

included
/85

/85
12

12

8 120
-X

-X
X

X
-P

-P

6 80
oly

VD

1-1/4" NPSM
pr

threaded cap 102 mm/ -X0 or


F
op

-X (0 thru 5) 4.0 in. -X1


3 40
yle

26.7 mm/
n

1.05 in.
e

°F 0 40 80 120 160 200 240


°C -18 4 27 49 71 93 115
Pipe Range:
1/2 to 4 in. -X0 = 104 mm/4.1 in.
5 to 8 in. -X1 = 137 mm/5.4 in. Standards & Approvals
10" and up -X2 = 213 mm/8.4 in. • Manufactured under ISO 9001 and ISO 14001
1/2 to 4 in. -X3 = 297 mm/11.7 in.
5 to 8 in. -X4 = 332 mm/13.1 in. Wet-tap -X0 = 152 mm/6.0 in. • CE
10" and up -X5 = 408 mm/16.1 in.
Lengths -X1 = 185 mm/7.3 in. • 515 Only: FM Class I, II, III/Div. I/Groups A-G
Inlet Outlet
2. Location of Fitting Flange Reducer 90° Elbow

Recommended sensor upstream/downstream 10x I.D. 5x I.D. 15x I.D. 5x I.D. 20x I.D. 5x I.D.
mounting requirements
2 x 90° Elbow
3 dimensions
2 x 90° Elbow Pump/Valve

25x I.D. 5x I.D. 40x I.D. 5x I.D. 50x I.D. 5x I.D.

3. Sensor Mounting Position -45° +45°

• Horizontal pipe runs: Mount sensor in the upright (0°) position for best performance. Mount
at a maximum of 45° when air bubbles are present (pipe must be full). Do not mount on the Process
bottom of the pipe when sediments are present. Pipe

• Vertical pipe runs: Mount sensor in any orientation. Upward flow is preferred to ensure full
pipe.

4. Standard Sensor Installation 3. Engage one thread of the sensor cap then turn the sensor
until the alignment tab is seated in the fitting notch. Hand
1. Lubricate the sensor O-rings with a silicone lubricant (e.g. tighten the sensor cap. DO NOT use any tools on the
GE silicone compound #G632 or equivalent). Do not use sensor cap or the cap threads and/or fitting flange threads
will be damaged, see Figure B.
black conduit sensor bale black senso
cap conduit bale
cap
tab
PROCESS PIPE
(TOP VIEW) direction of flow
notch Figure B

Figure A
any petroleum based lubricant that will attack the O-rings.
sensor
2. Using an alternating/twisting motion, lower the sensor into cap

the fitting, making sure the installation arrows on the black


cap are pointing in the direction of flow, see Figure A.
5. Sensor Wiring 515 Sensor Connections to Signet Instruments

Technical Notes Black


Frequency (-)
• Use 2-conductor shielded cable for cable extensions.
• Cable shield must be maintained through cable splice. Red
Frequency (+)
• Refer to your instrument manual for specific wiring details.
Shield
Ground
2536 Sensor Connections to Other Brand Instruments
Other Brands
black
+ 3.3 to 24 515 Sensor Connections to Signet Instruments

shield
10 kΩ - VDC
Black
Gnd. Other Frequency (-)
red instrument Red
Input
Frequency (+)
DC sensor power supplied from Signet instrument.
Shield
10KΩ Pull-up resistor may be required for non Signet brand instrument.
Ground

6. Rotor Replacement Procedure


1. To remove the rotor, insert a small screwdriver between the rotor and the ear of the sensor.

2. Twist the screwdriver blade to flex the ear outward enough to remove one end of the rotor and pin.
DO NOT flex the ear any more than necessary! If it breaks, the sensor cannot be repaired.

3. Install the new rotor by inserting one tip of the pin into the hole, then flex the opposite ear back
enough to slip rotor into place.
2 Signet 515/2536 Rotor-X Flow Sensors
7. K-Factors
A K-Factor is the number of pulses a sensor will generate for each engineering unit of fluid which passes the sensor. K-factors for
water are listed below in U.S. gallons and liters. For example, in a 1-inch PVC pipe, the 515 paddlewheel generates 174.67 pulses
per gallon of water passing the rotor. K-factors are listed for pipes up to 12 inches. For pipes over 12 inches, consult your Signet
distributor.
PIPE 515/8510-XX 2536/8512-XX PIPE 515/8510-XX 2536/8512-XX PIPE 515/8510-XX 2536/8512-XX
SIZE FITTING U.S. U.S. SIZE FITTING U.S. U.S. SIZE FITTING U.S. U.S.
(IN.) LITERS LITERS (IN.) LITERS LITERS (IN.) LITERS LITERS
GAL GAL GAL GAL GAL GAL
SCH 80 PVC TEES FOR SCH 80 PVC PIPE CARBON STEEL TEES ON SCH 40 PIPE STAINLESS STEEL WELDOLETS ON SCH 40 PIPE
1/2 PV8T005 480.19 126.87 991.71 262.01 1/2 CS4T005 370.20 97.808 756.00 199.74 2-1/2 CR4W025 18.800 4.9670 37.600 9.9339
3/4 PV8T007 257.72 68.090 545.14 144.03 3/4 CS4T007 212.06 56.027 438.69 115.90 3 CR4W030 12.170 3.2153 24.340 6.4306
1 PV8T010 174.67 46.148 352.44 93.114 1 CS4T010 141.14 37.289 286.78 75.768 4 CR4W040 6.9600 1.8388 13.920 3.6777
1-1/4 PV8T012 83.390 22.032 177.18 46.812 1-1/4 CS4T012 60.655 16.025 121.22 32.026 5 CR4W050 5.2600 1.3897 10.860 2.8692
1-1/2 PV8T015 58.580 15.477 117.85 31.137 1-1/2 CS4T015 45.350 11.982 91.139 24.079 6 CR4W060 3.6900 0.9749 7.5200 1.9868
2 PV8T020 32.480 8.5812 66.739 17.633 2 CS4T020 26.767 7.0717 54.468 14.391 8 CR4W080 2.1300 0.5627 4.3400 1.1466
2-1/2 PV8T025 21.833 5.7683 42.994 11.359 STAINLESS STEEL TEES ON SCH 40 PIPE 10 CR4W100 1.3500 0.3567 2.7600 0.7292
3 PV8T030 13.541 3.5775 26.652 7.0414 1/2 CR4T005 358.96 94.838 734.20 193.98 12 CR4W120 0.9600 0.2536 1.9400 0.5125
4 PV8T040 7.6258 2.0147 15.006 3.9645 3/4 CR4T007 202.61 53.530 412.10 108.88 CARBON STEEL WELDOLETS ON SCH 40 PIPE
SCH 80 CPVC TEES FOR SCH 80 CPVC PIPE 1 CR4T010 127.14 33.590 252.70 66.764 2-1/2 CS4W025 18.800 4.9670 37.600 9.9339
1/2 CPV8T005 480.19 126.87 991.71 262.01 1-1/4 CR4T012 61.910 16.357 128.12 33.849 3 CS4W030 12.170 3.2153 24.340 6.4306
3/4 CPV8T007 257.72 68.090 545.14 144.03 1-1/2 CR4T015 40.410 10.676 77.320 20.428 4 CS4W040 6.9600 1.8388 13.920 3.6777
1 CPV8T010 174.67 46.148 352.44 93.114 2 CR4T020 22.300 5.8917 45.780 12.095 5 CS4W050 5.2600 1.3897 10.860 2.8692
1-1/4 CPV8T012 83.390 22.032 177.18 46.812 GALVANIZED IRON TEES ON SCH 40 PIPE 6 CS4W060 3.6900 0.9749 7.5200 1.9868
1-1/2 CPV8T015 58.580 15.477 117.85 31.137 1 IR4T010 104.54 27.619 213.01 56.277 8 CS4W080 2.1300 0.5627 4.3400 1.1466
SCH 80 PVC SADDLES FOR SCH 80 PVC PIPE 1-1/4 IR4T012 62.979 16.639 127.75 33.751 10 CS4W100 1.3500 0.3567 2.7600 0.7292
2 PV8S020 32.480 8.5812 66.739 17.633 1 1/2 IR4T015 46.688 12.335 94.401 24.941 12 CS4W120 0.9600 0.2536 1.9400 0.5125
2-1/2 PV8S025 21.833 5.7683 42.994 11.359 2 IR4T020 29.459 7.7832 59.420 15.699 COPPER/BRONZE BRAZOLETS ON SCH 40 PIPE
3 PV8S030 13.541 3.5775 26.652 7.0414 BRONZE TEES ON SCH 40 PIPE 2-1/2 BR4B025 18.800 4.9670 37.600 9.934
4 PV8S040 7.6258 2.0147 15.006 3.9645 1 BR4T010 104.54 27.619 213.01 56.277 3 BR4B030 12.170 3.2153 24.340 6.431
6 PV8S060 4.1623 1.0997 8.3246 2.1994 1-1/4 BR4T012 62.979 16.639 127.75 33.751 4 BR4B040 6.9600 1.8388 13.920 3.678
8 PV8S080 2.3705 0.6263 5.0164 1.3253 1-1/2 BR4T015 46.688 12.335 94.401 24.941 5 BR4B050 5.2600 1.3897 10.860 2.869
10 PV8S100 1.5300 0.4042 3.0600 0.808 2 BR4T020 29.459 7.7832 59.420 15.699 6 BR4B060 3.6900 0.9749 7.5200 1.987
12 PV8S120 1.0600 0.2801 2.1600 0.571 COPPER TEE FITTINGS ON COPPER PIPE SCH K 8 BR4B080 2.1300 0.5627 4.3400 1.147
SCH 80 PVC SADDLE ON SCH 40 PVC PIPE 1/2 CUKT005 443.21 117.10 917.84 242.50 10 BR4B100 1.3500 0.3567 2.7600 0.729
2 PV8S020 27.350 7.2259 54.700 14.452 3/4 CUKT007 212.16 56.052 428.27 113.15 12 BR4B120 0.9600 0.2536 1.9400 0.513
2-1/2 PV8S025 18.874 4.9866 37.159 9.8175 1 CUKT010 127.18 33.600 256.43 67.749 SCH 80 IRON SADDLES ON SCH 80 PIPE
3 PV8S030 12.638 3.3389 23.697 6.2608 1-1/4 CUKT012 88.218 23.307 176.44 46.615 2 IR8S020 32.360 8.5495 64.720 17.099
4 PV8S040 6.7282 1.7776 13.456 3.5552 1-1/2 CUKT015 56.962 15.049 115.69 30.565 2-1/2 IR8S025 22.220 5.8705 42.480 11.223
6 PV8S060 3.7297 0.9854 7.4594 1.9708 2 CUKT020 29.370 7.7595 63.385 16.746 3 IR8S030 13.420 3.5456 26.420 6.980
8 PV8S080 2.1527 0.5688 4.5292 1.1966 COPPER TEE FITTINGS ON COPPER PIPE SCH L 4 IR8S040 7.6600 2.0238 14.700 3.884
10 PV8S100 1.3500 0.3567 2.8000 0.740 1/2 CUKT005 414.41 109.49 858.22 226.74 5 IR8S050 5.8600 1.5482 12.180 3.218
12 PV8S120 0.9600 0.2536 1.9800 0.523 3/4 CUKT007 191.09 50.485 385.74 101.91 6 IR8S060 4.0900 1.0806 8.4400 2.230
PP CLAMP-ON SADDLE ON SCH 80 PP PIPE 1 CUKT010 119.84 31.662 241.64 63.841 8 IR8S080 2.3300 0.6156 4.9000 1.295
10 PPS100 1.5300 0.4042 3.0600 0.808 1-1/4 CUKT012 85.451 22.576 170.90 45.152 10 IR8S100 1.5300 0.4042 3.0600 0.808
12 PPS120 1.0600 0.2801 2.1600 0.571 1-1/2 CUKT015 55.160 14.573 112.03 29.598 12 IR8S120 1.0600 0.2801 2.1600 0.571
PP CLAMP-ON SADDLE ON SCH 40 PP PIPE 2 CUKT020 28.605 7.5575 61.74 16.310 SCH 80 IRON SADDLE ON SCH 40 PIPE
10 PPS100 1.3500 0.3567 2.8000 0.740 2 IR8S020 26.820 7.0859 53.640 14.172
12 PPS120 0.9600 0.2536 1.9800 0.523 2-1/2 IR8S025 18.800 4.9670 37.600 9.934
3 IR8S030 11.990 3.1678 23.220 6.135
K-Factors DIN Pipes 4 IR8S040 6.8500 1.8098 13.260 3.503
5 IR8S050 5.3300 1.4082 11.040 2.917
515/8510-XX 2536/8512-XX
PIPE 6 IR8S060 3.7600 0.9934 7.2400 1.913
FITTING U.S. LITERS U.S. LITERS CODE
SIZE
GAL GAL 8 IR8S080 2.1300 0.5627 4.4000 1.162
POLYPROPYLENE FITTINGS (DIN/ISO AND BS AND ANSI) 10 IR8S100 1.3500 0.3567 2.8000 0.740
DN 15 PPMT005 481.55 127.23 952.87 251.75 198.150.522 12 IR8S120 0.9600 0.2536 1.9800 0.523
DN 20 PPMT007 277.09 73.207 563.10 148.77 198.150.523
DN 25 PPMT010 141.18 37.300 291.60 77.042 198.150.524 8. H-Dimensions
DN 32 PPMT012 83.540 22.071 169.22 44.709 198.150.525
DN 40 PPMT015 51.265 13.544 103.90 27.450 198.150.526 "H"
DN 50 PPMT020 29.596 7.8193 60.789 16.060 198.150.527
The plastic sensor insert in the Weldolet
DN 65 PPMT025 20.658 5.4579 41.498 10.964 198.150.560 fitting MUST be removed during the
DN 80 PPMT030 13.330 3.5218 26.786 7.0769 198.150.561 welding process. When reinstalled, it is
DN 100 PPMT040 8.7077 2.3006 17.415 4.6011 198.150.562
DN 125 PPMT050 5.0667 1.3386 10.168 2.6864 198.150.563
important that the insert be threaded to
DN 150 PPMT060 3.6892 0.9747 7.3119 1.9318 198.150.564 the proper height ("H" dimension).
DN 200 PPMT080 2.0398 0.5389 3.9946 1.0554 198.150.565
PVDF FITTINGS (DIN/ISO AND BS AND ANSI)
DN 15 SFMT005 420.87 111.19 827.26 218.56 198.150.529
DN 20 SFMT007 228.15 60.277 489.87 129.42 198.150.530
DN 25 SFMT010 136.70 36.116 283.55 74.915 198.150.531
DN 32 SFMT012 79.294 20.950 158.59 41.899 198.150.532 Weldolet “H” dimension Weldolet “H” dimension
DN 40 SFMT015 43.490 11.490 86.980 22.980 198.150.533 part number inches mm part number inches mm
DN 50 SFMT020 25.908 6.8450 50.385 13.312 198.150.534
DN 65 SFMT025 18.067 4.7732 36.133 9.5465 198.150.571
CS4W020 2.38 60.45 CS4W240 4.16 105.66
DN 80 SFMT030 12.357 3.2648 24.715 6.5297 198.150.572 CS4W025 2.33 59.18 CS4W360 4.10 104.14
DN 100 SFMT040 8.0599 2.1294 16.120 4.2589 198.150.573
CS4W030 2.32 58.92
DN 125 SFMT050 4.4312 1.1707 8.8624 2.3415 198.150.574
DN 150 SFMT060 3.2271 0.8526 6.4543 1.7052 198.150.575 CS4W040 2.30 58.42 CR4W020 2.38 60.45
DN 200 SFMT080 2.0360 0.5379 4.0720 1.0758 198.150.576 CS4W050 3.09 78.48 CR4W025 2.33 59.18
PVC FITTINGS (DIN/ISO) - EUROPE ONLY
DN 15 PVMT005 486.18 128.45 972.37 256.90 198.150.480 CS4W060 2.96 75.18 CR4W030 2.32 58.92
DN 20 PVMT007 242.85 64.160 485.69 128.32 198.150.481 CS4W080 2.73 69.34 CR4W040 2.30 58.42
DN 25 PVMT010 148.64 39.270 297.274 78.540 198.150.482
DN 32 PVMT012 85.125 22.490 170.249 44.980 198.150.483
CS4W100 5.48 139.19 CR4W050 3.09 78.48
DN 40 PVMT015 51.855 13.700 103.709 27.400 198.150.484 CS4W120 5.25 133.35 CR4W060 2.96 75.18
DN 50 PVMT020 29.750 7.8600 59.500 15.720 198.150.485
CS4W140 5.10 129.54 CS4W080 2.73 69.34
DN 65 PVMT025 17.487 4.6200 34.9734 9.2400 198.150.538
DN 80 PVMT030 12.491 3.3000 24.9810 6.6000 198.150.539 CS4W160 4.85 123.19 CR4W100 5.48 139.19
DN 100 PVMT040 8.1377 2.1500 16.2754 4.3000 198.150.540
CS4W180 4.60 116.84 CR4W120 5.25 133.35
DN 150 PVMT060 4.0878 1.0800 8.1756 2.1600 198.150.543
DN 200 PVMT080 2.0439 0.5400 4.0878 1.0800 198.150.545 CS4W200 4.38 111.25
Signet 515/2536 Rotor-X Flow Sensors 3
9. Signet Fittings
Type Description Type Description
Plastic tees 0.5 to 4 inch versions Iron, Carbon Steel, 0.5 to 2 in. versions
PVC or CPVC 316 SS Threaded Mounts on threaded pipe ends
tees

PVC Available in 10 and 12 inch sizes only Carbon steel & 2 to 4 inch, cut 1-7/16 inch hole in pipe
Glue-on Cut 2-1/2 inch hole in pipe stainless steel Over 4 inch, cut 2-1/8 inch hole in pipe
Saddles Weld in place using solvent cement Weld-on
Weldolets
PVC 2 to 4 inch, cut 1-7/16 inch hole in pipe
Saddles 6 to 8 inch, cut 2-1/8 inch hole in pipe Fiberglass 1.5 in. to 8 in. PVDF insert
tees & > 8 in. PVC insert
saddles: Special order 12 in. to 36 in.
FPT FPS
PP Available in 10 and 12 inch sizes only
Clamp-on Cut 2-1/8 inch hole in pipe Metric For pipes DN 65 to 200 mm
Saddles Wafer Fitting PP or PVDF

Iron 2 to 4 inch, cut 1-7/16 inch hole in pipe Metric For pipes from DN 15 to 50 mm
Strap-on Over 4 inch, cut 2-1/8 inch hole in pipe Union PP or PVDF
saddles Special order 12 in. to 36 in. Fitting

515/8510-XX 2536/8512-XX
Ordering Information Ordering Information Product Description
Part No. Code Part No. Code
P51530-P0 .......198 801 620 3-2536-P0 .........198 840 143 Sensor, Polypropylene, Titanium Rotor Pin, PVDF Rotor (black), to 4 Inch Pipe
P51530-P1 .......198 801 621 3-2536-P1 .........198 840 144 Sensor, Polypropylene, Titanium Rotor Pin, PVDF Rotor (black) 5 to 8 Inch Pipe
P51530-P2 .......198 801 622 3-2536-P2 .........198 840 145 Sensor, Polypropylene, Titanium Rotor Pin, PVDF Rotor (black) 10 to 36 Inch Pipe
P51530-P3 .......198 840 310 3-2536-P3 .........159 000 758 Sensor, Wet-Tap, Polypropylene, Titanium Rotor Pin, PVDF Rotor (black), ½ to 4 Inch Pipe
P51530-P4 .......198 840 311 3-2536-P4 .........159 000 759 Sensor, Wet-Tap, Polypropylene, Titanium Rotor Pin, PVDF Rotor (black) 5 to 8 Inch Pipe
P51530-P5 .......198 840 312 3-2536-P5 .........159 000 760 Sensor, Wet-Tap, Polypropylene, Titanium Rotor Pin, PVDF Rotor (black) 10 to 36 Inch Pipe
P51530-V0 .......198 801 623 3-2536-V0 .........198 840 146 Sensor, PVDF (natural), Hastelloy Rotor Pin, PVDF Rotor (natural), ½ to 4 Inch Pipe
P51530-V1 .......198 801 624 3-2536-V1 .........198 840 147 Sensor, PVDF (natural), Hastelloy Rotor Pin, PVDF Rotor (natural), 5 to 8 Inch Pipe
P51530-V2 .......198 801 625 N/A N/A Sensor, PVDF (natural), Hastelloy Rotor Pin, PVDF Rotor (natural), 10 to 36 Inch Pipe
P51530-T0 ........198 801 663 3-2536-T0 .........198 840 149 Sensor, PVDF (natural), PVDF (nat.) Rotor Pin, PVDF Rotor (nat.), ½ to 4 Inch Pipe
P51530-T1 ........198 801 664 N/A N/A Sensor, PVDF (natural), PVDF (nat.) Rotor Pin, PVDF Rotor (nat.), 5 to to 8 Inch Pipe
3-8510-P0 .........198 864 504 3-8512-P0 .........198 864 513 Sensor, Integral, PP, Titanium Rotor Pin, PVDF Rotor (black), ½ to 4 Inch Pipe
3-8510-P1 .........198 864 505 3-8512-P1 .........198 864 514 Sensor, Integral, PP, Titanium Rotor Pin, PVDF Rotor (black) 5 to 8 Inch Pipe
3-8510-T0 .........159 000 622 3-8512-T0 .........198 864 518 Sensor, Integral, PVDF (nat.), Hastelloy Rotor Pin, PVDF Rotor (nat.), ½ to 4 In. Pipe
3-8510-V0 .........198 864 506 3-8512-V0 .........198 864 516 Sensor, Integral, PVDF (nat.), PVDF (nat.) Rotor Pin, PVDF Rotor (nat.), ½ to 4 In. Pipe
3519/515-P3 .....159 000 819 3519/2536-P3 ...159 000 822 Sensor & Wet-Tap Assy., PP, Titanium Rotor Pin, PVDF Rotor (black), ½ to 4 In. Pipe
3519/515-P4 .....159 000 820 3519/2536-P4 ...159 000 823 Sensor & Wet-Tap Assy., PP, Titanium Rotor Pin, PVDF Rotor (black), 5 to 8 In. Pipe
3519/515-P5 .....159 000 821 3519/2536-P5 ...159 000 824 Sensor & Wet-Tap Assy., PP, Titanium Rotor Pin, PVDF Rotor (black), 10 to 36 In. Pipe

Accessories
M1538-2 ...........198 801 181 3-2536.320-1 ....198 820 052 Rotor, PVDF Black
P51547-3 ..........159 000 474 3-2536.320-2 ....159 000 272 Rotor, PVDF Natural
M1538-4 ...........198 820 018 3-2536.320-3 ....159 000 273 Rotor, Tefzel®
P51550-3 ..........198 820 043 3-2536.321 .......198 820 054 Rotor and Pin, PVDF Natural
3-0515.322-1 ....198 820 059 3-2536.322-1 ....198 820 056 Sleeved Rotor, PVDF Black
3-0515.322-2 ....198 820 060 3-2536.322-2 ....198 820 057 Sleeved Rotor, PVDF Natural
3-0515.322-3 ....198 820 017 3-2536.322-3 ....198 820 058 Sleeved Rotor, Tefzel®
M1546-1 ...........198 801 182 M1546-1 ...........198 801 182 Rotor Pin, Titanium
M1546-2 ...........198 801 183 M1546-2 ...........198 801 183 Rotor Pin, Hastelloy-C
M1546-3 ...........198 820 014 M1546-3 ...........198 820 014 Rotor Pin, Tantalum
M1546-4 ...........198 820 015 M1546-4 ...........198 820 015 Rotor Pin, Stainless Steel
P51545 .............198 820 016 P51545 .............198 820 016 Rotor Pin, Ceramic
1220-0021 ........198 801 186 1220-0021 ........198 801 186 O-Ring, FPM
1224-0021 ........198 820 006 1224-0021 ........198 820 006 O-Ring, EPDM
1228-0021 ........198 820 007 1228-0021 ........198 820 007 O-Ring, FFKM
P31536 .............198 840 201 P31536 .............198 840 201 Sensor Plug, Polypro
P31536-1 ..........198 840 202 P31536-1 ..........198 840 202 Sensor Plug, PVDF Metric
P31536-2 ..........159 000 649 P31536-2 ..........159 000 649 Sensor Plug, PVDF
P31542 .............198 801 630 P31542 .............198 801 630 Sensor Cap, Red (for use w/515)
---- ---- P31542-3 159 000 464 Sensor Cap, Blue (for use w/2536)
P31934 159 000 466 P31934 159 000 466 Conduit Cap
P51589 .............159 000 476 P51589 .............159 000 476 Conduit Adapter Kit
5523-0222 ........159 000 392 5523-0222 ........159 000 392 Cable (per foot), 2 cond. w/shield, 22 AWG

George Fischer Signet, Inc., 3401 Aerojet Avenue, El Monte, CA 91731-2882 U.S.A. • Tel. (626) 571-2770 • Fax (626) 573-2057
For Worldwide Sales and Service, visit our website: www.gfsignet.com • Or call (in the U.S.): (800) 854-4090

3-0515.090 E 8/04 English © George Fischer Signet, Inc., 2003 Printed in U.S.A. on recycled paper
Signet 8750-1 pH/ORP Transmitter English
*3-8750.090-1*
3-8750.090-1 Rev. G 10/06 English

10.20 pH
CAUTION! 25.0C

• Remove power to unit before wiring input and out- Signet pH/ORP
Transmitter
put connections.
• Follow instructions carefully to avoid personal injury. ENTER

1. Installation
ProcessPro transmitters are available in two styles: panel mount and field mount. The panel mount is supplied with the necessary
hardware to install the transmitter. This manual includes complete panel mounting instructions.
Field mounting requires a separate mounting kit. The 3-8050 Universal kit enables the transmitter to be installed virtually
anywhere. Detailed instructions for field installation options are included with the 3-8050 Universal kit.

1.1 Panel Installation


1. The panel mount transmitter is designed for installation using a 1/4 DIN Punch. For manual panel cutout, an adhesive
template is provided as an installation guide. Recommended clearance on all sides between instruments is 1 inch.
2. Place gasket on instrument, and install in panel.
3. Slide mounting bracket over back of instrument until quick-clips snap into latches on side of instrument.
4. To remove, secure instrument temporarily with tape from front or grip from rear of instrument. DO NOT RELEASE.
Press quick-clips outward and remove.

panel
gasket
mounting
terminals bracket

Optional
96 mm 82 mm Rear 92 mm
(3.8 in.)
8050 (3.23 in.) (3.6 in.)
Cover
latch 7
sr Gnd
SenIELD)
(SH
sr IN
SenD)
- 6 (RE
Pwr Output sr V+
System
p-
4 SenACK)
(BL
2 Loo
Pwr
5
System
p+ +
1 Loo
Output
3

96 mm 42 mm 64 mm 56 mm
(3.8 in.) 41 mm (2.2 in.)
(1.7 in.) (2.5 in.) (1.6 in.)
97 mm
106 mm (4.2 in.) (3.8 in.)
FRONT VIEW
SIDE VIEW SIDE VIEW
Field Mount & Panel Mount
Panel Mount Field Mount Panel Mount Installation Detail quick-clips

2. Specifications
General
Compatible electrodes: Current output:
Signet 3-2720 pH/ORP Preamplifier/3-271X Electrodes • 4 to 20 mA, isolated, fully adjustable and reversible
Accuracy: ± 0.03 pH, ± 2 mV ORP • Max loop impedance: 50 Ω max. @ 12 V
Enclosure: 325 Ω max. @ 18 V
• Rating: NEMA 4X/IP65 front 600 Ω max. @ 24 V
• Case: PBT • Update rate: 0.5 seconds
• Panel case gasket: Neoprene • Accuracy: ±0.03 mA @ 25°C, 24 V
• Window: Polyurethane coated polycarbonate Open-collector output:
• Keypad: Sealed 4-key silicone rubber • Isolated, 50 mA sink or source, 30 VDC max. pull-up voltage
• Weight: Approx. 325g (12 oz.) • Programmable for:
Display: • Hi or Lo w/adjustable hysteresis
• Alphanumeric 2 x 16 LCD • Proportional pulse (400 pulses per minute maximum)
• Contrast: User selected, 5 levels
• Update rate: 1 second Environmental
• Operating temperature: -10 to 70°C (14 to 158°F)
Electrical • Storage temperature: -15 to 80°C (5 to 176°F)
• Power: 12 to 24 VDC ±5%, regulated, 21 mA max. • Relative humidity: 0 to 95%, non-condensing
Sensor input range: • Maximum altitude: 2000 m (6562 ft)
• pH: 0.00 to 14.00 pH
• temp. (pH only) 3K Balco, -25 to 120°C (-13 to 248°F) Standards and Approvals
• ORP: -1000 to +2000 mV, isolated • CE, UL listed
(10KΩ I.D. resistance T+, T-) • Immunity: EN50082-2
• Emissions: EN55011 Class B
• Manufactured under ISO 9001 and ISO 14001
3. Electrical Connections
Caution: Failure to fully open terminal jaws before removing wire may permanently damage instrument.

Wiring Procedure 2
1. Remove 0.5 - 0.625 in. (13-16 mm) of insulation from wire end.
1
2. Press the orange terminal lever downward with a small screwdriver to open terminal jaws.
3. Insert exposed (non-insulated) wire end in terminal hole until it bottoms out.
4. Release orange terminal lever to secure wire in place. Gently pull on each wire to ensure a good connection.

Wiring Removal Procedure


1. Press the orange terminal lever downward with a small screwdriver to open terminal jaws.
2. When fully open, remove wire from terminal.

Wiring Tips:
• Do not route sensor cable in conduit containing AC power wiring. Electrical noise may interfere with sensor signal.
• Routing sensor cable in grounded metal conduit will help prevent electrical noise and mechanical damage.
• Seal cable entry points to prevent moisture damage.
• Only one wire should be inserted into a terminal. Splice double wires outside the terminal.

Terminals 9-12: Sensor connections


9-10 are mV (pH or ORP) input from the electrode.
11-12 are Temperature input from the electrode

Terminals 1 and 2: Loop Power


12-24 VDC ±10% system power and current
loop output.
Max. loop impedance: Temp -
50 Ω max. @ 12 V 12 (WHITE)
325 Ω max. @ 18 V Temp +
600 Ω max. @ 24 V 11 (GREEN)
Iso. GND
10 (BLUE)
mV Input
9 (BROWN)

System Pwr Earth


2 Loop - 8 GND
System Pwr Sensr Gnd
1 Loop + 4 Output - 7 (SHIELD)
V-
6 (BLACK)
V+
3 Output +
5 (RED)

Internal open-collector
output circuit Terminals 5-8: Preamplifier power and grounds
15Ω 5-6 are DC voltages from the 8750 to power the
S preamplifier.
Output --
7-8 are ground terminals for the sensor and for earth
Output + ground.
D
Isolation

Terminals 3 and 4: Open-collector Output


A transistor output, programmable in CALIBRATE menu as:
• High or Low setpoint with adjustable hysteresis
• Proportional pulse up to 400 pulses per minute
• May be disabled (Off) if not used.

2 8750-1 pH/ORP Transmitter


3.1 Sensor Input Connections

Terminals White (Temp) Preamp: Preamp:


12 Signet 2720 Signet 2760-1
Green (Temp) Transmitter
11 Signet 2760-2
Blue (ISO GND)
10
Brown (mV input) 10.20 pH

9
25.0C
Signet pH/ORP
Transmitter

* 8
Silver (Shield)
ENTER

7
6 Black (V-)
5 Red (V+) ≤ 400 ft. (122 m)
Twist-Lock DryLoc
* (connection of terminal 8 to Earth GND Electrodes Electrodes
may reduce electrical interference)

3.2 System Power/Loop Connections

Stand-alone application, no current loop used

Transmitter
Terminals
System Pwr Loop - 24 - Power
Supply
System Pwr Loop + 13 + 12-24 VDC

Connection to a PLC/Recorder, separate supply Connection to a PLC with built-in power supply

PLC or Recorder
Transmitter PLC Terminals
Transmitter
+ Loop Input
Terminals
Terminals
- 4-20 mA System Pwr Loop - 24 + Loop Input
4-20 mA
System Pwr Loop - 24 System Pwr Loop + 13 -
System Pwr Loop + 13
+ Power
- Power
-
Supply
12-24 VDC
Supply
+ 12-24 VDC Internal
PLC Connection

Example: Two transmitters connected to PLC/Recorder with separate power supply

PLC or Recorder

+ Channel 1
- 4-20 mA in

- Channel 2
Transmitter 1 Transmitter 2
Terminals + 4-20 mA in
Terminals

System Pwr Loop - 24 24 System Pwr Loop -


System Pwr Loop + 13 13 System Pwr Loop +

- Power
Supply
+ 12-24 VDC

8750-1 pH/ORP Transmitter 3


3.3 Open Collector Output
The Open Collector output can be used as a switch that responds • Proportional Pulsing
when the process value moves above or below a setpoint, or it The Open Collector output will generate a 100 mS pulse at the
can be used to generate a pulsing signal with a rate proportional rate defined by settings in the CALIBRATE menu (see page 6)
to the process value.
In the example below:
• Low: • The output will be 0 pulses/min. at pH values less than 5.0.
Output triggers when process variable is less than the setpoint. • The output will be 50 pulses/min. at 7.5 pH.
The output will relax when the process moves above the setpoint • The output will be 100 pulses/min. at pH values above 10 pH.
plus the hysteresis value.

• High:
Output triggers when process variable is greater than the
setpoint. The output will relax when the process variable moves
below the setpoint plus the hysteresis value.

:
in. ate
Process

s/m ut R
100 pulses

lse utp
Pu O
Hysteresis

0 or
10 ct

Pulse rate
to lle
0 Co
n
Low Setpoint

pe
O
Time

Relay energized 0 pulses


Relay relaxed 5 10
Starting point endpoint
Process

High Setpoint

Hysteresis

Time

VIEW Menu
• During normal operation, ProcessPro displays the VIEW menu.
10.20 pH
• When using the CALIBRATE or OPTIONS menus, ProcessPro will return to the VIEW menu if no activity 25.0C
occurs for 10 minutes. Signet pH/ORP
Transmitter
• To select the item you want displayed, press the UP or DOWN arrow keys. The items will scroll in a
continuous loop. Changing the display selection does not interrupt system operations. ENTER

• No key code is necessary to change display selection.


• Output settings cannot be edited from the VIEW menu.

View Menu for pH


Display Description

7.00 pH Monitor the Temperature input from the sensor.


12.6 ºC This is the permanent view display.
All of the displays below are temporary. The permanent display will return after ten minutes.

Input: Monitor the millivolt input from the electrode. Use this display to determine the
307 mV relative condition of your electrode during periodic calibration. (7 pH buffer = 0
mV, ±50 mV)

Loop Output: Monitor the 4-20 mA Loop output.


14.16 mA

Last CAL: Monitor date for scheduled maintenance or date of last calibration.
04-20-07 >

EASY Easy Cal is the fastest and simplest periodic calibration method. Requires 4 pH,
CAL: > 7 pH and 10 pH. (Any two)

4 8750-1 pH/ORP Transmitter


ProcessPro Editing Procedure:
Step 1. Press and hold ENTER key:
• 2 seconds to select the CALIBRATE menu
• 5 seconds to select the OPTIONS menu.
Step 2. The Key Code is UP-UP-UP-DOWN keys in sequence.
• After entering the Key Code, the display will show the first item in the selected menu.
Step 3. Scroll menu with UP or DOWN arrow keys.
Step 4. Press RIGHT ARROW key to select menu item to be edited.
• The first display element will begin flashing.
Step 5. Press UP or DOWN keys to edit the flashing element.
• RIGHT ARROW key advances the flashing element.
Step 6. Press ENTER key to save the new setting and return to Step 3.

Notes on Step 1: Notes on Step 2:


• The View Menu is normally displayed. If no key is pressed for 5 minutes while display is showing "Enter
• The CALIBRATE and OPTIONS menus require a KEY CODE. Key Code", the display will return to the VIEW menu.

CALIBRATE: ----
Press & Enter Key Code
ENTER
hold for
access: CALIBRATE: *---
Enter Key Code
CALIBRATE: **--
VIEW Enter Key Code
2s 5s CALIBRATE: ***-
CALIBRATE Enter Key Code

OPTIONS Set: First item in CALI-


Temperature > BRATE menu

Notes on Steps 3 and 4:


• Refer to pages 6 and 7 for complete listing of menu items and their use.
• From the Step 3 display, pressing the UP and DOWN keys simultaneously will Set:
return the display to the VIEW menu. Temperature >
• If no key is pressed for 10 minutes, display will also return to the VIEW menu.
Step 3

Step 3: Finished Editing? Output Setpnt:


Press the UP and DOWN keys simultaneously after 10.0 pH > Step 4
saving the last setting to return to normal operation.

Notes on Steps 5 and 6:


Output Setpnt:
• All output functions remain active during editing. 10.00 pH
• Only the flashing element can be edited.
Output Setpnt:
• RIGHT ARROW key advances the flashing element in a continuous loop. 00.00 pH Step 5
• Edited value is effective immediately after pressing ENTER key.
• If no key is pressed for 10 minutes unit will restore the last saved value and return to step 3.
• Step 6 (pressing ENTER key) always returns you to Step 3. Output Setpnt:
00.00 pH
• Repeat steps 3-6 until all editing is completed.

Output Setpnt:
9
0 .00 pH
Step 5: Made an Error?
ENTER

Press the UP and DOWN keys simultaneously Step 6


while any element is flashing. This will recall the Output Setpnt:
Saving
last saved value of the item being edited and
return you to Step 3. Output Setpnt:
9.00 pH >

8750-1 pH/ORP Transmitter 5


Calibrate Menu for pH
Display
Description
(Factory settings shown)

Set: Provides a maximum 25ºC offset to match temperature measurement to external reference.
Temperature >

Set: Applies a linear offset to the pH measurement. The ideal value is the average pH of your
application. (A sample of your application at process temperature is recommended.)
Standard >

Set: Applies a slope to the pH measurement. The slope value and the standard value must be at
least 2 pH units apart.
Slope > The ideal values are the minimum and maximum values of your process.

Loop Range: pH Select the minimum and maximum values for the 4-20 mA Current loop output.
0.00 → 14.00 >

Output Source: Select pH or Temperature as the source for the Open Collector Output.
pH >

Output Mode: Select the mode of operation for the Open Collector output: High, Low or proportional Pulse.
The signal may be disabled if not in use.
Low >

Output Setpnt: In Low or High Mode, the Open Collector output will be activated when the pH reaches this
value.
4.00 pH >

Output Hys: In Low or High mode, the Open Collector output will be deactivated at Setpoint ± Hysteresis,
depending on High or Low Setpoint selection. (See details on page 4.)
0.50 pH >

Output Range: pH
If the output is in PULSE mode, set the start and end point of the range and also set the
4.00 → 8.00 > maximum pulse rate. (The maximum PULSE rate setting is 400 pulses per minute.)
The combined Output Range and Pulse rate settings shown here indicate:
Output PlsRate: "Start pulsing when the pH value is 4 and increase the pulse rate up to the maximum of 120
pulses per minute when the pH value reaches 8"
120 Pulses/min >

Last CAL: Use this “note pad” to record important dates, such as annual recertification or scheduled
maintenance.
04-20-07 >

6 8750-1 pH/ORP Transmitter


EASY CAL Procedure - pH
• This procedure simplifies system calibration using standard 4.0, 7.0, 10.0 pH buffers only. If these pH buffers are not available,
calibrate the system via the CALIBRATE menu, using the STANDARD and SLOPE settings.
• Access the CALIBRATE menu and set sensor temperature before performing EASY CAL for new electrode installations.
• Access EASY CAL menu from the view menu.

EASY CAL: ---- Press UP, UP, UP, DOWN buttons in sequence to enter menu,
Enter Key Code ____
XXXX will appear during code entry.

To Calibrate: Response: To Accept:

Place Sensor in * 6.90 pH * 6.90 pH


Theoretical mV values
pH Buffer #1 -005 mV -005 mV pH @ 25°C mV
Place electrode tip in
2 +296
Allow for stabilization ENTER to accept
first pH buffer 3 +237
pH 7.0 = 0 mV 1
* 7.00 pH 4 +177
pH 4.0 = 177
pH 10 = -177 -005 mV 5 +118
30 seconds*
Limit ± 50 mV 6 +59
7 +0
8 -59
Place Sensor in * 3.93 pH * 3.93 pH 9 -118
pH Buffer #2 +179 mV +179 mV
10 -177
Place electrode tip Allow for stabilization Press ENTER to accept 11 -237
2
in second pH buffer. second buffer calibration. 12 -296
* 4.00 pH
+179 mV
30 seconds*

To exit menus and return to Display returns to VIEW Good Easy Cal
VIEW press UP and DOWN Menu in 10 minutes or Press <ENTER>
button at the same time when ENTER is pressed

Display
Description
(Factory settings shown)
Contrast: Adjust the LCD contrast for best viewing. A setting of 1 is lower contrast, 5 is higher.
Select lower contrast if the display is in warmer ambient surroundings.
3 >

Averaging: OFF provides the most instantaneous output response to changes in input value.
LOW averaging = 4 seconds, HIGH averaging = 8 seconds of input signal.
Off >

Output Active: Active HIGH: This setting is used to turn a device (pump, valve) ON at the setpoint.
Active LOW: This setting is used to turn a device OFF at the setpoint.
Low >
Temp Display:
Select temperature units: ºC or ºF.
ºC >

Loop Adjust: Adjust the minimum and maximum current output. The display value represents the
4.00 mA precise current output.
Adjustment limits:
• 3.80 mA < 4.00 mA > 5.00 mA
Loop Adjust: • 19.00 mA < 20.00 mA > 21.00 ma
20.00 mA > Use this setting to match the 8750 loop output to any external device.

Test Loop: Press UP or DOWN keys to manually order any output current value from 3.6 mA to
21.00 mA to test current loop output.
>

Test Output: Press UP or DOWN keys to manually toggle the state of the OPEN COLLECTOR
output.
>

8750-1 pH/ORP Transmitter 7


Calibrate Menu for ORP
Display
Description
(Factory settings shown)

Set: Applies a linear offset to the ORP measurement. The ideal value is the average pH of your
application. (A sample of your application at process temperature is recommended.)
Standard >

Set: Applies a slope to the ORP measurement. The slope value and the standard value must
be at least 120 mV apart. The ideal values are the minimum and maximum values of your
Slope > application.

Loop Range: mV Select the minimum and maximum ORP values for the 4-20 mA Current loop output.
Minimum range is -1000 mV; Maximum range is +2000 mV.
-1000 → +1000 >

Output Mode: Select the desired mode of operation for the Open Collector output: High, Low or
proportional Pulse. The signal may also be disabled if not in use.
Off >

Output Setpnt: In Low or High Mode, the Open Collector output will be deactivated when the ORP reaches
this value.
-500 mV >

Output Hys: In Low or High mode, the Open Collector output will be deactivated at Setpoint ± Hysteresis,
depending on High or Low Setpoint selection. (See details on page 4.)
10 mV >

Output Range: mV If the output is in PULSE mode, set the start and end point of the range and also set the
maximum pulse rate. (The maximum PULSE rate setting is 400 pulses per minute.)
-500 → +500 >
The combined Output Range and Pulse rate settings shown here indicate:
Output PlsRate: "Start pulsing when the ORP value is -500 and increase the pulse rate up to the maximum
of 120 pulses per minute when the ORP value reaches +500"
120 pulses/min >

Last Cal: Use this “note pad” to record important dates, such as annual recertification or scheduled
maintenance.
04-20-07 >

8 8750-1 pH/ORP Transmitter


EASY CAL Procedure - ORP
• This procedure simplifies system calibration using standard 4.0 pH and 7.0 pH buffers saturated with Quinhydrone. To calibrate
using any other ORP buffer solutions, use the Standard and Slope functions in the CALIBRATE menu.
• Access EASY CAL menu from the view menu.

EASY CAL: ---- Press UP, UP, UP, DOWN buttons in sequence to enter menu,
Enter Key Code
will appear during code entry.
*
To Calibrate: Response: To Accept: For best results, gently stir the
submerged electrode for approximately 5
Place Sensor in * ORP: + 84 mV * ORP: + 84 mV seconds during the stabilization period.
ORP Buffer #1 Input: + 82 mV Input: + 82 mV
Large temperature differences from pro-
Place electrode tip Allow for stabilization ENTER to accept cess fluids to buffers may require longer
in first pH buffer; 1 stabilization time.
* ORP: + 87 mV
pH 7.0 87 mV Input: + 82 mV Technical notes:
pH 4.0 264 mV 30 seconds*
The difference between the actual mV and
value shown is a good indication of the
condition of the electrode.
Place Sensor in * ORP: +262 mV * ORP: +262 mV
ORP Buffer #2 Input: +260 mV Input: +260 mV Differences in excess of 50 mV may indi-
cate a need to service the electrode.
Place electrode tip Allow for stabilization Press ENTER to accept
2
in second (different) second buffer calibration.
pH buffer. * ORP: +264 mV
Input: +260 mV
30 seconds*
pH 4.0 264 mV
pH 7.0 87 mV
To exit menus and return to Display returns to VIEW Good Easy Cal
VIEW press UP and DOWN Menu in 10 minutes or Press <ENTER>
button at the same time when ENTER is pressed

Options Menu for ORP


Display
Description
(Factory settings shown)
Contrast: Adjust the LCD contrast for best viewing. A setting of 1 is lower contrast, 5 is higher.
3 > Select lower contrast if the display is in warmer ambient surroundings.

Averaging: OFF provides the most instantaneous output response to changes in input value.
Off > LOW averaging = 4 seconds, HIGH averaging = 8 seconds of input signal.
Longer averaging produces more stable display and output response.

Output Active: Active HIGH: This setting is used to turn a device (pump, valve) ON at the setpoint.
Low > Active LOW: This setting is used to turn a device OFF at the setpoint.

Loop 1 Adjust:
Adjust the minimum and maximum current output. The display value represents the
4.00 mA > precise current output.
Adjustment limits:
• 3.80 mA < 4.00 mA > 5.00 mA
Loop 1 Adjust: • 19.00 mA < 20.00 mA > 21.00 ma
Use this setting to match the 8750 loop output to any external device.
20.00 mA >

Test Loop1:
Press UP or DOWN keys to manually order any output current value from 3.6 mA to
> 21.00 mA to test current loop output.

Test Output1:
Press UP or DOWN keys to manually toggle the state of the open collector output.
>

8750-1 pH/ORP Transmitter 9


Troubleshooting - pH

Display Condition Possible causes Suggested Solutions

During EasyCal: 1. Required 4, 7 or 10 buffers not being 1. Use pH 4, 7, 10 buffers


"Out of Range used. 2. Clean probe and retry EASY CAL.
Use Manual CAL" 2. Sensor is depleted too severely to 3. Use Manual calibration for Standard and
use EasyCal Slope if mV offset exceeds 50 mV.

During EasyCal: Sensor was not moved from buffer #1 to 1. Place sensor in correct buffer solution.
"Same Buffer" buffer #2. 2. Use fresh buffer.

During CALIBRATE Std: 1. pH Standard value within 2 pH units 1. Use pH values at least 2 pH units apart.
"Standard too close to of Slope value 2. Clean pH sensor; replace if necessary
Slope!" 2. pH Sensor efficiency is inadequate 3. Use fresh buffer.

During CALIBRATE Slope: 1. pH Slope value within 2 pH units of 1. Use pH values at least 2 pH units apart.
"Slope too close to Standard value 2. Clean pH sensor; replace if necessary
Standard!" 2. pH Sensor efficiency is inadequate 3. Use fresh buffer.

During CALIBRATE: 1. No temperature or mV signal from 1. Check all wiring, contacts in preamplifier.
"Out of Range sensor detected. 2. Verify sensor is securely installed.
Check Sensor" 2. No connection between pH sensor 3. Replace pH sensor.
and preamplifier.

During normal operation: mV input is less than 0 pH or greater than 1. Recalibrate system.
Constant "15.00 pH" 15 pH. 2. Replace pH sensor
or 3. Replace preamplifier.
constant "0.00 pH"
with good temp value

During normal operation: 1. No temperature or mV signal from 1. Check all wiring, contacts in preamplifier.
"Check Sensor?" sensor detected. 2. Verify sensor is securely installed.
2. No connection between pH sensor 3. Replace pH sensor.
and preamplifier.

The mV value from the sensor when placed in a 7 pH buffer represents the sensor offset. Signet recommends servicing/replacing the
sensor when the offset exceeds 50 mV.
The 3-2759 pH/ORP system tester allows simple system troubleshooting.

10 8750-1 pH/ORP Transmitter


Troubleshooting - ORP

Display Condition Possible causes Suggested Solutions

During EasyCal: 1. Required 4, 7 buffers with 1. Use pH 4, 7 buffers saturated with


"Out of Range quinhydrone not being used. quinhydrone.
Use Manual CAL" 2. Sensor is depleted too severely to 2. Clean probe and retry EASY CAL.
use EasyCal. 3. Use Manual calibration for Standard and
Slope if mV offset exceeds 50 mV.

During EasyCal: Sensor was not moved from buffer #1 to 1. Place sensor in correct buffer solution.
"Same Buffer" buffer #2. 2. Use fresh buffer.

During CALIBRATE Std: 1. ORP Standard value within 120 mV 1. Use ORP values at least 120 mV apart.
"Standard too close to of Slope value. 2. Clean ORP sensor; replace if necessary.
Slope!" 2. ORP Sensor efficiency is inadequate. 3. Use fresh buffer.

During CALIBRATE Slope: 1. ORP Slope value within 120 mV of 1. Use ORP values at least 120 mV apart.
"Slope too close to Standard value. 2. Clean ORP sensor; replace if necessary
Standard!" 2. ORP Sensor efficiency is inadequate. 3. Use fresh buffer.

1. No mV signal or sensor id from 1. Check all wiring, contacts in preamplifier.


During CALIBRATE: sensor detected. 2. Verify sensor is securely installed.
"Out of Range 2. No connection between ORP sensor 3. Replace ORP sensor.
Check Sensor" and preamplifier.

During normal operation: mV input is less than -999 or greater 1. Recalibrate system.
Constant "-1000" than +1999. 2. Replace ORP sensor.
or 3. Replace preamplifier.
constant ""+2000"

During normal operation: 1. No temperature or mV signal from 1. Check all wiring, contacts in preamplifier.
"Check Sensor?" sensor detected. 2. Verify sensor is securely installed.
2. No connection between ORP sensor 3. Replace ORP sensor.
and preamplifier.

8750-1 pH/ORP Transmitter 11


Ordering Information
Mfr. Part No. Code Description
3-8750-1 159 000 053 pH/ORP transmitter Field mount
3-8750-1P 159 000 054 pH/ORP transmitter Panel mount
3-8750-2 159 000 055 pH/ORP transmitter Field mount with relays
3-8750-2P 159 000 056 pH/ORP transmitter Panel mount with relays
3-8750-3 159 000 057 pH/ORP transmitter Field mount with single input/dual output
3-8750-3P 159 000 058 pH/ORP transmitter Panel mount with single input/dual output

Accessories
Mfr. Part No. Code Description
3-2714 198 844 300 Twist-Lock Flat pH electrode
3-2714-HF 198 844 305 Twist-Lock Flat pH hydrofluoric acid resistant electrode (<2%)
3-2716 198 844 302 Twist-Lock Bulb pH electrode
3-2716-DI 198 844 306 Twist-Lock Bulb pH electrode for process liquids (< I00 µs)
3-2715 198 844 301 Twist-Lock Flat ORP Electrode
3-2717 198 844 303 Twist-Lock Bulb ORP Electrode
3-2720 198 864 602 Twist-Lock Preamplifier, 1/4 in. NPT
3-2720-2 198 864 603 Twist-Lock Preamplifier, ISO 7/1-R 3/4
P31542 198 801 630 Red sensor cap for in-line installations
P31542-3 159 000 464 Blue sensor cap for in-line installations
3-2759 159 000 762 pH/ORP system tester (includes bypass adapter)
3-2759.393 159 000 765 2720 Adapter Cable
P31515-0P200 159 000 630 PVC Pipe Adapter
P31515-0C200 159 000 631 CPVC Pipe Adapter
P31515-0V200 159 000 459 PVDF Pipe Adapter
1220-0021 198 801 186 O-ring, FPM (standard)
1224-0021 198 820 006 O-ring, EPR
1228-0021 198 820 007 O-ring, Kalrez®
3-8050 159 000 184 Universal mounting kit
3-8050.395 159 000 186 Splashproof rear cover
3-8050.396 159 000 617 RC Filter kit (for relay use)
3-8052 159 000 188 3/4” Integral mounting kit
3-8052-1 159 000 755 3/4" NPT mount junction box
3-0000.596 159 000 641 Heavy duty wall mount bracket
3-0700.390 198 864 403 pH buffer kit
3-8050.392 159 000 640 Model 200 retrofit adapter
3-5000.598 198 840 225 Surface mount bracket
3-5000.399 198 840 224 5 x 5 inch adapter plate for +GF+ Signet retrofit
3-9000.392 159 000 368 Liquid-tight connector kit, 3 sets, 1/2 in. NPT
3-9000.392-1 159 000 839 Liquid-tight connector kit, 1 set, 1/2 in. NPT
3-9000.392-2 159 000 841 Liquid-tight connector kit, 1 set, PG 13.5
7300-7524 159 000 687 24 VDC Power Supply 7.5 Ω, 300mA
7300-1524 159 000 688 24 VDC Power Supply 15 Ω, 600mA
7300-3024 159 000 689 24 VDC Power Supply 30 Ω, 1.3 A
7300-5024 159 000 690 24 VDC Power Supply 50 Ω, 2.1 A
7300-1024 159 000 691 24 VDC Power Supply 100 Ω, 4.2 A
3-3719-11 159 000 804 pH/ORP Wet-Tap, 11/2 in. NPT
3-3719-21 159 000 805 pH/ORP Wet-Tap, 2 in. NPT
3-3719-12 159 000 806 pH/ORP Wet-Tap, ISO 7/1-R 1.5
3-3719-22 159 000 807 Wet-Tap Assembly, ISO 7/1-R 2
3-2716-WT 159 000 809 Twist-Lock pH Electrode (use with 3719 Wet-Tap)
3-2717-WT 159 000 811 Twist-Lock ORP Electrode (use with 3719 Wet-Tap)
2007-0225 159 000 812 PP Clamp-on Saddle, 2.5 in. x 11/2 in. (ASTM, NPT)
2007-0230 159 000 813 PP Clamp-on Saddle, 3 in. x 11/2 in. (ASTM, NPT
2007-0240 159 000 814 PP Clamp-on Saddle, 4 in. x 11/2 in. (ASTM, NPT)
2007-0260 159 000 815 PP Clamp-on Saddle, 6 in. x 2 in. (ASTM, NPT)
2007-0280 159 000 816 PP Clamp-on Saddle, 8 in. x 2 in. (ASTM, NPT)
2007-0210 159 000 817 PP Clamp-on Saddle, 10 in. x 2 in. (ASTM, NPT)
2007-0212 159 000 818 PP Clamp-on Saddle, 12 in. x 2 in. (ASTM, NPT)

George Fischer Signet, Inc., 3401 Aerojet Avenue, El Monte, CA 91731-2882 U.S.A. • Tel. (626) 571-2770 • Fax (626) 573-2057
For Worldwide Sales and Service, visit our website: www.gfsignet.com • Or call (in the U.S.): (800) 854-4090

3-8750.090-1 Rev. G 10/06 English © George Fischer Signet, Inc. 2001 Printed in U.S.A. on recycled paper
Signet 8750-2 pH/ORP Transmitter English

*3-8759.090-2*
3-8750.090-2 Rev. G 3/06 English

Contents
CAUTION! 1.Installation 10.20 pH
25.0 C
• Remove power to unit before wiring input and out-
2.Specifications Signet pH/ORP
put connections. Transmitter Relay 2
3.Electrical Connections Relay 1

• Follow instructions carefully to avoid personal injury.


4.Menu Functions ENTER

1. Installation
ProcessPro transmitters are available in two styles: panel mount and field mount. The panel mount is supplied with the necessary
hardware to install the transmitter. This manual includes complete panel mounting instructions.
Field mounting requires a separate mounting kit. The 3-8050 Universal kit enables the transmitter to be installed virtually
anywhere. Detailed instructions for field installation options are included with the 3-8050 Universal kit.

1.1 Panel Installation


1. The panel mount transmitter is designed for installation using a 1/4 DIN Punch. For manual panel cutout, an adhesive
template is provided as an installation guide. Recommended clearance on all sides between instruments is 1 inch.
2. Place gasket on instrument, and install in panel.
3. Slide mounting bracket over back of instrument until quick-clips snap into latches on side of instrument.
4. To remove, secure instrument temporarily with tape from front or grip from rear of instrument. DO NOT RELEASE.
Press quick-clips outward and remove.
panel
gasket
mounting
terminals bracket

Optional
96 mm 82 mm Rear 92 mm
(3.8 in.)
8050 (3.23 in.) (3.6 in.)
Cover
latch 7
sr Gnd
SenIELD)
(SH
sr IN
SenD)
- 6 (RE
Pwr Output sr V+
System
p-
4 Sen CK)
(BLA
2 Loo
Pwr
5
System
p+ +
1 Loo
Output
3

96 mm 42 mm 64 mm 56 mm
(3.8 in.) 41 mm (2.2 in.)
(1.7 in.) (2.5 in.) (1.6 in.)
97 mm
106 mm (4.2 in.) (3.8 in.)
FRONT VIEW
SIDE VIEW SIDE VIEW
Field Mount & Panel Mount
Panel Mount Field Mount Panel Mount Installation Detail quick-clips

2. Specifications
General Current output:
Compatible electrodes: Signet 2714-2717 Electrodes with 2720 • 4 to 20 mA, isolated, fully adjustable and reversible
pH/ORP Preamplifier, 2764-2767 and • Max loop impedance: 50 Ω max. @ 12 V
2774-2777 Electrodes with 2760-1,-2 325 Ω max. @ 18 V
pH/ORP Preamplifier 600 Ω max. @ 24 V
Accuracy: ±0.03 pH, ± 2 mV's ORP • Update rate: 0.5 seconds
Enclosure: • Accuracy: ±0.03 mA @ 25°C, 24 V
• Rating: NEMA 4X/IP65 front Relay outputs (2 sets mechanical SPDT contacts):
• Case: PBT • Maximum voltage rating: 5 A @ 30 VDC, or 5 A @ 250 VAC
• Panel case gasket: Neoprene resistive load
• Window: Polyurethane coated polycarbonate • Hi or Lo programmable with adjustable hysteresis
• Keypad: Sealed 4-key silicone rubber • Pulse programmable (maximum 400 pulses/minute)
• Weight: Approx. 325g (12 oz.)
Display: Environmental
• Alphanumeric 2 x 16 LCD • Operating temperature: -10 to 70°C (14 to 158°F)
• Contrast: User selected, 5 levels • Storage temperature: -15 to 80°C (5 to 176°F)
• Update rate: 1 second • Relative humidity: 0 to 95%, non-condensing
• Maximum altitude: 2000 m (6562 ft)
Electrical • Insulation category: II
Power: 12 to 24 VDC ±10%, regulated, 220 mA max. • Pollution degree: 2
Sensor input range:
• pH: 0.00 to 14.00 pH Standards and Approvals
• Temp. (pH only) 3K Balco, -25 to 120°C (-13 to 248°F) • CE, UL listed
• ORP: -1000 to +2000 mV, isolated • Immunity: EN50082-2
(10KΩ I.D. resistance T+, T-) • Emissions: EN55011 Class B
• Manufactured under ISO 9001 and ISO 14001
3. Electrical Connections
Caution: Failure to fully open terminal jaws before removing wire may permanently damage instrument.

Wiring Procedure
1. Remove 0.5 - 0.625 in. (13-16 mm) of insulation from wire end. 2
2. Press the orange terminal lever downward with a small screwdriver to open terminal jaws. 1
3. Insert exposed (non-insulated) wire end in terminal hole until it bottoms out.
4. Release orange terminal lever to secure wire in place. Gently pull on each wire to ensure a good connection.

Wiring Removal Procedure


1. Press the orange terminal lever downward with a small screwdriver to open terminal jaws.
2. When fully open, remove wire from terminal.

Wiring Tips:
• Do not route sensor cable in conduit containing AC power wiring. Electrical noise may interfere with sensor signal.
• Routing sensor cable in grounded metal conduit will help prevent electrical noise and mechanical damage.
• Seal cable entry points to prevent moisture damage.
• Only one wire should be inserted into a terminal. Splice double wires outside the terminal.

Terminals 5-10: Relay Outputs


Two sets mechanical SPDT contacts, Terminals 15-18: Sensor connections
programmable (see CALIBRATE menu) as: 15-16 are mV (pH or ORP) input from the electrode.
• High or Low with adjustable hysteresis 17-18 are temperature input from the pH electrode or
• proportional pulse based on pH or ORP 10KΩ identifying resistor from the ORP electrode.
• May be disabled (Off) if not used.

Terminals 3 and 4: Loop Power


12-24 VDC ±10% system power Temp -
and current loop output.
18 (WHITE)
Max. loop impedance: Temp +
50 Ω max. @ 12 V
17 (GREEN)
325 Ω max. @ 18 V Iso. GND
600 Ω max. @ 24 V 16 (BLUE)
Relay 2 mV Input
10 (NO) 15 (BROWN)
Relay 2
9 (COM)
System Pwr Relay 2 Earth
4 Loop - 8 (NC) 14 GND
System Pwr Relay 1 Sensr Gnd
3 Loop + 7 (NO) 13 (SHIELD)
AUX Relay 1 V-
2 Power - 6 (COM) 12 (BLACK)
AUX Relay 1 V+
1 Power + 5 (NC) 11 (RED)

Terminals 1 and 2: AUXILIARY power Terminals 11-14: Preamplifier power and grounds
Provides power for relay operation. 11-12 are DC voltages from the 8750 to power the
preamplifier.
13-14 are ground terminals for the sensor and for
earth ground

2 8750-2 pH/ORP Transmitter


3.1 Sensor Input Connections

White (Temp) Transmitter


Terminals 18
Green (Temp)
17 10.20 pH
25.0 C
Blue (ISO GND) Preamp: Preamp: Signet pH/ORP

16 Relay 1
Transmitter Relay 2

Brown (mV input) Signet 2720 Signet 2760-1


15
ENTER

* 14 Signet 2760-2
Silver (Shield)
13 ≤ 400 ft. (122 m)
12 Black (V-)
11 Red (V+)

* (connection of terminal 14 to Earth GND


may reduce electrical interference) Twist-Lock DryLoc
Electrodes Electrodes

3.2 System Power/Loop Connections

Stand-alone application, no current loop used


Transmitter
Terminals
System Pwr Loop - 44 Power
- Supply
System Pwr Loop + 33
+ 12-24 VDC
AUX Power - 22
AUX Power + 11

Connection to a PLC/Recorder, separate supply Connection to a PLC with built-in power supply

PLC or Recorder
Transmitter Transmitter PLC Terminals
Terminals
+ Loop Input Terminals
4-20 mA
- System Pwr Loop - 44 Loop Input
System Pwr Loop - 44 + 4-20 mA
33 System Pwr Loop + 33 -
System Pwr Loop +
22 Power AUX Power - 22 Power
AUX Power - - - Supply
Supply AUX Power + 11
AUX Power + 11
+ 12-24 VDC + 12-24 VDC
Internal
AUX power required for all 8750-2 systems PLC Connection

Example: Two transmitters connected to PLC/Recorder with separate power supply

PLC or Recorder

+ Channel 1
- 4-20 mA in

- Channel 2
Transmitter 1 Transmitter 2
4-20 mA in
Terminals + Terminals

System Pwr Loop - 4 44 System Pwr Loop -


System Pwr Loop + 3 33 System Pwr Loop +
AUX Power - 2 22 AUX Power -
AUX Power + 1 11 AUX Power +

Power
- Supply
+ 12-24 VDC

8750-2 pH/ORP Transmitter 3


3.3 Relay Output • Proportional Pulsing
The relay outputs can be programmed to respond when the pH/ The relay output will generate a 100 mS pulse at the rate defined
ORP value moves above or below a setpoint, or it can be used to by settings in the CALIBRATE menu (see page 6)
generate a pulse that is proportional to the pH/ORP value.
The relays can be disabled if not in use. In the example below:
• The output will be 0 pulses/min. at pH values less than 5.0.
• Low • The output will be 50 pulses/min. at 7.5 pH.
Relay triggers when the pH/ORP is less than the setpoint. • The output will be 100 pulses/min. at pH values above 10 pH.
The relay will relax when the pH/ORP moves above the setpoint
plus the hysteresis value.

• High
Relay triggers when the pH/ORPis greater than the setpoint.
The relay will relax when the pH/ORP drops below the setpoint 100 pulses

in. :
s/m te
lse Ra
plus the hysteresis value.

Pu ut
0 tp
10 Ou
Process

Pulse rate
to lay
Re
Hysteresis

0
Low Setpoint
0 pulses
Time
5 10
Relay energized Starting point endpoint
Relay relaxed
Process

High Setpoint

Hysteresis

Time

VIEW menu
• During normal operation, ProcessPro displays the VIEW menu.
• When using the CALIBRATE or OPTIONS menus, ProcessPro will return to the VIEW menu if no activity 10.20 pH
25.0 C
occurs for 10 minutes. Signet pH/ORP
• To select the item you want displayed, press the UP or DOWN arrow keys. The items will scroll in a continuous Relay 1
Transmitter Relay 2

loop. Changing the display selection does not interrupt system operations. ENTER

• No key code is necessary to change display selection.


• Output settings cannot be edited from the VIEW menu.

View Menu for pH


Display Description

7.00 pH Monitor the pH and the Temperature input from the sensor.
12.6 ºC This is the Permanent display.

All of the VIEW displays below are temporary. The permanent display will return after ten minutes.
Input: Monitor the millivolt input from the electrode. Use this display to determine the
307 mV relative condition of your electrode during periodic calibration.
(7 pH buffer = 0 mV, ±50 mV)

Loop Output: Monitor the 4-20 mA Loop output.


14.16 mA

Last CAL: Monitor date for scheduled maintenance or date of last calibration.
03-17-66 >

EASY Easy Cal is the fastest and simplest periodic calibration method. Requires
CAL: > 4 pH, 7 pH and 10 pH. (Any two)

4 8750-2 pH/ORP Transmitter


ProcessPro Editing Procedure:
Step 1. Press and hold ENTER key:
• 2 seconds to select the CALIBRATE menu
• 5 seconds to select the OPTIONS menu.
Step 2. The Key Code is UP-UP-UP-DOWN keys in sequence.
• After entering the Key Code, the display will show the first item in the selected menu.
Step 3. Scroll menu with UP or DOWN arrow keys.
Step 4. Press RIGHT ARROW key to select menu item to be edited.
• The first display element will begin flashing.
Step 5. Press UP or DOWN keys to edit the flashing element.
• RIGHT ARROW key advances the flashing element.
Step 6. Press ENTER key to save the new setting and return to Step 3.

Notes on Step 1: Notes on Step 2:


• The View Menu is normally displayed. If no key is pressed for 5 minutes while display is showing "Enter
• The CALIBRATE and OPTIONS menus require a KEY CODE. Key Code", the display will return to the VIEW menu.

CALIBRATE: ----
Press & Enter Key Code
hold for ENTER

access: CALIBRATE: *---


Enter Key Code
CALIBRATE: **--
VIEW Enter Key Code
2s 5s CALIBRATE: ***-
CALIBRATE Enter Key Code

OPTIONS Set: First item in CALI-


Temperature > BRATE menu

Notes on Steps 3 and 4:


• Refer to pages 6 and 7 for complete listing of menu items and their use.
• From the Step 3 display, pressing the UP and DOWN keys simultaneously will Set:
return the display to the VIEW menu. Temperature >
• If no key is pressed for 10 minutes, display will also return to the VIEW menu.
Step 3

Step 3: Finished Editing? Relay1 Setpnt:


Press the UP and DOWN keys simultaneously after 10.0 pH > Step 4
saving the last setting to return to normal operation.

Notes on Steps 5 and 6:


Relay1 Setpnt:
• All output functions remain active during editing. 10.00 pH
• Only the flashing element can be edited.
Relay1 Setpnt:
• RIGHT ARROW key advances the flashing element in a continuous loop. 00.00 pH Step 5
• Edited value is effective immediately after pressing ENTER key.
• If no key is pressed for 10 minutes unit will restore the last saved value and return to step 3.
• Step 6 (pressing ENTER key) always returns you to Step 3. Relay1 Setpnt:
00.00 pH
• Repeat steps 3-6 until all editing is completed.

Relay1 Setpnt:
9
0 .00 pH
Step 5: Made an Error?
ENTER

Press the UP and DOWN keys simultaneously Step 6


while any element is flashing. This will recall the Relay1 Setpnt:
Saving
last saved value of the item being edited and
return you to Step 3. Relay1 Setpnt:
9.00 pH >

8750-2 pH/ORP Transmitter 5


Calibrate Menu for pH
Display
Description
(Factory settings shown)
Set: Provides a maximum 25ºC offset to match temperature measurement to external reference.
Temperature >

Set: Applies a linear offset to the pH measurement. The ideal value is the average pH of your
application. (A sample of your application at process temperature is recommended.)
Standard >

Set: Applies a slope to the pH measurement. The slope value and the standard value must be
at least 2 pH units apart. The ideal values are the minimum and maximum values of your
Slope > process.

Loop Range: pH Select the minimum and maximum values for the 4-20 mA Current loop output.
0.00 › 14.00 >

Relay1 Source: Select pH or Temperature as the source for this relay.


pH >

Relay1 Mode: Select the mode of operation for this relay: High, Low or proportional Pulse.
The signal may be disabled if not in use.
Off >

Relay1 Setpnt: In Low or High Mode, the relay will be activated when the pH reaches this value.
4.00 pH >

Relay1 Hys: In Low or High mode, the relay will be deactivated at Setpoint ± Hysteresis, depending on
High or Low Setpoint selection. (See details on page 4.)
0.51 pH >

Relay1 Range: If Relay 1 is in PULSE mode, set the start and end point of the range and also set the
maximum pulse rate. (The maximum PULSE rate setting is 400 pulses per minute.)
4.00 → 8.00 >
The combined Relay1 Range and Relay1 Pulse rate settings shown here indicate:
Relay1 PlsRate: "Start pulsing when the pH value is 4 and increase the pulse rate up to the maximum of
120 pulses per minute when the pH value reaches 8"
120 Pulses/min >

Last CAL: Use this “note pad” to record important dates, such as annual recertification or scheduled
maintenance.
09-24-05 >

Settings repeat for Relay 2.

6 8750-2 pH/ORP Transmitter


EASY CAL Procedure - pH
• This procedure simplifies system calibration using standard 4.0, 7.0, 10.0 pH buffers only. If these pH buffers are not available,
calibrate the system via the CALIBRATE menu, using the STANDARD and SLOPE settings.
• Access the CALIBRATE menu and set sensor temperature before performing EASY CAL for new electrode installations.
• Access EASY CAL menu from the view menu.

EASY CAL: ---- Press UP, UP, UP, DOWN buttons in sequence to enter menu,
Enter Key Code ____
XXXX will appear during code entry.

To Calibrate: Response: To Accept:


Theoretical mV values
Place Sensor in * 6.90 pH * 6.90 pH
pH Buffer #1 -005 mV -005 mV pH @ 25°C mV
2 +296
Place electrode tip in Allow for stabilization ENTER to accept 3 +237
first pH buffer
pH 7.0 = 0 mV 1 4 +177
pH 4.0 = 177 * 7.00 pH 5 +118
pH 10 = -177 -005 mV
30 seconds* 6 +59
Limit ± 50 mV
7 +0
8 -59
9 -118
Place Sensor in * 3.93 pH * 3.93 pH
pH Buffer #2 +179 mV +179 mV 10 -177
11 -237
Place electrode tip Allow for stabilization Press ENTER to accept 12 -296
2
in second pH buffer. second buffer calibration.
* 4.00 pH
+179 mV
30 seconds*

To exit menus and return to Display returns to VIEW Good Easy Cal
VIEW press UP and DOWN Menu in 10 minutes or Press <ENTER>
button at the same time when ENTER is pressed

Options Menu for pH


Display
Description
(Factory settings shown)
Contrast: Adjust the LCD contrast for best viewing. A setting of 1 is lower contrast, 5 is higher.
Select lower contrast if the display is in warmer ambient surroundings.
3 >

Averaging: OFF provides the most instantaneous output response to changes in input value.
LOW averaging = 4 seconds, HIGH averaging = 8 seconds of input signal.
Off >

Temp Display: Select temperature units: ºC or ºF.


ºC >

Adjust the minimum and maximum current output. The display value represents the
Loop Adjust: precise current output.
4.00 mA Adjustment limits:
• 3.80 mA < 4.00 mA > 5.00 mA
• 19.00 mA < 20.00 mA > 21.00 ma
Loop Adjust: Use this setting to match the 8750 loop output to any external device.
20.00 mA >

Test Loop: Press UP or DOWN keys to manually order any output current value from 3.6 mA to
21.00 mA to test current loop output.
>

Test Relay 1: Press UP or DOWN keys to manually toggle the state of the relay output.
>

Test Relay 2: Press UP or DOWN keys to manually toggle the state of the relay output.

>

8750-2 pH/ORP Transmitter 7


Calibrate Menu for ORP
Display
Description
(Factory settings shown)
Set: Applies a linear offset to the ORP measurement. If you are using a single-point calibration,
use this function. The ideal value is the average pH of your application. (A sample of your
Standard > application at process temperature is recommended.)

Set: Applies a slope to the ORP measurement. This function should only be used in a two-point
calibration. The slope value and the standard value must be at least 2 pH units apart. The
Slope > ideal values are the minimum and maximum values of your application.

Loop Range: mV Select the minimum and maximum ORP values for the 4-20 mA Current loop output.
Maximum settings are -1000 mV to +2000 mV.
-1000 > +1000 >

Relay1 Mode: Select the mode of operation for this relay: High, Low or proportional Pulse.
The signal may also be disabled if not in use.
Off >

Relay1 Setpnt: In Low or High Mode, the relay will be activated when the ORP reaches this value.
-500 mV >

Relay1 Hys: In Low or High mode, the relay will be deactivated at Setpoint ± Hysteresis, depending on
High or Low Setpoint selection. (See details on page 4.)
10 mV >

Relay1 Range: mV
If Relay 1 is in PULSE mode, set the start and end point of the range and also set the
-500 → +500 > maximum pulse rate. (The maximum PULSE rate setting is 400 pulses per minute.)
Relay1 PlsRate: The combined Relay1 Range and Relay1 Pulse rate settings shown here indicate:
"Start pulsing when the ORP value is -500 and increase the pulse rate up to the maximum
120 pulses/min > of 120 pulses per minute when the ORP value reaches +500"

Last Cal: Use this “note pad” to record important dates, such as annual recertification or scheduled
maintenance.
09-24-05 >

8 8750-2 pH/ORP Transmitter


EASY CAL Procedure - ORP
• This procedure simplifies system calibration using standard 4.0 pH and 7.0 pH buffers saturated with Quinhydrone. To calibrate
using any other ORP buffer solutions, use the Standard and Slope functions in the CALIBRATE menu.
• Access EASY CAL menu from the view menu.

EASY CAL: ---- Press UP, UP, UP, DOWN buttons in sequence to enter menu,
Enter Key Code
will appear during code entry.
*
To Calibrate: Response: To Accept: For best results, gently stir the
submerged electrode for approximately 5
Place Sensor in * ORP: + 84 mV * ORP: + 84 mV seconds during the stabilization period.
ORP Buffer #1 Input: + 82 mV Input: + 82 mV
Large temperature differences from pro-
Place electrode tip Allow for stabilization ENTER to accept cess fluids to buffers may require longer
in first pH buffer; 1 stabilization time.
* ORP: + 87 mV
pH 7.0 Å 87 mV Input: + 82 mV Technical notes:
pH 4.0 Å 246 mV 30 seconds*
The difference between the actual mV and
value shown is a good indication of the
condition of the electrode.
Place Sensor in * ORP: +262 mV * ORP: +262 mV
ORP Buffer #2 Input: +260 mV Input: +260 mV Differences in excess of 50 mV may indi-
cate a need to service the electrode.
Place electrode tip Allow for stabilization Press ENTER to accept
2
in second (different) second buffer calibration.
pH buffer. * ORP: +264 mV
Input: +260 mV
30 seconds*
pH 4.0 Å 246 mV
pH 7.0 Å 87 mV
To exit menus and return to Display returns to VIEW Good Easy Cal
VIEW press UP and DOWN Menu in 10 minutes or Press <ENTER>
button at the same time when ENTER is pressed

Options Menu for ORP


Display
Description
(Factory settings shown)

Adjust the LCD contrast for best viewing. A setting of 1 is lower contrast, 5 is higher.
Contrast: Select lower contrast if the display is in warmer ambient surroundings.
3 >

OFF provides the most instantaneous output response to changes in input value.
Averaging: LOW averaging = 4 seconds, HIGH averaging produces more stable display and
Off > output response.

Loop Adjust: Adjust the minimum and maximum current output. The display value represents the
4.00 mA > precise current output.
Adjustment limits:
• 3.80 mA < 4.00 mA > 5.00 mA
Loop Adjust: • 19.00 mA < 20.00 mA > 21.00 ma
Use this setting to match the 8750 loop output to any external device.
20.00 mA >

Press UP or DOWN keys to manually order any output current value from 3.6 mA to
Test Loop: 21.00 mA to test current loop output.
>

Test Relay 1: Press UP or DOWN keys to manually toggle the state of the relay.

>

Press UP or DOWN keys to manually toggle the state of the relay.


Test Relay 2:
>
8750-2 pH/ORP Transmitter 9
Troubleshooting - pH

Display Condition Possible causes Suggested Solutions

During EasyCal: 1. Required 4, 7 or 10 buffers not being 1. Use pH 4, 7, 10 buffers.


"Out of Range used. 2. Clean probe and retry EASY CAL.
Use Manual CAL" 2. Sensor is depleted too severely to use 3. Use Manual calibration for Standard and
EasyCal. Slope if mV offset exceeds 50 mV.

During EasyCal: 1. Sensor was not moved from buffer #1 to 1. Place sensor in correct buffer solution.
"Same Buffer" buffer #2. 2. Use fresh buffer.
2. Buffer is contaminated

During CALIBRATE Std: 1. pH Standard value within 2 pH units of 1. Use pH values at least 2 pH units apart.
"Standard too close to Slope value. 2. Clean pH sensor; replace if necessary.
Slope!" 2. pH Sensor efficiency is inadequate. 3. Use fresh buffer.

During CALIBRATE Slope: 1. pH Slope value within 2 pH units of 1. Use pH values at least 2 pH units apart.
"Slope too close to Standard value. 2. Clean pH sensor; replace if necessary
Standard!" 2. pH Sensor efficiency is inadequate. 3. Use fresh buffer.

During CALIBRATE: 1. No temperature or mV signal from 1. Check all wiring, contacts in preamplifier.
"Out of Range sensor detected. 2. Verify sensor is securely installed.
Check Sensor" 2. No connection between pH sensor and 3. Replace electrode pH sensor.
preamplifier.

During normal operation: mV input is less than 0 pH or greater than 1. Recalibrate system.
Constant "15.00 pH" 15 pH. 2. Replace pH sensor.
or 3. Replace preamplifier.
constant "0.00 pH"
with good temp value

During normal operation: 1. No temperature or mV signal from 1. Check all wiring, contacts in preamplifier.
"Check Sensor?" sensor detected. 2. Verify sensor is securely installed.
2. No connection between pH sensor 3. Replace pH sensor.
and preamplifier.

The mV value from the sensor when placed in a 7 pH buffer represents the sensor offset. Signet recommends servicing/replacing the
sensor when the offset exceeds 50 mV.
The 3-2759 pH/ORP system tester allows simple system troubleshooting.

10 8750-2 pH/ORP Transmitter


Troubleshooting - ORP

Display Condition Possible causes Suggested Solutions

During EasyCal: 1. Required 4, 7 buffers with 1. Use pH 4, 7 buffers saturated with


"Out of Range quinhydrone not being used. quinhydrone.
Use Manual CAL" 2. Sensor is depleted too severely to 2. Clean probe and retry EASY CAL.
use EasyCal. 3. Use Manual calibration for Standard and
Slope if mV offset exceeds 50 mV.

During EasyCal: 1. Sensor was not moved from buffer #1 1. Place sensor in correct buffer solution.
"Same Buffer" to buffer #2. 2. Use fresh buffer.
2. Buffer is contaminated

During CALIBRATE Std: 1. ORP Standard value within 120 mV 1. Use ORP values at least 120 mV apart.
"Standard too close to of Slope value. 2. Clean ORP sensor; replace if necessary.
Slope!" 2. ORP Sensor efficiency is inadequate. 3. Use fresh buffer.

During CALIBRATE Slope: 1. ORP Slope value within 120 mV of 1. Use ORP values at least 120 mV apart.
"Slope too close to Standard value. 2. Clean ORP sensor; replace if necessary
Standard!" 2. ORP Sensor efficiency is inadequate. 3. Use fresh buffer.

1. No mV signal or sensor id from 1. Check all wiring, contacts in preamplifier.


During CALIBRATE: sensor detected. 2. Verify sensor is securely installed.
"Out of Range 2. No connection between ORP sensor 3. Replace ORP sensor.
Check Sensor" and preamplifier.

During normal operation: mV input is less than -999 or greater 1. Recalibrate system.
Constant "-1000" than +1999. 2. Replace pH sensor.
or 3. Replace preamplifier.
constant ""+2000"

During normal operation: 1. No temperature or mV signal from 1. Check all wiring, contacts in preamplifier.
"Check Sensor?" sensor detected. 2. Verify sensor is securely installed.
2. No connection between ORP sensor 3. Replace ORP sensor.
and preamplifier.

8750-2 pH/ORP Transmitter 11


Ordering Information
Mfr. Part No. Code Description
3-8750-1 159 000 053 pH/ORP transmitter Field mount
3-8750-1P 159 000 054 pH/ORP transmitter Panel mount
3-8750-2 159 000 055 pH/ORP transmitter Field mount with relays
3-8750-2P 159 000 056 pH/ORP transmitter Panel mount with relays
3-8750-3 159 000 057 pH/ORP transmitter Field mount with single input/dual output
3-8750-3P 159 000 058 pH/ORP transmitter Panel mount with single input/dual output

Accessories
Mfr. Part No. Code Description
3-2714 198 844 300 Twist-Lock Flat pH electrode
3-2714-HF 198 844 305 Twist-Lock Flat pH hydrofluoric acid resistant electrode (<2%)
3-2716 198 844 302 Twist-Lock Bulb pH electrode
3-2716-DI 198 844 306 Twist-Lock Bulb pH electrode for process liquids (< I00 µs)
3-2715 198 844 301 Twist-Lock Flat ORP Electrode
3-2717 198 844 303 Twist-Lock Bulb ORP Electrode
3-2720 198 864 602 Twist-Lock Preamplifier, 1/4 in. NPT
3-2720-2 198 864 603 Twist-Lock Preamplifier, ISO 7/1-R 3/4
P31542 198 801 630 Red sensor cap for in-line installations
P31542-3 159 000 464 Blue sensor cap for in-line installations
3-2759 159 000 762 pH/ORP system tester (includes bypass adapter)
3-2759.393 159 000 765 2720 Adapter Cable
P31515-0P200 159 000 630 PVC Pipe Adapter
P31515-0C200 159 000 631 CPVC Pipe Adapter
P31515-0V200 159 000 459 PVDF Pipe Adapter
1220-0021 198 801 186 O-ring, FPM (standard)
1224-0021 198 820 006 O-ring, EPR
1228-0021 198 820 007 O-ring, Kalrez®
3-8050 159 000 184 Universal mounting kit
3-8050.395 159 000 186 Splashproof rear cover
3-8050.396 159 000 617 RC Filter kit (for relay use)
3-8052 159 000 188 3/4” Integral mounting kit
3-8052-1 159 000 755 3/4" NPT mount junction box
3-0000.596 159 000 641 Heavy duty wall mount bracket
3-0700.390 198 864 403 pH buffer kit
3-8050.392 159 000 640 Model 200 retrofit adapter
3-5000.598 198 840 225 Surface mount bracket
3-5000.399 198 840 224 5 x 5 inch adapter plate for Signet retrofit
3-9000.392 159 000 368 Liquid-tight connector kit, 3 sets, 1/2 in. NPT
3-9000.392-1 159 000 839 Liquid-tight connector kit, 1 set, 1/2 in. NPT
3-9000.392-2 159 000 841 Liquid-tight connector kit, 1 set, PG 13.5
7300-7524 159 000 687 24 VDC Power Supply 7.5 Ω, 300mA
7300-1524 159 000 688 24 VDC Power Supply 15 Ω, 600mA
7300-3024 159 000 689 24 VDC Power Supply 30 Ω, 1.3 A
7300-5024 159 000 690 24 VDC Power Supply 50 Ω, 2.1 A
7300-1024 159 000 691 24 VDC Power Supply 100 Ω, 4.2 A
3-3719-11 159 000 804 pH/ORP Wet-Tap, 11/2 in. NPT
3-3719-21 159 000 805 pH/ORP Wet-Tap, 2 in. NPT
3-3719-12 159 000 806 pH/ORP Wet-Tap, ISO 7/1-R 1.5
3-3719-22 159 000 807 Wet-Tap Assembly, ISO 7/1-R 2
3-2716-WT 159 000 809 Twist-Lock pH Electrode (use with 3719 Wet-Tap)
3-2717-WT 159 000 811 Twist-Lock ORP Electrode (use with 3719 Wet-Tap)
2007-0225 159 000 812 PP Clamp-on Saddle, 2.5 in. x 11/2 in. (ASTM, NPT)
2007-0230 159 000 813 PP Clamp-on Saddle, 3 in. x 11/2 in. (ASTM, NPT
2007-0240 159 000 814 PP Clamp-on Saddle, 4 in. x 11/2 in. (ASTM, NPT)
2007-0260 159 000 815 PP Clamp-on Saddle, 6 in. x 2 in. (ASTM, NPT)
2007-0280 159 000 816 PP Clamp-on Saddle, 8 in. x 2 in. (ASTM, NPT)
2007-0210 159 000 817 PP Clamp-on Saddle, 10 in. x 2 in. (ASTM, NPT)
2007-0212 159 000 818 PP Clamp-on Saddle, 12 in. x 2 in. (ASTM, NPT)

George Fischer Signet Inc., 3401 Aerojet Avenue, El Monte, CA 91731-2882 U.S.A. • Tel. (626) 571-2770 • Fax (626) 573-2057
For Worldwide Sales and Service, visit our website: www.gfsignet.com • Or call (in the U.S.): (800) 854-4090

3-8750.090-2 Rev. G 3/06 English © George Fischer Signet Inc. 2001 Printed in U.S.A. on recycled paper
ENGLISH
‡ SIGNET 2714-2717 Twist-Lock pH and ORP Electrodes

3-2714.090-1 G-1/02 English


SAFETY INSTRUCTIONS
1. Depressurize and vent system prior to installation or removal.
2. Confirm chemical compatibility before use.
3. Do not exceed maximum temperature/pressure specifications.
4. Wear safety goggles or faceshield during installation/service.
5. Do not alter product construction.
6. When using chemicals or solvents care should be taken and appropriate eye, face, hand, body,
and/or respiratory protection should be used.

1. Technical Data BAR PSI


1.1 General 7 100
Compatibility: +GF+ SIGNET 2720 Twist-Lock Preamplifier

Pipe Size Range: 5 75

2714-HF
2714
• 1/2 in. and up.
• Use +GF+ SIGNET installation fittings to 4 in.
3 50
• Use pipe adapter in pipes over 4 in.
• Submersion with 2720 pre-amplifier requires 3/4 in. NPT or
ISO 7-R 3/4 in. male threaded extensions 2 25
Efficiency: >97% @ 25°C (77° F) 0 10 25 50 75 °C
Wetted Materials: CPVC Body
Glass 32 50 77 122 167 °F
FPM O-rings
Porous UHMW Polyethylene reference 1.4 Temperature and pressure specifications
junctions ORP electrode operating Temperature/Pressure
ORP: Platinum sensing surface • 6.89 bar @ 0°C to 65ºC (100 psi @ 32° to 149° F)
• 4.00 bar @ 66ºC to 85°C (58 psi @150° to 185°F)
Primary Functions: 2714, 2715: Flat surface resists fouling
2716, 2717: Bulb surface for general use 2716 and 2716-DI pH electrode operating Temperature/Pressure
2714-HF: Extended use in applications • 6.89 bar @ 0°C to 65ºC (100 psi @ 32° to 149° F)
with trace hydrofluoric acid (<2%) • 4.00 bar @ 66ºC to 85°C (58 psi @150° to 185°F)
2716-DI: Extended use in pure waters
(<100 µS) 2714 pH electrode operating Temperature/Pressure
• 6.89 bar @ 10°C to 65ºC (100 psi @ 50° to 149° F)
Secondary Junction: Nylon Filament • 4.00 bar @ 66ºC to 85°C (58 psi @150° to 185°F)
Element: Ag/AgCl
Shipping Weight: 0.2 kg (0.4 lb) 2714-HF pH electrode operating Temperature/Pressure
• 6.89 bar @ 0°C to 50ºC (100 psi @ 32° to 122° F)
1.2 2714 and 2716 pH Electrodes
Operating Range: 0 to 14 pH (2714-HF: 0 to 12 pH) Storage Temperature: > -12° C (11° F)
Reference: Electrolyte: Solidified Acrylamide Gel
3.5M KCI (2714, 2714-HF, 2716) 1.5 Dimensions
1.0 in. 1.0 in.
0.1 M KCl (2716-DI) (27 mm) (27 mm)
Temperature Sensor: 3KΩ Balco (3000Ω = 25°C)
ResponseTime: <5 s for 95% of signal change
Response Time, τ: 140 s (2714), 196 s (2716)
1.2 in. 1.2 in.
1.3 2715/2717 ORP Electrodes (30.5 mm) (30.5 mm)
Operating Range: -999 to +999 mV
Reference: Electrolyte: Solidified Acrlyamide Gel 3.8 in. 4.1 in.
(97 mm) (104 mm)
3.5M KCL
Response Time: Application dependent
2.6 in. 2.6 in.
(65 mm) (65 mm)
3.4 in. 3.4 in.
(86 mm) (86 mm)

0.9 in.
(23 mm) 0.9 in.
(23 mm)

Flat electrode Bulb electrode


‡ SIGNET 2714-2717 Twist-Lock pH and ORP Electrodes page 1 of 4
2. Electrode care and application
pH/ORP electrodes are similar to batteries; they age with time and usage. The following information will help maximize electrode life.

2.1 Conditions to Avoid:


• High temperatures, strong acids or caustics will elevate electrochemical reactions and speed electrode aging.
• Coatings on the glass or junction surfaces (i.e. proteins) cause extended response time and inaccurate measurement.
• Never store the electrode tip in deionized (DI) water.
• Never expose electrode to temperatures below -12 °C (10 °F) or allow it to dehydrate. These conditions will damage the electrode.
• Never scrape or sand the glass electrode surface.
• Treat glass electrode surfaces with care. The glass is very thin and requires care to prevent accidental breakage.

2.2 Submersible Installation Tips:


• Mount electrodes in a location with ample clearance for removal for YES
YES
periodic cleaning and recalibration. Choose a location that keeps the
electrode glass completely submerged at all times.
• Place the electrode tip in pH 4 buffer during system maintenance or
storage to avoid dehydration.
• Mount the electrode near tank outlet away from reagent addition areas.
30° 30°
2.3 In-Line Installation Tips: NO NO
• pH and ORP electrodes respond best in moving fluids.
• The internal measuring electrode chamber contains a wire within a liquid
and a slight amount of air. The electrode must be mounted at least 30°
from horizontal to ensure proper sensing. Mounting angles less than 30°
NO
will impede performance.

3. pH Electrode Calibration
All pH electrodes are designed to ensure linearity during their lifespan. The following
Theoretical mV Values @ 25°C
sections define proper electrode operation.
pH mV
2 + 295 mV
3.1 Offset (STD) 3 + 236 mV
Electrode offsets occur due to: 4 +177 mV
• Clogged reference junction 5 +118 mV
• Aged or contaminated reference solution/wire 6 + 59 mV
7 0 mV
Check offsets in a pH 7 buffer @ 25 °C. The theoretical output is 0 mV. Any deviation from 8 - 59 mV
9 - 118 mV
0 mV is the pH electrode offset.
10 - 177 mV
11 - 236 mV
pH Electrode Offset pH 7 buffer @ 25°C Theoretical: 7.0 pH (0.0 mV) 12 - 295 mV
New: pH 7 ± 0.25 pH (±15 mV)
Reliable: pH 7 ± 0.85 pH (± 50 mV)
Electrode offsets greater than 0.85 pH (50 mV) indicate the electrode requires cleaning or replacement. See section 5: Maintenance and
cleaning.
°C pH Error
3.2 Slope (SLP)
2 3 4 5 6 7 8 9 10 11 12
Electrode slope is the number of mV per pH unit. At 25°C the
theoretical slope is 59.16 mV per pH. Temperature has an 15 0.15 0.12 0.09 0.06 0.03 0 0.03 0.06 0.09 0.12 0.15
appreciable affect on electrode slope. Reliable instrumentation 25 0 0 0 0 0 0 0 0 0 0 0
includes temperature compensation. The graph below illustrates 35 0.15 0.12 0.09 0.06 0.03 0 0.03 0.06 0.09 0.12 0.15
potential pH error when a temperature compensated instrument
45 0.3 0.24 0.18 0.12 0.06 0 0.06 0.12 0.18 0.24 0.3
is not used.
55 0.45 0.36 0.27 0.18 0.09 0 0.09 0.18 0.27 0.36 0.45
Recommendations:
• Calibrate temperature before calibrating the standard and slope.
• The mV offset will track across the entire pH range. The slope is usually not affected by offset changes.
(i.e. pH 7= +10 mV, pH 4= +187 mV); slope = 59 mV
• Coatings on the glass may affect sensor slopes. See section 5 maintenance and cleaning.
• A constant output near 0 mV in all buffer solutions indicates a shorted electrode that must be replaced.

3.3 Response Time/Stability


Response time and stability are affected by the condition of the pH electrode's glass surface (ORP electrode - Platinum surface),
reference junction, and reference solution. Restoration to acceptable levels can often be accomplished by cleaning the electrode's glass
surface (ORP electrode - Platinum surface) and reference junction.

Electrode mV values should remain stable ±3 mV. Conditions that may cause fluctuations are:
1. Electrode coating
2. Ground fault: If proper operation is observed in the beaker, but is unstable in the application, a ground fault probably exists.
• Using instrumentation with isolated inputs and outputs may restore stable operation.
• Solution grounding may also restore stable operation.
page 2 of 4 ‡ SIGNET 2714-2717 Twist Lock pH and ORP Electrodes
4. ORP Electrode Calibration
All ORP electrodes are designed to ensure linearity during their lifespan. The following sections define proper electrode operation.

4.1 Offset (STD)


Electrode offsets occur due to:
• Clogged reference junction
• Aged or contaminated reference solution/wire

Offsets are easily checked in pH 7 buffer saturated with quinhydrone @ 25 °C; since the theoretical output is +87 mV. Any deviation
from +87 mV is the ORP electrode offset (i.e. +90 mV). Quinhydrone is the oxidizer measured by the ORP electrode and is required for
calibration. To guarantee buffer saturation, mix 1/8g quinhydrone per 50 mL of pH buffer.

ORP Electrode Offset:


Solution: pH 7 or pH 4 buffer saturated with Quinhydrone @ 25 °C

pH 7 + Quinhydrone pH 4 + Quinhydrone
Theoretical mV: + 87 mV + 264 mV
New: 87 ± 15 mV +264 ± 15 mV
Reliable: 87 ± 50 mV +264 ± 50 mV

Electrode offsets greater than ±50 mV indicate the electrode requires cleaning or replacement, see section 5.2.

4.2 Slope (SLP)


ORP slope errors are generally caused by contamination of the platinum electrode surface. Cleaning the electrode surface will usually
restore proper values, response time, and stability.

Common ORP Values


Reaction mV

Cr → Cr2+ + 2e- - 913


Fe → Fe2+ + 2e- - 440
Cr2+ →Cr3+ + e- - 407
4OH- → O2 + 2H2O + 4e - 401
2I- → I2 + 2e- - 400
Ti2+ → Ti3+ + e- - 370
Ni → Ni2+ + 2e- - 250
Pb → Pb2+ + 2e- - 126
Fe → Fe3+ + 3e- - 37
H2 → 2H+ + 2e- 0
Fe2+ → Fe3+ + e- + 771
Ag → Ag+ + e- + 799
Pb → Pb4+ + 4e- + 800
3Br- → Br3- + e- + 1060
2Br- → Br2 + 2e- + 1066
ClO2- → ClO2 + e- + 1160
Pt → Pt2+ + 2e- + 1188
Ag → Ag2+ + 2e- + 1369

Many systems require both pH and ORP calibration. To conserve calibration reference solutions, use pH 7 and 4 buffers for pH
calibration first. ORP calibration can be performed with the same buffers by adding quinhydrone.

5. Maintenance and Cleaning


5.1 Maintenance

Variables can affect long term pH or ORP electrode life. For this reason, a maintenance log is recommended for trend analysis. When
storing boxed sensors, lay the sensor flat to maximize hydration of the glass surface. Keep the glass surface wet at all times. Soak the
sensor tip in pH 4.0 buffer during system maintenance intervals. In-line applications should be plumbed with a depression (trap) so liquid
is maintained around the sensor tip. If the sensor dehydrates, soak the sensor tip in pH 4 buffer for 24 to 48 hours, then visually inspect
the electrode for surface cracks, swelling, or discoloration. Severely dehydrated electrodes cannot be restored to normal operation.

‡ SIGNET 2714-2717 Twist-Lock pH and ORP Electrodes page 3 of 4


5.2 Cleaning
Cleaning techniques vary depending on the type of coating present on the glass electrode surface or reference junction.
• Soft coatings can be removed by vigorous stirring, or with directed spray of an applicable detergent or solvent onto the glass
electrode surface. Chlorine bleach or mild detergent may be used to remove soft coatings. Always rinse electrode tip in clean water
after cleaning.
• Hard coatings can be chemically removed. Use the least harsh chemical which will remove the contaminant within two (2) minutes
without attacking the materials of construction. e.g. calcium carbonate may be removed with a 5% HCL (muriatic acid) solution.
• Oily or organic coatings can be removed with detergents or an appropriate solvent that does not attack the materials of
construction e.g. isopropyl alcohol may be used but acetone must be avoided to prevent damage to the CPVC sensor body.
• ORP electrode surface (platinum rod) can be gently sanded with 600 grit wet and dry silicone or carbide sandpaper, jewelers rouge,
crocus cloth, or very fine steel wool.

WARNING!
Wear appropriate eye, face, hand, body, and respiratory protection when using chemicals or solvents.

6. Replacement parts and accessories 3-2759 pH/ORP


Simulator/System Tester
Mfr. Part No. Code Description
3-2714 198 844 300 Flat pH Electrode
3-2714-HF 198 844 305 Flat pH Electrode, HF Resistsant
3-2715 198 844 301 Flat ORP Electrode
3-2716 198 844 302 Bulb pH Electrode
3-2716-DI 198 844 306 Bulb pH Electrode, DI Resistant
3-2717 198 844 303 Bulb ORP Electrode
3-2759 159 000 762 pH/ORP Simulator/System Tester
3-2759.393 159 000 765 Adapter Cable for use with 2720
3-2720 198 864 602 Preamplifier, 3/4 in. NPT ORP

3-2720-2 198 864 603 Preamplifier, ISO 7-R 3/4 in. pH

P31515-0P200 159 000 630 PVC Pipe Adapter


P31515-0C200 159 000 631 CPVC Pipe Adapter
P31515-0V200 159 000 459 PVDF Pipe Adapter
3-0700.390 198 864 403 pH Buffer Kit
1220-0021 198 801 186 O-ring, FPM (standard)
1224-0021 198 820 006 O-ring, EPR
1228-0021 198 820 007 O-ring, Kalrez

a b
o c
n
CAUTION!
m d
Apply O-ring lubricant to sensor O-rings prior to assembly.
Unlubricated O-rings may score the sealing surface in the 2720.
c
Technical Features
l
a) Male BNC connector i) 3K Balco thermistor
b) Keyed for a simple sure fit j) Solidified acrylamide reference k
c) Viton® O-rings electrolyte j
d) Silicone-bushing seal k) Ag/AgCl measuring element
e) Double junction l) Large reference volume i e
f) Ag/AgCl reference element m) Epoxy seal f
g) Platinum sensing surface (ORP) or flat pH glass n) Shielding h g
h) Porous UHMW polyethylene reference junction o) 10KΩ I.D. resistor for ORP sensor

‡ SIGNET
Signet Scientific Company, 3401 Aerojet Avenue, El Monte, CA 91731-2882 U.S.A. • Tel. (626) 571-2770 • Fax (626) 573-2057
For Worldwide Sales and Service, visit our website: www.gfsignet.com • Or call (in the U.S.): (800) 854-4090

GEORGE FISCHER ‡ Piping Systems


3-2714.090-1/(G-1/02) English © Signet Scientific Company 2001 Printed in U.S.A. on recycled paper

page 4 of 4 ‡ SIGNET 2714-2717 Twist Lock pH and ORP Electrodes


Signet 2720 Twist-Lock pH/ORP Preamplifier English
*3-2720.090-1*
3-2720.090-1 D 8/04 English

SAFETY INSTRUCTIONS FOR IN-LINE ELECTRODE INSTALLATION


1. Do not remove from pressurized lines.
2. Do not exceed maximum temperature/pressure specifications.
3. Wear safety goggles or face shield during installation/service.
4. Do not alter product construction.
Failure to follow safety instructions may result in severe personal injury!

1. Wiring
Preamplifier: Preamplifier:
Silver (earth ground) Silver (earth ground)

Brown Brown
(mV Input) (mV Input)
Blue 6 7 8 Blue
(Iso. Gnd) ALARM 1

2
4
pH
10

12
ALARM 2

(Iso. Gnd)
Green Black
(T+) 0 14
(V-)
White Red Signet
(T-) (V+)
Green 8710
Red ENTER

(T+)
(V+)
Black White
(V-) Signet (T-)
pH ORP 5700 pH ORP
Electrodes: Electrodes: Electrodes: Electrodes:
2714 2715 2714 2715 ENTER

2714-HF 2717 2714-HF 2717


2716 2716 Signet
2716-DI 2716-DI 8750

Preamplifier: Preamplifier:
Silver (earth ground) Silver (earth ground)
Red Red
(#10) V+ (#10) V+
Black pH CONTROLLER Black ORP CONTROLLER

(#11) V- RLY 1 (#11) V- RLY 1


RLY 2

Green
RLY 2
RLY 3
Green RLY 3
RLY 4

(#12) T+ RLY 4
N/C
Brown ENTER MOD
pH mV
White ENTER MOD
ORP mV

(#13) Ain CAL RELAY OUTPUT


TEMP
N/C CAL RELAY OUTPUT

White Brown
(#14) ISO (#13) Ain
Blue Blue
(#14) ISO Signet (#14) ISO Signet
pH 9030 ORP 9040
• Use X1 gain selection • Use X1 gain selection
Electrodes: Electrodes:
2714 2715
2714-HF 2717
2716
2716-DI

Technical Notes:
• Use 6-conductor shielded cable for cable extensions to 120 m (400 ft)
• Shield must be maintained through cable splice

2. Signet Fittings

Type Description Type Description


Plastic tees • 0.5 to 4 in. Carbon steel • 2 to 4 in, use 1-7/16 in. hole in pipe
• PVC or CPVC weld-on • Remove insert before welding
• Mounts via glue-on fittings weldolets • Installed by certified welder only

• 2 to 4 in., use 1-7/16 in. hole in pipe Carbon steel • 0.5 to 2 in.
PVC saddles
• Align wedge arrows with saddle threaded tees • Mounts on threaded pipe ends
arrows during assembly.

Iron • 2 to 4 in., use 1-7/16 in. hole in pipe Universal • For existing pipe fittings 2 in. and up
strap-on pipe adapter • External 1-1/4 inch NPT male threads
saddles for large pipes,
#P31515-OV200

Consult your local Signet distributor for additional fitting information.


3. Recommended Position
Customer supplied:
• 3/4 in. NPT threaded
Customer supplied:
3/4 in. NPT OR C. pipe (A)
• 3/4 in. NPT nipple (male)
ISO 7/1-Rc 3/4 • J-box (B) B.
• J-box
female threads B. • Flex conduit (C)
• flex conduit
• Quick release pipe
C.
D. clamp (D)
• Tank flange (E)
A. A.

0 E.

+60 2 in.
-60 min.
In-Line

Process
pipe Open Closed
tanks tanks

• Vertical (0 ) position optimum Caution: If liquid level is not constant, always ensure
• 3m/s (10ft/s) or less for max. performance and sensor life liquid contact with electrode tip

4. Installation
In-line Applications Submersible Applications

1 2 1 2

Sealant
Preamplifier Preamplifier Customer
supplied
pipe
3/4 in. NPT or
ISO 7/1-Rc 3/4
A. O-ring lubricant A. O-ring lubricant
recommended C. B. Align recommended C. B. Align Sealant
Hand
(factory applied) marks tighten (factory applied) marks
only!

#P31542 Sensor Cap


Fitting
(purchased separately)
inlet
3

Fill with
3 to 4 in.
of sealant

Attach 3/4 in. watertight pipe to the top of the 2720. Secure the threaded connection to prevent any leakage. For additional defense against possible accu-
mulation of condensation at the back seal area of the sensor, fill the lower 3 to 4 inches of conduit or extension pipe with a flexible sealant such as silicone.

2 Signet 2720 Twist-Lock pH/ORP Preamplifier


5. Accessories

Part no. Description Material Code

P31542 Sensor PP 198 801 630


cap

CAUTION!
1220-0021 Sensor O-ring, FPM 198 801 186
1224-0021 When replacing O-rings, apply O-ring lubricant to sensor O-
2 required EPR 198 820 006
1228-0021 FFKM 198 820 007 rings prior to preamplifier/electrode assembly. Unlubricated
O-rings may score the preamplifier sealing surface.

6. Specifications
Signet 2720 Twist-Lock pH/ORP Preamplifier Signet pH/ORP Electrodes
Housing material: CPVC
Compatible sensors: 2714 Flat Surface pH Electrode General Specifications
2714-HF Flat Surface pH Electrode Wetted parts:
2715 Flat Surface ORP Electrode Sensor body: CPVC
2716 Bulb pH Electrode O-rings: FPM
2716-DI Bulb pH Electrode Electrode junction: Porous UHMW polyethylene
2717 Bulb ORP Electrode Quality standard: CE
Input Impedance: >1011 Ω
Operating temp.: 0 to 80°C Maximum pressure/temperature ratings:
Gain: X1 (unity) • 7 bar (100 psi) max. @ 65°C (149°F)
Input power: ±4.5 to ±8 VDC, dual supply • 4 bar (58 psi) max. @ 85°C (185°F)
Current consumption: <1 mA, dual supply
Quality standard: CE BARPSI

7 100

5 75
Dimensions:
3 50
3/4 in. NPT OR 2 25
ISO 7/1-Rc 3/4
Std.15 ft/ female threads F° 77 122 167 212
4.6 m cable C° 25 50 75 100

SAFETY INSTRUCTIONS FOR IN-LINE


3.6 in./ ELECTRODE INSTALLATION
91 mm 1. Do not remove from pressurized lines.
2. Do not exceed maximum temperature/pres-
sure specifications.
3. Do not install/service without following installa-
tion instructions (see sensor manual).
4. Wear safety goggles and faceshield during
1.8 in./
46 mm installation/service.
5. Do not alter product construction.
6. Failure to follow safety instructions could result
in severe personal injury!

7. Preamplifier Troubleshooting
Procedure: Simulator Actual displayed
A. Install sensor adapter into preamplifier Input mV
4.00, +177 mV ________________________
B. With preamplifier and instrument connected, simulate pH 4, 7, and 10 7.00, 0 mV ________________________
and record displayed mV readings (right) and approximate preamplifier 10.00, -177 mV ________________________
response time between simulations. Preamplfier response time: ________________________
C. Refer to table on next page for preamplifier troubleshooting tips.

Signet 2720 Twist-Lock pH/ORP Preamplifier 3


With simulator Error Condition Possible Cause Possible Remedy
connected
A) mV output stuck A) Shorted input signal A) Check preamplifier cable connections and shielding.
at zero B) Faulty preamplifier or wiring B) Verify preamplifier shield connections. Verify cable
B) mV output eratic C) Faulty preamplifier shield wire has been maintained through each cable
C) mV output stuck splice.
at 1.4 VDC C) Replace preamplifier

Okay with A) mV output stuck A) Cracked electrode glass


simulator near zero B1) Poor contact between A) Replace electrode
connected B) mV output eratic electrode and preamplifier B1) Check contacts between electrode and preamplifier
but fails with C) Output stuck at connectors Contacts must be clean and dry.
electrode 1.4 VDC B2) Fouled electrode reference B2) Clean electrode, see electrode manual
or aged electrode B3) Isolate electrode in test beaker. If output is stable,
B3) Ground loop ground loops may exist causing erratic behavior; isolate
C) Faulty preamplifier instrument outputs (i.e. 4 to 20 mA, 0 to 5 VDC).

8. Electrode Maintenance and Cleaning


8.1 Maintenance
Variables can affect long term pH or ORP electrode life. For this • Hard coatings: can be chemically removed. Always use the
reason, a maintenance log is recommended for trend analysis. least harsh chemical which will remove the contaminant within
When storing boxed sensors, lay the sensor flat to maximize two (2) minutes without attacking the materials of construction.
hydration of the glass surface. Keep the glass surface wet at all e.g. calcium carbonate may be removed with a 5% HCL (muri
times. Soak the sensor tip in pH 4.0 buffer during system main- atic acid) solution.
tenance intervals. In-line applications should be plumbed with a
depression (trap) which ensures liquid is maintained around the • Oily or Organic Coatings: can be removed with detergents or
sensor tip. If sensor dehydration has occurred, soak the sensor tip an appropriate solvent that does not attack the materials of
in pH 4 buffer for 24 to 48 hours, then visually inspect the elec- construction e.g. isopropyl alcohol may be used but acetone
trode for surface cracks, swelling, or discoloration. must be avoided to prevent damage to the CPVC sensor body.

• ORP electrode surface (platinum rod): can be gently sanded


8.2 Cleaning with 600 grit wet and dry silicone or carbide sandpaper, jewel
Cleaning techniques vary depending on the type of coating pres- ers rouge, crocus cloth, or very fine steel wool.
ent on the glass electrode surface or reference junction.

• Soft coatings: can be removed by vigorous stirring, or with


directed spray of an applicable detergent or solvent onto the WARNING!
glass electrode surface. Chlorine bleach or mild detergent When using chemicals or solvents care should be taken
may be used to remove soft coatings. Always rinse electrode and appropriate eye, face, hand, body, and/or respiratory
tip in clean water after cleaning. protection should be used.

9. Replacement parts and accessories 3-2759 pH/ORP


Simulator/System Tester
Mfr. Part No. Code Description
3-2720 198 864 602 Preamplifier, 3/4 in. NPT
3-2720-2 198 864 603 Preamplifier, ISO 7-R 3/4 in.
3-2714 198 844 300 Flat pH Electrode
3-2714-HF 198 844 305 Flat pH Electrode, HF Resistsant
3-2715 198 844 301 Flat ORP Electrode
3-2716 198 844 302 Bulb pH Electrode
3-2716-DI 198 844 306 Bulb pH Electrode, DI Resistant
3-2717 198 844 303 Bulb ORP Electrode
3-2759 159 000 762 pH/ORP Simulator/System Tester ORP

3-2759.393 159 000 765 Adapter Cable for use with 2720
3-0700.390 198 864 403 pH Buffer Kit pH

Signet
MODEL 2759
pH/ORP SIMULATOR

George Fischer Signet, Inc. 3401 Aerojet Avenue, El Monte, CA 91731-2882 U.S.A. • Tel. (626) 571-2770 • Fax (626) 573-2057
For Worldwide Sales and Service, visit our website: www.gfsignet.com • Or call (in the U.S.): (800) 854-4090

3-2720.090-1 D 8/04 English © George Fischer Signet, Inc. 2002 Printed in U.S.A. on recycled paper
Dwg. No. 101023 450 PSI
Rev. B/0 MEGA-SIDE PORT
ENGINEERING DRAWING PACKET
MODEL PRO-8-450-MSP

DESIGN PRESSURE at 120ºF 450 PSI OPERATING pH RANGE 3-11


MINIMUM OPERATING TEMP.* 20ºF CLEANING pH RANGE 2-12
(less than 30 minutes)
MAXIMUM OPERATING TEMP. 120ºF
APPLICATION TYP. BRACKISH WATERS
FACTORY TEST PRESSURE 495 PSI
FEEDWATER TDS <= 10,000 ppm Max.
BURST PRESSURE 2700 PSI
INTENDED USE
The PROTEC Model PRO-8-450-MSP Pressure Vessel is The filament-wound reinforced plastic shell of this vessel must
designed for continuous use as a housing for membrane filtration be allowed to expand under pressure. Any undue restraint at the
elements to purify typical brackish waters at any positive support points or piping connections can cause non-repairable
pressure up to 450 PSI. The PRO-8-450-MSP will leaks to develop in the shell. This vessel must not be subjected
accommodate any make of eight-inch nominal diameter spiral- to excessive stress caused by bending moments acting at the
wound element as well as many hollow fiber elements. The side ports in the fiberglass shell.
element interface hardware for the specified element is supplied
The end closures of the vessel must be kept dry and free of
with the vessel.
corrosion at all times. Failure to do so may result in deterioration
The Model PRO-8-450-MSP has been designed to meet the that can lead to catastrophic failure of the vessel heads.
standards of the American Society of Mechanical Engineers
(ASME), Boiler and Pressure Vessel Code, Section X. At an When requested, Bekaert Progressive Composites will assist the
purchaser in determining the suitability of this standard vessel
additional cost, vessels can be inspected during fabrication by an
design for their operating environment. However, the final
ASME Authorized Inspector and Code stamped.
determination including the evaluation of the materials of
The Model PRO-8-450-MSP must be installed, operated and construction for use in the specific corrosive environment shall
maintained using good industrial practice and following the be the responsibility of the purchaser. Alternate materials of
precautions listed in order to help assure safe operation and a construction may be available on special order.
long service life. Misuse, improper installation or operation may
Before using this engineering packet for system design or vessel
result in severe bodily harm or property damage and will void the installation, please verify that it is the latest revision by consulting
vessel warranty. Therefore, review and follow the safeguards the factory. Specifications are subject to change without notice.
listed below before placing the vessels into service.
PRECAUTIONS
Follow all instructions. Never support other components with the vessel.
Failure to take every precaution listed will void the vessel Hanging piping manifolds or supporting other components with
warranty and may result in vessel failure. the vessel may result in vessel damage.
Mount shell using furnished hardware. Do not over tighten the Permeate Port connection.
Following the recommended span(s), mount the vessel on Tightening the connection more than one turn past hand tight
saddles provided. Tighten straps to one ft-lb maximum. will damage the port.
Align the side ports with the manifold. Ensure that the Thrust Ring is installed downstream.
Center each vessel with the manifold and correct the causes Operating without a thrust ring may cause membrane damage.
of misalignment for each and every vessel. Double check end closure installation.
Use flexible type groove-end pipe couplings. Ensure that retaining ring is in place and fully seated.
Use Victaulic™ style 75 or equal couplings at each side port Never operate the vessel in excess of its ratings.
and allow a gap between each port /manifold connection as This practice will void the vessel warranty, shorten vessel life
specified by coupling manufacturer. and could lead to bodily harm or property damage.
Maximize the connection flexibility. Do not operate the vessel permeate port over 125 psi.
Position the vessel and the piping so that the vessel can grow Permeate pressure in excess of 125 psi must be approved by
in length and diameter under pressure without any undue the factory prior to operation.
restraint. ∆DIA = 0.014 in. (0.4mm) and ∆L = 0.25 in. (6mm) Operate the vessel in only positive pressure applications.
for a length code –7 vessel. This vessel is not designed for vacuum conditions.
Provide overpressure protection. Flush the vessel before system shut down.
Set the safety device at not more than 105% design pressure. Some feed waters may cause corrosion under static
Inspect end closures regularly. conditions. Flushing with non-corrosive permeate is
Replace damaged or deteriorated components and correct the recommended.
cause of any corrosion. Operate the vessel within the recommended pH range.
Relieve system pressure before working on the vessel. The vessel is designed for continuous use at a pH of 3 -11 and
Working on vessels that are under pressure may result in for intermittent cleaning (less than 30 min. at a pH of 2 -12).
bodily harm and/or property damage.

*Please inform the factory when continuous operating temperature is less than 45°F.
HEAD LOADING PROCEDURE
Step 1 Inspect The Shell Step 5 Remove Head
Before installing the head, check the inside surface of the shell While holding the permeate port with your hand, simply pull the
for any imperfections or foreign matter. Remove all foreign matter head from the shell. In some instances it may be required to
using a mild soap solution and rinse with clean water. To remove thread a connection onto the permeate port and gently rock the
imperfections, lightly sand the surface of the vessel with 600-grit head up and down to release the head from the shell.
sandpaper and soapy water and then rinse with water can.
SIDE PORT SEAL REPLACEMENT
Step 2 Head Seal And Shell Lubrication While it is possible to replace the side port seal without removing
Ensure that the head seal is covered with a thin layer of glycerin the port, port removal is the best way to ensure that the seal
and is free from any dirt or dust contamination. Then lubricate the gland is not damaged and to inspect/recondition the gland as
inside of the shell starting directly inboard of the retaining ring required. Before this procedure is started, it is strongly
groove and up the energizing ramp into the vessel bore. Only a recommended that a replacement retaining ring and a new port
thin layer is required. Silicone lubricants can also be used; seal be purchased to ensure correct port installation.
however, care should be taken to use as little as possible. Check
with your membrane supplier before using these lubricants as Step 1 Remove Retaining Ring
they can foul membranes. Carefully remove the metal retaining ring from the side port as to
not damage the ring or the port.
Step 3 Install Head
Holding the head square to the axis of the shell, slowly push the Step 2 Remove Side Port
head into the shell until the seal passes the retaining ring g roove. Mark the port and the shell to indicate correct port location for
As a resistance is felt, two hands may be required. Push the installation. Rotate the vessel, until the port is in the 2 O’clock
head into shell until the head clears the retaining ring groove. position. Place a soft towel into the vessel bore to prevent any
possible damage. Using a rubber mallet, lightly tap on the port
Step 4 Install Retaining Ring from the outside of the vessel while holding the port from inside
Remove any moisture from the retaining groove before the vessel. Continue to tap on the port until it is removed.
proceeding. Carefully place the end of the retaining ring into the
groove on the shell. After the ring is started, slowly push the ring Step 3 Inspect Port
towards the groove. As the ring enters the groove, continue Inspect inside the port for any corrosion and remove any deposits
pushing as your hand slowly rotates counter-clockwise around with a mild abrasive. Ports that have pitting or crevice corrosion
the inside diameter of the shell. Be careful to prevent the ring should be replaced. Inspect the sealing area of the port for areas
from snapping against your finger as it enters the groove that may create sealing problems. Imperfections can be sanded
with 600-grit sandpaper and soap solution. If any imperfections
Step 5 Reconnect Permeate Port cannot be removed in this manner, port replacement is required.
Reconnect the permeate manifolding to the permeate port.
Step 4 Inspect Shell
Step 6 Pressurize System Inspect the sealing area of the shell for areas that may create
Before starting the system, double check that each head has sealing problems. Imperfections can be lightly sanded with 600-
been correctly installed and that all piping connections are in grit sandpaper and a mild soap solution. If any imperfections
place. After ensuring that all required precautions have been cannot be removed in this manner the port may leak. If this is
taken, start the system. found to be the case, the vessel will require a factory technician
to repair the damaged area. Contact the factory for further
Step 7 Check For Leaks
After system start up, verify that all connections are leak free. Fix information.
any leaks at this time to prevent corrosion that may lead to Step 5 Install The Port
component deterioration and possibly unsafe operation. Using the clocking marks from the port removal, install the port
into the vessel wall by pushing it from the inside toward the
HEAD REMOVAL PROCEDURE outside of the vessel. Push the port into position until the snap
ring groove clears the outside of the shell.
Step 1 Shut Down System Step 6 Install The New Retaining Ring
Shut down system and take all steps necessary to relieve Carefully install the new retaining ring being very careful not to
system pressure from the vessel. stretch it out of shape. Feed one end of the ring into the groove.
Then walk the ring into the groove by pushing on the ring with a
Step 2 Disconnect Permeate Piping small tool such as a screwdriver until the ring is completely
Carefully disconnect the permeate piping from the permeate port. installed into the groove.
Set this piping in a secure place for re-assembly.
Step 7 Lubricate The New Seal
Step 3 Check End Closure Lubricate the new seal with a thin layer of glycerin. Silicone
Examine the end closure for any corrosion or damage. Remove lubricants can also be used; however, use as little as possible.
any corrosion with a wire brush and flush away the deposits with Check with your membrane supplier before using these
clean water. Order replacement components as required. lubricants as they can foul membranes.
Step 4 Remove Retaining Ring Step 8 Install The New Seal
Pull the retaining ring out of the groove in the shell. After the ring With the tongue depressor, push the seal all the way down at two
is removed from the groove for ¼ turn, stop pulling. Finish points across from each other. Then repeat the process in the
removing the ring by running your finger behind the ring and opposite direction. The seal should now be installed at four
carefully pulling the ring from groove. It is best to follow the ring corners. Carefully continue to push the seal into the gland by
in a clock-wise direction while removing to avoid stretching the alternating sides until the entire seal is installed.
ring.
HEAD REBUILDING the vessel before tightening the straps allows each end to handle
.030. Do this with each vessel.
Prior to following this procedure, remove the head following the Allow one concentrate manifold to float. In some systems,
procedure listed. the manifold can be connected to the vessels and supported by
Step 1 Remove Adapter the floor but allowed to float in the axial direction to provide room
Pull the adapter from the permeate port by slowly pulling on the for vessel growth under pressure.
adapter body. Let the manifold span be longer than the vessel span.
Remember that the vessel will grow in length under pressure.
Step 2 Remove Permeate Port Setting the manifold span on the long side is another way to
Carefully remove the metal retaining ring from the permeate port provide room for vessel growth under pressure.
as to not damage the ring or the port. A new retaining ring may Check each connection for acceptable misalignment.
be required to assemble the head. After the ring is removed, By installing the Victaulic™ connection without the gasket and
carefully slip the bearing plate off the permeate port and set it drawing the bolts snug, the connector should be able to rotate by
aside. Then simply pull the permeate port from the sealing plate. hand. On some systems this test may not be practical. In these
cases the Victaulic™ connections must be able to be tightened
Step 3 Remove Seals without the need of excessive force. Force would indicate a
Remove the seal from the permeate port and set aside. Using a major misalignment that could damage the vessel.
small tool, such as a screwdriver or a paper clip, remove the seal When in doubt, contact the factory.
from the inside of the permeate port and set aside.
Step 4 Clean All Components MULTIPLE PORT
Using a mild soap solution, clean each component, rinse with
fresh water and then dry with compressed air or a lint free towel.
RECOMMENDATIONS
Multiple port vessels are those specified by the user to have
Step 5 Inspect Components more than one high-pressure port per end. This feature allows
Examine each component for corrosion or damage that may vessels to be directly connected together allowing water to flow
affect the performance of the vessel. Replace any components through one vessel into another. This piping method has
that have corrosion or visual damage. In addition, carefully become an acceptable way to provide superior system designs
inspect each seal for damage or wear. It is recommended to while reducing system costs.
replace each seal at this time. Please be aware that seal While the thought of directly bolting vessels together is easily
condition may affect system performance. understood, there are several guidelines that must be followed in
order to have a good long-term system design. These are as
Step 6 Lubricate Seals follows:
Using extreme care, coat each seal with a thin layer of glycerin. Flow-balance the system.
Only a thin layer is required. Silicone lubricants can also be used; When supplying feed water from one side of the vessels, take the
however, care should be taken to use as little as possible. Check concentrate from the opposite side. This will prevent more water
with your membrane supplier before using these lubricants as from flowing through the first vessel and starting the second and
they can foul membranes. third. This practice will help equalize feed flow to each vessel.
Step 7 Reassemble Head Minimize pressure drop.
As water passes through each vessel, a pressure drop occurs.
Reversing the removal procedure, reassemble the head. Please
note that a new permeate port retaining ring may be required to This will result in the last vessel in a connected pass receiving
ensure correct component performance. less pressure than the first. Increasing port size reduces this
effect.
Optimize the water velocity through the ports.
PIPING RECOMMENDATIONS The speed of the water through the ports should be kept within a
PROTEC pressure vessels are the most durable side port vessel reasonable range to ensure proper long-term performance
available today. Unlike vessels with less durable designs, (typically 5-15 ft. per sec.) Speeds that are too fast result in port
connecting PROTEC side ported vessels to manifolding or to erosion while speeds that are too slow will promote corrosion.
each other is easily done if some very basic rules are followed. Consider feeding from the center of a pass or from both
These are as follows: ends.
Use two flexible Victaulic™ connections when manifold This practice may eliminate problems with velocities that are too
accuracy is questionable. high for proper system performance.
The tolerance required for side-ported vessels should be a total Avoid the temptation to use smaller ports.
per port of .030. For retrofitting side-ported vessels into older Even though the thought of adding on an extra vessel with small
systems or when manifold tolerances can simply not be ports sounds reasonable, it can result in a pressure drop
guaranteed, the two-connection method is the safest approach. problem.
Use a single flexible Victaulic™ connection when manifold Take caution when using more than one port size.
accuracy is not a problem. This is possible when manifold to Changing ports sizes in a second or third pass requires careful
vessel misalignment can be held to within .030 in any direction. evaluation of pressure drop that can affect system performance.
However, it is important to note that these flexible connections Check with your membrane supplier.
allow angular but not lateral misalignment. Therefore, any It is a good idea to let your membrane supplier evaluate the
misalignment must be kept to a minimum. performance of your proposed system.
Use intermediate Victaulic™ connections in the manifolds Don’t assume that we endorse the use of multiple ports for
when required. This practice allows more flexibility in the your system.
system resulting in easier to install manifolds. Just because vessels can be ported together does not make
Center the vessel between the manifolds. This is very basic them the best choice for your system. Bekaert Progressive
but commonly overlooked. If the port on one end is directly Composites is not responsible for the misapplication of the
aligned with the manifold and the opposite is .060 off, centering multiple port option.
450 PSI
L SIDE PORT

ITEM QTY P/N DESCRIPTION MATERIAL NOTES:


DIMENSIONS IN INCHES (MM APPROX.)
1 1 4080223 Shell Filament Wound, Epoxy FRP
Shell L P S Empty Weight
FOR REFERENCE ONLY, NOT FOR CONSTRUCTION UNLESS CERTIFIED
Length inch inch Span lb 2 2 4080030 Bearing Plate 6061-T6 Aluminum, SB-221, Anodized
Code (mm) (mm) in (mm) (kg)
3 2 4080177-2 Sealing Plate Thermoplastic SHIMMING OF THE SADDLES MAY BE REQUIRED
58.7 47 1 @ 28 76 4 2 4080195-1 Feed/Concentrate Port Stainless Steel, 316L, SA-312 CENTER VESSEL ON 2 OR 3 SUPPORTS AT SPAN(S) "S". 3 SUPPORTS
-1
(1491) (1194) (711) (35) REQUIRED FOR LENGTHS -4 AND OVER
5 4 6200343 Retaining Ring, F/C Port Stainless Steel, 300 Series
78.7 67 1 @ 42 88
-1.5 INCORRECT MANIFOLDING WILL CAUSE SEVERE LOCAL STRESS AROUND PORT
(1999) (1702) (1067) (40) 6 2 6110237 Seal, F/C Port Ethylene Propylene AND MAY RESULT IN LEAKS AND PREMATURE FAILURE. TAKE EVERY
99 7 2 4080204-2 Seal Spacer Polyurethane PRECAUTION LISTED IN THIS PACKET.
98.7 87 1 @ 56
-2 (2507) (2210) (1422) (45) INTERNAL PERMEATE PRESSURE MUST NOT EXCEED 125 PSI.
8 2 4080012-1 Permeate Port PVC Thermoplastic
138.7 127 1 @ 80 122
-3 9 2 6100442 Head Seal Ethylene Propylene ASME SECTION X, RP CODE STAMP OPTIONAL
(3523) (3226) (2032) (55)
145 10 2 6110229 Permeate Port Seal Ethylene Propylene SPECIFICATIONS SUBJECT TO CHANGE WITHOUT NOTICE
178.7 167 2 @ 64
-4
(4539) (4242) (1626) (66) 11 2 4080054 Retaining Ring w/ Finger Pull Stainless Steel, 300 Series
218.7 207 2 @ 78 168 12 2 6121200 Retaining Ring, Permeate Port Stainless Steel, 300 Series
-5
(5555) (5258) (1981) (76)
13 2* 4080174 Support Saddle TPR BEKAERT PROGRESSIVE COMPOSITES
258.7 247 2 @ 92 191
-6 14 2 4080040 Strap Assembly Stainless Steel, 300 Series
(6571) (6274) (2337) (87)

298.7 287 2 @ 106 214 15 4 6150001 Strap Screw Stainless Steel, 18-8
-7
(7587) (7290) (2692) (97) 16 2 A/R Adapter PVC Thermoplastic (Upstream Solid)
318.7 307 2 @ 114 226
-7.5 17 1 4080165-1 Thrust Cone PVC Thermoplastic PRO 8-450-MSP
(8095) (7798) (2896) (103)
18 2 6110326 Adapter Seal Ethylene Propylene
338.7 327 2 @ 120 237
-8
(8603) (8306) (3048) (108) 19 A/R - PWT Seal Ethylene Propylene

*3 each with shell length -4 and longer


PORT SPECIFICATION CHART

This chart is used to specify the location of the ports for each different vessel configuration in
7 the system. Always use this chart to specify proper side port locations. If you have any
questions, call the factory. Please use this chart as follows:
6 8
1) Determine proper port sizes using the multiple port guide.
5 2) Determine the proper port location for each vessel.
3) Starting at the serial number end, enter the location of the first port followed by the
port size. Repeat this for each port on the serial number end.
4) Moving to the opposite end, enter the location of the first port followed by the port
size. Repeat this for each port on this end.
5) Enter this information at the bottom of the ordering page for each vessel
configuration.
6) Sign and date the ordering page before you send it in.

NOTE: Two ports per end maximum, diametrically opposed

Port Size Code


J 2-1/2” Grooved End
K 3” Grooved End
3
2 4
Serial Number End
1
Opposite end

EXAMPLE
6 8 This example is provided to show you the proper way to specify your port locations. Please
understand this example before filling out the ordering page. For questions concerning the use
of this chart, please call the factory.

2 J 4 K
Serial Number End

Opposite end 6 J 8 K

2 4
Calculated Pressure Drop into Vessel from Side Port Calculated Pressure Drop From Vessel into Side Port
1.75 0.80

3" pipe 3" pipe


1.5" pipe 2" pipe 2.5" pipe
0.70 2.5" pipe
1.50 1.5" pipe 2" pipe

0.60
1.25

0.50
1.00

0.40

0.75
0.30

Pressure Drop (psi)


Pressure Drop (psi)
0.50
0.20
INLET
0.25 OUTLET
0.10

0.00 0.00

0
0

10
20
30
40
50
60
70
80
90
10
20
30
40
50
60
70
80
90

100
110
120
130
140
150
160
170
180
190
200
210
220
230
240
250
260
270
280
290
300
310
320
330
340
350
360
370
100
110
120
130
140
150
160
170
180
190
200
210
220
230
240
250
260
270
280
290
300
310
320
330
340
350
360
370

Flow Rate (gpm) Flow Rate (gpm)

MULTIPLE PORT DIAGRAM Velocity vs. Flow Rate in schedule 40 pipe


17.00
16.00
15.00 1.5" pipe 2" pipe 2.5" pipe
3" pipe
14.00
13.00
IN L E T
12.00
11.00
10.00
9.00
O UTLET
8.00
7.00
Velocity (ft/s)

6.00
5.00

IN L E T 4.00
3.00
2.00
FEED 1.00
0.00
0
10
20
30
40
50
60
70
80
90
100
110
120
130
140
150
160
170
180
190
200
210
220
230
240
250
260
270
280
290
300
310
320
330
340
350
360
370

CALCULATE THE VELOCITY AND PRESSURE DROP AT EACH PORT USING THE CALCULATED
INFORMATION PROVIDED HERE Flow Rate (gpm)
Membrane Element SWC5
Performance: Permeate Flow: 9,000 gpd (34.1 m3/d)
Salt Rejection:
nominal: 99.8 %
minimum: 99.7 %
Boron Rejection (nominal): 92.0 %†

Type Configuration: Spiral Wound


Membrane Polymer: Composite Polyamide
Nominal Membrane Area: 400 ft2

Application Data* Maximum Applied Pressure: 1200 psig (8.27 MPa)


Maximum Chlorine Concentration: < 0.1 PPM
Maximum Operating Temperature: 113 °F (45 °C)
Feedwater pH Range: 3.0 - 10.0
Maximum Feedwater Turbidity: 1.0 NTU
Maximum Feedwater SDI (15 mins): 5.0
3
Maximum Feed Flow: 75 GPM (17.0 m /h)
Minimum Ratio of Concentrate to
Permeate Flow for any Element: 5:1
Maximum Pressure Drop for Each Element: 10 psi
* The limitations shown here are for general use. The values may be more conservative for specific projects to
ensure the best performance and longest life of the membrane.

Test Conditions
The stated performance is initial (data taken after 30 minutes of operation), based on the following conditions:

32,000 ppm NaCl


800 psi (5.5 MPa) Applied Pressure
77 °F (25 °C) Operating Temperature
10% Permeate Recovery
6.5 - 7.0 pH Range

A
C

B FEED PERMEATE

CONCENTRATE

A, inches (mm) B, inches (mm) C, inches (mm) Weight, lbs. (kg)


40.0 (1016) 7.95 (201.9) 1.125 (28.6) 36 (16.4)
Notice: Permeate flow for individual elements may vary + or - 15 percent. All membrane elements are supplied with a brine seal, interconnector, and o-rings. Elements
are vacuum sealed in a polyethylene bag containing less than 1.0% sodium meta-bisulfite solution, and then packaged in a cardboard box.

When tested at standard test conditions at pH = 7 with 5.0ppm Boron in feed solution.

Hydranautics believes the information and data contained herein to be accurate and useful. The information and data are offered in good faith, but without guarantee, as
conditions and methods of use of our products are beyond our control. Hydranautics assumes no liability for results obtained or damages incurred through the application of the
presented information and data. It is the user's responsibility to determine the appropriateness of Hydranautics' products for the user's specific end uses. 11/27/05
Technical Service Bulletin June 2008 TSB 105.05

REVERSE OSMOSIS AND NANOFILTRATION MEMBRANE ELEMENT


PRECAUTIONS

PERMEATE VALVE OPERATION

The membrane element shall not, at any time, be exposed to permeate back pressure
(where permeate static pressure exceeds feed static pressure). There shall be no
permeate back pressure at shutdown.

At no time during operation of a membrane element system should the permeate valve(s)
be closed. This includes pre-start up flushing, pre-shutdown flushing, cleaning(s) and
standard operation.

Closing the permeate valve during any phase of operation causes a pressure differential
across the tail end of the system and will likely result in irreparable damage to the glue lines
of the tail element(s). This damage will cause immediate increase in salt passage of the
system.

NOTE: Permeate valve(s) may be closed during shutdown after the system has been
flushed and/or when input of the feed water is stopped. In many cases this is necessary to
prevent an aerobic environment in the pressure vessels. The permeate valve (as well as
the concentrate) should be fully re-opened prior to re-introducing feed water.

Reference also Technical Service Bulletin 118.

CONCENTRATE VALVE OPERATION TO SET RECOVERY RATE

During start up of any system, the concentrate valve should be in the fully open position.
This valve should be moved towards the closed position after start up in order to obtain the
desired system recovery. NEVER START A SYSTEM WITH THE CONCENTRATE VALVE
CLOSED AND THEN OPENING IT UNTIL THE SYSTEM RECOVERY IS ACHIEVED.

NOTE: System recovery should be set to the design setpoint as recommended by


Hydranautics’ Rodesign Software.

PRESENCE OF FREE CHLORINE IN FEED WATER OF THIN FILM (POLYAMIDE)


MEMBRANE ELEMENTS

At no time should there be a Free Chlorine residual in the feed water. Even very low levels
of chlorine in the feed stream will result in irreparable oxidation damage of the membrane.
Therefore, operators should ensure that oxidant does not enter the RO system. To ensure
that membranes are not harmed by oxidant, Hydranautics recommends that the feed to the
RO/NF system is equipped with a ORP (Oxidation-Reduction Potential) meter. The
feedwater can then be continuously monitored for the presence of oxidant. Except in
wastewater applications where chloramines are used, the ORP meter reading should
always be below 300 mV. If it exceeds 300 mV, the plant operator should receive a warning
that a dangerous level of oxidant is getting to the membrane and should take action, such
as adding or increasing the dose of SBS, to reduce the oxidant concentration. If the ORP
value reaches 350 mV, the plant should be shut down until the oxidant concentration can be
reduced to a safe value (ORP < 300 mV). Please contact your system provider for various
methods of removing Free Chlorine prior to the membrane system.

NOTE: The oxidative effects of Free Chlorine are strongly catalyzed in the presence of
transition metals such as iron and manganese. If transition metals are present, it is
recommended that there be NO Free Chlorine in the feed water.

LUBRICATION OF O-RINGS AND BRINE SEALS

At no time should petroleum based lubricants be used when lubricating interconnector o-


rings, end adapter o-rings or the membrane element brine seal. Acceptable lubricants
include glycerin, silicon-based Molykote III, or other silicone-based lubricants which contain
no hydrocarbons.

Safe Operation at High Temperature and Pressure

Since membranes are made from plastic materials, they are subject to plastic creep
under certain high temperature and high pressure operating conditions. For reverse
osmosis membranes, the primary concern is that the porous polysulfone support
(Figure 1) may undergo compression at these conditions, which decreases the porosity
of the intermediate layer. This results in greater resistance to water flow through this
layer. The end result is that the apparent permeability of the composite membrane will
decrease and the pressure required to achieve permeation rates at the reference
temperature of 25 C will thus increase. Hydranautics recommends that customers
operate their systems in accordance to the Temperature-Pressure limitations given in
Figure 2. This chart gives the maximum pressure that is allowed for a given feed
temperature. The RO elements are designed to run at up to 45 C. If the operator
desires to run at temperatures in excess of 40C, they should first contact the
Hydranautics Technical Department for advice on safe operation.

Figure 1 Magnified Cross-Section of a Typical Composite Polyamide Membrane

Polysulfone Porous Support

Polyester Nonwoven
Backing
Figure 2a Temperature versus Pressure Operation Limits for Seawater Membranes *
English Values:
Maximum Membrane Feed Pressure vs Temperature
Operational Curve

1250

1200
Maximum Pressure - psi

1150

1100

1050

1000
Contact Hydranautics
950 if operation above
40 deg. C
900
0 5 10 15 20 25 30 35 40 45
Temperature

Figure 2b Temperature versus Pressure Operation Limits for Seawater Membranes- *


Metric Values:
Maximum Membrane Feed Pressure vs Temperature
Operational Curve

84

82
Maximum Pressure - bar

80 Contact Hydranautics
if operation above
78 40 deg. C

76

74
Pressure (Bar)
72

70

68
0 5 10 15 20 25 30 35 40 45
Temperature

* Brackish water elements shall not be operated above 600 psi (41.4 bar).

Hydranautics
401 Jones Rd.
Oceanside, CA 92058
Tel: (760) 901-2500
Fax: (760) 901-2664
email: info@Hydranautics.com
TSB109.02 Page 1

Technical Service Bulletin November 2000 TSB109.02


Vessel Shimming Procedure

To reduce the risk of having disconnects between elements within a pressure vessel, it is
advisable to shim the vessel properly. Shimming is the process of placing pieces of
material (shims) between two parts to take up free space and help to prevent movement.
For membrane systems, plastic or PVC washers are used as shims. This TSB outlines
the procedure to shim a vessel.
Note: Before beginning the shim procedure, ensure that the spacer tube (called the
thrust ring on HydraCode pressure vessels) is in place on the downstream end of the
vessel.

1. Remove the end plate on the feed end of the pressure vessel.
2. Push elements firmly into the vessel, and ensure that there is no free space
between elements.
3. Place an inboard connector on the lead element.
4. Obtain washer-like pieces of plastic (or other approved materials) 1/8” to
1/4” in thickness with an inner diameter larger than the outer diameter of the
adapter. These are the shims.
5. Place the shims by trial and error method over the adapter and then replace
the endplate. Shims should be added until the endplate will not fit entirely in
place. Then remove a shim so that the total thickness of the shims is just
enough to allow the endplate to fit.
6. Repeat this procedure for all vessels.
HYDRANAUTICS
401 Jones Rd.
Oceanside, CA 92054
Tel# (760) 901-2500
Fax# (760) 901-2578
e:mail: info@hydranautics.com
www.membranes.com
Technical Service Bulletin July 2008 TSB108.09

General Storage Procedures for Composite Polyamide (ESPA, ESNA,


CPA, LFC, SWC) and Polyvinyl Derivative (PVD) RO Membrane Elements
This bulletin provides guidelines for storing Hydranautics' Composite Polyamide Reverse
Osmosis (RO) membrane elements.

Note: Before undertaking any long-term or short-term storage operation, contact


Hydranautics for specific instructions related to the local environment.

Scope
The general storage procedures included in this bulletin are as follows:

1. Short-term storage of RO membrane elements in place in pressure


tubes.
2. Long-term storage of RO membrane elements in place in pressure tubes.
3. Dry storage of RO membrane elements as spares or before start-up of
an RO plant.

Note: The composite polyamide type of RO membrane elements may not be exposed
to chlorinated water under any circumstances. Any such exposure will cause
irreparable damage to the membrane. Absolute care must be taken following
any disinfection of piping or equipment or the preparation of cleaning or storage
solutions to ensure that no trace of chlorine is present in feedwater to the RO
membrane elements. If there is any doubt about the presence of chlorine,
perform chemical testing to make sure. Neutralize any chlorine residual with a
sodium bisulfite solution, and ensure adequate contact time to accomplish
complete dechlorination.

Short-Term Storage

Short-term storage is for periods where an RO plant must remain out of operation for more
than five days, but fewer than thirty days, with the RO elements in place. Prepare each RO
train as follows:

1. Flush the RO section with feedwater, while simultaneously venting any


gas from the system. Flushing with RO permeate water instead of
feedwater may help remove build up of foulant (reference TSB 107) .
2. When the pressure tubes are filled, close the appropriate valves to
prevent air from entering the system.
TSB108.07 Page 2

3. Reflush as described above at 5-day intervals.


Note: Short term storage with RO permeate can have added benefits, please
refer to TSB107 for details.

Long-Term Storage
Long-term storage is for periods where an RO plant must remain out of operation for more
than thirty days with the RO elements in place. Prepare each RO train as follows:

1. Clean the RO membrane elements in place.


2. Flush the RO section with an approved biocide (see TSB110 or check
with Hydranautics for recommendations and approvals of currently
available products) prepared from permeate.
3. When the RO section is filled with this solution (make sure that it is
completely filled), close the valves to retain the solution in the RO
section.
4. Repeat Steps 2 and 3 with fresh solution every thirty days if the
temperature is below 80°F (27°C), or every fifteen days if the
temperature is above 80°F (27°C).
5. When the RO system is ready to be returned to service, flush the system
for approximately one hour using low-pressure feedwater with the
product dump valve open to drain; then flush it at high pressure for 5 to
10 minutes with the product dump valve open to drain. Before returning
the RO system to service, check for any residual biocide in the product.

Prior To Installation

When RO elements are stored prior to installation, they should be protected from direct
sunlight and stored in a cool, dry place with an ambient temperature range of 40°F to 95°F
(4.4°C to 35°C). During the period of transit between the factory and the plant site, the
elements should not be exposed to temperatures below freezing, 32°F (0°C), or above
113°F (45°C). New Elements are enclosed in a sealed polyethylene bag containing a
storage solution, and then packaged in a cardboard box. Large shipments may come
packaged in crates strapped to pallets containing 25 single elements. When storing the
pallets of elements, they may be stacked 2 high. Pallets should NOT exceed 2 high.

HYDRANAUTICS
401 Jones Rd.
Oceanside, CA 92058
Tel# (760) 901-2500
Fax# (760) 901-2664
Email: info@hydranautics.com
www.membranes.com
Element Loading Guidelines November 2000 TSB122.01

The following provides general information for installing Hydranautics elements to provide
optimally reliable performance.

Flushing
If the system is new, it is strongly recommended to flush the system first before loading
elements. This allows any debris, solvents, or chlorine to be cleared so that they do not
come in contact with the membranes.

Vessel Preparation
Clean the inside of the vessels before loading. This will remove any dust and debris that
could collect on the membrane surface. Hosing down the insides of the vessels usually will
not be sufficient to clean the vessels. Use of a sponge ball wrapped in a towel and soaked
in a 50% solution of glycerin and water is highly recommended. The sponge ball can be
pulled through the vessel with a piece of rope. Alternatively, the sponge ball can be pushed
through the length of the tube with a piece of 2 inch PVC pipe with a PVC flange attached
to the end.
Caution: Be sure to avoid scraping the pipe along the vessel surface.

Storage
If elements cannot be loaded upon delivery, store elements out of direct sunlight. Do not
allow the elements to freeze. (Please refer to Hydranautics Technical Service Bulletin 101
for cellulose acetate elements or Technical Service Bulletin 108 for composite elements).

Lubricants
• When loading elements into a system, do NOT use oil, grease, or petroleum jelly
based compounds to lubricate o-rings and brine seals.
• Use silicone based gel or a mixture of 50% glycerin in water to lubricate 0-rings and
brine seals.

(Rev. B)
Shimming
Due to inconsistencies in vessel length, it is highly recommended to shim elements to take
up free space in the vessel. This helps to prevent elements from moving when the system
is shut down and restarted. The appearance of leaks between elements is also minimized
when the elements are shimmed.
To shim, simply place PVC “washers” of varying thickness (1/8” to 3/8”) over the FEED
side inboard adapter. Add as many shims as necessary until the end plate fits snugly
against the shims. If necessary a shim may be removed if the end cap is difficult to
reinstall. A gap of 1/4 inch between the end plate and the shims will not cause problems in
performance.

Operation
With all composite membranes, do not expose the membrane to chlorine or other strong
oxidants. A concentration of chlorine in excess of 0.1 PPM can cause irreversible damage
to the membrane.
With cellulose acetate (CAB) membranes, operate in the pH range of 4-6. Operation
outside of this range will cause premature degradation of the membrane.
Note: Assure that flush sequences are within these pH ranges. Failure to do so
may cause severe damage to the membranes.

For further information on the installation and care of Hydranautics products, contact your
Sales Representative or the Technical Support department at Hydranautics.

Hydranautics
401 Jones Rd.
Oceanside, CA 92054
Tel: (760) 901-2500 Fax: (760) 901-2578
e:mail: info@hydranautics.com
Internet: www.membranes.com

(Rev. B)
TSB118.10 Page 1

Technical Service Bulletin November 2007 TSB118.10

Membrane Start-up, Shutdown, and Preservative Flushing Guidelines


This Technical Service Bulletin provides information related to starting up and shutting down an
RO system with Hydranautics membranes, and for flushing composite elements prior to use.

Preservative Flushing Introduction


To preserve elements from biological growth and to help maintain performance over time,
Hydranautics composite type membranes (CPA, ESPA, ESNA, LFC, and SWC) are stored in
either a 0.99% sodium bisulfite solution, or a combination of 0.99% sodium bisulfite and 10%
propylene glycol solution. It is therefore advised to flush membranes prior to use to eliminate
residual preservatives in the product stream. The standard model types that are stored in the
sodium bisulfite and propylene glycol solution are the CPA2-4040, ESNA1-4040, ESPA1-4040,
ESPA3-4040, ESPA4-4040, ESPA1, ESPA3, and ESPA4. All other standard model types are
stored in sodium bisulfite only.

Once the elements have had the preservatives flushed from them, they would need to
have preservatives re-applied for long-term storage. Please refer to TSB108 which
details our short-term and long-term storage procedures for our composite membranes.

Preservative Flushing during Start-up


Once elements have been loaded and vessels sealed, it is recommended to flush the system
to drain with feedwater at design operating pressure for a minimum of 2 hours. If the elements
are to be used in systems requiring ultrapure water, a minimum flushing time of 24 hours is
recommended to reduce the TOC concentration to below 50 ppb (assuming zero TOC in the
feedwater).

Warning: For potable applications using models that are preserved with both
sodium bisulfite and propylene glycol, discard the product water for at
least 24 hours prior to drinking or using in food applications. Ingestion
of the preservative may cause irritation to the gastrointestinal tract,
colic, diarrhea, or other similar symptoms.

For potable applications using models that are preserved with sodium
bisulfite only, discard the product water for at least 2 hours prior to
drinking or using in food applications.
TSB118.10 Page 2
RO System Start-up

It is important to be sure that the elements are loaded and shimmed correctly to remove any
excess slack that may cause disconnects (see TSB122 - Element Loading Guidelines). A low
pressure flush to purge air from the membranes is always recommended before a high
pressure startup. This can be accomplished through the use of a soft-start mechanism, or a
variable frequency drive. Failure to do this can result in a water shock wave (water hammer)
that can cause physical damage to the RO membranes. The permeate valves should always
be open to drain during this flush to prevent damage to the membranes.

After the air has been purged from the system the feed pressure should be increased gradually
up to the working pressure of the RO unit. Pressurization (and depressurization) of the
membrane elements should not exceed ten (10) psi/second (0.7 bar/second) at any time.

RO System Shutdown

Brackish Systems
Upon shutdown for brackish systems, a flush with the feed water at low recovery (brine valve
wide open) is usually sufficient to remove the high concentration of salts from the membranes.
The permeate valves should be open to drain during this flush to prevent damage to the
membranes.

Seawater Systems
Upon shutdown for seawater systems, a flush with RO permeate is recommended to remove
the high concentration of salts from the membranes. The permeate valves should be open to
drain during this flush to prevent damage to the membranes. If RO permeate is temporarily
unavailable, the membranes should be flushed with RO feed at low recovery (with brine valve
wide open). The membranes should then be flushed with RO permeate as soon as it is
available. The seawater RO system should not be left unflushed with a high concentration
brine on the membrane surface.
NOTE:
The quantity of water used in both normal RO System Start-up and RO System Shutdown
flushing should be equal to or greater than that which is retained in the system. For standard
16-inch X 40 inch elements assume thirty-four (34) gallons (130 L) per element. For standard
8-inch X 40-inch elements assume ten (10) gallons (37.85L) per element. For standard 4-inch
X 40-inch elements assume three (3) gallons (11.35L) per element.

If further information is required, please relay questions to the Technical Support department at
our corporate headquarters.

Hydranautics
401 Jones Rd.
Oceanside, CA 92058
Tel: (760) 901-2500
Fax: (760) 901-2664
email: info@Hydranautics.com
Internet: www.membranes.com
Technical Service Bulletin May 1998 TSB114.02

Procedure for Pressure Vessel Probing

This bulletin provides general instructions for probing a pressure vessel containing
reverse osmosis membrane elements. Probing a pressure vessel allows you to
determine where there is a problem in a particular vessel. The problem may be either a
poorly performing membrane element, an O-ring leak at an interconnector or end adapter,
or possibly even a cracked adapter. Probing consists of inserting semi-rigid tubing into
the permeate channel of the pressure vessel and measuring the water quality at different
areas along the length of the pressure vessel.

Test Equipment Set Up (8.0 and 8.5 inch Pressure Vessels)

1. Shut down the RO system.

2. Remove the permeate cap from the pressure vessel that you wish to probe. (The
cap should be on the opposite end of the vessel from where you are collecting the
permeate).

3. Connect a 1 1/4" threaded coupling to the permeate port. Thread in a 1 1/4" by


1/2" threaded reducer bushing into the coupling. Thread in a 1/2" nipple and 1/2"
ball valve. Finally, thread in a 1/2" Parker Fast & Tite male connector (for 3/8"
tubing - Part # P6MC8). Remove the metal collar and O-ring from the Fast & Tite
fitting.

4. Obtain a piece of 3/8" outside diameter natural colored polyethylene tubing. The
tubing should be several feet longer than the length of the vessel. Using a
permanent marker, mark the total length of tubing needed to place the end of the
tubing at the point where the farthest element connects to the adapter. Then, mark
the tubing in 20" increments from this point.
TSB114.02 Page 2

Test Procedure

1. Close the ball valve on the probing fittings. Restart the RO system.

2. After the system has run for 15 minutes, insert the tubing into the Fast & Tite fitting
while opening up the ball valve. Push the tubing in until the “total length” mark is
reached.

3. After 1 minute, measure the conductivity of the water coming out of the tubing.
Recheck several times to make sure the value is constant. Record the
conductivity and note the location.

4. Pull the tubing out 20" using your black marks as a guide, wait 1 more minute, and
repeat the measurement procedure. You may slightly close the ball valve to hold
the tubing in place. When the end of the tubing comes out of the vessel, close the
ball valve, and continue to the next vessel.

5. Chart the value of the permeate conductivity over the length of the vessel. A
steady trend should be observed as a function of position.

Interpreting Probing Data

Evaluation of the data can be done by reviewing the conductivity values along the length
of the permeate channel for individual pressure vessels, and by comparing the trends of
parallel vessels against one another. Since individual situations and systems are unique,
it is best to contact Hydranautics for consultation in analysing data.

In many cases, a sudden increase in the permeate conductivity at a junction between


elements indicates an O-ring problem or a disconnect between elements and
interconnectors. Replace faulty O-rings and ensure that elements are properly shimmed
(TSB109) to eliminate one possible source of a problem. If the problem should persist
following these corrective actions, contact Hydranautics for specific information on
troubleshooting a particuliar system.

Hydranautics
401 Jones Rd.
Oceanside, CA 92054
Tel: (760) 901-2500
Fax: (760) 901-2578
Technical Service Bulletin June 2006 TSB110.08

Biocides for Disinfection and Storage of Hydranautics Membrane


Elements
This bulletin provides general information about biocides that may be used with
Hydranautics membrane elements for disinfection and/or storage. Before storage or
disinfection of Hydranautics elements, one should become familiar with Technical
Service Bulletins 101, 103, and 108 which describe the general storage procedures for
the CAB, CPA, ESPA, ESNA, SWC, LFC and PVD membrane elements. Also, one
should confirm which type of membrane elements are actually in the system. Since
elements may be composed of either cellulose acetate, composite polyamide
membrane, or polyvinyl derivative, it is imperative to be certain of the type to be
disinfected.

SOME OF THE FOLLOWING PROCEDURES, ESPECIALLY THE USE OF FREE


CHLORINE, ARE APPLICABLE TO CELLULOSE ACETATE MEMBRANE
ELEMENTS ONLY AND WILL DAMAGE THE COMPOSITE POLYAMIDE
MEMBRANE ELEMENTS.

If any uncertainty exists regarding the type of elements in use, please contact
Hydranautics for confirmation of compatibility of specific procedures with membrane
types.

If the feed water contains any hydrogen sulfide or dissolved iron or manganese, the
oxidating disinfectants (chlorine and hydrogen peroxide) should not be used. Please
contact Hydranautics for alternative methods of disinfection.

Warning: Some of the biocides listed in this procedure are toxic in some
degree to humans. Allow ample time for system flushing to
remove the presence of the biocides before commencing
normal operation. Hydranautics assumes no liability for the
misuse of any chemical listed herein, and all safety issues are
the responsibility of the end user. Consult manufacturers’
material safety data sheets (MSDS’s) for proper handling and
disposal of any of the listed chemicals.
TSB110.08 Page 2

Biocides for Cellulose Acetate (CAB) Membrane Elements

Free Chlorine
Free chlorine is used at a concentration of 0.1 to 1.0 ppm. Free chlorine may be
applied continuously or on an intermittent basis. If necessary, "shock" chlorination may
be used with cellulose acetate membranes. In this procedure, the membrane elements
are exposed to water which contains up to 5.0 ppm of free chlorine for a period of one
hour in biweekly intervals. If corrosion products are present in the feed water, free
chlorine may cause membrane degradation. If corrosion is present, chloramine, used
at up to 10 ppm, is recommended instead of free chlorine.

Formaldehyde
A formaldehyde solution of 0.1 to 1.0% concentration may be used for system
disinfection and as a preservative for long term storage.

Glutaraldehyde
A glutaraldehyde solution of 0.1 to 1.0% concentration may be used for system
disinfection and as a preservative for long term storage.

Isothiazolin
Isothiazolin is distributed by manufacturers of water treatment chemicals under the
trade name Kathon. The commercial solution contains 1.5% of the active ingredient.
The recommended concentration of Kathon for disinfection and storage is 15 to 25
ppm.

Biocides which can be used with Composite Polyamide (ESPA, ESNA,


CPA, LFC, SWC) and Polyvinyl Derivative (PVD) Membrane Elements

Formaldehyde
A formaldehyde solution of 0.1 to 1.0% concentration may be used for system
disinfection and as a preservative for long term storage. The membrane elements
should be operated for at least 24 hours before being exposed to formaldehyde. (See
NOTE below.)
TSB110.08 Page 3

Glutaraldehyde
A glutaraldehyde solution of 0.1 to 1.0% concentration may be used for system
disinfection and as a preservative for long term storage. The membrane elements
should be operated for at least 24 hours before being exposed to glutaraldehyde. (See
NOTE below.)

NOTE: Addition of formaldehyde and/or gluteraldehyde to new elements may


cause flux reduction of 10-20%. To minimize the chances of flux reduction,
membrane elements should be run for a minimum of 24-hours prior to exposure
to formaldehyde and or gluteraldehyde. Regardless, first time exposure to
formaldehyde and/or gluteraldehyde may result in permanent flux loss.
Subsequent exposure to formaldehyde and/or gluteraldehyde will result in
additional temporary flux loss and will require significant flushing to return to
pre-exposure flux rates.

Isothiazolin
Isothiazolin is distributed by manufacturers of water treatment chemicals under the
trade name Kathon. The commercial solution contains 1.5% of the active ingredient.
The recommended concentration of Kathon for disinfection and storage is 15 to 25
ppm.

DBNPA
DBNPA (2,2 dibromo-3-nitrilo-propionamide) is an effective biocide that comes in
several different forms. For slug dosing, the recommended concentration of DBNPA is
10 to 30 ppm of active ingredient, usually circulated through the membranes using the
cleaning system for 30 minutes to 2 hours. For continuous dosing, a DBNPA
concentration of 0.5 to 1 ppm is recommended. Although DBNPA is useful as a
disinfectant, it should not be used for storage since it will degrade the membrane and
lower the rejection.

Sodium Bisulfite
TSB110.08 Page 4

Sodium bisulfite can be used as an inhibitor of biological growth. To control biological


growth with sodium bisulfite, it is applied at a dosing rate of 500 ppm for 30 to 60
minutes daily. Sodium bisulfite at a 1% concentration can also be used as a
preservative during long term storage of the membrane elements.

Hydrogen Peroxide
Hydrogen peroxide or a solution of hydrogen peroxide with paracetic acid can be used
for disinfection. Special care must be taken that transition metals (Fe, Mn) are not
present in the feed water, since in the presence of transition metals oxidation of the
membrane surface may occur resulting in membrane degradation. The concentration
of hydrogen peroxide in the disinfecting solution should not exceed 0.2%. Hydrogen
peroxide should not be used as a preservative for long term storage of membrane
elements. During application of hydrogen peroxide the water temperature should not
exceed 25°C.

HYDRANAUTICS
401 Jones Rd.
Oceanside, CA 92054
Tel# (760) 901-2500
Fax# (760) 901-2578
e:mail: info@hydranautics.com
www.membranes.com
Technical Service Bulletin May 1998 TSB113.02

Procedure for Measuring Silt Density Index (SDI)

This bulletin provides general instructions for measuring the silt density index
(SDI). The SDI is a popular method for determining feed water quality in RO
applications. It is based on the time required to filter a volume of feedwater
through a 0.45 µm filter pad at a feed pressure of 30 psig.

Test Equipment Set Up


1. Assemble the test equipment per figure 1.
2. Locate a sample tap on the feedwater piping and install the test
equipment.
3. Adjust the pressure regulator to 30 PSI with a filter pad installed.
Use a fresh filter for the actual test.
Note: For best results:
• Use dull tweezers when positioning the filter to prevent puncturing
the filter.
• Ensure that the O-ring is clean and in good condition, and is properly
positioned.
• Avoid touching the filter with fingers.
• Flush the apparatus to remove any contaminants that may be held
within it.

Test Procedure

1. Take the temperature of the feedwater. The temperature should not


vary more than + 1 °C between the start and end of the test.
2. Bleed any entrained air in the filter holder. Depending on the model
of the filter holder, either open the bleed valve, or loosen the filter
TSB113.02 Page 2

holder while cracking the ball valve. Then close the bleed valve or
filter holder.
3. Place a 500 ml graduated cylinder under the filter to measure the
amount of water that passes through the filter.
4. Open the ball valve fully, and measure the time required to collect
100 ml and 500 ml* from the time the ball valve is opened. Record
these times, leaving the valve open and letting the flow continue.
5. After 5 minutes, repeat the time measurement required to collect 100
ml and 500 ml samples. Repeat again after 10 and 15 minutes of
elapsed time.
6. If the time required to obtain a 100 ml sample is greater than about
60 seconds, pluggage will be about 90%, and it is not necessary to
continue the test.
7. Measure the water temperature again to ensure that it did not vary
by more than 1 °C from the initial temperature.
8. After completing the test and disconnecting the apparatus, the filter
paper may be saved in a plastic bag for future reference.

Calculations
SDI = P30 / Tt = 100 * (1 - Ti / Tf) / Tt

where SDI = Silt Density Index


P30 = % pluggage at 30 psig feed pressure**
Tt = Total test time in minutes (usually 15 minutes, but may be less if
75% pluggage** occurs in less than 15 minutes).
Ti = initial time in seconds required to obtain sample.
Tf = time required to obtain sample after 15 minutes (or less).

NOTES
* Time to collect 500 ml should be approximately 5 times greater than the time to
collect 100 ml. If 500 ml collection time is much greater than 5X, SDI should be
calculated using 100 ml collection times.
** For accurate SDI measurements, P30 should not exceed 75%. If P30 exceeds
this value, re-run test and obtain Tf at a shorter time, (T).
TSB113.02 Page 3

Figure 1. Apparatus

Feed

Ball Valve
or 1st Stage
Regulator

Pressure
Regulator
30 psi

Pressure Gauge

Bleed

0.45 micron filter O-ring


TSB107.15 Page 1

Technical Service Bulletin July 2008 TSB107.15

Foulants and Cleaning Procedures


for composite polyamide RO Membrane Elements
(ESPA, ESNA, CPA, LFC, and SWC)
This bulletin provides general information about the usual foulants affecting the performance of
Hydranautics' Composite Polyamide Reverse Osmosis (RO) membrane elements and the removal of these
foulants. The information in this bulletin applies to 4-inch, 6-inch, 8-inch, 8.5-inch, and 16-inch diameter
RO membrane elements.

Note: The Composite Polyamide type of RO membrane elements may not be exposed to
chlorinated water under any circumstances. Any such exposure will cause irreparable
damage to the membrane. Absolute care must be taken following any disinfection of piping
or equipment or the preparation of cleaning or storage solutions to ensure that no trace of
chlorine is present in the feedwater to the RO membrane elements. If there is any doubt
about the presence of chlorine, perform chemical testing to make sure. Neutralize any
chlorine residual with a sodium bisulfite solution, and ensure adequate mixing and contact
time to accomplish complete dechlorination. Dosing rate is 1.8 to 3.0 ppm sodium bisulfite
per 1.0 ppm of free chlorine.

Note: It is recommended that all RO membrane cleaning operations should be closely coordinated
with Hydranautics during the RO membrane element warranty period. Hydranautics field
service personnel are available to be on site for cleaning assistance, should the need arise.
Please contact Hydranautics for current charges for this service.

Note: The use of cationic surfactant should be avoided in cleaning solutions, since irreversible
fouling of the membrane elements may occur.

If additional information is needed, please contact the Technical Services Department at:

HYDRANAUTICS
401 Jones Rd.
Oceanside, CA 92058
Tel# (760) 901-2500
Fax# (760) 901-2664
e-mail: info@hydranautics.com
Internet: www.membranes.com
TSB107.15 Page 2

RO Membrane Fouling and Cleaning


During normal operation over a period of time, RO membrane elements are subject to fouling by
suspended or sparingly soluble materials that may be present in the feedwater. Common examples of
foulants are:
• Calcium carbonate scale
• Sulfate scale of calcium, barium or strontium
• Metal oxides (iron, manganese, copper, nickel, aluminum, etc.)
• Polymerized silica scale
• Inorganic colloidal deposits
• Mixed inorganic/organic colloidal deposits
• NOM organic material (Natural Organic Matter)
• Man-made organic material (e.g. antiscalant/dispersants, cationic polyelectrolytes)
• Biological (bacterial bioslime, algae, mold, or fungi)

The nature and rapidity of fouling depends on a number of factors, such as the quality of the feedwater and
the system recovery rate. Typically, fouling is progressive, and if not controlled early, will impair the RO
membrane element performance in a relatively short time. Cleaning is should accur when the RO shows
evidence of fouling, just prior to a long-term shutdown, or as a matter of scheduled routine maintenance.
The elements shall be maintained in a clean or “nearly clean” condition to prevent excessive fouling by the
foulants listed above. Some fouling is allowed as long as:

- normalized permeate flow decrease is less than 10%

- normalized permeate quality decrease is less than 10%


.
- normalized pressure drop, as measured between the feed and concentrate headers, increase is less
than 15%.

Cleaning should be carried out before these values are exceeded to maintain the elements in a clean or
“nearly clean” condition. Effective cleaning is evidenced by the return of the normalized parameters to their
initial, Start-up, value. In the event you do not normalize your operating data, the above values still apply if
you do not have major changes in critical operating parameters. The operating parameters that have to
stay constant are permeate flow, permeate back-pressure, recovery, temperature, and feed TDS. If these
operating parameters fluctuate, then it is highly recommended that you normalize the data to determine if
fouling is occurring or if the RO is actually operating normally based on the change in a critical operating
parameter. Hydranautics offers a free normalization software program called ROData, which can be
downloaded from our web site at www.membranes.com.

Monitoring overall plant performance on a regular basis is an essential step in recognizing when
membrane elements are becoming fouled. Performance is affected progressively and in varying degrees,
depending on the nature of the foulants. Table 1 “RO Troubleshooting Matrix” provides a summary of the
expected effects that common foulants have on performance.

RO cleaning frequency due to fouling will vary by site. A rough rule of thumb as to an acceptable cleaning
frequency is once every 3 to 12 months. If you have to clean more than once a month, you should be able
to justify further capital expenditures for improved RO pretreatment or a re-design of the RO operation. If
the cleaning frequency is every one to three months, you may want to focus on improving the operation of
your existing equipment but further capital expenditure may be harder to justify.

It is important to clean the membranes when they are only lightly fouled, not heavily fouled. Heavy fouling
can impair the effectiveness of the cleaning chemical by impeding the penetration of the chemical deep into
the foulant and in the flushing of the foulant out of the elements. If normalized membrane performance
drops 30 to 50%, it may be impossible to fully restore the performance back to baseline conditions.
TSB107.15 Page 3

When inorganic coagulants are used in the pretreatment process, there can often be incomplete reaction of
the inorganic salt and thus insufficient formation of a filterable floc. The user should ensure that excessive
amounts of inorganic coagulant are not fed to the RO system. Excessive amounts of coagulant can be
measured by using SDI filter equipment. In the case of iron, the iron on the SDI filter pad should typically
be 3 µg/pad and never above 5 µg/pad.
In addition to the use of turbidity and SDI, particle counters are also very effective to accurately measure
the suitability of the feedwater for NF/RO elements. The measure of particles greater than 2 microns in
size should be < 100 particles per millilitre.
One RO design feature that is commonly over-looked in reducing RO cleaning frequency is the use of RO
permeate water for flushing foulants from the system. Soaking the RO elements during standby with
permeate can help dissolve scale and loosen precipitates, reducing the frequency of chemical cleaning.

What you clean for can vary site by site depending on the foulant. Complicating the situation frequently is
that more than one foulant can be present, which explains why cleanings frequently require a low pH and
high pH cleaning regiment.

Note: The membrane elements shall not be exposed to feed water containing oil, grease, or other foreign
matter which proves to chemically or physically damage the integrity of the membrane.
TSB107.15 Page 4

Table 1: RO Troubleshooting Matrix


(Pressure Drop is defined as the Feed pressure minus the Concentrate pressure)
Possible Possible Pressure Feed Salt
Cause Location Drop Pressure Passage
Metal Oxide Fouling 1st stage Rapid Rapid increase Rapid
(e.g. Fe,Mn,Cu,Ni,Zn) lead elements increase increase
Colloidal Fouling 1st stage Gradual Gradual Slight
(organic and/or lead elements increase increase increase
inorganic complexes)
Mineral Scaling Last stage Moderate Slight increase Marked
(e.g. Ca, Mg, Ba, Sr) tail elements Increase increase
Polymerized Silica Last stage Normal to Increased Normal to
tail elements increased increased
Biological Fouling Any stage, Marked Marked Normal to
usually lead increase increase increased
elements
Organic Fouling All stages Gradual Increased Decreased
(dissolved NOM) increase
Antiscalant Fouling 2nd stage most Normal to Increased Normal to
severe increased increased
Oxidant damage 1st stage Normal to Decreased Increased
(e.g Cl2, ozone,KMnO4) most severe decreased
Hydrolysis damage All stages Normal to Decreased Increased
(out of range pH) decreased
Abrasion damage 1st stage Normal to Decreased Increased
(carbon fines, etc) most severe decreased
O-ring leaks Random Normal to Normal to Increased
(at interconnectors or (typically at decreased decreased
adapters) feed adapter)
Glue line leaks 1st stage Normal to Normal to Increased
(due to permeate back- most severe decreased decreased
pressure in service or
standby)
Glue line leaks Tail element Increased Increased Increased
(due to closed of a stage (based on prior (based on prior
permeate valve while fouling & high fouling & and
cleaning or flushing) delta P) high delta P)
TSB107.15 Page 5

Discussion on Foulants

Calcium Carbonate Scale: Calcium carbonate is a mineral scale and may be deposited from almost any
feedwater if there is a failure in the antiscalant/dispersant addition system or in the acid injection pH control
system that results in a high feedwater pH. An early detection of the resulting calcium carbonate scaling is
absolutely essential to prevent the damage that crystals can cause on the active membrane layers.
Calcium carbonate scale that has been detected early can be removed by lowering the feedwater pH to
between 3.0 and 5.0 for one or two hours. Longer resident accumulations of calcium carbonate scale can
be removed by a low pH cleaning with a citric acid solution.

Calcium, Barium & Strontium Sulfate Scale: Sulfate scale is a much “harder” mineral scale than
calcium carbonate and is harder to remove. Sulfate scale may be deposited if there is a failure in the
antiscalant/dispersant feed system or if there is an over feed of sulfuric acid in pH adjustment. Early
detection of the resulting sulfate scaling is absolutely essential to prevent the damage that crystals can
cause on the active membrane layers. Barium and strontium sulfate scales are particularly difficult to
remove as they are insoluble in almost all cleaning solutions, so special care should be taken to prevent
their formation.

Calcium Phosphate Scale: This scale is particularly common in municipal waste waters and polluted
water supplies which may contain high levels of phosphate. This scale can generally be removed with
acidic pH cleaners. At this time, phosphate scaling calculations are not performed by the Hydranautics
RO Design software. As a rule of thumb, contact Hydranautics technical department if phosphate levels in
the feed are 5 ppm or higher.

Metal Oxide/Hydroxide Foulants: Typical metal oxide and metal hydroxide foulants are iron, zinc,
manganese, copper, aluminum, etc. They can be the result of corrosion products from unlined pipes and
tanks, or result from the oxidation of the soluble metal ion with air, chlorine, ozone, potassium
permanganate, or they can be the result of a pretreatment filter system upset that utilizes iron or aluminum-
based coagulant aids.
Polymerized Silica Coating: A silica gel coating resulting from the super-saturation and polymerization of
soluble silica can be very difficult to remove. It should be noted that this type of silica fouling is different
from silica-based colloidal foulants, which may be associated with either metal hydroxides or organic
matter. Silica scale can be very difficult to remove by traditional chemical cleaning methods. Contact
Hydranautics technical department if the traditional methods are unsuccessful. There does exist harsher
cleaning chemicals, like ammonium biflouride, that have been used successfully at some sites but are
considered rather hazardous to handle and can damage equipment.

Colloidal Foulants: Colloids are inorganic or mixed inorganic/organic based particles that are suspended
in water and will not settle out due to gravity. Colloidal matter typically contains one or more of the
following major components: iron, aluminum, silica, sulfur, or organic matter.

Dissolved NOM Organic Foulants: The sources of dissolved NOM (Natural Organic Matter) foulants are
typically derived from the decomposition of vegetative material into surface waters or shallow wells. The
chemistry of organic foulants is very complex, with the major organic components being either humic acid
or fulvic acid. Dissolved NOMs can quickly foul RO membranes by being absorbed onto the membrane
surface. Once absorption has occurred, then a slower fouling process of gel or cake formation starts. It
should be noted that the mechanism of fouling with dissolved NOM should not be confused with the
mechanism of fouling created by NOM organic material that is bound up with colloidal particles.

Microbiological Deposits: Organic-based deposits resulting from bacterial slimes, fungi, molds, etc. can
be difficult to remove, particularly if the feed path is plugged. Plugging of the feed path makes it difficult to
TSB107.15 Page 6

introduce and distribute the cleaning solutions. To inhibit additional growth, it is important to clean and
sanitize not only the RO system, but also the pretreatment, piping, dead-legs, etc. The membranes, once
chemically cleaned, will require the use of a Hydranautics approved biocide and an extended exposure
requirement to be effective. For further information on biocides, refer to Hydranautics Technical Service
Bulletin TSB-110 “Biocides for Disinfection and Storage of Hydranautics Membrane Elements”.

Selection and Use of Cleaning Chemicals


There are a number of factors involved in the selection of a suitable cleaning chemical (or chemicals) and
proper cleaning protocol. The first time you have to perform a cleaning, it is recommended to contact the
manufacturer of the equipment, the RO element manufacturer, or a RO specialty chemical and service
supplier. Once the suspected foulant(s) are identified, one or more cleaning chemicals will be
recommended. These cleaning chemical(s) can be generic or can be private-labeled proprietary
chemicals. Typically, the generic chemicals can be of technical grades and are available from local
chemical supply companies. The proprietary RO cleaning chemicals can be more expensive, but may be
easier to use and you cannot rule out the advantage of the intellectual knowledge supplied by these
companies. Some independent RO service companies can determine the proper chemicals and cleaning
protocol for your situation by testing at their facility a fouled element pulled from your system.

It is not unusual to use a number of different cleaning chemicals in a specific sequence to achieve the
optimum cleaning. Typically, a high pH cleaning is used first to remove foulants like oil or biological matter,
followed by a low pH cleaning to remove foulants like mineral scale or metal oxides/hydroxides fouling.
There are times that order of high and low pH cleaning solutions is reversed or one solution only is required
to clean the membranes. Some cleaning solutions have detergents added to aid in the removal of heavy
biological and organic debris, while others have a chelating agent like EDTA added to aid in the removal of
colloidal material, organic and biological material, and sulfate scale. An important thing to remember is that
the improper selection of a cleaning chemical, or the sequence of chemical introduction, can make the
foulant worse.

Hydranautics recommends that the membrane system operator thoroughly investigate the signs of fouling
before they select a cleaning chemical and a cleaning protocol. Some forms of fouling (iron deposits and
scaling commonly associated with well waters) may require only a simple low pH cleaning. However, for
most complex fouling phenomena, Hydranautics recommends the following sequence:
1. Flushing with permeate with addition of non oxidizing biocide (DBNPA or similar type) at the end of
the flushing.
2. High pH CIP – Temperature versus pH as per recommendations in this TSB
3. Flushing with permeate until pH on the brine side is below pH 8.5
4. Low pH CIP
5. Acid flushing with permeate and non oxidizing biocide (DBNPA or similar type)

General Precautions in Cleaning Chemical Selection and Usage


• If you are using a proprietary chemical, make sure the chemical has been qualified for use with your
Hydranautics membrane by the chemical supplier. The chemical supplier’s instructions should not be
in conflict with Hydranautics recommended cleaning parameters and limits listed in this Technical
Service Bulletin.
• If you are using generic chemicals, make sure the chemical has been qualified for use with your
Hydranautics membrane in this Technical Service Bulletin.
• Use the least harshest cleaning regiment to get the job done. This includes the cleaning parameters of
pH, temperature, and contact time. This will optimize the useful life of the membrane.
• Clean at the recommended target temperatures to optimize cleaning efficiency and membrane life.
TSB107.15 Page 7

• Use the minimal amount of chemical contact time to optimize membrane life.
• Be prudent in the adjustment of pH at the low and high pH range to extend the useful life of the
membrane. A “gentle” pH range is 4 to 10, while the harshest is 2 to 12.
• Oil and biologically -fouled membranes should not use a low pH clean-up first as the oil and biological
matter will congeal.
• Cleaning and flushing flows should be in the same direction as the normal feed flow to avoid potential
telescoping and element damage.
• When cleaning a multi-stage RO, the most effective cleaning is one stage at a time so cleaning flow
velocities can be optimized and foulants from upstream stages don’t have to pass through down-
stream stages.
• Flushing out detergents with higher pH permeate can reduce foaming problems.
• Verify that proper disposal requirements for the cleaning solution are followed.
• If your system has been fouled biologically, you may want to consider the extra step of introducing a
sanitizing biocide chemical before and after a successful cleaning. Biocides can be introduced before
and immediately after cleaning, periodically (e.g. once a week), or continuously during service. You
must be sure that the biocide is compatible with the membrane, does not create any health risks, is
effective in controlling biological activity, and is not cost prohibitive.
• For safety reasons, make sure all hoses and piping can handle the temperatures, pressures and pH’s
encountered during a cleaning.
• For safety reasons, always add chemicals slowly to an agitated batch of make-up water.
• For safety reason, always wear safety glasses and protective gear when working with chemicals.
• For safety reasons, don’t mix acids with caustics. Thoroughly rinse the 1st cleaning solution from the
RO system before introducing the next solution.

Selecting a Cleaning Solution


Table 2 lists the recommended generic chemical solutions for cleaning an RO membrane element based
on the foulant to be removed.
Important: It is recommended that the MSDS of the cleaning chemicals be procured from
the chemical supplier and that all safety precautions be utilized in the handling and storage
of all chemicals.

Table 2: Hydranautics Recommended Chemical Cleaning Solutions

Foulant Gentle Cleaning Solution Harsher Cleaning Solution


Calcium carbonate scale 1 4
Calcium, barium or strontium sulfate scale 2 4
Metal oxides/hydroxides (Fe, Mn, Zn, Cu, Al) 1 5
Inorganic colloidal foulants 1 4
Mixed Inorganic/organic colloidal foulants 2 6
Polymerized silica coating None 7
Biological matter 2 or 3 6
NOM organic matter (naturally occurring) 2 or 3 6
TSB107.15 Page 8

Table 3 “Hydranautics Recipes for Cleaning Solutions” offers instructions on the volumes of bulk chemical
to be added to 100 U.S. gallons (379 liters) of make-up water. Prepare the solutions by proportioning the
amount of chemicals to the amount of make-up water to be used. Make-up water quality should be of RO
permeate or deionized (DI) quality, and be free of chlorine and hardness. Before forwarding the cleaning
solution to the membranes, it is important to thoroughly mix it, adjust the pH according to the target pH, and
stabilize the temperature at the target temperature. Unless otherwise instructed, the cleaning design
parameters are based on a chemical recirculation flow period of one hour and an optional chemical soak
period of one hour.

Table 4 “Hydranautics Maximum pH and Temperature Limits for Cleaning” highlights the maximum pH and
temperature limits for specific membranes, after which irreparable membrane damage can occur. A
suggested minimum temperature limit is 70 F (21 C), but cleaning effectiveness and the solubility of the
cleaning chemical is significantly improved at higher temperatures.

Description of Cleaning Solutions

Note: The notation (w) denotes that the diluted chemical solution strength is based on the actual weight of
the 100% pure chemical or active ingredient.

Solution 1: This is a low pH cleaning solution of 2.0% (w) citric acid (C6H8O7). It is useful in removing
inorganic scale (e.g. calcium carbonate, calcium sulfate, barium sulfate, strontium sulfate) and metal
oxides/hydroxides (e.g. iron, manganese, nickel, copper, zinc), and inorganic-based colloidal material.
Note: Citric acid is available as a powder.

Solution 2: This is a high pH cleaning solution (target pH of 10.0) of 2.0% (w) of STPP (sodium
tripolyphosphate) (Na5P3O10) and 0.8% (w) of Na-EDTA (sodium salt of ethylaminediaminetetraacetic acid).
It is specifically recommended for removing calcium sulfate scale and light to moderate levels of organic
foulants of natural origin. STPP functions as an inorganic-based chelating agent and detergent. Na-EDTA
is an organic-based chelating cleaning agent that aids in the sequestering and removal of divalent and
trivalent cations and metal ions. STPP and Na-EDTA are available as powders.

Solution 3: This is a high pH cleaning solution (target pH of 10.0) of 2.0% % (w) of STPP (sodium
tripolyphosphate) (Na5P3O10) and 0.025% (w) Na-DDBS (C6H5(CH2)12-SO3Na) (sodium salt of
dodecylbenzene sulfonate). It is specifically recommended for removing heavier levels of organic foulants
of natural origin. STPP functions as an inorganic-based chelating agent and detergent. Na-DDBS
functions as an anionic detergent.

Solution 4: This is a low pH cleaning solution (target pH of 2.5) of 0.5% (w) of HCL (hydrochloric) acid. It
is useful in removing inorganic scale (e.g. calcium carbonate, calcium sulfate, barium sulfate, strontium
sulfate and metal oxides/hydroxides (e.g. iron, manganese, nickel, copper, zinc) and inorganic-based
colloidal material. This cleaning solution is considered to be harsher than Solution 1. HCL acid, a strong
mineral acid, is also known as muriatic acid. HCL acid is available in a number of concentrations: (18 0
Baume = 27.9%), (20 0 Baume = 31.4%), (22 0 Baume = 36.0%).

Solution 5: This is a lower pH cleaning solution (natural pH is between pH 4 and 6. No pH adjustment is


required) 1.0% (w) of Na2S2O4 (sodium hydrosulfite). It is useful in the removal of metal oxides and
hydroxides (especially iron fouling), and to a lesser extent calcium sulfate, barium sulfate and strontium
sulfate. Sodium hydrosulfite is strong reducing agent and is also known as sodium dithionite. The solution
will have a very strong odor so proper ventilation is required. Sodium hydrosulfite is available as a powder.
TSB107.15 Page 9

Solution 6: This is a high pH cleaning solution (target pH of 11.5) of 0.1% (w) of NaOH (sodium
hydroxide) and 0.03% (w) of SDS (sodium dodecylsulfate). It is useful in the removal of organic foulants of
natural origin, colloidal foulants of mixed organic/inorganic origin, and biological material (fungi, mold,
slimes and biofilm). SDS is a detergent that is an anionic surfactant that will cause some foaming. This is
considered to be a harsh cleaning regiment.

Solution 7: This is a high pH cleaning solution (target pH of 11.5) of 0.1% (w) of NaOH (sodium
hydroxide). It is useful in the removal of polymerized silica. This is considered to be a harsh cleaning
regiment.

Important: It is recommended that the MSDS of the cleaning chemicals be procured from
the chemical supplier and that all safety precautions be utilized in the handling and storage
of all chemicals.
TSB107.15 Page 10

Table 3: Hydranautics Recipes for Cleaning Solutions


The quantities listed below are to be added to 100 U.S.gallons (379 liters) of dilution water.

Cleaning Bulk Ingredients Quantity Target Target


Solution pH Adjustment Temp.
1 Citric acid 17.0 pounds No pH adjustment is 104 F (40 C)
(as 100% powder) (7.7 kg) Required.
2 STPP 17.0 pounds Adjust to pH 10.0 with 104 F (40 C)
(sodium tripolyphosphate) (7.7 kg) sulfuric or hydrochloric
(as 100% powder) acid.
Na-EDTA 7.0 pounds
(Versene 220 or equal) (3.18 kg)
(as 100% powder)
3 STPP 17 pounds Adjust down to pH 104 F (40 C)
(sodium tripolyphosphate) (7.7 kg) 10.0 with sulfuric or
(as 100% powder) hydrochloric acid.
Na-DDBS 0.21 pounds
Na-dodecylbenzene sulfonate (0.1 kg)
4 HCl acid 0.47 gallons Slowly adjust pH down 95 F (35 C)
(hydrochloric acid (1.78 liters) to 2.5 with HCL acid.
(as 220 Baume or 36% HCL) Adjust pH up with
sodium hydroxide.
5 Sodium hydrosulfite 8.5 pounds No pH adjustment is 95 F (35 C)
(as 100% powder) (3.86 kg) required.
6 NaOH (sodium hydroxide) Slowly adjust pH up to 86 F (30 C)
(as 100% powder) 0.83 pounds 11.5 with sodium
(0.38 kg) hydroxide. Adjust pH
(or as 50% liquid) 0.13 gallons down to 11.5 by
(0.49 liters) adding HCL acid.
SDS
(sodium dodecylsulfate) 0.25 pounds
(0.11 kg)
7 NaOH (sodium hydroxide) Slowly adjust pH up to 86 F (30 C)
(as 100% powder) 0.83 pounds 11.5 with sodium
(0.38 kg) hydroxide. Adjust pH
(or as 50% liquid) 0.13 gallons down to 11.5 by
(0.49 liters) adding HCL acid.
TSB107.15 Page 11

Table 4: Hydranautics pH and Temperature Limits for Cleaning


(See Table 3 for target pH and temperatures)

Membrane 45 C (113 F) 40 (105 F) 30 C (86 F)


CPA 2-10 2-11.5 2-12
ESPA 2-10 2-11.5 2-12
LFC 2-10 2-11.5 2-12
SWC 2-10 2-11.5 2-12
ESNA 3-10 2-11.5 2-12

Note: The above cleaning parameters denote the maximum temperature limits for a corresponding range of
pH. Cleaning operations performed at the extremes may result in a more effective cleaning, but can
shorten the useful life of the membrane due to hydrolysis. To optimize the useful life of a membrane, it is
recommended to use the least harshest cleaning solutions and minimize the contact time whenever
possible.

Table 5: Cleaning and Flushing Flow Rates per RO Pressure Tube


(Pressures are not to exceed 60 psi (4 bar) at inlet to tubes.)

Element Diameter GPM LPM


4-inches 6 to 10 23 to 38
6-inches 12 to 20 46 to 76
8-inches 24 to 40 91 to 151
8.5-inches 27 to 45 102 to 170
16-inches 96 to 160 360 to 600

Table 6: Cleaning Solution Volume Requirement per RO Element


(these volumes do not include volumes required for piping, filters, etc)
(these volumes do not include initial 20% of volume dumped to drain)
Normal Heavy Normal Heavy
Element Size Fouling Fouling Fouling Fouling
(Gallons) (Gallons) (Liters) (Liters)
4 x 40 inches 2.5 5 9.5 19
6 x 40 inches 5 10 19 38
8 x 40 inches 9 18 34 68
8.5 x 40 inches 10 20 38 76
16 x 40 inches 36 72 136 272
TSB107.15 Page 12

RO Cleaning Skid

The successful cleaning of an RO on-site requires a well designed RO cleaning skid. Normally this skid is
not hard piped to the RO skid and uses temporary hosing for connections. It is recommended to clean a
multi-stage RO one stage at a time to optimize cross-flow cleaning velocity. The source water for chemical
solution make-up and rinsing should be clean RO permeate or DI water and be free of hardness, transition
metals (e.g. iron), and chlorine. Components must be corrosion proof. Major cleaning system components
are:

RO Cleanup Skid

10-micron RO Stage
Clean-up Filter
RO Clean-up Pump
Tank

Concentrate

Permeate

• RO Cleaning Tank: This tank needs to be sized properly to accommodate the displacement of water in
the hose, piping, and RO elements. The table below denotes the amount of chemical solution that
needs to be made for a single RO element. The tank should be designed to allow 100 % drainage,
easy access for chemical introduction and mixing, a recirculation line from the RO Cleaning Pump,
proper venting, overflow, and a return line located near the bottom to minimize foam formation when
using a surfactant.
• RO Cleaning Pump: This pump needs to be sized to develop the proper cross-flow velocity to scrub
the membrane clean. The maximum recommended pressure is 60 psi (4 bar) at the inlet to the
pressure vessels to minimize the production of permeate during cleaning and reduce the convective
redeposition of foulant back on to the membrane surface. The table below denotes the flow rate
ranges for each pressure tube.
• RO Cleaning Cartridge Filter: Normally 5 to 10-micron and is designed to remove foulants that have
been displaced from the cleaning process.
• RO Tank Heater or Cooler: The maximum design temperature for cleaning is 1130 F (450 C). It should
be noted that heat is generated and imparted by the RO Cleaning Pump during recirculation.
• RO Tank Mixer: This is recommended to get optimal mixing of chemical, though some designers rely
solely on the slow introduction of chemical while maintaining a recirculation through the RO Cleaning
Pump back to the tank.
• Instrumentation: Cleaning system instrumentation should be included to monitor flow, temperature,
pressure, and tank level.
• Sample Points: Sample valves should be located to allow pH and TDS measurements off the RO
Cleaning Pump discharge and the concentrate side recirculation return line.
TSB107.15 Page 13

• Permeate Return Line: A small amount of the cleaning solution can permeate through the membranes
and so a permeate-side return line back to the RO Cleaning Tank is required.

Important: The permeate line and any permeate valves must always be open to atmospheric pressure
during the cleaning and flushing steps or damage to RO elements can occur. If the permeate line is
closed, the permeate pressure can build up and become higher than the feed-side pressure of the tail
elements. This can result in excessive permeate back-pressure which can damage the membrane
glue lines in the tail elements.

RO Membrane Element Cleaning and Flushing Procedures

The RO membrane elements can be cleaned in place in the pressure tubes by recirculating the cleaning
solution across the high-pressure side of the membrane at low pressure and relatively high flow. A
cleaning unit is needed to do this. RO cleaning procedures may vary dependent on the situation. The time
required to clean a stage can take from 4 to 8 hours.

A general procedure for cleaning the RO membrane elements is as follows:

1. Perform a low pressure flush at 60 psi (4 bar) or less of the pressure tubes by pumping clean
water from the cleaning tank (or equivalent source) through the pressure tubes to drain for
several minutes. Flush water should be clean water of RO permeate or DI quality and be
free of hardness, transition metals, and chlorine.

2. Mix a fresh batch of the selected cleaning solution in the cleaning tank. The dilution water
should be clean water of RO permeate or DI quality and be free of hardness, transition
metals, and chlorine. The temperature and pH should be adjusted to their target levels.

3. Circulate the cleaning solution through the pressure tubes for approximately one hour or the
desired period of time. At the start, send the displaced water to drain so you don’t dilute the
cleaning chemical and then divert up to 20% of the most highly fouled cleaning solution to
drain before returning the cleaning solution back to the RO Cleaning Tank. For the first 5
minutes, slowly throttle the flow rate to 1/3 of the maximum design flow rate. This is to
minimize the potential plugging of the feed path with a large amount of dislodged foulant.. For
the second 5 minutes, increase the flow rate to 2/3 of the maximum design flow rate, and
then increase the flow rate to the maximum design flow rate. If required, readjust the pH
back to the target when it changes more than 0.5 pH units.

4. An optional soak and recirculation sequence can be used, if required. The soak time can be
from 1 to 8 hours depending on the manufacturer’s recommendations. Caution should be
used to maintain the proper temperature and pH. Also note that this does increase the
chemical exposure time of the membrane.

5. Upon completion of the chemical cleaning steps, a low pressure Cleaning Rinse with clean
water (RO permeate or DI quality and free of hardness, transition metals, and chlorine) is
required to remove all traces of chemical from the Cleaning Skid and the RO Skid. Drain and
flush the cleaning tank; then completely refill the Cleaning Tank with clean water for the
TSB107.15 Page 14

Cleaning Rinse. Rinse the pressure tubes by pumping all of the rinse water from the
Cleaning Tank through the pressure tubes to drain. A second cleaning can be started at this
point, if required.

6. Once the RO system is fully rinsed of cleaning chemical with clean water from the Cleaning
Tank, a Final Low Pressure Clean-up Flush can be performed using pretreated feed water.
The permeate line should remain open to drain. Feed pressure should be less than 60 psi (4
bar). This final flush continues until the flush water flows clean and is free of any foam or
residues of cleaning agents. This usually takes 15 to 60 minutes. The operator can sample
the flush water going to the drain for detergent removal and lack of foaming by using a clear
flask and shaking it. A conductivity meter can be used to test for removal of cleaning
chemicals, such that the flush water to drain is within 10-20% of the feed water conductivity.
A pH meter can also be used to compare the flush water to drain to the feed pH.

7. Once all the stages of a train are cleaned, and the chemicals flushed out, the RO can be
restarted and placed into a Service Rinse. The RO permeate should be diverted to drain until
it meets the quality requirements of the process (e.g. conductivity, pH, etc.). It is not unusual
for it to take from a few hours to a few days for the RO permeate quality to stabilize,
especially after high pH cleanings.

Hydranautics
401 Jones Rd.
Oceanside, CA 92058
Tel: (760) 901-2500
Fax: (760) 901-2664
e-mail: info@Hydranautics.com

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