Observation Sheet for TMT Steel Chemical Test

As Per IS : 6226 (Part-1,2), 228 (Part-1,3) Reaffirmed – 2018,19, & STH/SOP/CE/LAS/03

I.D. No : Details of sample :

Condition of sample : Date of sample received :

Type of sample : Date of Testing :

ID Mark/ No. : Temperature :

Dia ……. 6mm

S.No. Parameter of Chemical Properties Test -1 Test-2
1 Determination of Carbon
  Sample Taken in gm 1.0065 2
  Burette Reading for Blank, ( Initial Reading) B= 0.35 0.34
  Burette Reading for Sample, ( Final Reading) A= 0.515 0.78
  Temperature in oC = 22 32
  Pressure in mm Hg = 724 740
  Correction Factor for temp and Pressure (IS 228 P1) F = 0.912 0.894

  Carbon as (C) % by mass = (A – B) x F/Wt of Sample, gm 0.150 0.197

2 Determination of Sulphur
  Weight of sample Taken in gm D = 1.0045 5
  ml of NaOH Sulphur burette Reading used in blank , B = 0 20
  ml of NaOH Sulphur burette Reading used in sample, A = 0.048 16.9
  Diffrence (A-B) 0.048 0.03
  Sulphur as (S) % by mass = (A - B) / D 0.048 0.030

3 Determination of Phosphorus    
  Weight of sample Taken in gm D = 2.0562 2
  ml of used in blank titration, B = 19.6 20.3
  ml of HNO3 used in sample titration, A = 24.8 24.8
  Phosphorous Equivalent 1.0 ml of HNO3 , C = 0.0001347 0.0001347
  Phosphorus as (P) %by mass = (B-A) x C x100/ D 0.034 0.030

4 Determination of Sulphur & Phosphorus (2 + 3) = 0.082 0.060

Tested By Checked By

Format. No. : STH/OS/Steel /9.2C

Issue Date : 02/03/2021 Rev. No. : 00
Issue No. : 01 Rev. Date : 00
Control Copy Issued By : Technical Manager Sr. No.
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