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Composites: Part A 39 (2008) 154–163


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Improving performance of GFRP/aluminum single lap joints


using bolted/co-cured hybrid method
Ryosuke Matsuzaki a,*, Motoko Shibata b,1, Akira Todoroki b,1
a
Department of Mechanical Sciences and Engineering, Tokyo Institute of Technology, 2-12-1-I1-66, O-okayama Meguro-ku, Tokyo 152-8552, Japan
b
Department of Mechanical Sciences and Engineering, Tokyo Institute of Technology, 2-12-1-I1-58, O-okayama Meguro-ku, Tokyo 152-8552, Japan

Received 28 May 2007; received in revised form 26 October 2007; accepted 18 November 2007

Abstract

The present study proposes a bolted/co-cured hybrid joining method, and experimentally investigates the joint strength. The bolted/
co-cured hybrid joints combine co-cured adhesive joints and bolted joints without damaging reinforcing fibers. The method allows for
low scatter strength in static and fatigue loading for easily manufactured co-cured joints. Testing of the static tensile lap-shear and fatigue
strengths is performed using aluminum alloy A5052-F and knit fabric glass epoxy composites. The results show that the hybrid joints
have 1.84 times higher maximum shear strength and a quarter of the standard deviation compared with conventional co-cured joints.
Furthermore, less stress concentration and undamaged glass fibers in the hybrid joints contribute to a much higher fatigue strength than
that of the bolted joint.
Ó 2007 Elsevier Ltd. All rights reserved.

Keywords: A. Glass fibers; A. Hybrid; E. Joints/joining; Co-cure

1. Introduction design of large FRP structures are lacking because of the


complex failure modes, anisotropic properties and relative
Fiber reinforced plastic (FRP) composites are superior newness of the material compared with metals. For these
to metals in terms of specific strength and stiffness, corro- reasons, metals are still important materials especially for
sion resistance, and formability. Composite materials, large structures; large vessels are usually made of hybrid
therefore, are used for primary structures of small or structures composed of composites and metals [2]. Since
mid-sized nautical vessels [1], and aerospace structures. composite/metal hybrid structures are the key technology
Although FRP is more expensive than major metals, glass in realizing high stiffness, light weight, and high reliability,
fibers are relatively inexpensive compared with carbon and they are now seen in many structures: automotive drive
aramid fibers, so that glass fiber reinforced plastics (GFRP) shafts [3–5], headstocks of grinding machines [6], and
are widely used for vessel structures. However, since larger robotic structures [7].
vessels are subjected to larger vertical bending moments in There are two major methods for joining different mate-
a seaway, the GFRP hull girder stiffness is not sufficient in rials: mechanical fastening and adhesive bonding. Mechan-
the case of large vessels. Furthermore, design rules, empir- ical fastening using bolts or rivets is simple, and it is
ical data and simple-to-use models for optimizing the possible to obtain high joining strength with small scatter;
thereby it is widely used in metal structures. The disadvan-
tages of mechanical joints are an increase in weight of the
*
Corresponding author. Tel./fax: +81 3 5734 3184. whole structure and low sealing performance. In addition,
E-mail addresses: rmatsuza@ginza.mes.titech.ac.jp (R. Matsuzaki),
presence of the bolt holes of mechanical joints decreases the
mshibata@ginza.mes.titech.ac.jp (M. Shibata), atodorok@ginza.mes.tite-
ch.ac.jp (A. Todoroki). cross-sectional area of structures, and increases stress con-
1
Tel./fax: +81 3 5734 3178. centration. Especially in the case of the FRP structures, a

1359-835X/$ - see front matter Ó 2007 Elsevier Ltd. All rights reserved.
doi:10.1016/j.compositesa.2007.11.009
R. Matsuzaki et al. / Composites: Part A 39 (2008) 154–163 155

drilling process to fabricate bolt holes breaks reinforcing Hence, methods to increase the joint strength of co-cured
glass fibers, and causes (1) peeling of the higher plies at joints are highly sought after. Melograna and Grenestedt
the entry of the hole, (2) fiber wrenching and resin degrada- proposed perforation [25] and tongue-and-groove [26]
tion on the wall of the hole, and (3) delamination of the last methods; Matsuzaki et al. [27] proposed dimple treatment
plies in the laminate [8,9]. Since these damages can initiate for GFRP/aluminum co-cured joints. However, these
fatigue cracks, mechanical fastening in FRP structures methods require special skills to fabricate the perforation,
severely decreases fatigue strength. tongue-and-groove, and dimple, and are still affected by
Using adhesive bonding, the weight of a structure is less the adherend surface conditions.
than if mechanical joints are used. The adhesive joint has a The present study proposes a bolted/co-cured hybrid
sealing effect, no stress concentration due to bolt holes, and joining method, and experimentally investigates the joint
no damage in the FRP from the bonding process. These strength. The bolted/co-cured hybrid joints combine co-
advantages allow the adhesive joints to have high fatigue cured adhesive joints and bolted joints to realize a high
strength. In the adhesive joints, however, each adherend strength with low scatter in static and fatigue loading and
has its own suitable adhesive. The selection of adhesive is easy-to-use co-cured joints. Testing of the static tensile
difficult for joints of different materials. In addition, degre- lap-shear and fatigue strengths is performed using speci-
asing and etching are necessary in order to obtain high mens of bolted/co-cured hybrid joints between aluminum
joining strength during the general bonding process of alloy A5052-F and knit fabric glass epoxy composites.
metal adherends. Although chemical treatment brings high For comparison, co-cured joints and bolted joints are also
bonding strength, the adhesive surface would be oxidized tested.
and polluted after a few hours. The degradation of the
adhesive surface highly decreases the bonding strength 2. Bolted/co-cured hybrid joints
[10]. For these reasons, obtaining high joint strength with
low scatter is difficult for adhesive joints. A schematic illustration of the bolted/co-cured hybrid
To overcome the potential weakness of adhesive bond- joints is shown in Fig. 1. Since the proposed bolted/co-
ing, bonded/bolted hybrid joints were proposed [11–14]. cured hybrid joints are reinforced with bolt fastening,
In the hybrid joint, mechanical fastening is added to the unlike conventional co-cured joints, the static joint strength
bonded joints to improve the joining strength. Kelly may improve and the scatter in strength may decrease. Fur-
[15,16] investigated the strength and fatigue life of the thermore, the proposed method requires only one curing
bonded/bolted hybrid single lap joints with CFRP using process for the GFRP itself and the co-cure bonding. The
different modulus adhesives; the hybrid joints with lower method, therefore, has higher manufacturing efficiency
modulus adhesives allowed for load sharing between the than that of conventional bonded/bolted hybrid joints.
adhesive and the bolts, and were shown to have greater In the manufacturing of bolted/co-cured hybrid joints,
strength and fatigue life in comparison to adhesive bonded bolts are inserted in the dry (unimpregnated) glass fiber
joints. Kweon et al. [17] also investigated failure loads of composite laminate before the co-curing process. This bolt
the bonded/bolted hybrid joints between composite and inserting process utilizes the space between glass fiber bun-
aluminum; the hybrid joining improves joint strength when dles; it does not break the glass fibers, and the glass fibers
the mechanical fastening is stronger than the bonding. are continuous even around the bolt holes as shown in
However, fiber damage and delamination due to fabricat- Fig. 1. Since the clearance between the bolts and bolt holes
ing bolt holes are still problematic for the conventional is filled with excessive resin, stress concentration may
bonded/bolted hybrid joints between FRP and metals. decrease. These benefits prevent a decrease in fatigue
Another problem of the adhesive joining of FRP is that strength of the bolted/co-cured hybrid joints. In addition,
manufacturing requires curing time for the bonding process since the bolts are covered with the resins during the co-
in addition to the curing of the FRP itself. This increases curing process, the method has better sealing performance
manufacturing time and cost. In addition, since a high tem- and corrosion resistance; thus, the method is suitable for
perature for the curing process causes thermal deformation joints in vessel structures.
in the FRP at room temperature, highly accurate fit-up
between adherend components becomes difficult, especially 3. Experimental procedures
for complicated shape structures made to a recent weight
saving design. To overcome these problems, co-curing 3.1. Specimen preparation
has been developed as a joining method [18–24]. The co-
cured joint utilizes excessive resin of FRP as the adhesive, The specimens of the bolted/co-cured joints are single
so that adhesive and FRP adherend are united. Thus, both lap joints, designed based on Japanese Industrial Standards
the curing and joining process for composite structures can (JIS) K6850: testing methods for shear strength of adhesive
be achieved simultaneously. Although the reduction of bonds by tensile loading. The GFRP adherend is made
labor for the additional curing process is favorable, we can- from [(0/90)3]T laminate. The 0° direction of the GFRP is
not expect a dramatic increase of joining strength com- along the longitudinal direction of the specimen; thus the
pared with the conventional adhesively bonded joint. 90° ply is in contact with the aluminum alloy surface.
156 R. Matsuzaki et al. / Composites: Part A 39 (2008) 154–163

Fig. 1. Schematic illustration of the bolted/co-cured hybrid joint between aluminum and GFRP laminate.

The glass fibers used are knit fabric WF-800-127 made by Aluminum adherends are pre-cut prior to co-curing. The
FRP Service and Company, while the matrix is two-com- four bolts are inserted into the bolt holes of the aluminum
ponent cold setting epoxy resin Z2/H07 by Kokusai Chem- alloy adherend. The dry knit fabric glass fiber lamina is
ical Co. Ltd. Since the knit fabric GFRP has large stacked on the aluminum alloy adherend by hand lay-up;
clearance between adjacent glass fiber bundles compared here, the bolts are inserted between the nets of the fabric
with cloth fabric, adverse flexure of the glass fibers around so as not to damage glass fibers. Then, epoxy resin is
the bolt holes is suppressed as shown in Fig. 2. The metal impregnated into the glass fabric. After three sheets of glass
adherend is aluminum–magnesium alloy A5052-F. A sche- fiber fabric are laminated, a silicon sheet that has holes for
matic configuration showing the dimensions of the hybrid the bolt and nut space is placed on the specimen; a nut is
joint is illustrated in Fig. 3a: single row and double rows tightened manually just for contact (finger tightened).
of bolt specimens. Steel bolts of M2  12 mm (JIS B The specimens are then placed on an aluminum molding
1111) are used for the bolt fastening. Two pairs of bolts jig, and cured at 25 °C for 24 h and 80 °C for 2 h at a pres-
are placed at 5 (and 13 mm in double rows) from the alu- sure of 0.7 MPa in an electric oven. After the co-curing
minum adherend edge as shown in Fig. 3a so that the process, the specimens are cut into the proper size using
width-to-diameter and end distance-to-diameter are set at a diamond cutter as shown in Fig. 3a. Fig. 3b shows a pho-
2.5. The bolt holes are made using a drilling machine with tograph of a typical fabricated bolted/co-cured hybrid joint
a diameter of 1.6 mm, then the screw threads (0.4 mm specimen.
pitch) are shaved. The surfaces of the aluminum alloy To compare with joining strengths of conventional
adherend are polished using P240 waterproof abrasive joints, we also fabricated co-cured GFRP/aluminum joints
paper (JIS R 6253), and are wiped off with acetone. A without bolt fastening, and bolt fastened joints without
chemical treatment was not applied to the aluminum sur- adhesive bonding. The type and size of adherends and
face, being hardly feasible for large-scale marine structures. the bolts are the same as for the bolted/co-cured hybrid
joints.

3.2. Static tensile lap-shear tests

Static tensile lap-shear tests are carried out on the basis


of JIS K 6850 using a tensile testing machine AG-1 by Shi-
madzu Co., in order to evaluate the static strength of joints.
In the static tests, five co-cured joints, three bolted joints,
and six hybrid joints are tested. Stroke speed is 1.0 mm/
min. Strength is evaluated using maximum shear strength
Smax, given by
P max
S max ¼ ð1Þ
A
where Pmax is the maximum applied load during the test
and A is the bonded area. In general, the bearing strength
of a bolted joint is defined as the maximum load divided by
Fig. 2. Photograph showing stacking process of the bolted/co-cured the compressed area (the thickness of the joint times the
hybrid joint using knit fabric GFRP. The bolts are inserted between glass diameter of the bolted hole). For comparisons between
fiber warp and weft bundles without cutting fibers. co-cured, bolted, and bolted/co-cured hybrid joints, the
R. Matsuzaki et al. / Composites: Part A 39 (2008) 154–163 157

a GFRP Aluminum alloy

5 8 Bolt

25
5
t = 2.5 20 38
100
unit: mm

Fig. 3. Specimen of the bolted/co-cured hybrid joint between GFRP and aluminum: (a) specimen configuration (dimensions in mm) and (b) photograph
of top view.

joint strength is defined as Eq. (1) regardless of the joining 4. Results and discussion
method, in this study. The reduction in area due to the
presence of the holes is not included in the calculation of 4.1. Static tensile lap-shear tests
the joint strength.
When the adhesive failure of a bolted/co-cured hybrid First, the differences in crack arrest performance
joint occurs before reaching the maximum load, the between the bolted/co-cured hybrid joint and the co-cured
strength of adhesive failure is defined as joint were observed using two bolts at the edge of the alu-
P af minum adherend. Since translucence of the GFRP adher-
S af ¼ ð2Þ end surfaces at the bonded area turns white when the
A
crack occurs between the adherends, the progressive crack
where Paf is the applied load at the adhesive (co-cure bond- front can be observed by monitoring the GFRP surface
ing) failure. Note that the adhesive failure may include a during the tests. Fig. 4a shows the crack propagation of
small amount of cohesive failure in composites in actual the co-cured joints; the crack begins from the aluminum
tests. edge. The crack propagates toward to the GFRP edge until
the joint completely breaks. On the contrary, Fig. 4b shows
3.3. Tensile lap-shear fatigue tests the case of the bolted/co-cured joint with two bolts; it indi-
cates that when the crack from the aluminum edge pro-
Tensile lap-shear fatigue tests are performed based on gresses close to the bolts, it is arrested, probably because
JIS K 6864: test methods for fatigue properties of struc- a larger portion of the applied load is transferred to the
tural adhesives in tensile shear using MTS servo material bolts.
testing machine Model 312.21. The objective of the fatigue The crack starts again from the GFRP edges; finally
tests is to demonstrate failure trends of the bolted and adhesive failure occurs. This would suggest the presence
bolted/co-cured hybrid joints rather than the generation of the bolts in the bolted/co-cured hybrid joints contribute
of comprehensive S–N curves. The stroke frequency is to the prevention of crack propagation. In case of the four-
from 10 to 20 Hz; it was confirmed that the specimen does bolts specimen, the crack from the GFRP edges also is also
not generate excessive heat even at 20 Hz. The maximum arrested for a while.
shear stress smax and minimum stress smin are defined as Fig. 5 shows typical stress–displacement diagrams of the
maximum and minimum applied loads divided by the bolted/co-cured hybrid joint (TP2) compared with the co-
bonded area, respectively; the stress ratio (smin/smax) is con- cured joint and the bolted joint. The abscissa is crosshead
stant at 0.1 in all fatigue tests. The mean stress displacement while the ordinate is applied stress, the force
sm=(smax + smin)/2 is set to be in the range from 0.25 to divided by the bonded area.
0.5 sR where sR is the static tensile shear strength of each In the bolted joint in Fig. 5, the applied stress increases
joint obtained in the static tests. Fatigue failure is defined steadily until a maximum stress Smax of 5.96 MPa at a dis-
here as the perfect separation between two adherends. placement of 1.50 mm; the joint breaks with some steps.
158 R. Matsuzaki et al. / Composites: Part A 39 (2008) 154–163

Fig. 4. Crack propagation of GFRP/aluminum single lap joint during tensile shear tests: (a) co-cured joint and (b) bolted/co-cured hybrid joint. The solid
line shows the edges of aluminum and GFRP adherends; the dashed line shows the crack front.

Fig. 6 shows the failure surfaces of the bolted joint; the not specifically developed for bonding between composites
bearing failure in the GFRP adherend and the bolt failures and aluminum.
are observed. The bearing failure involves delamination, Fig. 7 shows the failure surfaces of the co-cured joint. A
fiber breakage, and surface splitting; most of the delamina- few glass fibers and epoxy matrix exist on the aluminum
tion spreads toward 90°, which corresponds to the fiber ori- adherend; the failure mode is a mixture of adhesive failure
entation or splitting direction of the ply contacting the and a small amount of cohesive failure of the GFRP.
aluminum adherend. Since the four bolts do not break at The bolted/co-cured hybrid joint has approximately the
the same time, the stress decreases step-by-step after the same stiffness as the co-cured joint until adhesive failure at
maximum stress corresponding to points B1, B2, and B3 a displacement of 0.554 mm and stress Saf of 3.94 MPa
in Fig. 5. (Fig. 5 C2). After the applied stress decreases sharply at
From the stress–displacement diagram of the co-cured a displacement of 0.554 mm, the stress increases again
joint in Fig. 5, the applied stress increases steadily as the though the stiffness decreases; then the joint has a maxi-
displacement increases until catastrophic joint failure mum stress Smax of 5.97 MPa at a displacement of
occurs at a displacement of 0.365 mm and stress Smax of 1.48 mm. From visual observation, the crack occurs at
2.51 MPa. There are some good adhesives that have similar the edge of aluminum adherend at point C1 in Fig. 5; the
joint strength as the bolted joints. However, the strength of crack stops at the bolt once; then the crack makes progress
the co-cured bonding is usually low because the matrix is again from the GFRP edge. The adhesive failure occurs at
R. Matsuzaki et al. / Composites: Part A 39 (2008) 154–163 159

Bolted/co-cured joint C3
6 B1
Applied stress (MPa)

C2
4
C4
Bolted joint
C1 A2
2 A1 B2 B3

Co-cured joint

0
0 0.5 1 1.5 2
Displacement (mm)

Fig. 5. Applied stress and displacement diagram of GFRP/aluminum co-


cured, bolted, bolted/co-cured hybrid joints.

Fig. 7. Failure surfaces of the GFRP/aluminum co-cured joint after static


tensile shear tests: (a) GFRP adherend and (b) aluminum adherend.

and C4) like the bolted joint. The slight difference between
stress vs displacement of bolted and hybrid joints is caused
because not all the adhesive area of the hybrid joints failed
in C2, and small amount of adhesive bonding still existed
around the bolts and failed gradually between C2 and
C3. This was observed as the stiffness decreasing between
C2 and C3. The maximum tensile shear stress of the
bolted/co-cured hybrid joint is approximately the same as
that of the bolted joint. Despite some fibers may damage
due to adhesive failure in C2, the broken fibers in the
hybrid joint do not adversely affect static strength.
Fig. 8 shows the failure surfaces of the bolted/co-cured
hybrid joint. It indicates that both bolt failure and bearing
failure with delamination and fiber breakage occur as is the
case with the bolted joint; the cohesive failure of GFRP
also occurs as with the co-cured joint. Contrary to the
bolted joint, the delamination of the hybrid joints spreads
Fig. 6. Failure surfaces of the GFRP/aluminum bolted joint after static not only along the fiber orientation (90°) but along the
tensile shear tests: (a) GFRP adherend and (b) aluminum adherend.
loading direction; this is due to the peeling stress induced
by co-cure adhesion.
point C2. After that, the bolts bear the applied stress; the Fig. 9 shows the average static tensile shear strengths
hybrid joint behaves as the bolted joint. As a consequence, Smax of co-cured, bolted/co-cured, and bolted joints as well
the progressive bolt failures are also observed (Fig. 5 C3 as the adhesive failure stress Saf of the bolted/co-cured
160 R. Matsuzaki et al. / Composites: Part A 39 (2008) 154–163

7
Smax
6

Tensile shear strength (MPa)


5

4
Saf

0
Co-cured Bolted joint
joint Bolted/co-cured
hybrid joint
Fig. 9. Average static tensile shear strengths of GFRP/aluminum co-
cured, bolted/co-cured hybrid, and bolted joints. Smax and Saf of the
hybrid joint indicate the maximum (bolt failure) and adhesive failure
strengths, respectively. The error bar indicates the standard deviations.

The reason for the large strength scatter in the co-cured


joints is that the strength is easily affected by surface (oxi-
dation, pollution, and roughness), curing (temperature,
time, and pressure) conditions, joint alignment, the overlap
length and the surplus of resin at the overlap ends. On the
other hand, the strength of the bolted joints is not affected
by such conditions, which are difficult to control, but
affected by the tightening torque, which is easily controlled.
Thereby the strength scatter of the bolted joints is smaller.
Although the adhesive failure strength of the hybrid
joints is also affected by surface and curing conditions
and has a large strength scatter, the hybrid joints bear
the applied loads as bolted joints in the final stage, and
therefore the scatter of the maximum tensile shear strength
Fig. 8. Failure surfaces of the GFRP/aluminum bolted/co-cured hybrid of the hybrid joints is as small as that of the bolted joints.
joint after static tensile shear tests: (a) GFRP adherend and (b) aluminum Considering the loss of water tightness due to the adhesive
adherend.

hybrid joints. Saf is in correspondence of the point of load 6


drop (C2) in Fig. 5. The error bars indicate the standard Bolted joint
Maximum shear stress, τmax (MPa)

deviations. As can be seen from Fig. 9, the hybrid joints Bolted/co-cured joint
have a maximum tensile shear strength Smax of 6.09 MPa 5
with a standard deviation of 0.25 MPa, similar to the
bolted joints, for which Smax is 6.21 MPa with a standard
deviation of 0.36 MPa. Compared with co-cured joints 4
(Smax is 3.37 MPa with a standard deviation of 0.86
MPa), the hybrid joints have 1.84 times higher tensile
strength and a quarter of the standard deviation. However, 3 Bolted Bolted/co-cured
the adhesive failure stress Saf (3.61 MPa with a standard
deviation of 0.89 MPa) of the hybrid joints is as small as
that of the co-cured joints. From Kelly [15], the lower mod- 2
ulus matrix of the hybrid joints may allow for more load
103 104 105 106
sharing between the adhesive and the bolts, and improve
the adhesive strength in comparison to co-cured joints. Number of cycles to failure, N (cycles)
Note that the bolt diameter was lower than the ones gener- Fig. 10. Maximum shear stress and number of cycles to failure of the
ally used in marine application, so that the joint strength GFRP/aluminum bolted and bolted/co-cured hybrid joints. The stress
may decrease in a real case. ratio R is 0.1.
R. Matsuzaki et al. / Composites: Part A 39 (2008) 154–163 161

Fig. 11. Failure surfaces of the GFRP/aluminum bolted joint after fatigue failure: (a) GFRP adherend and (b) aluminum adherend. The maximum shear
stress smax = 3.5 MPa; N = 7777 cycles.

Fig. 12. Failure surfaces of the GFRP/aluminum bolted/co-cured hybrid joint after fatigue failure: (a) GFRP adherend; (b) aluminum adherend; and (c)
side view of the aluminum adherend. The maximum shear stress smax = 4.4 MPa; N = 13547 cycles.
162 R. Matsuzaki et al. / Composites: Part A 39 (2008) 154–163

failure, the hybrid joints should be used in the stress level of joint when the final joint failure occurred. Adhesive failure
less than Saf. However, if the higher load is applied to the and shear-out failure of the GFRP are also observed.
joint, the joint does not break as catastrophic failure until Therefore, the failure mode of the bolted/co-cured hybrid
Smax, thus the method highly improves the reliability of the joints is a mixture of adhesive failure, shear-out failure
structure. and delamination between GFRP plies. Plastic deforma-
tion of the bolts is also observed for the hybrid joints,
4.2. Tensile lap-shear fatigue tests but bolt breakage does not occur, unlike for the bolted
joints. Compared with the bolted joints, the failure mode
Fig. 10 shows the S–N curves of the fatigue tests using of the hybrid joints involves a large amount of damages
bolted and bolted/co-cured hybrid joints. The abscissa is of GFRP itself. In other words, the hybrid joints survived
the logarithmic of the number of cycles, while the ordinate until the GFRP adherend failure.
is the maximum stress smax. Compared at the same maxi- Fig. 13 illustrates the failure mechanisms of the (a)
mum stress level around 3.5 MPa, the bolted joints break bolted and (b) bolted/co-cured hybrid joints. Since the
within 104 cycles (7777 cycles at 3.5 MPa), whereas the maximum stress level was higher than Saf, the debonding
bolted/co-cured hybrid joints survive more than 105 cycles between the GFRP and aluminum surfaces occurred early
(113,648 cycles at 3.66 MPa). Although comprehensive S– stage in case of the hybrid joints. However, not whole area
N curves are not obtained in Fig. 13, it can be said that of interface was debonded and GFRP still adhered to the
the bolted/co-cured hybrid joints have a higher fatigue aluminum by co-cure bonding at the fringe of the bolts.
strength than that of the bolted joints. In addition to that, since the stress level was less than the
Fig. 11 shows the failure surfaces of the bolted joints; bolt failure Smax, the fatigue loads gradually damaged the
the number of cycles to failure N is 7777, and smax is fiber and matrix around the bolts in the hybrid joints.
3.5 MPa. The failure mode of the bolted joints is a mixture The bolted joint bears the applied load at the small contact
of bolt failure and bearing failure involving delamination point of the bolt whereas the bolted/co-cured hybrid joint
and fiber breakage. On the other hand, Fig. 12 shows the bears the load by the surrounding area of the bolt owing
failure surfaces of the bolted/co-cored hybrid joints; N is to co-cure adhesion. Therefore, the adhesion reduces stress
13547 cycles, and smax is 4.4 MPa. As can be seen from concentration factors at the bolts in the hybrid joints com-
Fig. 12, one ply of GFRP laminate delaminates and sticks pared with the bolted joints; less stress concentration pre-
to the aluminum alloy surface (cohesive failure of GFRP). vents bolt failure in the hybrid joint during the fatigue
This indicates that a part of interface bonding between tests. Furthermore, delamination, resin degradation, and
GFRP and aluminum adherends still existed in the hybrid glass fiber damage occurred in the bolted joints due to

a
Bolt hole

Applied load is concentrated


at the bolt contact point.

Delamination and resin GFRP


degradation due to drilling

Load
Aluminum

Bearing failure & Bolt failure


Load

b Bolt hole

Applied load is distributed around


the bolt hole owing to adhesion.

GFRP
Bolt/hole clearance is
filled with epoxy resin.
Load
Aluminum

GFRP cohesive failure


Load

Fig. 13. Schematic illustrations of fatigue failure mechanisms: (a) bolted joints and (b) bolted/co-cured hybrid joints.
R. Matsuzaki et al. / Composites: Part A 39 (2008) 154–163 163

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