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  • Equ35-I-01 App 1 Carryover Guide

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    This document describes a carryover study to evaluate an analytical method. It involves running replicates of a low concentration sample and a high concentration sample in a specific order. The carryover is calculated and compared to an error limit based on the standard deviation of the low concentration sample results to determine if the method passes.

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    Equ35-I-01_App_1_Carryover_Guide (3)

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    This document describes a carryover study to evaluate an analytical method. It involves running replicates of a low concentration sample and a high concentration sample in a specific order. The carryover is calculated and compared to an error limit based on the standard deviation of the low concentration sample results to determine if the method passes.

    Copyright:

    © All Rights Reserved
    Download as XLS, PDF, TXT or read online from Scribd
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    23 views2 pages

    Equ35-I-01 App 1 Carryover Guide

    Uploaded by

    benchmark Innovation
    This document describes a carryover study to evaluate an analytical method. It involves running replicates of a low concentration sample and a high concentration sample in a specific order. The carryover is calculated and compared to an error limit based on the standard deviation of the low concentration sample results to determine if the method passes.

    Copyright:

    © All Rights Reserved
    Download as XLS, PDF, TXT or read online from Scribd
    Flag for inappropriate content
    of 2

    Carryover Study

    Method being evaluated:


    Analyte:
    Units: Date:
    Low Conc.: High Conc.

    • Choose a sample (H) with a very high concentration of the analyte, and a sample (L) with a very low concentration.

    • Run eleven replicates of the low sample, and ten replicates of the high sample, in the following order: Do not run any
    other samples within the series
    • A passing status is given if the Carryover is less than the Error Limit which is based upon three times the Low-Low SD.

    Sample Result Low-Low High-Low Analysis


    L1 High - Low Mean: #DIV/0!
    L2 Low - Low Mean: #DIV/0!
    L3 Carryover: #DIV/0!
    H1 Error Limit: #DIV/0!
    H2 Status: #DIV/0!
    L4
    H3
    H4
    L5
    L6
    L7
    L8
    H5
    H6
    L9
    H7
    H8
    L10
    H9
    H10
    L11
    Mean #DIV/0! #DIV/0!
    SD #DIV/0! #DIV/0!

    Comment:

    Analyst: Date:
    Accepted by: Date:

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