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Summary Report

Page 1
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

Surface Area
Single Point Surface Area at p/po=0.20000: 418.465 (m2/g)
BET Surface Area: 415.877 (m2/g)
Langmuir Surface Area: 425.420 (m2/g)
t-Plot Micropore Area: 11.017 (m2/g)
t-Plot External Surface Area: 404.860 (m2/g)
BJH Adsorption Cumulative Surface Area: 365.835 (m2/g)
BJH Desorption Cumulative Surface Area: 401.461 (m2/g)
Pore Volume
Total Pore Volume at p/p0 = 0.99000: 0.744 (cm3/g)
t-Plot Micropore Volume: 0.015 (cm3/g)
BJH Adsorption Cumulative Volume: 0.700 (cm3/g)
BJH Desorption Cumulative Volume: 0.715 (cm3/g)
DR Micropore Volume: 0.000 (cm3/g)
Pore Size
Average Pore Diameter (4V/A): 7.152 (nm)
BJH Adsorption Average Pore Diameter (4V/A): 7.651 (nm)
BJH Adsorption Most Frequent Pore Diameter (dV/dD): 8.865 (nm)
BJH Desorption Average Pore Diameter (4V/A): 7.123 (nm)
BJH Desorption Most Frequent Pore Diameter (dV/dD): 6.863 (nm)
HK/SF Micropore Analysis (< 2 nm)
Micropore Volume: 0.176 (cm3/g)
Most Frequent Pore Diameter: 1.251 (nm)
Median Pore Diameter: 0.697 (nm)

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


Isotherm Report
Page 2
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

ID p (mmHg) p/p0 V (cm3/g STP) p0 (mmHg) Time


1 7.00388060 0.00941962 69.16441 743.542 08:27:28
2 30.74915025 0.04137430 89.33609 743.194 08:35:09
3 62.52072883 0.08412817 100.98374 743.160 08:37:38
4 89.92791189 0.12101188 107.97604 743.133 08:39:47
5 117.59451705 0.15827959 114.01482 742.954 08:41:44
6 145.20008172 0.19543111 119.50178 742.973 08:43:44
7 173.20240962 0.23312066 124.77652 742.973 08:45:43
8 200.64011293 0.27009519 129.30915 742.850 08:48:35
9 227.43689102 0.30619855 134.14638 742.776 08:51:17
10 261.03968449 0.35149724 140.27018 742.651 08:53:50
11 293.55900916 0.39530898 146.64599 742.606 08:56:23
12 324.52180115 0.43707409 153.25850 742.487 08:59:03
13 354.23326296 0.47706147 159.92246 742.532 09:01:48
14 383.02911732 0.51591032 166.99308 742.434 09:04:30
15 417.97480173 0.56292042 176.79622 742.511 09:07:32
16 451.31817309 0.60783454 187.19906 742.502 09:10:44
17 483.01345105 0.65068395 198.58741 742.317 09:13:57
18 513.62526019 0.69199661 212.18388 742.237 09:17:33
19 543.44354286 0.73224443 229.50642 742.161 09:22:33
20 564.15153140 0.76029991 266.98678 742.012 09:29:48
21 574.16217287 0.77382613 326.13471 741.978 09:39:52
22 585.72934701 0.78974170 382.92808 741.672 09:52:08
23 608.61953330 0.82071948 428.66891 741.568 10:04:23
24 641.00151685 0.86472625 449.83947 741.277 10:11:44
25 677.61055479 0.91406441 463.28216 741.316 10:15:47
26 716.49335125 0.96677815 473.84653 741.115 10:18:47
27 736.46885382 0.99428016 481.87960 740.706 10:38:38
--- --- --- --- --- ---
1 736.46885382 0.99428016 481.87960 740.706 10:38:38
2 700.47022084 0.94572906 469.62807 740.667 10:45:12
3 661.70950538 0.89339994 457.65191 740.664 10:49:45
4 622.79618868 0.84105620 443.31260 740.493 10:53:16
5 585.43940465 0.79072174 434.86220 740.386 10:57:08
6 549.01348820 0.74161593 422.70631 740.294 11:02:38
7 530.53347779 0.71678730 373.09203 740.155 11:19:24
8 522.29301073 0.70622221 297.87098 739.559 11:37:47
9 513.70156081 0.69466877 232.21410 739.491 11:52:42
10 502.60745052 0.68013098 208.27876 738.986 12:07:18
11 475.78015218 0.64384055 196.76859 738.972 12:12:20
12 445.77874801 0.60329819 186.14836 738.903 12:17:13

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


Isotherm Report
Page 3
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

ID p (mmHg) p/p0 V (cm3/g STP) p0 (mmHg) Time


13 417.01341390 0.56436529 177.13087 738.907 12:21:13
14 388.12599880 0.52522060 168.93457 738.977 12:25:29
15 358.73499960 0.48552659 161.46314 738.858 12:29:02
16 328.77937580 0.44499476 154.57849 738.839 12:32:12
17 298.97635325 0.40471311 148.13491 738.737 12:35:12
18 269.41749268 0.36472123 142.19464 738.694 12:37:59
19 231.22140182 0.31301732 135.06819 738.686 12:40:55
20 196.29097753 0.26578258 128.78048 738.540 12:43:37
21 160.56702679 0.21748552 122.58835 738.288 12:46:10
22 127.83406039 0.17314923 116.21094 738.288 12:48:36

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


Isotherm Report
Page 4
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

Isotherm Plot
Adsorption Desorption
530.07

477.06

424.05
Quantity Adsorbed(cm3/g STP)

371.05

318.04

265.03

212.03

159.02

106.01

53.01

0.00
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0
p/p0

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


Isotherm Report
Page 5
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

Isotherm Log Plot


Adsorption
530.07

477.06

424.05
Quantity Adsorbed(cm3/g STP)

371.05

318.04

265.03

212.03

159.02

106.01

53.01

0.00
1e-2 1e-1
p/p0

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


BET Surface Area Report
Page 6
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

BET Surface Area Report

Single Point Surface Area at p/p0 = 0.20000: 418.46494 m2/g


BET Surface Area: 415.87692 m2/g
Slope: 0.01046
Y-Intercept: 0.00001 cm3/g STP
Vm: 95.54653 cm3/g STP
C: 1059.84170
Correlation Coefficient: 0.99963

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


BET Surface Area Report
Page 7
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

ID p/p0 V (cm3/g STP) 1/[V(Po/P-1)]


3 0.08413 100.98374 0.00091
4 0.12101 107.97604 0.00128
5 0.15828 114.01482 0.00165
6 0.19543 119.50178 0.00203
7 0.23312 124.77652 0.00244
8 0.27010 129.30915 0.00286

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


BET Surface Area Report
Page 8
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

BET Surface Area Plot


0.00315

0.00283

0.00252

0.00220

0.00189
1/[V(p0/p-1)]

0.00157

0.00126

0.00094

0.00063

0.00031

-0.00000
0.000 0.030 0.059 0.089 0.119 0.149 0.178 0.208 0.238 0.267 0.297
p/p0

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


Langmuir Surface Area Report
Page 9
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

Langmuir Surface Area Report

Langmuir Surface Area: 425.41951 m2/g


Slope: 0.01023
Y-Intercept: 0.00004 cm3/g STP
Vm: 97.73892 cm3/g STP
Correlation Coefficient: 1.00000

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


Langmuir Surface Area Report
Page 10
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

ID p/p0 V (cm3/g STP) p/p0/V


1 0.00942 69.16441 0.00014
2 0.04137 89.33609 0.00046

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


Langmuir Surface Area Report
Page 11
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

Langmuir Surface Area Plot


0.00051

0.00046

0.00041

0.00036

0.00031
p0/p/V

0.00025

0.00020

0.00015

0.00010

0.00005

0.00000
0.00 0.00 0.01 0.01 0.02 0.02 0.03 0.03 0.04 0.04 0.05
p/p0

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


t-Plot Report
Page 12
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

t-Plot Report

External Surface Area: 404.86041 m2/g


Micropore Area: 11.01651 m2/g
Micropore Volume: 0.01485 cm3/g
Slope: 261.70569
Y-Intercept: 9.59637 cm3/g STP
Correlation Coefficient: 0.99650

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


t-Plot Report
Page 13
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

ID p/p0 t (nm) V (cm3/g STP)


7 0.23312 0.43141 124.77652
8 0.27010 0.45532 129.30915
9 0.30620 0.47772 134.14638
10 0.35150 0.50584 140.27018
11 0.39531 0.53122 146.64599
12 0.43707 0.55247 153.25850
13 0.47706 0.57517 159.92246
14 0.51591 0.59953 166.99308
15 0.56292 0.63144 176.79622

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


t-Plot Report
Page 14
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

t-Plot
194.5

175.0

155.6
Quantity Adsorbed(cm3/g STP)

136.1

116.7

97.2

77.8

58.3

38.9

19.4

0.0
0.000 0.069 0.139 0.208 0.278 0.347 0.417 0.486 0.556 0.625 0.695
t (nm)

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


BJH Adsorption Pore Distribution Report
Page 15
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

Kelvin Equation
rk = -0.414/ln(P/Po)
Broekhoff-de Boer Equation
log(p/p0) = 0.1682 exp(-0.1137t) - 16.11/t^2

BJH Adsorption Pore Distribution Report

BJH Adsorption Cumulative Pore Volume: 0.69978 cm3/g


Most Frequent Pore Width (dV/dD): 8.86482 nm
Most Frequent Pore Width (dV/dlogD): 8.86482 nm
Median Pore Width: 7.65134 nm

Pore Volume Percentage Report

ID Pore Size Range Pore Volume (cm3/g) Percentage (%)


1 2.00-10.00 0.54702 78.17
2 10.00-20.00 0.12217 17.46
3 20.00-50.00 0.01827 2.61
4 >50.00 0.01233 1.76

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


BJH Adsorption Pore Distribution Report
Page 16
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

ID Pore Size Range D (nm) dV sum_dV dV/dD dV/dlogD


7 1.98-2.17 2.07 0.00265 0.00952 0.01362 0.06501
8 2.17-2.37 2.27 0.00162 0.01115 0.00833 0.04348
9 2.37-2.57 2.47 0.00392 0.01507 0.01968 0.11174
10 2.57-2.84 2.70 0.00518 0.02025 0.01926 0.11970
11 2.84-3.12 2.98 0.00784 0.02808 0.02783 0.19056
12 3.12-3.41 3.26 0.01099 0.03907 0.03766 0.28271
13 3.41-3.73 3.57 0.01031 0.04938 0.03244 0.26628
14 3.73-4.08 3.90 0.01073 0.06011 0.03036 0.27269
15 4.08-4.58 4.33 0.01552 0.07563 0.03098 0.30855
16 4.58-5.16 4.87 0.01604 0.09168 0.02763 0.30951
17 5.16-5.84 5.50 0.01781 0.10949 0.02618 0.33121
18 5.84-6.67 6.25 0.02165 0.13114 0.02622 0.37710
19 6.67-7.69 7.18 0.03148 0.16262 0.03092 0.51009
20 7.69-8.60 8.14 0.07957 0.24219 0.08674 1.62500
21 8.60-9.13 8.86 0.13402 0.37620 0.25587 5.22132
22 9.13-9.83 9.48 0.12716 0.50337 0.18175 3.96415
23 9.83-11.50 10.66 0.09894 0.60231 0.05912 1.44863
24 11.50-15.20 13.35 0.04240 0.64471 0.01147 0.35038
25 15.20-24.07 19.63 0.02419 0.66890 0.00273 0.12107
26 24.07-61.10 42.58 0.01794 0.68684 0.00048 0.04435
27 61.10-338.39 199.74 0.01294 0.69978 0.00005 0.01741

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


BJH Adsorption Pore Distribution Report
Page 17
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

BJH Adsorption Pore Size Distribution Plot (dV/dD)


0.28146

0.25331

0.22517

0.19702

0.16887
dV/dD

0.14073

0.11258

0.08444

0.05629

0.02815

0.00000
1e+0 1e+1 1e+2
D (nm)

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


BJH Adsorption Pore Distribution Report
Page 18
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

BJH Adsorption Pore Size Distribution Plot (dV/dlogD)


5.74345

5.16910

4.59476

4.02041

3.44607
dV/dlogD

2.87172

2.29738

1.72303

1.14869

0.57434

0.00000
1e+0 1e+1 1e+2
D (nm)

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


BJH Adsorption Pore Distribution Report
Page 19
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

BJH Adsorption Pore Size Distribution Plot (sum_dV)


0.76976

0.69278

0.61581

0.53883
sum_dV(cm3/g)

0.46186

0.38488

0.30790

0.23093

0.15395

0.07698

0.00000
1e+0 1e+1 1e+2
D (nm)

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


BJH Desorption Pore Distribution Report
Page 20
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

BJH Desorption Pore Distribution Report

BJH Desorption Cumulative Pore Volume: 0.71485 cm3/g


Most Frequent Pore Width (dV/dD): 6.86252 nm
Most Frequent Pore Width (dV/dlogD): 7.12874 nm
Median Pore Width: 7.12254 nm

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


BJH Desorption Pore Distribution Report
Page 21
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

ID Pore Size Range D (nm) dV sum_dV dV/dD dV/dlogD


1 338.39-37.99 188.19 0.00000 0.71485 0.00000 0.00000
2 37.99-19.33 28.66 0.01951 0.71485 0.00006 0.02055
3 19.33-12.97 16.15 0.02064 0.69534 0.00111 0.07037
4 12.97-9.87 11.42 0.02695 0.67470 0.00424 0.15555
5 9.87-7.97 8.92 0.01664 0.64774 0.00537 0.14038
6 7.97-7.26 7.61 0.02565 0.63110 0.01347 0.27572
7 7.26-7.00 7.13 0.11827 0.60545 0.16688 2.92391
8 7.00-6.73 6.86 0.18597 0.48718 0.70607 11.58849
9 6.73-6.41 6.57 0.16275 0.30121 0.60488 9.55673
10 6.41-5.72 6.07 0.05531 0.13846 0.17436 2.63688
11 5.72-5.10 5.41 0.01433 0.08315 0.02082 0.29054
12 5.10-4.60 4.85 0.01306 0.06882 0.02090 0.26004
13 4.60-4.17 4.38 0.01060 0.05576 0.02120 0.23639
14 4.17-3.80 3.99 0.00978 0.04517 0.02294 0.23145
15 3.80-3.47 3.63 0.00895 0.03539 0.02408 0.22088
16 3.47-3.18 3.32 0.00765 0.02644 0.02304 0.19267
17 3.18-2.92 3.05 0.00857 0.01879 0.02981 0.22801
18 2.92-2.61 2.76 0.00487 0.01022 0.01844 0.12934
19 2.61-2.34 2.47 0.00339 0.00535 0.01087 0.06905
20 2.34-1.87 2.10 0.00148 0.00196 0.00567 0.03227
21 1.87 1.87 --- --- --- ---

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


BJH Desorption Pore Distribution Report
Page 22
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

BJH Desorption Pore Size Distribution Plot (dV/dD)


0.77668

0.69901

0.62134

0.54367

0.46601
dV/dD

0.38834

0.31067

0.23300

0.15534

0.07767

0.00000
1e+0 1e+1 1e+2
D (nm)

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


BJH Desorption Pore Distribution Report
Page 23

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


BJH Desorption Pore Distribution Report
Page 24
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

BJH Desorption Pore Size Distribution Plot (sum_dV)


0.78634

0.70771

0.62907

0.55044
sum_dV(cm3/g)

0.47180

0.39317

0.31454

0.23590

0.15727

0.07863

0.00000
1e+0 1e+1 1e+2
D (nm)

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


DR Micropore Volume Report
Page 25
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

DR Micropore Volume Report

DR Micropore Volume: 0.00000 cm3/g


Slope: inf
Y-Intercept: -inf cm3/g STP

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


DR Micropore Volume Report
Page 26
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

ID p/p0 [lg(p0/p)]^2 V (cm3/g STP) lgV


1 0.0094196 4.10454 69.16441 1.83988
2 0.0413743 1.91343 89.33609 1.95103
3 0.0841282 1.15575 100.98374 2.00425
4 0.1210119 0.84120 107.97604 2.03333
5 0.1582796 0.64092 114.01482 2.05696
6 0.1954311 0.50269 119.50178 2.07737
7 0.2331207 0.39995 124.77652 2.09613
8 0.2700952 0.32317 129.30915 2.11163
9 0.3061985 0.26419 134.14638 2.12758
10 0.3514972 0.20619 140.27018 2.14697
11 0.3953090 0.16246 146.64599 2.16627
12 0.4370741 0.12920 153.25850 2.18542
13 0.4770615 0.10331 159.92246 2.20391
14 0.5159103 0.08261 166.99308 2.22270
15 0.5629204 0.06228 176.79622 2.24747
16 0.6078345 0.04675 187.19906 2.27230
17 0.6506839 0.03483 198.58741 2.29795
18 0.6919966 0.02557 212.18388 2.32671
19 0.7322444 0.01832 229.50642 2.36079
20 0.7602999 0.01416 266.98678 2.42649
21 0.7738261 0.01240 326.13471 2.51340
22 0.7897417 0.01051 382.92808 2.58312
23 0.8207195 0.00736 428.66891 2.63212
24 0.8647263 0.00398 449.83947 2.65306
25 0.9140644 0.00152 463.28216 2.66585
26 0.9667782 0.00022 473.84653 2.67564
27 0.9942802 0.00001 481.87960 2.68294

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


DR Micropore Volume Report
Page 27
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

DR Plot
2.951

2.656

2.361
Quantity Adsorbed(cm3/g STP)

2.066

1.771

1.476

1.180

0.885

0.590

0.295

0.000
0.000 0.451 0.903 1.354 1.806 2.257 2.709 3.160 3.612 4.063 4.515
log(p0/p)^2

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


DA Micropore Volume Report
Page 28
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

DA Equation
dV/dr = 6 * Vo * (Ks/E)^2 * r^(-7) * exp^[-(Ks/E)^2 * r^(-6)]

r(nm) dV/dr
0.40000 nan
0.45000 nan
0.50000 nan
0.55000 nan
0.60000 nan
0.65000 nan
0.70000 nan
0.75000 nan
0.80000 nan
0.85000 nan
0.90000 nan
0.95000 nan
1.00000 nan
2.00000 nan
3.00000 nan

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


MP Pore Size Distribution Report
Page 30
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

MP Pore Size Distribution Report

MP Cumulative Pore Volume: 0.00001 cm3/g


Most Frequent Pore Width: 95.54653 nm
Median Pore Width: 1059.84170 nm

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


MP Pore Size Distribution Report
Page 31
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

ID Pore Range dS dV sum_dV dV/dD


1 0-0.99055 415.71769 0.20590 0.20590 0.41572
2 0.99055-1.29775 0.10657 0.00006 0.20596 0.00005
3 1.29775-1.52304 0.03244 0.00002 0.20598 0.00002
4 1.52304-1.72716 0.02388 0.00002 0.20600 0.00001
5 1.72716-1.92624 0.00193 0.00000 0.20600 0.00000

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


MP Pore Size Distribution Report
Page 32
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

MP Pore Size Distribution Plot (dV/dD)


0.000

0.000

0.000

0.000

0.000
dV/dD

0.000

0.000

0.000

0.000

0.000

0.000
0.000 0.212 0.424 0.636 0.848 1.059 1.271 1.483 1.695 1.907 2.119
DD (nm)

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


MP Pore Size Distribution Report
Page 33
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

MP Pore Size Distribution Plot (sum_dV)


0.227

0.204

0.181

0.159
sum_dV(cm3/g)

0.136

0.113

0.091

0.068

0.045

0.023

0.000
0.000 0.212 0.424 0.636 0.848 1.059 1.271 1.483 1.695 1.907 2.119
DD (nm)

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


HK/SF Pore Size Distribution Report
Page 34
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

HK/SF Pore Size Distribution Report

HK/SF Cumulative Pore Volume (< 2 nm): 0.17638 cm3/g


Most Frequent Pore Width: 1.25084 nm
Median Pore Width: 0.69660 nm

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


HK/SF Pore Size Distribution Report
Page 35
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

ID Pore Size Range D (nm) dV sum_dV dV/dD


1 0.9325 0.10700 0.10700 0.1147488
2 1.2508 0.03121 0.13820 0.0980117
3 1.5338 0.01802 0.15622 0.0636721
4 1.7510 0.01082 0.16704 0.0498076
5 1.9657 0.00934 0.17638 0.0435247
6 2.1832 0.00849 0.18487 0.0390151
7 2.4132 0.00816 0.19303 0.0354800
8 2.6524 0.00701 0.20004 0.0293162
9 2.9030 0.00748 0.20753 0.0298633

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


HK/SF Pore Size Distribution Report
Page 36
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

HK/SF Pore Size Distribution Plot (dV/dD)


0.108

0.097

0.086

0.075

0.065
dV/dD

0.054

0.043

0.032

0.022

0.011

0.000
0.000 0.306 0.611 0.917 1.222 1.528 1.833 2.139 2.444 2.750 3.055
DD (nm)

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


HK/SF Pore Size Distribution Report
Page 37
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

HK/SF Pore Size Distribution Plot (sum_dV)


0.228

0.205

0.183

0.160
sum_dV(cm3/g)

0.137

0.114

0.091

0.068

0.046

0.023

-0.000
0.000 0.306 0.611 0.917 1.222 1.528 1.833 2.139 2.444 2.750 3.055
DD (nm)

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


DFT Pore Size Distribution Report
Page 38
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

DFT Pore Size Distribution Report

DFT Cumulative Pore Volume (< 10 nm): 0.02926 cm3/g


Most Frequent Pore Width: 0.50000 nm
Median Pore Width: 0.00000 nm

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


DFT Pore Size Distribution Report
Page 39
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

ID p/p0 V (cm3/g STP) Vcal.(cm3/g STP)


1 0.00941962 3.08770 3.41109
2 0.04137430 3.98822 3.75367
3 0.08412817 4.50820 4.13139
4 0.12101188 4.82036 4.80793
5 0.15827959 5.08995 5.36477
6 0.19543111 5.33490 5.69118
7 0.23312066 5.57038 5.94681
8 0.27009519 5.77273 6.14552
9 0.30619855 5.98868 6.31934
10 0.35149724 6.26206 6.52810
11 0.39530898 6.54670 6.75555
12 0.43707409 6.84190 7.05270
13 0.47706147 7.13940 7.49418
14 0.51591032 7.45505 7.98609
15 0.56292042 7.89269 8.38762
16 0.60783454 8.35710 8.68585
17 0.65068395 8.86551 8.98978
18 0.69199661 9.47249 9.68168

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


DFT Pore Size Distribution Report
Page 40

0.76

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


DFT Pore Size Distribution Report
Page 41
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

ID D (nm) dV sum_dV dV/dD


1 0.50000 0.01577971 0.01577971 0.31559420
2 0.59375 0.00036524 0.01614495 0.00615133
3 0.68750 0.00036285 0.01650780 0.00527785
4 0.87500 0.00036002 0.01686782 0.00411454
5 0.96875 0.00035495 0.01722277 0.00366401
6 1.06250 0.00035316 0.01757593 0.00332389
7 1.15625 0.00035133 0.01792727 0.00303856
8 1.25000 0.00034685 0.01827412 0.00277480
9 1.34375 0.00034226 0.01861638 0.00254709
10 1.43750 0.00033862 0.01895500 0.00235558
11 1.53125 0.00033475 0.01928975 0.00218614
12 1.62500 0.00032852 0.01961827 0.00202164
13 1.71875 0.00032217 0.01994044 0.00187444
14 1.81250 0.00031900 0.02025944 0.00176000
15 1.90625 0.00031552 0.02057496 0.00165518
16 2.00000 0.00031076 0.02088571 0.00155378
17 2.09375 0.00030650 0.02119221 0.00146387
18 2.18750 0.00030320 0.02149541 0.00138607
19 2.28125 0.00029846 0.02179387 0.00130832
20 2.37500 0.00029430 0.02208817 0.00123916
21 2.45000 0.00029059 0.02237876 0.00118607
22 2.56250 0.00028746 0.02266622 0.00112179
23 2.65625 0.00028392 0.02295014 0.00106887
24 2.75000 0.00028144 0.02323158 0.00102342
25 2.84375 0.00027916 0.02351074 0.00098165
26 2.93750 0.00027863 0.02378937 0.00094853
27 3.03125 0.00027805 0.02406742 0.00091728
28 3.12500 0.00027340 0.02434082 0.00087488
29 3.31250 0.00027351 0.02461433 0.00082570
30 3.50000 0.00027014 0.02488447 0.00077183
31 3.68750 0.00026746 0.02515193 0.00072532
32 3.87500 0.00026255 0.02541448 0.00067756
33 4.25000 0.00025911 0.02567360 0.00060968
34 4.62500 0.00025194 0.02592554 0.00054473
35 5.00000 0.00024065 0.02616618 0.00048129
36 5.37500 0.00023659 0.02640277 0.00044017
37 5.75000 0.00024517 0.02664795 0.00042639
38 6.12500 0.00021446 0.02686241 0.00035014
39 6.50000 0.00022641 0.02708882 0.00034832
40 6.87500 0.00024218 0.02733100 0.00035227

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


DFT Pore Size Distribution Report
Page 42
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

ID D (nm) dV sum_dV dV/dD


41 7.25000 0.00022052 0.02755152 0.00030416
42 7.62500 0.00019605 0.02774757 0.00025712
43 8.00000 0.00021141 0.02795898 0.00026426
44 8.37500 0.00023602 0.02819499 0.00028181
45 8.75000 0.00024639 0.02844138 0.00028159
46 9.12500 0.00023616 0.02867754 0.00025881
47 9.50000 0.00020566 0.02888320 0.00021648
48 9.87500 0.00018877 0.02907197 0.00019116
49 10.25000 0.00018880 0.02926077 0.00018420

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


DFT Pore Size Distribution Report
Page 43

11.27

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039


DFT Pore Size Distribution Report
Page 44
Model: BK112 Method: static volumetric method
Project: des 2021-Sample Lab. Sample: PT5%_SBA15
Adsorbate: N2 Charge Number: #1
Bath Temperature: 77.35 K Sample Weight: 0.0338(g)
Operator: Degas Conditions: 300
Started: 2021-12-24 08:00:17 Completed: 2021-12-24 12:58:24

DFT Pore Size Distribution Plot (sum_dV)


0.03219

0.02897

0.02575

0.02253
sum_dV(cm3/g)

0.01931

0.01609

0.01287

0.00966

0.00644

0.00322

0.00000
0.00 1.13 2.25 3.38 4.51 5.64 6.76 7.89 9.02 10.15 11.27
D (nm)

Beijing JWGB Sci. and Tech. Co., Ltd. Tel: 400-600-5039

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