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ORIGINAL ARTICLE
ABSTRACT that the MMEs that are reported from the calc-alkaline to felsic
Mafic microgranular enclaves (MMEs) and Syn-plutonic dykes intrusives are the product of the magma mixing and mingling processes
(SPD) are commonly observed in granitoids and are believed to (Perugini et al. 2003; Jayananda et al. 2009).
have a similar period of origin as that of the host. Here the MMEs and SPD are reported from many EDC granitic plutons,
petrographical and mineralogical characteristics of the MMEs and which compositionally exhibit mafic to intermediate hybrid magma
Syn-plutonic dykes from Sircilla granite pluton (SGP), eastern composition and occur at various stages of felsic magma chamber
Dharwar craton (EDC), Southern India is presented. The contact evolution (Jayananda et al. 2014). In the present work, a comprehensive
relationships of MMEs with the host granite are diffusive or mineral chemistry of host granite, MMEs, and SPD are provided to
gradational, implying under-cooling and disaggregation of MMEs. estimate the physicochemical conditions, oxygen fugacity (fO2), and
Petrographic features such as quartz ocelli, bladed biotite, and petrogenesis.
acicular apatite grains in mafic enclaves suggest magma mixing/
mingling-related processes. Consequently, crystallization GEOLOGICAL SETTING
temperature and pressure of hornblende and biotite from SPD The Dharwar craton is divided into two broad tectonic domains
indicate rapid undercooling and hence suggest their emplacement (Fig. 1a), namely the western Dharwar craton (WDC) and the eastern
towards the final stage of pluton evolution. Mineral chemistry Dharwar craton (EDC), depending on crustal thickness, metamorphic
studies reveal that the plagioclase in host SGP compositionally grade, and geochronological data. The two blocks are separated by
varies from An 23 -An 27, while the Fe# in biotite vary from 0.47- the Chitradurga shear zone (Ramakrishnan, and Vaidyanadhan, 2008;
0.52. The composition of plagioclase and mafic phases in MMEs Chardon et al., 2011). The WDC comprises tonalite–trondhjemite–
and the SPDs exhibit variation in compositional range, plagioclase granodiorite (TTG) (3.45 to 3.23 Ga) suites (Guitreau et al. 2017) in
(An 26 -An 30), hornblende Mg# (0.42-0.55), and biotite Fe# (0.46- association with a wide range of greenstone belts (3400 to 2700 Ma)
0.54). A decreasing trend in fO2 value in MMEs and SPD during (Maya et al. 2017). The EDC is defined by widespread late Archaean
progressive crystallization suggest an orogenic tectonic setting of tonalitic to granodioritic gneisses and calc-alkaline granite plutons
magma formation. Intermediate composition of biotite and (Peucat et al. 2013) interlayered with ca. 2700 Ma narrow greenstone
plagioclase from MMEs suggest control of magma mixing processes belts and carries tracks of older (3140 to 3000 Ma) crust (Peucat et al.
for their formation. 2013; Dey et al. 2018; Jayananda et al. 2019). The Neoarchean
magmatism of EDC is characterized by NS to NNW trending calc-
INTRODUCTION alkaline plutons consisting of TTG gneisses, biotite granites, and syn-
Mafic microgranular enclaves (MME) and syn-plutonic dykes to late-kinematic high-Mg diorites or sanukitoids (Jayananda et al.
(SPD) are associated with the granite plutons (Ahmad 2011; Jayananda 2019).
et al. 2014; Elangovan et al. 2017) and are believed to have a similar The northern part of EDC is mainly composed of tonalitic to
age as that of their host rocks. During their ascent from the deeper granodioritic gneisses with age from 2.7 Ga – 2.54 Ga and N-S trending
crustal sources, the mafic and the felsic components mix at various 2.57 Ga-2.52 Ga calc-alkaline plutonic belts, which are likely to be
stages of their compositional evolution. Magma mixing represents associated with the Karimnagar granulite belt (KGB). The KGB
mixing of melts from two or more different sources, having different corresponds to the zone of accumulation of several smaller granitic
temperatures, density, crystallinity, viscosity, and rheological behavior plutons that run along the NW- SE trending Pranahita-Godavari rift
(Perugini and Poli 2012). Consequently, the study of felsic and mafic basin (Fig. 1b). The lithology of KGB granitoid plutons are akin to
rocks can contribute valuable information on the petrogenesis, physical EDC granitoids, which represents that KGB is a part of the EDC. The
and chemical environments of magma mixing in relation to KGB is typically made of granite gneiss, charnockites, and calc-alkaline
temperature, pressure, and oxygen fugacity (Barbarin 2005; Kocak et granites. These constitute the supra crustal rocks as enclaves include
al. 2011; Azadbakht et al. 2020). Most of the previous studies show charnockite-enderbite gneiss, amphibolite, banded magnetite quartzite
Fig.2. (a) Sub-rounded shaped MME associated with host granite; (b) A disrupted syn-plutonic dyke exhibiting gradational to diffusive contact
with host granite; (c) Amphibolite supra crustal rock occur as enclave associated with Sircilla granite pluton (SGP).
due to the dissolution of pre-existing crystals in the host granite due (Supplementary Table 2 and Fig. 4a). In addition, the host granite
to the high temperature of the injected mafic magmas and the contains some K-feldspar, and it falls in the orthoclase field (Fig. 4a).
subsequent abrupt cooling, which results in the development of The plagioclase composition from MMEs and SPDs vary from
amphibole and biotite (Hibbard 1991; Vernon 1991; Baxter 2002). Ab73-67–An28-26–Or5-0.5 to Ab69-72–An30-25–Or2.8-0.2, respectively. The
The presence of poikilitic quartz in hornblende, biotite, and plagioclase plagioclase from the host granite has Ab 76-72–An27-23–Or 1.2-0.6.
in MME, as well as SPDs, is most likely the consequence of injected Amphiboles are only observed in the MMEs and SPD and not in
mafic magmas acquiring early crystallized quartz (Jayananda et al. the host. Amphibole and biotite structural formula calculated based
2014). The unusual bladed biotite morphology, which is highly on 23 and 11 oxygen per atom respectively are provided in
elongated in one direction, is observed from MMEs and SPD supplementary tables 3 and 4. A comparison between Na+K+Ca (apfu)
(Fig. 3a). Bladed biotite provides evidence for physically constrained and Si (apfu) indicates that amphiboles are plotted in the igneous field
rapid development in undercooled conditions (Hibbard 1981; Jeen et (Sial et al. 1998). Amphiboles from the enclaves varies distinctly
al. 2002). Acicular and stubby apatite crystals are abundant in the (Fig. 4b) from magnesian hornblende to Tschermak-Pargasite (Leake
MME and SPD, while apatite in felsic hosts has mainly a stubby et al. 1997, 2004), whereas amphiboles from the SPD show Mg-
habit (Fig. 3c). It forms rapidly in a quenched mixing environment hornblende composition (Fig. 4c).
(Hibbard 1991; Kumar 1995). Although biotite grains from all three lithologies fall in the Mg-
biotite field of (Fig. 4d) (Foster, 1960), biotites from granite and SPD
METHODOLOGY form clusters at the lower and upper ends, respectively, and biotites
Polished thin sections were obtained for the petrographic from MMEs are scattered in between the two ends. Particularly, biotites
characterization and microprobe analytical investigations. Mineral from the syn-plutonic dykes are more Mg-rich than the host granite,
chemistry was determined using Cameca SX-100 electron microprobe and the biotite composition from MME fall in between them. The Fe#
equipment equipped with wavelength-dispersive spectrometers at a for biotites from the host granite varies from 0.43-0.60, whereas it
voltage of 15 kV and a current of 20 nA. Standards include a variety varies from 0.4-0.44 and 0.43-0.50 for SPDs and MMEs, respectively.
of natural minerals and oxides. The electron microprobe analyses of Biotites from the syn-plutonic dykes and host granite are plotted in
plagioclase, amphibole and biotite from the selected MME, SPD the “re-equilibrated biotite” field in Fig. 4e (Nachit et al. 2005), whereas
and host samples were carried out at CSIR-National Geophysical biotites from MMEs fall in the primary as well as in the reequilibrated
Research Institute, Hyderabad. fields. Nachit et al. (2005), demonstrated that only primary biotites
can be used to determine the temperature, pressure, and fugacity change
MINERAL CHEMISTRY during magmatic evolution. The reequilibrated and neo form (or
The plagioclase feldspar from the host granite (syeno-monzo secondary) biotites show modification due to post magmatic events
granite), MMEs (granodiorite), and syn-plutonic dykes (quartz diorite) and hydrothermal events, respectively, and hence can’t be used for the
have compositional variation from oligoclase to andesine purposes as mentioned above. However, they also showed that
Fig.4. (a) Classification diagram of Or-Ab-An for the plagioclase from granite, mafic magmatic enclave, and syn-plutonic dyke; (b) Si (apfu) vs
Na+Ca+K (apfu) defines classification of amphibole in MME and syn-plutonic dyke; (c) Si (apfu) vs Mg/Mg+Fe2+ diagram showing classification
of hornblende from the MME and syn-plutonic dyke; (d) (AlVI + Fe3+ Ti)-Mg-(Fe2+ + Mn) ternary compositional variation diagram of biotite
from Sircilla granite pluton (SGP) rock types.A, phlogopite; B, Mg-biotite; C, Fe+2 biotite; D, siderophyllites and lepidomelane; (e) TiO2-FeOt-
MgO triangular diagram of SGP biotites explains primary and re-equilibrated conditions; (f) MgO-FeO-Al2O3 discrimination-plot displays
biotites from the SGP rock types are formed within the calc-alkaline magmatism.
Fig.5. (a) Binary log fO2 vs temperature diagram for amphibole revel the MMEs and syn-plutonic dyke are formed under NNO buffer(Ridolfi et
al. 2010); (b) The temperature versus fO2 discrimination diagram (Wones 1972, 1980) for magmatic biotites explains that SGP rock types are
formed under the NNO buffer; (c) An (mol%)versus Ab (mol%) diagram indicating a magma mixing in the SGP; (d) Na + K vs. Aliv diagram
showing substitutions between pargasite (Prg) and hornblende (Hbl), and Ed: Edenite (Hterenbn et al. 1974).