All units mentioned in this file in (%Wt).

The uncertainty calculations using top down approach have been done within the laboratory du
within the laboratory during (Period) to (Periood).
 Reference TOTL-SP07-F02

Office Egypt
ISO / IEC 17025 Form Issue n° 00
Clause 7.2 & 7.6 Date 1-Apr-19
Selection, verification and validation of methods Author / Approver M. Saleh / M. Abd Elrazek
and measurement uncertainty

Analysis Uncertainty Calculations

Test Metod: ISO 20483 : 2013 Test Name: Crude Protein in Cereals and Pulses

Month Week Range 1 Range 2 Name P.T Results P.TActual Value Bias values
8.43 11.72 9.49 9.77 0.279999999999999
8.56 11.94 9.44 9.77 0.33
8.46 11.77
8.61 11.91
B1Sep-22 3rd week 8.51 11.86 Bahaa Eldin Mohamed

8.49 11.78
8.46 11.75
8.52 11.91
8.44 11.85
8.55 11.79 9.46 9.77 0.309999999999999
8.54 11.91 9.5 9.77 0.27
8.49 11.77
8.43 11.72
B1Oct-22 1 st week 8.51 11.86 M.A
8.47 11.91
8.55 11.89
8.45 11.77
8.62 11.90
8.51 11.86 9.5 9.77 0.27
8.49 11.78 9.45 9.77 0.32
8.46 11.75
8.52 11.91
B1Oct-22 2nd week 8.44 11.84 Bahaa Eldin Mohamed
8.55 11.78
8.54 11.91
8.49 11.77
8.43 11.72
8.51 11.86 9.44 9.77 0.33
8.47 11.92 9.46 9.77 0.31
8.55 11.89
8.46 11.72
B1Oct-22 2nd week 8.62 11.88 M.A
8.53 11.92
8.49 11.89
8.46 11.77
8.52 11.90
8.42 11.86 9.5 9.77 0.27
8.58 11.78 9.45 9.77 0.32
8.46 11.75
B1Oct-22 3rd week 8.62 11.91 Bahaa Eldin Mohamed
8.51 11.84
8.49 11.79
8.49 11.91
8.52 11.76
8.44 11.72 9.46 9.77 0.309999999999999
8.55 11.86 9.5 9.77 0.27
8.53 11.92
B1Oct-22 4th week 8.49 11.86 M.A
8.43 11.78
8.51 11.75
8.47 11.91
8.39 11.74
Mean 8.5005769231 11.831153846 9.47083333333 9.77 0.33
SD 0.0541390172 0.0709502407 0.02503028469 0.0250302846870577
SD^2 0.0029310332 0.0050339367 0.00062651515
RSD 0.0063688639 0.0059968995 0.00264288092 0.0026428809172432
RSD % 0.6368863864 0.5996899508 0.26428809172 0.264288091724323
Ustd %(max) 0.6368863864
Bias 0.33
Bias % 3.3776867963
U Certificate 0.32
(U(cref))% 1.6376663255
(RSD/√n)^2 0.07629
Ubias% 3.7545358928
Uc% 3.8081706947
(U)exp 7.6163413894

((U)exp)2 58.008656159