Ab

Munshiganj, Bangladesh

HPLC Column Requisition List

Project Name of Stage Test Name Column Brand Name Manufacturer Packing/Phase Length (mm) Dia (mm) P. Size (µ)

Intermediate Purity

In Process Purity Xterra MS Waters L1 250 4.6 5

AZD
Impurities
Finished
Assay Asahipak ODP-50 Shodex L67 250 4.6 5

Intermediate-1 Purity

Intermediate-3 Purity ZORBAX RX-C8 Agilent L7 250 4.6 5

In Process-1 Purity

ASC In Process-2 Purity Synergi Polar-RP Phenomenex L11 250 4.6 4

Enantiomeric Purity CHIRALPAK AD Daicel Chiral Technologies L51 250 4.6 5

Finished Impurities Synergi Polar-RP Phenomenex L11 250 4.6 4

Assay ZORBAX RX-C8 Agilent L7 250 4.6 5

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 Ab
Munshiganj, Bangladesh

HPLC Column Requisition List

Project Name of Stage Test Name Column Brand Name Manufacturer Packing/Phase Length (mm) Dia (mm) P. Size (µ)

Intermediate Purity Inertsil ODS-3 GL Science L1 150 3 3

In Process Purity Inertsil ODS-3 GL Science L1 150 3 3

Enantiomeric Purity CHIRALCEL OJ-RH Daicel Chiral Technologies L107 150 4.6 5
RSC
Impurity L InertSustain C8 GL Science L7 150 4.6 2.7
Finished
Impurities Inertsil ODS-3 GL Science L1 150 3 3

Assay Inertsil ODS-3 GL Science L1 150 3 3

Intermediate-1 Purity Hypersil BDS Thermo Scientific L1 100 4.6 3

Intermediate-2 Purity Hypersil BDS Thermo Scientific L1 100 4.6 3

In Process-1 Purity Hypersil BDS Thermo Scientific L1 100 4.6 3

DMM
In Process-2 Purity Hypersil BDS Thermo Scientific L1 100 4.6 3

Intermediate-3 Purity Hypersil BDS Thermo Scientific L1 100 4.6 3

Finished Impurities Hypersil BDS Thermo Scientific L1 100 4.6 3

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 Ab
Munshiganj, Bangladesh

GC Column Requisition List

Name of Column Film
Project Test Name Manufacturer Composition Length (m) Dia (mm)
Stage Brand Name thickness (µ)
Residual Mid-polar 6% cyanopropyl/phenyl, 94%
DB-624 Agilent 30 0.53 3
Solvent polydimethylsiloxane
AZD Finished
DMF
DB-WAX Agilent High-polarity, polyethylene glycol (PEG) 30 0.25 0.25
Content
Nonpolar and low-bleed,
Intermediate-2 Purity DB-1 Agilent 30 0.32 1
100%Dimethylpolysiloxane
ASC
Residual Mid-polar 6% cyanopropyl/phenyl, 94%
Finished DB-624 Agilent 30 0.53 3
Solvent polydimethylsiloxane
Residual Mid-polar 6% cyanopropyl/phenyl, 94%
RSC Finished DB-624 Agilent 30 0.53 3
Solvent polydimethylsiloxane
Residual Mid-polar 6% cyanopropyl/phenyl, 94%
DB-624 Agilent 30 0.53 3
Solvent polydimethylsiloxane
DMM Finished
Acetic Acid DB-WAX Agilent High-polarity, polyethylene glycol (PEG) 30 0.25 0.25

Name Designation Signature Date

Prepared by Mohammad Nur Sharif Senior Executive, ARD
Reviewed by Md. Tarikul Islam Tuhin Deputy Manager, QC
Reviewed by Md. Asanul Haque Manager, R&D

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