Document No.

SPC-UTE-20-115-003

Sheet 1 of 6

TITLE SHOP PAINTING SPECIFICATION

CAKASA
CLIENT
(NIG.) COMPANY LTD

SPHERE 8.180 M³
PROJECT
STOCKGAP FUELS

ORDER 8776F dtd 30/01/2020

2 18/05/20 Revised where indicated UTE UTE DTO

1 12/05/20 Revised where indicated UTE UTE DTO

0 25/03/20 Issued for approval UTE UTE DTO

REV DATE DESCRIPTION COMP. CONT. APPR.

 Document No.
SPC-UTE-20-115-003
SHOP PAINTING SPECIFICATION
SPHERE 8.180 M³
Sheet 2 of 6

INDEX

1. SCOPE ...................................................................................................................................................................................... 3

2. GENERAL INFORMATION........................................................................................................................................................ 3

3. REFERENCE DOCUMENTS AND STANDARDS ..................................................................................................................... 3

4. SHOP PAINTING ....................................................................................................................................................................... 3

5. REPORTING.............................................................................................................................................................................. 6

6. ATTACHMENTS ........................................................................................................................................................................ 6
 Document No.
SPC-UTE-20-115-003
SHOP PAINTING SPECIFICATION
SPHERE 8.180 M³
Sheet 3 of 6

1. SCOPE

This specification describes the methods to be followed for shop surface preparation and shop paint application for site
assembled LPG storage sphere TK-G03 for STOCKGAP Terminal at Rumuolumeni, Nigeria.

MAX SPHERE
GEOMETRIC SPHERE AUXILIARY STEEL FIRE FIGHTING
OPERATING EXTERNAL
ITEM CAPACITY INSULATION INTERNAL STRUCTURES SYSTEMS
TEMP. (°C) SURFACES
(MC) PAINTING TREATMENT TREATMENT
PAINTING
TK-G03 50 8181 No Inorganic Primer Inorganic Primer Inorganic Primer Hot Dip Galvanized

2. GENERAL INFORMATION

Before starting activities, a brief procedure with the method statement of how-to-do the job with particular care about safety
and pollution will be issued.

3. REFERENCE DOCUMENTS AND STANDARDS

• ISO 2409 – Paints And Varnishes – Cross-Cut Test

• ISO 2808 - Paints And Varnishes – Determination Of Film Thickness

• ISO 8501 – Preparation Of Steel Substrates Before Application Of Paints And Related Products – Visual
Assessment Of Surface Cleanliness

• ISO 8502– Preparation Of Steel Substrates Before Application Of Paints And Related Products – Test For
Assessment Of Surface Cleanliness

• ISO 8503– Preparation Of Steel Substrates Before Application Of Paints And Related Products –Surface
Roughness Characteristics Of Blast-Cleaned Steel Substrates

• ISO 19840 – Paints And Varnishes – Corrosion Protection Of Steel Structures By Protective Paint Systems

• ISO 1461 - Hot dip galvanized coatings on fabricated iron and steel articles — Specifications and test methods

4. SHOP PAINTING

4.1. SURFACE PREPARATION

The metallic surface to be protected by paint shall comply with ISO 8501-3 grade P2 (steel preparation).
Before starting any de-rusting operation or painting application, the surface shall be cleaned from grease, oil and dirt.
These matters shall be removed according to SSPC SP6.
Abrasive containing silica sand or free silica and copper slag are not allowed. Abrasive shall contain a maximum quantity of
salts corresponding to 25 ppm of chlorides.
Steel grit for carbon steel shall be used (see attachments 2).
Areas which are blast cleaned but not painted (all plates edges)will be protected with adhesive tape 5 cm wide.
 Document No.
SPC-UTE-20-115-003
SHOP PAINTING SPECIFICATION
SPHERE 8.180 M³
Sheet 4 of 6

4.2. PAINT APPLICATION

The painting shall be carried out in accordance with ISO 8502-4 and the following conditions:

• Air temperature: 5 ÷ 40 °C Min value of 10 °C for two components catalyses paints;

• Air relative humidity: ≤ 85%. Min value of 50% for zinc primer application;

• Steel temperature: at least 3 °C above the dew point temperature of the surrounding air.

Temperature and humidity shall be continuously monitored.

Painting shall not be carried out under the rain or in a misty atmosphere or in presence of dew and on moist surfaces.
The surface painted shall be protected by: rain, condensation, dust, salts and pollution during both application and curing.
The minimum dry film thickness shall suit to the requested value.
Additional coats shall be applied when the request value is not obtained.
The maximum dry film thickness shall suit to the value indicated in the technical data sheet of the product.
Dry film thickness higher than the max allowed by technical data sheet shall be repaired as per paint manufacturer
recommendation.
Paint application shall be performed within 4 hours from surface preparation and before any visible rusting occurs.
Application method shall be as indicated on product technical datasheet.
The stripe coating shall be applied for each layer on all critical area (e.g. welds, angles, corners, bolt, holes, etc).

2 4.3. SHOP PAINTING SYSTEMS

List of items to be painted:

PAINTING SURFACE PRODUCT TO BE FINAL APPLICATION

SYSTEM SURFACES PREPARATION APPLIED AND COLOUR
No. (ISO 8501 - 1) THICKNESS (RAL)
Workshop
Primer: Interzinc 22 -
inorganic zinc primer
Manufacturer
1 All External Surfaces of Sphere Sa 2.5 (or equivalent)
Std
1x70 µm
Workshop
Hot dip galvanized as per
Gratings
2 - ISO 1461 -
Fire-fighting system

Primer: Interzinc 22 - Site

All Internal Surfaces of Sphere inorganic zinc primer
Manufacturer
3 All External surfaces of auxiliary Sa 2.5 (or equivalent)
Std
steel structures
1x70 µm
 Document No.
SPC-UTE-20-115-003
SHOP PAINTING SPECIFICATION
SPHERE 8.180 M³
Sheet 5 of 6

4.4. SHOP INSPECTION AND TESTING

Testing and inspections will be carried out during production, in accordance with the following table.
Before all activities a visual check for presence of grease, oils and contaminants shall be carried out.
Paint which has coagulated or otherwise deteriorated during storage shall not be used.

Test Type Method Frequency Acceptance Criteria Consequence

Visual ISO8501-3 Defects to be
100% of all surfaces As per grade P2
examination Grade P2 repaired

ISO 8502-4
Ambient and steel Before start of each shift and In accordance para. 3 & 4
Environmental Neither blasting
temperature min. twice per shift during and with products data
Conditions nor coating
Relative Humidity blasting, painting and curing sheets
Dew point

ISO 8501-1 100% visual of all surfaces Sa 2 ½ Reblasting

Cleanliness Re-cleaning and
ISO 8502-3 2/3 check per day of production Rating 2 retesting until
acceptable
Roughness ISO 8503-1/2/4 2/3 check per day of production Segment 2 Reblasting

Max conductivity Recleaning and

Salt test ISO 8502-6 1 check per day of production corresponding to 50 mg/m2 retesting until
NaCl acceptable

Dust test ISO 8502-3 Per each piece Grade 2 Cleaning

Visual to determine:
Curing
Visual Contaminations
examination of Solvent retention 100% of surface after each coat No defect Repair of defects
coating Pinholes/popping
Sagging
Surface defects
- Arithmetic mean of DFTs
not less than specified
Per each peace for plates (NDFT) Repair, additional
Film thickness ISO 19840 Per lot for auxiliary structures - No single DFT less than coats or recoating
and accessories 80% of NDFT as appropriate
- Max DFT as indicated by
Paint Manufacturer
One per painting system per day
(or lot) of production to be
carried out, after curing, on Coating to be
Adhesion test ISO 2409 Segment 1
reference panel blasted and rejected
coated at the same time and
condition than item
 Document No.
SPC-UTE-20-115-003
SHOP PAINTING SPECIFICATION
SPHERE 8.180 M³
Sheet 6 of 6

5. REPORTING

The painting activity reporting will be made up of all Painting Application Reports (Attachment 1).

6. ATTACHMENTS

1- Sample of Paint Application Report (1 sheet)

2- Abrasive Product GH050 data sheet certified by Wheelabrator Allevard Co. (1 sheet ) used for shop activities

3- INTERNATIONAL Interzinc 22 data sheet (4 sheets)

 Rapporto N. / Report N.

Foglio / Sheet Segue / Follow

Rapporto Controllo del Trattamento Protettivo giornaliero

Report Daily Check of Protective Treatment

Cliente / Customer Progetto / Project Comm. / Job .

Disegno / Drawing Procedura / Procedure P.C.Q. / I.T.P.

e
Serbatoio / Tank :
Componente/ Component :

Richiesto Prodotti Controllato

Condizioni amb. / Environ. conditions

Ispezione visiva
Sabbiatura
Rugosità
/ Visual examination

/ Sandblasting

/ Roughness

Contaminazione da sali / salt test

pl Required
Iso 8502-4
Iso 8501-3
Iso 8501-1 & 8502-3
ASTM D4417 Method C
Iso 8502-6 & 9
Product Checked
m
Contaminazione abrasivo /
ASTM D4940
Abrasive contamination
1° mano sp./ 1° coat thk

2° mano sp./ 2° coat thk

3° mano sp./ 3° coat thk

Ispezione visiva trattamento /
Visual examination of coating
Spessore umido / Wet film thk ASTM D1212
Sa

Spessore / Film thk SSPC-PA2

Discontinuità / Holiday test ASTM D5162
Test di aderenza / adhesion test ASTM D4541

Risultato Dell’ispezione  Conforme  Non Conforme

Result of Inspection Conforme Not Conforme

Ispettore /
Eseguito / Performed Controllato / Checked Cliente / Customer
Inspector

Firma / Sign. Firma / Sign. Firma / Sign. Firma / Sign.

Data / Date Data / Date Data / Date Data / Date

Mod.PRS-028/3
.

TECHNICAL DATA SHEET

Version : 4 Date : 6/11/2000 Page : 1

PRODUCT : GH050

SHAPE : GRIT

GRADING CHEMICAL COMPOSITION

SIEVES SPECIFICATIONS ELEMENT CONTENT (%)

SPECIFICATIONS % TOTAL REJECTED Min Max
N° Openning Min Max C 0,800 1,200
(mm)

20 0,850 TP Si 0,400 1,200

25 0,710 10 Mn 0,600 1,000

30 0,600 S 0,050

35 0,500 P 0,050

40 0,425
HARDNESS
45 0,355 80 UNIT HV1 HRC

50 0,300 90 Min 840,0 65,2

80 0,180 Max

Deviation
DENSITY ( g/cm3 )

Min Max SHAPE FACTOR

SPECIFICATION 7,60 _ METHODE

BULK % MIN good shape

MICROSTRUCTURE

MARTENSITE
FINE AND HOMOGENEOUS

Etablished by : RQ Approved by : CV
PHILIPPE SERT
Interzinc® 22
Inorganic Zinc-Rich Silicate
PRODUCT Part of the Interzinc 22 Series of products.
DESCRIPTION
A two component, rapid recoat, fast curing solvent based inorganic zinc rich ethyl silicate primer, containing 85% zinc
by weight in the dry film. Conforms to SSPC Paint 20 Level 1.

Available in ASTM D520, Type II (low lead) zinc dust version as standard

INTENDED USES A zinc rich primer suitable for use with a wide range of high performance systems and topcoats in both maintenance
and new construction of bridges, tanks, pipework, offshore structures and structural steelwork. Interzinc 22 can also
be used as tank coating suitable for the carriage of different chemical cargoes (e.g. styrene) according to
International Paint’s chemical resistance guide.

Provides excellent corrosion protection for correctly prepared steel substrates, up to temperatures of 1004°F (540°C)
when suitably topcoated.

Fast curing primer capable of application in a wide range of climatic conditions.

PRACTICAL Color Green Gray

INFORMATION FOR
INTERZINC 22 Gloss Level Matte

Volume Solids 63%

Typical Thickness 2-3 mils (50-75 microns) dry equivalent to 3.2-4.8 mils (79-119 microns) wet

Theoretical Coverage 337 sq.ft/US gallon at 3 mils d.f.t and stated volume solids
8.40 m²/liter at 75 microns d.f.t and stated volume solids
Practical Coverage Allow appropriate loss factors

Method of Application Airless Spray, Air Spray

Drying Time
Overcoating Interval with
recommended topcoats
Temperature Touch Dry Hard Dry Minimum Maximum

41°F (5°C) 30 minutes 3 hours 18 hours Extended¹

59°F (15°C) 20 minutes 90 minutes 9 hours Extended¹
77°F (25°C) 10 minutes 1 hour 4.5 hours Extended¹
104°F (40°C) 5 minutes 30 minutes 1.5 hours Extended¹

¹ See International Protective Coatings Definitions & Abbreviations

The drying times quoted have been determined at the quoted temperature and 55% relative humidity. The 41°F
(5°C) time was determined at 60% relative humidity. Prior to overcoating, verify a value of 4 via ASTM D4752
MEK rub test. See Product Characteristics section for more details on overcoating.

REGULATORY DATA Flash Point (Typical) Part A 66°F (19°C); Mixed 66°F (19°C)
Product Weight 20.4 Ib/gal (2.44 kg/l)

VOC 3.92 lb/gal (470 g/lt) EPA Method 24

216 g/kg EU Solvent Emissions Directive
(Council Directive 1999/13/EC)

See Product Characteristics section for further details

Protective Coatings Worldwide Product

Page 1 of 4
Issue Date:11/23/2016
Ref:4518
Interzinc® 22
Inorganic Zinc-Rich Silicate
SURFACE All surfaces to be coated should be clean, dry and free from contamination. Prior to paint application, all surfaces
PREPARATION should be assessed and treated in accordance with ISO 8504:2000. Oil or grease should be removed in accordance
with SSPC-SP1 solvent cleaning.
Abrasive Blast Cleaning
Abrasive blast clean to a minimum of SSPC-SP6 or Sa2½ (ISO 8501-1:2007), (or SSPC-SP10 for optimum
performance). If oxidation has occurred between blasting and application of Interzinc 22, the surface should be
reblasted to the specified visual standard.
Surface defects revealed by the blast cleaning process, should be ground, filled, or treated in the appropriate
manner.
A surface profile of 1.6-3.0 mils (40-75 microns) is recommended.
Shop Primed Steelwork
Interzinc 22 is suitable for application to unweathered steelwork freshly coated with zinc silicate shop primers. If the
zinc shop primer shows extensive or widely scattered breakdown, or excessive zinc corrosion products, overall
sweep blasting will be necessary. Other types of shop primer are not suitable for overcoating and will require
complete removal by abrasive blast cleaning.
Weld seams and damaged areas should be blast cleaned to SSPC-SP6 or Sa2½ (ISO 8501-1:2007).
Damaged/Repair Areas
All damaged areas should ideally be blast cleaned to SSPC SP6 or Sa2½ (ISO 8501:2007). However, it is
acceptable that small areas can be power tool cleaned to SSPC SP11 or Pt3 (JSRA SPSS:1984), provided the area
is not polished. Repair of the damaged area can then be carried out using a recommended zinc epoxy primer -
consult International Protective Coatings for specific advice.

APPLICATION Mixing Interzinc 22 is supplied in two parts, a liquid Binder base component QHA285 (Part A) and a
Powder component (Part B). The Powder (Part B) should be slowly added to the liquid Binder
(Part A) whilst stirring with a mechanical agitator. DO NOT ADD LIQUID TO POWDER. Material
should be filtered prior to application and should be constantly agitated in the pot during
spraying. Once the unit has been mixed it should be used within the working pot life specified.
Mix Ratio 3.1 part(s) : 1 part(s) by volume
Mix ratio is given for advice; always mix the product in the proportions supplied.

Working Pot Life 41°F (5°C) 59°F (15°C) 77°F (25°C) 104°F (40°C)
12 hours 8 hours 4 hours 2 hours

Airless Spray Recommended Tip Range 15-21 thou (0.38-0.53 mm)

Total output fluid pressure at spray tip not less than 1593 psi
(112 kg/cm²)

Air Spray Recommended Typical pump Graco X-Treme 40:1 or similar

(Pressure Pot) Gun DeVilbiss MBC-510/JGA-510 (Binks 2100)
Air Cap 704 or 765 (Binks 66SD or 68PB)
Fluid Tip E (1.8mm or D (2.2mm) or Binks 66,67

Brush Suitable - Small areas only Typically 1.0-2.0 mils (25-50 microns) can be achieved

Roller Not recommended

Thinner International GTA803, As regionally available. Do not thin more than allowed by local
International GTA415 or environmental legislation
International GTA138
Cleaner International GTA803, As regionally available.
International GTA138 or
International GTA415
Work Stoppages Do not allow material to remain in hoses, guns or spray equipment. Thoroughly flush all
equipment with International GTA803/International GTA415 /International GTA138. Once units
of paint have been mixed they should not be resealed and it is advised that after prolonged
stoppages work recommences with freshly mixed units.

Clean Up Clean all equipment immediately after use with International GTA803/International
GTA415/International GTA138. It is good working practice to periodically flush out spray
equipment during the course of the working day. Frequency of cleaning will depend upon
amount sprayed, temperature and elapsed time, including any delays.
All surplus materials and empty containers should be disposed of in accordance with
appropriate regional regulations/legislation.

Page 2 of 4
Interzinc® 22
Inorganic Zinc-Rich Silicate
PRODUCT Prior to overcoating, Interzinc 22 must be clean, dry and free from both soluble salts and excessive zinc corrosion
CHARACTERISTICS products.
Surface temperature must always be a minimum of 5°F (3°C) above dew point.
When applying Interzinc 22 in confined spaces, ensure adequate ventilation.
The minimum overcoating interval is dependent upon the relative humidity during cure.
If thinning is required to assist spray application in warmer climates, (typically >82°F (28°C)), it is recommended that
International GTA803 thinners are used.
It is recommended that prior to overcoating a solvent rub test to ASTM D4752 should be undertaken. A value of 4
indicates a satisfactory degree of cure for overcoating purposes.
At relative humidities below 55%, curing will be retarded. Humidity may be increased by the use of steam or water
spraying. However, cure at relative humidities below 55% is more effectively achieved by incorporating the Low
Humidity Cure Accelerator*; some example overcoating times at 59ºF (15ºC) are detailed below;
Relative Humidity (%) 20 30 40
Minimum Overcoating Interval 24 hours 10 hours 10 hours
The Interzinc 22 Application Guidelines contain further information on expected cure times at lower relative
humidities.
Excessive film thickness and/or over-application of Interzinc 22 can lead to mudcracking, which will require complete
removal of the affected areas by abrasive blasting and re-application in accordance with the original specification.

Care should be exercised to avoid the application of dry film thicknesses in excess of 5.0 mils (125 microns).

For high temperature systems the thickness of Interzinc 22 should be restricted to 2 mils (50 microns) d.f.t.
Continuous dry temperature resistance of Interzinc 22 is 752°F (400°C) if left untopcoated, however, if this product is
used as a primer for Intertherm 50, the dry temperature resistance will be 1004°F (540°C).

Untopcoated Interzinc 22 is not suitable for exposure in acid or alkaline conditions or continuous water immersion.

This product has the following specification approvals:

• AISC Specification 348-04 Research Council for Structural Connections Class B Coating
• UNE 48293 (Spain)

Note: VOC values are typical and are provided for guidance purpose only. These may be subject to variation
depending on factors such as differences in color and normal manufacturing tolerances.

Low molecular weight reactive additives, which will form part of the film during normal ambient cure conditions, will
also affect VOC values determined using EPA Method 24.

*Only available in Europe, China, Middle East, Africa and Russia.

SYSTEMS When it is necessary for Interzinc 22 is to be overcoated by itself due to low dry film thickness the coating surface
COMPATIBILITY must be fresh and unweathered. A minimum of 2 mils (50 microns) d.f.t. of any subsequent coat of Interzinc 22 is
needed to ensure good film formation.
Before overcoating with recommended topcoats ensure the Interzinc 22 is fully cured (see above) and if weathering
has occurred all zinc salts should be removed from the surface by fresh water washing, and if necessary scrubbing
with bristle brushes.
Typical topcoats and intermediates are:
Intercure 200 Intergard 475HS
Intercure 420 Intertherm 50
Intergard 251 Interseal 670HS
Intergard 269 Intertherm 715
Intergard 345
In some cases it may be necessary to apply a mist coat of suitable viscosity to minimize bubbling. This will depend
upon the age of the Interzinc 22, surface roughness and ambient conditions during curing and application.
Alternatively, an epoxy sealer coat, such as Intergard 269, can be used to reduce bubbling problems.
For other suitable topcoats/intermediates, consult International Protective Coatings.

Page 3 of 4
 Interzinc® 22
Inorganic Zinc-Rich Silicate
D ADDITIONAL Further information regarding industry standards, terms and abbreviations used in this data sheet can be found in the
following documents available at www.international-pc.com:
et INFORMATION
ai • Definitions & Abbreviations
l
T • Surface Preparation
o • Paint Application
p
• Theoretical & Practical Coverage

• Interzinc 22 Application Guidelines

Individual copies of these information sections are available upon request.

SAFETY This product is intended for use only by professional applicators in industrial situations in accordance with the advice
PRECAUTIONS given on this sheet, the Material Safety Data Sheet and the container(s), and should not be used without reference to
the Material Safety Data Sheet (MSDS) which International Protective Coatings has provided to its customers.

All work involving the application and use of this product should be performed in compliance with all relevant
national, Health, Safety & Environmental standards and regulations.

In the event welding or flame cutting is performed on metal coated with this product, dust and fumes will be emitted
which will require the use of appropriate personal protective equipment and adequate local exhaust ventilation.

If in doubt regarding the suitability of use of this product, consult International Protective Coatings for further advice.

Rect Top
PACK SIZE Unit Size Part A Part B
Vol Pack Vol Pack
13.78 liter 10.42 liter 15 liter 3.36 liter 20 liter
5 US gal 3.78 US gal 5 US gal 1.22 US gal 5 US gal

For availability of other pack sizes contact International Protective Coatings

SHIPPING WEIGHT Unit Size Part A Part B

(TYPICAL) 13.78 liter 11.6 kg 25.8 kg
5 US gal 34.4 lb 72.4 lb

STORAGE Shelf Life Part A 6 months minimum at 77°F (25°C).

Part B 12 months minimum at 77°F (25°C).
Subject to re-inspection thereafter. Store in dry, shaded conditions away from sources
of heat and ignition.

Rect
Bottom
Disclaimer
The information in this data sheet is not intended to be exhaustive; any person using the product for any purpose other than that specifically recommended in this data sheet without first
obtaining written confirmation from us as to the suitability of the product for the intended purpose does so at their own risk. All advice given or statements made about the product (whether in
this data sheet or otherwise) is correct to the best of our knowledge but we have no control over the quality or the condition of the substrate or the many factors affecting the use and application
of the product. Therefore, unless we specifically agree in writing to do so, we do not accept any liability at all for the performance of the product or for (subject to the maximum extent permitted
by law) any loss or damage arising out of the use of the product. We hereby disclaim any warranties or representations, express or implied, by operation of law or otherwise, including, without
limitation, any implied warranty of merchantability or fitness for a particular purpose. All products supplied and technical advice given are subject to our Conditions of Sale. You should request
a copy of this document and review it carefully. The information contained in this data sheet is liable to modification from time to time in the light of experience and our policy of continuous
development. It is the user's responsibility to check with their local representative that this data sheet is current prior to using the product.

This Technical Data Sheet is available on our website at www.international-marine.com or www.international-pc.com, and should be the same as this document. Should there be any
discrepancies between this document and the version of the Technical Data Sheet that appears on the website, then the version on the website will take precedence.

Copyright © AkzoNobel, 11/23/2016.

All trademarks mentioned in this publication are owned by, or licensed to, the AkzoNobel group of companies.

www.international-pc.com

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