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Keywords: This paper investigated the experimental study on the axial compressive behavior of glass fiber-reinforced
Glass fiber-reinforced polymer (GFRP) polymer (GFRP)-confined concrete, including cement-based seawater coral aggregate concrete (CAC) and slag-
Alkali-activated seawater coral aggregate based alkali-activated seawater coral aggregate concrete (AACAC). The axial compression characteristics of
concrete (AACAC)
the CAC and AACAC cylinders wrapped with different GFRP layers (i.e., 0, 2, 4, and 6 layers) were tested and
Axial compressive behavior
Ultimate strength model
analyzed. Experimental results showed that both CAC and AACAC specimens had a fairly similar failure pattern.
The ultimate strain increment ratios are significantly higher than the ultimate strength ones, and AACAC
exhibited a higher strain enhancement ratio than CAC. Moreover, the ultimate strength and axial strain gradually
improved as the thickness of FRP increased. Approximately 2.88- and 5.79-times improvements in the ultimate
axial strain were observed for the 6-ply CAC and AACAC specimens, respectively, compared with their un-
confined companions, demonstrating that FRP jackets can effectively improve the axial deformation capacity
of concrete cylinders. Additionally, experimental results were compared with some representative empirical
models and then preliminary ultimate strength and strain models were proposed for GFRP-confined CAC and
AACAC.
* Corresponding author.
E-mail addresses: 220201322@seu.edu.cn (F. Li), baizhang1120@126.com (B. Zhang), alice_zhuhong@seu.edu.cn (H. Zhu).
https://doi.org/10.1016/j.conbuildmat.2022.128437
Received 19 February 2022; Received in revised form 12 June 2022; Accepted 7 July 2022
Available online 28 July 2022
0950-0618/© 2022 Elsevier Ltd. All rights reserved.
F. Li et al. Construction and Building Materials 347 (2022) 128437
the marine environment, demonstrating its promising applications for 2. Raw materials
marine engineering constructions. However, the current investigation is
less involved in the utilization of AAMs or geopolymer binders in marine 2.1. GFRP sheets
concrete construction [19,20]. Therefore, more research is worth con
ducting to promote the development of marine concrete structures. The adopted glass fiber-reinforced polymer (GFRP) sheets used for
Fiber-reinforced polymer (FRP) is widely regarded as a high- concrete wrapping were manufactured by the fiber winding process in a
performance material, characterized by enhanced mechanical proper bidirectional direction, as shown in Fig. 1(a). The GFRP sheet has a
ties, including high strength-to-weight ratio and superior durability nominal thickness of 0.200 mm. In terms of the GFRP sheet, the polymer
performance, which can be introduced to prevent corrosion issues of matrix used was epoxy impregnation resin and the tensile strength,
traditional steel bars [21–23]. The external FRP jacket/tube confine elasticity modulus, and ultimate tensile strain provided by the manu
ment for concrete has been actively researched and currently become facturer were 85 MPa, 3.5 GPa, and 3.5%, respectively.
one of the mainstream FRP applications. The mechanism of FRP The GFRP sheets were tested using a flat coupon sample following
confinement is that the FRP confinement of the passive type provides ASTM D3039/D3039M [35] to obtain the tensile ultimate strength, ul
increasing pressure as a result of the lateral expansion of concrete under timate strain, and elastic modulus. The GFRP tensile coupons with 25
compression. With FRP confinement, it shows that the strength and mm width and 250 mm length were prepared and the loading speed was
deformability of confined concrete can be greatly enhanced due to the 1.5 mm/min. To avoid premature failure of the coupon ends during the
good confinement efficiency of FRP jackets [24,25]. Currently, re test, two pairs of customized aluminum gripping pieces were used. The
searches on the FRP-confined NAC have been well documented [26–28]. tested results of GFRP sheets are shown in Table 1.
In addition, the performance of FRP-confined recycled aggregate con
crete (RAC) with circular and square cross-sections was compared by Xie
and Ozbakkaloglu [29]; Tang and Li et al. [30,31] investigated the 2.2. Alkali-activated materials (AAMs) and OPC
compressive behavior of sustainable geopolymeric RAC confined by
carbon fiber-reinforced polymer (CFRP) jackets. It was concluded that The used precursor materials were comprised of ground blast furnace
the compressive strength and ultimate strain of geopolymer concrete slag (GBFS), fly ash (FA), and silica fume (SF), with a weight ratio of
were remarkably enhanced by CFRP confinement. Little information has 80:15:5, based on our previous optimization study [36]. Grade 42.5
been concerned about the study of the FRP-confined CAC [32–34], ordinary Portland cement (OPC) was also prepared as the control
especially those prepared by AAMs or geopolymer binders. It should be mixture to replace the ground blast furnace slag (GBFS). The chemical
pointed out that, no study has been carried out to investigate the compositions of the unreacted GBFS, FA, SF, and OPC were detected by
behavior of FRP-confined CAC incorporating slag-based alkali-activated X-ray fluorescence (XRF) and the results are summarized in Table 2.
materials, to the best knowledge of the authors. According to the analysis, the unreacted OPC contained a relatively
Therefore, this study conducted an experimental investigation, as lower Al/Si ratio and a higher Ca/Si ratio compared to the GBFS, which
well as a theoretical analysis of GFRP-confined CAC and AACAC. Axial makes it one of the reasons for the differences in the hydration pro
compressive behavior was investigated. Additionally, four different duction of pastes [5].
thicknesses of GFRP jackets, (i.e., 0, 2, 4, and 6 layers) were selected to The pre-prepared artificial seawater, anhydrous NaOH flakes, and
assess the effectiveness of the FRP confinement on cylinder specimens of
CAC and AACAC. Finally, based on the test results, some typical models Table 1
to predict the ultimate condition of FRP-confined concrete were selected The physical and tensile properties of GFRP sheets.
and compared with the proposed models of GFRP-confined CAC and Type of Nominal Ultimate Elastic Ultimate
AACAC. FRP sheet thickness strength ffrp modulus Efrp strain εfrp (%)
(mm) (MPa) (GPa)
2
F. Li et al. Construction and Building Materials 347 (2022) 128437
Table 2
The SF, FA, GBFS, and OPC chemical compositions detected by XRF (wt. %).
Material Chemical composition
SiO2 CaO Al2O3 TiO2 Fe2O3 SO3 P2O5 MnO MgO Na2O K2 O
SF 95.41 0.456 0.485 0.004 0.837 0.149 0.102 0.021 0.066 0.448 1.68
FA 50.94 4.05 34.18 1.48 0.747 0.811 0.265 0.033 4.79 0.838 1.67
GBFS 29.86 40.48 15.5 1.78 9.02 1.53 0.026 0.491 0.401 0.510 0.365
OPC 21.08 60.2 7.1 0.374 2.11 3.85 0.17 0.15 3.45 0.214 1.16
instant dissolved Na2SiO3 powder with a modulus of 2.85 (59.6 wt% procedure was conducted in line with the Chinese code (GB/T 50081-
SiO2, 21.6 wt% Na2O) were incorporated to make an alkali activator (Ms 2019) [39]. The tested results of CAC and AACAC are summarized in
= SiO2/Na2O = 2.85). The detailed chemical composition of seawater is Table 5. The slumps of CAC and AACAC were 60 mm and 158 mm,
detailed in Table 3. It is noted that the corporation of seawater will exert respectively. The possible reason why AACAC achieved a higher slump
a beneficial effect on the hydration reaction due to the existence of than CAC may be the higher water absorption of OPC than slag material.
inorganic salts (e.g., NaCl and CaCl2) compared to fresh water [5,37]. It can be observed that AACAC achieved a higher splitting tensile
The required activator solution finally achieved a modulus of 1.2, strength (ft) and elastic modulus (Ec) compared to those of CAC. Also,
adjusted by adding anhydrous NaOH flakes to the Na2SiO3 solution. The the calculated flexural-to-compressive ratios (ft/fcu) are 0.076 for CAC
alkaline content (Na2O-to-binder ratio by mass) of 4% was also ach and 0.08 for AACAC respectively with the discrepancy within 5%,
ieved. It is worth noting that half of the total water content was showing trivial differences.
consumed in preparation of the alkali activator. The detailed procedure
for making an activator solution can be found in our previous study [15]. 3. Experimental program
The coral aggregates used herein to prepare the CAC and AACAC are A total of 18 GFRP-confined concrete cylinders, as well as 6 un-
the same as used in the authors’ previous papers [38], which contained confined specimens, were prepared for the axial compressive test, as
two categories: coral sand (CS) and coral coarse aggregate (CCA), as listed in Table 6. Two different concrete types including CAC and
shown in Fig. 1(b and c). They were sourced from the South China Sea AACAC were cast. The height of the cylinders is 300 mm and the
island and their basic properties and grading curves are provided in diameter of the cylinder section is 150 mm. The number of layers of
Table 4 and Fig. 2, respectively. The continuously graded coral coarse GFRP in each concrete type consists of 0-layer, 2-layer, 4-layer, and 6-
aggregate had a maximum particle size of 25 mm, and coral sand had a layer, respectively, and each series contains three identical specimens.
fineness modulus of 2.63. It is noticeable that the coral aggregates All plain specimens were taken out from the curing room after 28
possessed high void content and crush index value, and had a rough and days for the purpose of GFRP wrapping and the detailed procedure of
porous surface, which are reasons for an increase in binder content and GFRP-confined cylinder specimens is as follows, as also illustrated in
water consumption in concrete preparation. Fig. 4. Firstly, all plain specimens were cleaned with alcohol, and then
wrapped with 300 mm-length GFRP sheet along the hoop direction of
2.4. Concrete mix proportion the cylinders using the wet lay-up procedure. It is worth noting that the
epoxy impregnation resin was chosen as an adhesive and an overlap
According to our previous study [38], it was determined that the length of 150 mm was performed to give a better wrapping effect.
adopted mixtures for CAC and AACAC had a total water-to-binder ratio Subsequently, excessive resin and air bubbles were eliminated by roll
of 0.60, a total cementitious material content of 500 kg⋅m− 3, and a ing. Afterward, the two ends of confined specimens were wrapped in a
volume sand rate of 55%. It is important to note that all mixtures had the two-layer GFRP sheet with 30-mm width to avoid premature end failure.
same net water-to-binder ratio of 0.3 and half of the seawater is used in
pre-soaking coral aggregates, and the other half is used for preparing the 3.2. Axial compression test
alkaline solution or mixing CAC. The mixture proportions and basic
properties for CAC and AACAC are detailed in Table 5. All the compression cylinder specimens were tested by a 1000 kN
For the preparation of AACAC specimens, the mixing process is servo-hydraulic universal testing machine to conduct the axial
summarized as follows: 1) dry-mix the coral coarse aggregate and coral compressive tests after the GFRP-wrapped cylinders were cured for 14
sand for 2 min; 2) dump half of the total seawater into the coral ag days under the laboratory environment. The loading rate for all speci
gregates and blend them for 3 min for coral pre-wetting; 3) pour the mens was 0.5 mm/min with displacement control under axial
precursor materials (i.e., GBFS, FA, and SF) into the mixed materials and compression, referring to the AS 1012.9:2014 specification [40]. A force
blend them adequately for 2 min; 4) put the activator liquid into the transducer was used in the machine to capture the applied load. The
mixtures and stir them for 3 min, as illustrated in Fig. 3. applied loading procedure was terminated when the axial stress dropped
The compressive strength (fcu) and splitting tensile strength (ft) were to approximately 60% of the axial compressive strength. In the middle
determined by 150 mm × 150 mm × 150 mm concrete cubic specimens. zone of the tested specimens, two linear variable displacement trans
Prism specimens (150 mm × 150 mm × 300 mm) were also prepared to ducers (LVDTs) mounted on a customized cage were placed covering a
obtain the elastic modulus (Ec) of CAC and AACAC. The specimens were height of 150 mm, as shown in Fig. 5. Moreover, the axial strains of the
taken out from the molds and cured at 25 ± 5◦ C one day after casting. specimens were collected by two strain gauges with a 80 mm length
When the samples reached the preset curing age (i.e. 28 d), the testing located at the middle height of the FRP jacket, and the hoop strains were
measured by two horizontally arranged strain gauges with a 50 mm
length, as shown in Fig. 5.
Table 3
Chemical composition required for seawater preparation (g/L).
NaCl MgCl2 Na2SO4 CaCl2 KBr KCl NaHCo3
3
F. Li et al. Construction and Building Materials 347 (2022) 128437
Table 4
Basic properties of the coral sand (CS) and coral coarse aggregate (CCA).
Aggregate Bulk density (kg⋅m− 3) Apparent density (kg⋅m− 3) 1 h Water absorption (%) Crush index (%) Void content (%) Fineness modulus (Mx)
As shown in Fig. 6a) and e), the plain concrete cylinder specimens
reach the failure as a result of the occurrence of a main diagonal crack
and soon lost load capacity after hitting the peak load. As for the GFRP-
confined specimens, all of them failed when the rupture of the GFRP
jacket happened under transverse tension. Moreover, the location of FRP
rupture for three different thickness specimens was quite similar, char
acterized by the rupture along the axial direction from the mid-height to
the end or through both ends as a result of a bidirectional GFRP sheet.
Table 5
Mixture proportions and mechanical properties of CAC and AACAC.
Concrete type Mix proportion (kg/m3) Ec (×104N/mm2) ft (MPa) fcu (MPa) Slump (mm)
4
F. Li et al. Construction and Building Materials 347 (2022) 128437
Table 6
Axial compression results of GFRP-confined CAC and AACAC specimens.
Specimen Concrete type Number of FRP plies fco or fcc (MPa) εco or εcc εh,rup fcc/fco εcc/εco
Ind. Avg. Ind. Avg. Ind. Avg.
Note: “Ind.” and “Avg.” are the individual value and average value of three identical specimens for each series, respectively. The test data of specimen CAC-P2-S3 was
lost due to a malfunction of the testing machine during the test.
rapidly after the peak stress due to the propagation of diagonal crack and specimens showed three obvious stages: linear ascending stage, hard
spalling of surface concrete, presenting poor ductility of the un-confined ening stage, and descending stage. At the initial stage, the axial stress
specimens. Overall, the curves of the un-confined specimens were and strain showed linear growth and then the confined specimens
characterized by two-stage: linear ascending stage and descending stage. experienced a hardening stage from the inflection point, the strain value
While for the GFRP-confined specimens, the peak stress was clearly of which was approximately equal to the ultimate axial strain of the un-
improved as well as the corresponding strain. The curves of the confined confined specimen (εco), demonstrating that FRP confinement mainly
5
F. Li et al. Construction and Building Materials 347 (2022) 128437
Fig. 7. Tested axial stress-strain curves of GFRP-confined CAC and AACAC specimens.
6
F. Li et al. Construction and Building Materials 347 (2022) 128437
Fig. 8. Axial stress to hoop strain relationship curves of GFRP-confined CAC and AACAC specimens.
Fig. 9. Tested axial-hoop strain relationship curves of GFRP-confined CAC and AACAC specimens.
specimen AACAC-P6 had a larger second stage slope than that of the concrete and non-uniformly circumferential strain distribution in the
AACAC-P4, leading to a larger hoop rupture strain than other specimens. FRP composites [24].
This may be associated with the non-uniformly transverse expansion of
Fig. 10. Tested axial compressive strength and corresponding axial strain:(a) axial compressive strength;(b) ultimate axial strain.
7
F. Li et al. Construction and Building Materials 347 (2022) 128437
4.3. Axial compressive strength and ultimate axial strain 4.4. Ultimate strength and strain models for GFRP-confined CAC and
AACAC
The axial compressive strength and ultimate axial strain of CAC and
AACAC specimens are presented in Fig. 10, and the effect of the number Currently, the modeling of the ultimate strength and strain of FRP-
of layers on axial compressive behavior is shown in Fig. 11 and Fig. 12. A confined concrete under axial compression has been actively under
detailed comparison and discussion of the tested results are conducted in taken and some of these empirical models [32,44–47] are selected, as
this section. shown in Table 7. The FRP thickness and the FRP rupture strain affect
As can be seen from Fig. 10(a), the axial compressive strength of CAC the effectiveness of FRP confinement, which can be characterized by the
and AACAC was gradually improved with the increase of GFRP thick actual confining pressure (fl ), as expressed in Eq.(1).
ness. It can be concluded from Fig. 10 that both CAC and AACAC can be
2Efrp tfrp εh,rup εh,rup
adequately confined by the FRP sheet. As is shown in Fig. 10(a), CAC and fl = , kε = (1)
D εfrp
AACAC specimens with 6-ply FRP jackets gained approximately 1.63-
and 1.39-times enhancement (fcc/fco) in ultimate strength respectively
where Efrp and tfrp are the elastic modulus and the thickness of the FRP
compared with the un-confined specimens. And differences in fcc/fco
jacket, respectively; D is the diameter of the cylinders; εh,rup and εfrp are
between CAC and AACAC became more pronounced as the number of
the hoop rupture strain and ultimate strain of the FRP jacket obtained
layers increased (see Fig. 11(b)). The CAC specimens achieved a higher
from the coupon test, respectively; and kε is the hoop strain reduction
fcc/fco than that of the AACAC specimens because of a relatively higher
factor.
axial compressive strength (fco) of AACAC under the same cube
The FRP hoop rupture strains of GFRP-confined CAC and AACAC
compressive strength (fcu). This may be attributed to the AAMs char
specimens are shown in Table 8. Table 8 shows that there was an overall
acterized by a denser interfacial transition zone between the paste ma
increase in average hoop rupture strain when the number of layers
trix and the aggregates than OPC [5]. These improved microstructures
increased both for CAC and AACAC specimens, but the average rupture
help improve the porosity of coral aggregates and delay the propagation
strain was not significantly affected by the layers and concrete type,
of the cracks inside the specimens under compressive stress. However,
which is in line with previous studies [26,47,48]. In this study, the
the gap in axial compressive strength between CAC and AACAC became
average hoop rupture strain of 0.0038 was used in Eq.(1) for further
smaller with the thickness of GFRP increased (see Fig. 11).
analysis.
As is shown in Fig. 10(b), the specimens were under a three-
In general, the ultimate strength and ultimate strain models for FRP-
dimensional state of stress due to the confinement of the GFRP jacket,
confined concrete can be respectively expressed as [47]:
and the peak axial strain was significantly improved. CAC and AACAC
specimens with 6-ply FRP jackets gained approximately 2.88- and 5.79- fcc fl
= 1 + k1 ( )m (2)
times enhancements (εcc/εco) respectively in deformation capacity fco fco
compared with the un-confined specimens. Compared with the strength
enhancement ratio (fcc/fco), the ultimate strain enhancement ratio (εcc/ εcc fl
= 1 + k2 ( )p (3)
εco) was relatively distinct ranging from 1.39 to 5.79, especially for εco fco
AACAC specimens, indicating that wrapping FRP jackets can effectively
where the k1, k2, m, and p are fitting factors that can be obtained by
improve the axial deformation capacity. It can be seen that the ultimate
regression analysis.
axial strain between the CAC and AACAC exerted a tiny difference for 0-
To determine the suitability of the existing models for the tested
ply and 2-ply FRP confinement, and the differences became progres
results of GFRP-confined CAC and AACAC specimens, six ultimate
sively apparent from 2-ply onwards. Overall, a greater ultimate strain
strength and strain models that can provide accurate predictions for
enhancement (εcc/εco) was observed in AACAC compared to CAC, as
FRP-confined NAC [44–47], CAC [32], and geopolymer concrete [31]
illustrated by 5.79 for AACAC and 2.88 for CAC under 6-ply
are selected, as plotted in Fig. 13. It is noticeable that both the strength
confinement.
enhancement ratio (fcc/fco) and strain enhancement ratio (εcc/εco) were
Overall, the axial compressive behavior is affected by the type of
basically in direct proportion to the confinement ratio (fl/fco). As the fl/
concrete, with AACAC exhibiting a similar strength enhancement ratio
fco ratio was aggrandized, the fcc/fco and εcc/εco ratios were gradually
and a higher strain enhancement ratio than CAC.
increased. It can be seen from Fig. 11 that the selected models cannot
predict well both the ultimate strength and stain of FRP-confined
AACAC. Teng’s model can produce good values in the strain
Fig. 11. Effect of the number of FRP layers on axial compressive strength of CAC and AACAC specimens.
8
F. Li et al. Construction and Building Materials 347 (2022) 128437
Fig. 12. Effect of the number of FRP layers on the ultimate axial strain of CAC and AACAC specimens.
9
F. Li et al. Construction and Building Materials 347 (2022) 128437
Fig. 13. Relationship of fcc/fco and εcc/εco with fl/fco with different empirical models.
Table 9
The accuracy of the proposed model in the ultimate compressive strength and ultimate axial strain.
Specimen fcc(MPa) Test (fcc/fco) Calculation (fcc/fco) Δ(%) Test (εcc/εco) Calculation (εcc/εco) Δ(%)
Note: fco represents the ultimate compressive strength of the un-confined specimens; εco means the ultimate axial strain of the un-confined specimens corresponding to
fco; The symbol ‘‘Δ” means the deviation.
Fig. 14. Performance of proposed model in predicting the ultimate compressive strength and ultimate axial strain of CAC and AACAC specimens.
2.88- and 5.79-times improvements in the ultimate axial strain concrete, with AACAC exhibiting a similar strength enhancement
were observed for the 6-ply CAC and AACAC specimens, ratio (fcc/fco) but a higher strain enhancement ratio (εcc/εco) than
respectively, compared with their un-confined companions, CAC.
demonstrating that FRP jackets can effectively improve the axial (3) It shows that there was an overall increase in average hoop
deformation capacity. There was an increase of about 63% and rupture strain (εh,rup) when the number of layers increased both
39% for 6-ply CAC and AACAC in the ultimate strength. It is for CAC and AACAC specimens, but the average rupture strain
noticeable that the stress-strain behavior is affected by the type of
10
F. Li et al. Construction and Building Materials 347 (2022) 128437
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