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The characterisation of unsaturated intermediate and coarse-grained soils faces some practical
difficulties because undisturbed sampling is not easy. Geophysical methods provide useful information
as they can be applied on site for testing geo-materials in their natural state. Moreover their repeated
application over time is effective and efficient for monitoring purposes. A procedure for evaluating
porosity and degree of saturation on the basis of electrical resistivity and wave velocities measure-
ments is proposed. The approach is based on an electro-seismic model that utilises Archie’s law to
describe the electrical behaviour of soils and a recent formulation of elastic wave propagation in
unsaturated soils. The proposed procedure is applied to laboratory data, and shows promising results.
KEYWORDS: geophysics; laboratory tests; partial saturation; suction; waves and wave loading
278
COSENTINI AND FOTI 279
seismic and electrical resistivity measurements. The pro- change with respect to a change in matric suction; Kw and
posed electro-seismic model is based on a simplified formu- Ka are the bulk moduli of water and air respectively; rs , rw
lation of wave propagation in unsaturated soils proposed by and ra are the densities of the solid phase, water phase and
Conte et al. (2009) and on the Archie’s law (Archie, 1942) air phase respectively. The low frequency assumption is
that links electrical resistivity of soil with porosity, degree of justified by the relatively low operational frequency of
saturation and electrical resistivity of the fluid. The model is seismic sources used for geophysical tests.
applied to laboratory data to check its applicability. The coefficient of volume change for the water phase
(mw2 ) can be obtained experimentally from the water reten-
tion curve. The water volume content can be described
DESCRIPTION OF THE PROPOSED MODEL analytically by van Genuchten’s equation (van Genuchten,
Theoretical background 1980)
Wave velocities (VP and VS ) and electrical resistivity (r) in
soils depend to a varying degree on porosity, saturation, (Łsat Łr )
Ł ¼ S r ¼ þ Łr (4)
fabric, stress, mineralogy, pore fluid and temperature (Mavko ½1 þ (Æł)n m
et al., 1998; Santamarina et al., 2001; Mitchell & Soga,
2005). An electro-seismic model is a system of equations where Łr and Łsat are residual and saturated values of the
that links some hydrological and mechanical parameters of volumetric water content Ł; ł is the matric suction; Æ, n
soil to geophysical parameters. For example, Carrara et al. and m are experimental parameters.
(1994) proposed a model based on the scheme of a rock The coefficient mw can be evaluated by deriving
2
mass as a polycomponent medium made up of matrix, clay, equation (4)
water and air. Their model was based on the time-average
model proposed by Wyllie et al. (1956) for seismic velocity @Ł n m Æ(Æł)n1
and the model of parallel resistors proposed by Patnode & mw
2 ¼ ¼ (Łsat Łr ) (5)
@ł ½1 þ (Æł)n mþ1
Wyllie (1950) for electrical resistivity.
The model proposed in this paper utilises Archie’s law to
Combining equation (4) and equation (5), it is possible to
describe the electrical behaviour of soils and the recent
write
formulation of wave propagation in unsaturated soils pro-
posed by Conte et al. (2009). The Archie’s law, which holds 1=m 2 3m
Ł Łr 1
for porous media with non-conductive solid grains (e.g. mw ¼ (Ł Łr )nmÆ 6 17
clean sands), can be written as
2
Łsat Łr 4 Ł Łr 1=m 5
¼ w p S qr (1) Łsat Łr
(6)
where and w are respectively the soil and interstitial fluid
electrical conductivities, is the porosity, Sr is the degree of
saturation, and p and q are two parameters that take into
account the geometry of the interconnected porosity. Formulas for porosity and degree of saturation
The formulation of wave propagation, developed by Conte The system of equations (1)–(3) and (6) allows the
et al. (2009), is based on the theory of linear poro-elasticity porosity and the degree of saturation to be evaluated from
in conjunction with the constitutive relationships originally measured wave velocities (VP , VS ) and electrical conductivity
proposed by Fredlund & Morgenstern (1976) to describe the (). Indeed, in the previous equations rs , rw , ra , Kw , Ka can
volume changes of unsaturated soils caused by changes in be considered as physical parameters with standard values;
total stress and suction. The theory predicts the existence of while the coefficients of Archie’s law and van Genuchten’s
three compressional waves and one shear wave in unsatu- equation can be evaluated through laboratory tests. The
rated porous media. The waves are dispersive, that is, their Archie’s law parameters can be inferred with a simple meas-
speed of propagation is frequency dependent (Coussy, 2004). urement of electrical conductivity at different porosities and
The fastest compressional wave is considered in the follow- water contents. The parameters of van Genuchten’s law can
ing as it is the one that is measured in laboratory and field be estimated by fitting data of the water retention curve
experiments. The expressions of VP and VS are obtained by obtained with well-documented techniques (e.g. pressure
applying the formulation of Conte et al. (2009) to the case plate extractor, suction controlled oedometer cell, filter paper
of low-frequency excitations method) (Fredlund & Rahardjo, 1993; Murray & Sivakumar,
8 " # 9 2010). Recently Cosentini et al. (2012) used electrical tomo-
>
> sk 2 >
>
< K a K w mw 3(1 2 )S r = graphic reconstructions in the laboratory to infer van Gen-
2
2(1 þ )Gsk uchten’s parameters.
>
>
: >
>
; Substitution of equations (1), (3) and (6) in equation (2)
2(1 sk ) þ S r (1 S r )½K w S r þ K a (1 S r ) yields
Gþ 8 9
1 2sk
> ½K S þ K (1 S r ) >
a w
> " r
> >
#> 2Æsk G þ ½(K a K w B þ D)=(L B þ C)
>
< sk 2 =
> V 2P ¼ (7)
3(1 2 )S r R
3 mw
>
>
2
2(1 þ sk )G > > where
>
> >
>
: ;
2 þ S r (1 S r )
2
R ¼ (1 )rs þ ˆQþ1 rw þ (1 ˆQ )ra
VP ¼
(1 )rs þ S r rw þ (1 S r )ra
L ¼ K a ˆQ þ K w (1 ˆQ )
(2) h im
½(1=m)þ1 1=m 1
G B ¼ M(ˆQþ1 Łr ) º (ˆQþ1 Łr ) º 1
V 2S ¼ (3)
(1 )rs þ S r rw þ (1 S r )ra
3sk 2 2Q
ˆ
G
where G is the shear modulus; vsk is the Poisson’s ratio of
the soil skeleton; mw C ¼ ˆQþ2 (1 ˆQ )
2 denotes the coefficient of water volume
280 EVALUATION OF POROSITY AND DEGREE OF SATURATION FROM SEISMIC AND ELECTRICAL DATA
D ¼ ˆQþ1 (1 ˆQ ) K w ˆQ þ K a (1 ˆQ ) (p ua ) þ ł b
1=q G ¼ A f (e) (10)
pr
ˆ¼
w where A is a stiffness index, p is the mean total stress, ua is
p the air pressure, ł is the suction, pr is a reference pressure,
Q¼ b is a fitting parameter and f (e) is a function of void ratio e.
q
Several expressions are available for the void ratio function
1 sk
f (e) as reported in Mitchell & Soga (2005).
Æsk ¼
1 2sk Equation (7) can be used to plot a diagram where each
1 2 sk curve describes how the electrical conductivity () and the
sk ¼ P-wave velocity (VP ) change when porosity is fixed and the
2(1 þ ) sk
degree of saturation is increased, or vice versa. Fig. 1 reports
M ¼ Æmn an example for sand. The set of parameters used to draw
1 this diagram is reported in Table 1 with related references.
º¼ Table 2 presents the assumed standard values of physical
(Łsat Łr ) 1=m
parameters: rs , rw , ra , Kw , Ka : In the diagram the range of
porosity is limited to 0.2–0.8, typical values for soils,
Equation (7) is a non-linear function of porosity. There- whereas the degree of saturation is assumed to vary between
fore, the porosity has to be evaluated numerically by solving 0.01 and 1.00.
an inverse problem with an iterative procedure. The objective
function to be minimised expresses the discrepancy between 10⫺6 v sk ⫽ 0·15
the observed and predicted system responses. In this specific v sk ⫽ 0·35
case, it is a measure of the difference between the predicted 0·20
φ
and the measured compressional wave velocities. The L1 10⫺5 0·40
norm of the misfit has been chosen as the objective function 0·80
0·60
to limit the weight of outliers (Menke, 1989) 0·01
10⫺4
minjje1 jj ¼ V 2 V 2
P P obs (8)
σ: mS/cm
Sr
where V P and V P obs are the calculated and measured values, 10⫺3
respectively.
The porosity obtained by equation (8) can be used to
evaluate the degree of saturation by 10⫺2
0·20
S r ¼ ˆ Q
(9)
0·40 0·20
10⫺1
0
1·0
The shear modulus (G), which is needed to solve the φ
0·60 0·40
inverse problem of equation (8), depends on the stiffness of 0·80 0·60
the granular skeleton. At constant effective confinement, the 0·80
100
stiffness of the soil skeleton varies with the degree of 100 1000
saturation. In general, an increase of the stiffness is observed VP: m/s
with decreasing saturation due to contact-level capillary
forces, which leads to the development of suction in the Fig. 1. Examples of velocity–conductivity diagram as a function
of porosity and degree of saturation for two values of Poisson ratio
pore water.
of the soil skeleton
To take into account the influence of suction on the shear
modulus (G), an appropriate relationship is needed to evalu-
ate equation (7). Table 2. Assumed values of the physical constants for determining
Many authors have proposed relationships to account for porosity and degree of saturation
the influence of suction on shear modulus: Wu et al. (1984),
Qian et al. (1993), Marinho et al. (1995), Mancuso et al. rs : kN.s2 /m4 2.767
(2002), Fratta et al. (2005), Kawajiri et al. (2011), Oh & rw : kN.s2 /m4 1.000
ra : kN.s2 /m4 0.001
Vanapalli (2011).
Ka : kPa 1.45 3 102
For example, neglecting anisotropy effects, for normally Kw : kPa 2.25 3 106
consolidated materials a power equation can be used vsk 0.15 4 0.35
(Mancuso et al., 2002)
Table 1. Parameters of Archie’s law, van Genuchten’s equation and equation (10) used to
plot the velocity–conductivity diagram in Fig. 1
Suction, ψ: kPa
vsk ¼ 0.15 (dashed lines) and vsk ¼ 0.35 (continuous lines) 100
100 000
grained soils). Cho & Santamarina (2001) provided possible
explanations for this observed difference.
A new relationship which describes the influence of suc- 80 000
tion on shear modulus is proposed below
8 2 3
< n m
4łres łaev @Ł 5 60 000
G(S) ¼ Gsat :1 þ ł 2 1m
2pr @ł
9 40 000
=
3 (1 S r )(m=1þm)
;
20 000
(11) 0 0·2 0·4 0·6 0·8 1·0
Degree of saturation, Sr
where Gsat is the shear modulus under saturated condition, Fig. 3. Shear modulus plotted against degree of saturation:
łres is the residual suction value, łaev is the air entry value, comparison between experimental data by Wu et al. (1984) and
pr is a reference pressure, and n and m are the parameters of the proposed relationship (equation (11))
van Genuchten’s equation. This expression reproduces the
stiffness variation with the degree of saturation with a
continuous function and without introducing additional para- LABORATORY EXPERIMENTAL DATA
meters. Laboratory data are used to verify the proposed approach.
The relation given by equation (11) takes into account The data are taken from the work of Comina et al. (2010).
that the evolution of suction depends on the variation of Main features of the experiments are described below. The
degree of saturation; therefore, the effects of suction on experiments were conducted on uniform quartz sand samples
shear stiffness have to be associated with the soil water (range of particle diameter was from 0.08 to 0.4 mm,
retention curve. uniformity coefficient CU ¼ 2.7 and specific gravity of solids
Equation (11) has been validated using the experiments by Gs ¼ 2.767).
Wu et al. (1984) on Glacier Way silt (particle size distribu-
tion between 0.0001 and 0.2 mm with a uniformity coeffi-
cient CU ¼ 125). The parameters n, m, łsat and łaev were Water retention curve
evaluated fitting the water retention curve by Wu et al. The water retention curve was obtained by measuring
(1984) with van Genuchten’s equation (Fig. 2). The experi- matric suction using the filter paper method (ASTM D 5298-
mental points of the water retention curve (Fig. 2) were 94 (ASTM, 1997)) on duplicate samples prepared by com-
obtained by pressure plate extractor. Fig. 3 shows that equa- pacting a mixture of soil and preselected quantities of
tion (11) closely follows the variation of shear modulus distilled water with the moist tamping technique at a poros-
plotted against degree of saturation that Wu et al. (1984) ity ¼ 0.4. Whatman No. 2 filter papers were placed in
observed in their resonant column tests. direct contact with the samples, as prescribed by the standard
282 EVALUATION OF POROSITY AND DEGREE OF SATURATION FROM SEISMIC AND ELECTRICAL DATA
procedure. Each specimen with filter paper was then placed internal boundary: 16 are equally spaced on the sidewall,
in an airtight container and left in a temperature-controlled and 13 are on each base and top plates. On each plate, there
room (20 18C) for 7 d. The ASTM (1997) filter paper are a bender element and an extender plate for the measure-
calibration curve (ASTM D 5298-94) was used. Experimen- ment of S- and P-wave velocities, respectively.
tal data and van Genuchten’s fitting equation are shown in The samples were prepared by mixing soil and 0.1 M
Fig. 4, while the fitting parameters are reported in Table 4. potassium chloride in water solution at given degrees of
saturation in the range between 20 and 100%. Salt solution
was used as the liquid phase to ensure a constant value of
Seismic and electrical measurements interstitial fluid electrical conductivities (w ) during electri-
Seismic and electrical measurements were performed in a cal resistivity measurements. To obtain samples with height
special oedometer cell, designed to perform geophysical tests of 4 cm and homogeneous density, the soil was compacted
(Comina et al., 2008). The cell is equipped for three- in four layers at an average porosity ¼ 0.4 directly in the
dimensional (3D) electrical resistivity tomography (ERT) oedometer cell using the moist tamping technique.
and to measure the velocity of compression (P) and shear
(S) seismic waves. The cell has 42 electrodes located on its
100 M ⫽ 0·50
electrodes that apply electrical current are on the sidewall and
the measuring electrodes are on the plates. This sequence
allows a good reconstruction of the distribution of the
10 ψaev
electrical conductivity within the sample. Details on least-
squares inversion algorithm can be found in Borsic et al.
ψres (2005).
1 The tomographic reconstructions showed an almost homo-
geneous distribution of conductivity for each sample, so the
average conductivity was considered in the present work
(Table 3). The electrical conductivity plotted against degree of
0·1 saturation relationship is shown in Fig. 5 in non-dimensional
0 0·1 0·2 0·3 0·4 form (/w ). Since the soil is a quartz sand, the assumption of
Volumetric water content, θ
‘non-conductive particle model’ (Mitchell & Soga, 2005) is
Fig. 4. Observed and calculated water retention curve for the justified, and Archie’s law can be appropriately applied to fit
investigated soil (range of the particle diameter is from 0.08 to these experimental data. The p and q exponents of the
0.4 mm). Archie’s law are reported in Table 4.
Table 3. Values of conductivity (ó) and P- and S-wave velocities measured in laboratory
tests. Values of shear modulus G estimated with equation (3) are also reported
Table 4. Fitting parameters of Archie’s law, van Genuchten and equation (11) for the
laboratory specimens
150 000
1600
Experimental data
P-wave S-wave Equation (11)
P-wave and S-wave velocity, VP,S: m/s
1200
Shear modulus, G: kPa
100 000
800
50 000
400
0
0 0·2 0·4 0·6 0·8 1·0
0·2 0·4 0·6 0·8 1·0 Degree of saturation, Sr
Degree of saturation, Sr
Fig. 7. Shear modulus plotted against degree of saturation for the
Fig. 6. Seismic wave velocities measured at different degrees of laboratory test: comparison between experimental data and the
saturation in the laboratory proposed relationship (equation (11))
284 EVALUATION OF POROSITY AND DEGREE OF SATURATION FROM SEISMIC AND ELECTRICAL DATA
0·6
0·20 0·30
φ ⫹10%
0·1
0·40
0·30
0·5 ⫺10%
0·40 0·50
Calculated porosity, φ
0·50
σ: mS/cm
Sr 0·60
0·70 0·4
0·80
0·90
1
0·3
1·00
In Figs 9(a) and 9(b) the values of porosity and degree of 0·9 ⫹20%
saturation imposed in the experimental tests are compared to
the values inferred with the proposed approach on the basis of Calculated degree of saturation, Sr 0·8
geophysical measurements. The figures show that the average ⫺20%
error in the evaluation of porosity is 10%, whereas the error 0·7
is higher for the evaluation of the degree of saturation.
0·6
The difference between calculated and imposed porosity
plotted against measured degree of saturation is shown in 0·5
Fig. 10(a), while the difference for the degree of saturation
is plotted in Fig. 10(b). Larger discrepancies are observed 0·4
for degree of saturation lower than 0.80.
The principal causes of the disagreement may be asso- 0·3
ciated with
0·2
(a) errors in the evaluation of seismic velocities
(b) errors in the measurements of average conductivity 0·1
(c) choice of soil skeleton Poisson ratio
(d ) errors in the evaluation of the water retention curve. 0
0 0·1 0·2 0·3 0·4 0·5 0·6 0·7 0·8 0·9 1·0
The first three causes appear to be negligible for the Measured degree of saturation, Sr
following reasons. (b)
(a) For P-wave velocity measurements, first arrival picking Fig. 9. Comparison between experimental and calculated (a)
porosity and (b) degree of saturation of laboratory specimens
was operated on traces recorded with an oscilloscope
with a sampling time of 1 s. The height of each sample
was measured with a tolerance of 0.5 mm. Therefore, the Eventually, errors in the water retention curve may be
maximum errors in P-wave velocity measurements can considered the most plausible cause of discrepancies in Fig.
generate maximum errors of 2% on the degree of 10. Indeed, suction measurements are not easy; they are very
saturation and of 0.5 % on the porosity, which are much time consuming and sensitive to testing technique. In the
less than those observed in Figs 9(a), 9(b) and 10. present tests, the measurements of suction were performed
Moreover, these errors can be considered independent of using the filter paper method. This technique estimates the
the saturation, otherwise the trend of Fig. 10 would not suction of soil indirectly by simple measurements of the
have been observed. Analogous considerations apply for moisture content of a filter paper at the same suction as
S-waves velocity measurements. the soil. Although this method is very simple, careful
(b) The average electrical conductivity was calculated with a procedures must be used to avoid erroneous measurements
largely redundant number of electrical resistivity meas- (e.g. a room with constant temperature and a sufficient
urements acquired for ERT, hence it is possible to equilibration time are required) (Bulut & Leong, 2008). The
consider this measurement very accurate. Furthermore, suction of soil is obtained from the calibration curve of the
maximum errors in electrical conductivity should be filter paper water content with suction. Supposing a careful
recorded at low saturation, but Fig. 10 shows that the setting of the method, the evaluation of moisture content of
maximum errors in the evaluation of unknowns ( and Sr ) filter paper is the principal cause of errors in the suction
are not at low saturation. measurements. The major errors can be committed when
(c) Figure 1 shows that the assumption on the soil skeleton measuring small masses of the filter paper moisture, because
Poisson ratio affects the porosity independently from the on the basis of the calibration curve, small differences of
degree of saturation, hence a wrong assumption on filter paper moisture correspond to large values of suction.
Poisson ratio cannot explain the larger discrepancies for Another source of error can be associated with the
intermediate saturation degree observed in Fig. 10. difference between the experimental data of the water reten-
COSENTINI AND FOTI 285
0·10
validated according to the literature data and then used to fit
the available experimental data for the present study.
0·05 Geophysical measurements performed in the laboratory on
(φcal ⫺ φmeas)
Fig. 10. Errors in the evaluation of (a) porosity and (b) degree of NOTATION
saturation plotted against measured degree of saturation of A stiffness index
laboratory specimens b fitting parameter of equation (10)
e void ratio
f (e) function of void ratio
tion curve and the values predicted by the van Genuchten’s G shear modulus
expression. Indeed the latter is used in the seismo-electric Gsat shear modulus under saturated condition
model and these discrepancies at intermediate degrees of Ka bulk modulus of air
saturation may justify the observed trends of Fig. 10. From Kw bulk modulus of water
this point of view, other analytical expressions of the water m parameter of van Genuchten’s equation
retention curve may provide an improvement on the seismo- mw2 coefficient of water volume change with respect to a
electric model. change in matric suction
Although some differences between experimental data and minjje1 jj minimum of L1 norm of the misfit
n parameter of van Genuchten’s equation
the model can be observed, such discrepancies can be con-
p parameter of Archie’s law
sidered acceptable from an engineering viewpoint. Indeed, p ua net total stress
the method allows the evaluation of the porosity and degree pr reference pressure
of saturation for coarse-grained soils, where it is complicated q parameter of Archie’s law
to obtain undisturbed samples and where the traditionally Sr degree of saturation
adopted methods (e.g. empirical correlations with penetration VP seismic P-wave velocity
tests) are affected by large uncertainties. V P obs measured value of seismic P-wave velocity
VS seismic S-wave velocity
Æ parameter of van Genuchten’s equation
@Ł
CONCLUSIONS derivative of volumetric water content with regard to the
A procedure has been presented for an evaluation of @ł matric suction
porosity and degree of saturation of unsaturated soils from Ł volumetric water content
electrical conductivity and seismic wave velocities measure- Łr residual value of the volumetric water content
ments. The proposed procedure is relevant in geotechnical Łsat saturated value of the volumetric water content
engineering practice, considering that it may be very useful vsk Poisson ratio of the soil skeleton
r electrical resistivity
when undisturbed sampling is not feasible.
ra density of air phase
It requires measurements of electrical conductivity and P- rs density of solid phase
and S-wave velocities. These quantities can be obtained by rw density of water phase
geophysical tests, which allow soils to be investigated in soil electrical conductivity
their natural state on site. Other parameters required for the w interstitial fluid electrical conductivity
calibration of the electro-seismic model may be obtained in 09 effective confining pressure
the laboratory on disturbed samples, or alternatively through soil porosity
the use of empirical relationships or, better, with additional ł matric suction
information, as for example measurements of suction (e.g. łaev air entry value
tensiometer) or moisture content (e.g. capacitance/frequency- łres residual suction value
domain reflectometry probes (FDR), time-domain reflecto-
metry probes (TDR), dual needle heat pulse probes).
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