Atish Dipankar University of Science & Technology

Lab Report

Course Title: CSE

Course Code: CSE-122
Section: Sec-01

Submitted By: Submitted To:

MD Nasim Howladar Mahmudur Rahman Roni

Coordinator
ID : 223-0459-203
Department of Computer Science and
Department of Computer Science and
Engineering
Engineering

Submission Date : 05/12/2023

 Introduce of Titration
Objective:—
The object of this experiment is to make us familiar with
neutralization reaction of acid or base and

Also to introduce us with some important terms such as titration,

standardization, indicator, acid-base reaction, etc.

The main purpose of the experiment is to determine the strength of a

base with the help of a standard acid solution.

Theory:—
In this experiment we shall determine the strength of solution by a
standard solution of this is done by means of “Titration”. The
important matters that are related with the

Experiment is stated below:

Titration: —
In presence of a suitable indicator, the volumetric analysis in which a
standard solution

Is added in another solution (whose strength is not known) to reach its

end point to determine the

Strength of that solution is called ‘titration’.

Standard Solution: — A solution of known concentration is

called a ‘standard solution’.
Indicator: — in our acid-base titration there is an important use of
indicator. An ‘indicator’ is a chemical substance that detects the
equivalent point (i.e. the end point) of reaction by changing its color.

Equivalent Point: — the ‘equivalent point’ is the point in a

titration when a stoichiometric amount of reactant has been added.

Molarity: - In current practice, concentration is most often

expressed as molarity. Molarity (symbol

M) Is defined as the number of moles of solute per liter of solution. If

n is the number of moles of

Solute and V liters the volume of solution,

Molarity= Moles of solute/ Volume in liters

Or, M= n/V (in liters)

Here, n= x (in gm.)/ Molecular weight

Normality (N) = gm. equivalent of solute /liters per solution.

In this experiment the reaction we shall use is as follows:

HOOC-COOH + 2NaOH ——> NaOOC-COONa + 2H2O

The formula required to determine the strength of NaOH solution is:-

V × S = V × S, acid acid

Base or ,V × S = V × Sab ba Where ‘V’ represents volume and ‘S’

represents strength
Why Phenolphthalein is used as indicator: In this experiment,
Phenolphthalein’ is selected as indicator whose working pH range is
8.3-10.0 i.e. it is works when the environment is acid. This indicator
gives pink color in basic solution and becomes colorless when the
base is neutralized.

Apparatus:

. Conical flask,. Burette,. Pipette,-Volumetric flasks,. Stand

Solve the experiment: 01

Data and calculation:-

Standardization of NaOH solution with standard Oxalic Acid

Solution

Solution Volume of Initial Final Base

number: acid (v1) reading bullet (v2)
reading
01 10 0 15.1

02 10 15.1 30.2 15.57

03 10 30.2 46.7

V1=10ml, V2=15.57ml

S1=0.1N, S2=?
 v 1s1 10∗0.1
V2 S2= V1 V2 , S2 = v2 S = 15.57
,
2

S2=0.064ml (Answer)