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Construction and Building Materials 207 (2019) 548–562

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Construction and Building Materials


journal homepage: www.elsevier.com/locate/conbuildmat

Assessment of parameters governing the steel fiber alignment in fresh


cement-based composites q
Víctor Pérez Villar a,⇑, Nelson Flores Medina c,d, M.M. Alonso b, Sara Gismera Diez b, Francisca Puertas b
a
Escuela Técnica Superior de Arquitectura de Madrid (ETSAM) – Universidad Politécnica de Madrid, Avenida de Juan de Herrera, 4, 28040 Madrid, Spain
b
Instituto de Ciencias de la Construcción Eduardo Torroja (IETcc), Spanish National Research Council (CSIC) (IETcc-CSIC), Calle de Serrano Galvache, 4, 28033 Madrid, Spain
c
Escuela de Arquitectura, Ingeniería y Diseño, Universidad Europea de Canarias, c/ Inocencio García 1, La Orotova, 38300 Santa Cruz de Tenerife, Spain
d
Departamento de Construcción Arquitectónica, Escuela de Arquitectura, Universidad de Las Palmas de Gran Canaria, Campus Universitario de Tafira, 35017 Las Palmas de Gran
Canaria, Spain

h i g h l i g h t s

 The torque to rotate a steel fiber immersed into cement-based composites has been determined.
 Induced torque can explain fiber alignment successful in fresh cementitious materials.
 The influence of mixture parameters of cementitious composites has been analyzed.
 Fiber geometry parameters, like shape and aspect ratio, affect the induced torque needed to rotate fibers.
 Particle size distribution and packing density affects the induced torque exerted on fiber.

a r t i c l e i n f o a b s t r a c t

Article history: The main aim of this paper is to measure the induced torque needed to rotate a steel fiber, hence an
Received 14 August 2018 experimental and parametrical analysis of factors governing steel fiber alignment in cement pastes
Received in revised form 4 February 2019 and mortar, rotating from static position and rotating in a dynamic fluid is here presented. To aim this
Accepted 5 February 2019
objective, a set of rheological tests has been conducted to assess the torque necessary to rotate steel fibers
immersed into different fresh cement paste and mortar mixes with Bingham fluid behaviour. Fibers of
different aspect ratios (length/width) and different geometry, straight and hooked-end, have been eval-
Keywords:
uated as they are the more commonly used. On the other hand, different parameters (type of mixture,
Concrete rheology
Steel fiber
size of aggregates, volume fraction of aggregates) affecting cement mixtures are also analysed and their
Fiber suspensions influence in fiber orientation discussed.
Fibre orientation Fiber alignment depends on external torques applied to fibers, immersed into a cement-water-
Fiber alignment aggregate viscous system, that can be produced during or after casting. The flowability of the fresh sus-
Bingham fluid pension with fibers produces a load/pressure that generates a torque that can align them. Fiber alignment
SFRC is a main goal to pump the fresh material. Hence, the factors that govern fiber alignment are studied
Yield stress which increase the post-cracking strength of cement-based composites under load along its life service
Plastic viscosity
due to casting or pumping. To that end, a set of tests has been conducted to assess the torque necessary
Self-compacting concrete
to rotate steel fibers immersed into different fresh cement paste and mortar mixes with Bingham fluid
behaviour. Fibers of different aspect ratios(length/width) and different geometry (straight and hooked-
end) have been evaluated. On the other hand, different parameters (type of mixture, size of aggregates,
volume fraction of aggregates) affecting cement mixtures are also analysed and their influence on fiber
orientation is discussed. The values obtained here are between 1 and 14 N  mm of dynamic yield torque
and 0.1 and 0.5 N  mm min for viscoplastic torque per fiber, depending on fiber geometry, are helpful to
improve the fiber alignment in cement-based composites reinforced with fibers through a design and
production based on these parameters.
Ó 2019 Published by Elsevier Ltd.

q
This document is a collaborative effort.
⇑ Corresponding author.
E-mail addresses: victor.perez.villar@alumnos.upm.es (V.P. Villar), nelson.flores@universidadeuropea.es (N.F. Medina), mmalonso@ietcc.csic.es (M.M. Alonso),
sgismera@ietcc.csic.es (S.G. Diez), puertasf@ietcc.csic.es (F. Puertas).

https://doi.org/10.1016/j.conbuildmat.2019.02.036
0950-0618/Ó 2019 Published by Elsevier Ltd.
V.P. Villar et al. / Construction and Building Materials 207 (2019) 548–562 549

Nomenclature
DMax max. aggregate size
List of symbols d fiber deflection
c_ shear rate T(x) induced torque
l1 plastic viscosity S viscoplastic torque
T ðosÞ static yield torque
sðodÞ dynamic yield stress
T ðodÞ dynamic yield torque
sðosÞ static yield stress
s0 yield stress Tf torque due one fiber
s shear stress T Ref torque due probe
vf volume fraction Tb homogenized torque
b
S homogenized visc. torque
x rotation speed

1. Introduction [27]. In some cases prediction of rheological parameters in SCC


with fiber geometry, such as plastic viscosity from experimental
Steel fibers are used increasingly as a discrete reinforcement in values in cementitius pastes have been researched to be included
composites with a brittle cement matrix, to enhance their tensile in software simulations [20]. Under this line of research, to know
strength or flexural strength, ductility, toughness, fatigue and the predicted rheological parameters of fiber inclusions, helps to
impact resistance [45,21,51,3],2. Fibers reduce also shrinkage and simulate the fiber alignment during flow introducing them into
cracking due to hardening of concrete in service. However, they the governing equations. Some research has been done to predict
must be aligned or orientated respect to a tensile principal stress fiber orientation in slump flow and L-Box test using Lagrangian
trajectories, which produces a final strength on the material reach- Smooth particle Hydrodynamics (SPH) [15,16]. Much of the
ing a better mechanical targeted behaviour. On the other hand, also research found in the literature regards to the composite rein-
steel fibers randomly orientated in cement-based composites forced with fibers as a whole, but the behaviour of a fiber itself
enhance the mechanical properties, like tensile strength and has not been described yet within the cementitious composite.
toughness [41]. The effect of flowability of FRCC has been also studied, because
The mechanical efficiency of a Fiber Reinforced Cementitious it is one of the parameters that can increase the volume fraction vf
Composite (FRCC) depends not only on the volume fraction (vf ) of aligned fibers [10]. Moreover, the higher the vf of fibers aligned
but mainly on the percent of them aligned with the reduced stress the better the workability of the fresh FRCC, which helps to
supported [5]. Furthermore, the fiber design depends on anchorage increase the amount of fibers added as reinforcement or the suc-
necessary to develop the required bond when the composite is cess of placing and pumping the composite. Therefore, flowability
stressed under load: straight, hooked, crimped, double dueform, is also studied to pump FRCC as it also concerns to the construction
paddled, etc . . .[7]. However, straight and hooked are the most industry [19]. Nowadays, pumping is a common way to place con-
common shapes used [32]. Moreover, induced fiber orientation crete, and the risks associated with concrete pumping increase
also results in a higher effectiveness of crack-width control, which when fibers are added to a composite which has to pass a pipe.
depends on the individual performance of all fibers crossing a crack Under these conditions, concrete flow depends on slip-layer forma-
[54]. Therefore, fiber alignment has become a research issue in the tion and occurrence of dynamic segregation. Pumping can generate
last decades in order to increase the performance of the FRCC, Edg- segregation, bleeding of concrete, but concrete can cause also
ington and Hannant [17,44] such as Fiber Reinforced Concrete blockage in the pump pipe. This situation will be more pronounced
(FCR), Self-Compacting Fiber Reinforced Concrete (SCFRC), Ultra in FRCC, because stiff steel fibers increase the viscosity and also can
High Performance Fiber Reinforced Cementitious Composites cause balling-up [30] & 26. Moreover, the settlement of aggregates
(UHPFRCC) [45,21,51,54,1]. Nevertheless there are still more field and fibers is also a major concern [34].
to research linking the rheology to the fiber dynamics in order to Fiber alignment in FRCC depends on many factors, like fiber
define the fiber alignment processes. properties (shape, material, aspect ratio) and on the fresh proper-
Several researchers studied methods to predict the fiber align- ties of the cementitious fresh material (shear stress (s), yield stress
ment [27,18] based on anisotropic physical properties of hardened (s0 ), plastic viscosity (l1 ) and on the placing and casting method,
concrete. These methods are based on how to determine the main as it will modify the velocity of the fluid and hence the shear rate of
fiber orientation direction after hardening. Some of these methods the material (c_ ) defined also as @u/@y. Orientation of rigid fibers
are based on electrical conductivity [33,46], on measuring ultra- can be externally induced only when the cement-based composite
sonic waves velocity [8], on X-ray tomography [23], and also is still a fluid. This early stage, after mixing, by assessment of the
destructive testing based on slicing hardened samples [37,14]. rheological properties of such cementitious composites, fibers
The relation between fiber alignment and the mechanical beha- can be rotated through an external torque T, that must to overcome
viour has also been analysed through test, [48,50,42,5] meso- the initial static yield shear stress of the fresh cementitious mate-
mechanical models [53], through modeling the pull-out behaviour rials [39].
[45], modeling the split tensile strength [21]. The constitutive equation of Bingham shear rate (c_ ) is com-
Different mechanisms can induce torque-fiber alignment in monly expressed as a two parameter model (so and l1 ). To model
fresh concrete. The procedure of concrete placement into a mould the stress-deformation behaviour of viscoplastic fluids:
has been recognized to have a major impact on fiber orientation,
both due to the casting direction and due to preferential fiber  
@u 0; s < s0
alignment induced by the casting element itself [47]. Moreover, c_ ¼ ¼ ð1Þ
@y ðs  s0 Þ=l1 ; s P s0
vibration during compaction can rotate and align fibers into planar
orientations, some experiences have been reported in literature The steel fiber considered, rotates in a fresh cementitious com-
[37,52]. The flow has also been identified to play a major role on posites which is a non-newtonian fluid. On the other hand, fresh
fiber alignment, as for example self-consolidating concrete (SCC) cement-based composites can be considered as suspensions
550 V.P. Villar et al. / Construction and Building Materials 207 (2019) 548–562

behaving as Bigham fluid Banfill and Tattersall [6]. The rotation paste, which had different mix designs and different rheological
dynamics of ellipsoidal bodies, immersed in newtonian fluids, parameters. The work of a single fiber was analysed, as fibers in
was first described theoretically by [24]. Subsequently, Brenner a volume fraction around a 2% are considered in a dilute solution,
addressed the dynamics in case of general body shape [11]. If a with low possibility of interaction between fibers [30]. From the
steel fiber is considered equivalent of a small cylinder (rod), with results obtained, the behaviour of fibers in FRCC was analysed
similar aspect ratio: ‘/d (length divided by section diameter), and parameters for future design of FCC were set. The rheometer
immersed in a non-newtonian fluid with yield stress, it is neces- tests applied provide the viscous torque value T and factors affect-
sary define all these rheological parameters to asses the overall vis- ing the fiber torque, and hence design parameters are obtained to
cous torque T. Lack of empirical tests, or numerical modeling, has increase the fiber alignment in fiber reinforced cementitious con-
been observed in the literature by the authors. Nevertheless to crete (FRCC).
asses experimentally this torque value T, rheometer measurements
provide useful information to explain the fiber dynamics in fresh
cementitious materials. 2. Experimental program
Some experimental procedures based on torsional pendulum
have been applied by [52] to measure the torque induced due a The main aim of this study was to measure the induced torque
magnetic field in short-fiber-reinforced composites. However, the on a steel fiber immersed into a controlled rotating fresh cement-
use of rheometers is becoming more common and they increases water-aggregate system. This section contains the description of
the knowledge about the rheological behaviour of fresh cementi- the experiments conducted.
tious composites, thanks to their high precision and ease of calibra-
tion. Applying a rotational rheometer with modified probe, [49]
have been studied the alignment of hooked-end fibres in matrices 2.1. Materials
with similar rheological behaviour to cementitious composites due
to homogeneous magnetic fields, using different concentrations of An ordinary Portland cement type CEM I 52.5R, according to
CarbopolÒ 940 as a fluid with yield stress similar to the pastes and UNE-EN 197-1:2011-Part 1: Composition, specifications and con-
mortars presented here. formity criteria for common cements, has been used. The cement
Attention should be drawn to the fact that the fresh cement had a specific weight of 3.077 g=cm3 , a specific Blaine fineness of
pastes and mortars is often characterized by thixotropic behaviour 3552 m2 =kg; its chemical composition is presented in Table 1.
Roussel [38]. Applying shear stress, over time, the plastic viscosity The particle distribution of the cement has been obtained through
l1 begins to decrease due to progressive breakdown of the inter- a sample suspended in ethanol with a Mastersizer S, Malvern par-
nal structure of particle-particle network through shear thinning. ticle size analyser (Fig. 2). The initial and final setting times were
However, after shearing the structure begins to rebuild. The result 118 and 178 min respectively.
is shear rate can form hysteresis loop, increasing and decreasing A quartz CEN-standard sand, complying with DIN EN 196-1 and
the value of shear stress (See Fig. 1). DIN EN ISO 679, was used to mix the all the mortars considered in
The variation of yield stress under thixotropic conditions can be rheological tests. The moisture content was tested around to 0.07
measured at two points. Initially the structure is able to admit a wt% in all the cases. Chemical composition and mineralogical
certain amount of stress before it is broken down and starts to phase analysis of this sand (determined on a Bruker AXS D8 Advance
ðsÞ
flow, this amount is usually called the static yield stress so (also
X-ray diffractometer and Rietveld refinement method) values are pre-
refered to as shear-growth shear stress). Under shear flow, the
structure and bonding network is broken down, resulting in lower sented in Tables 1 and 2.
ðdÞ The characteristic of CEN-Standard Sand is their own specific
yield stress: dynamic yield stress s [39,36].
o
grain size distribution. It ranges between 0.08 and 2.00 mm and
This research work aims at assessing the rheological parameters
the different sand fractions are blended in defined portions to be
governing the effect of external induced torque on fiber rotation, to
compliant with DIN EN 196-1. The maximum aggregate size DMax
understand the factors governing the phenomenon of fiber align-
was established sieving with square mesh widths, obtaining three
ment. This assessment was performed as follows: industrial fibers
samples with 2 mm, 1 mm and 0.5 mm maximum aggregate size.
with different aspect ratios and geometries (hooked-end and
The particle size distribution of the different series of sand samples
straight) were fixed to a probe of a commercial rheometer
through differential sieving procedure is presented in Fig. 3 (see
(Fig. 6). Fibres were immersed in a set of plain mortars and cement
Table 3).
In order to understand the influence of sand with different max-
imum diameters of the particle suspension affecting the fiber rota-
tion, a reference cement paste with a maximum particle size (Dmax )
of 0.063 mm and three mortars with same concentrations of sand
but different maximum aggregate size (Dmax ), of 0.5 mm, 1 mm,
2 mm, were tested. On the other hand, the role of aggregate con-
centration on the fiber due rotation was also studied. Hence, one
reference cement paste (0% aggregate concentration), and three
mortars with 2 mm maximum aggregate diameter and 0%, 50%
66% and 75% aggregate volume where also tested. Five different
mortars and one reference cement paste were designed in order
to obtain similar rheological parameters and their proportions
are presented in Table 4 all of them with the same CEM I 52.5R
Portland cement.
On the other hand, seven different steel fibers were used for
experiments. The two main geometric parameters considered in
Fig. 1. The flow curve of paste/mortars determination of the hysteresis loop due steel fibers are: aspect ratio (‘/d) and type (straight and hooked-
thixotropy. end).
V.P. Villar et al. / Construction and Building Materials 207 (2019) 548–562 551

Table 1
Chemical composition of CEM I 52.5R used. (%-weight percent). LOI*: Loss on ignition IR*: Insoluble residue.

SiO2 Al2 O3 Fe2 O3 MnO MgO CaO SO3 Na2 O K2O TiO2 P 2 O5 Cl SrO ZrO LOI* IR*

% 19.65 5.24 2.78 0.06 0.85 63.52 3.44 0.12 1.04 0.23 0.06 0.009 0.07 0.02 2.90 0.007

37 and 67 approximately (See Table 5). In Table 5 a code to distin-


guish the fibers during the tests was applied, by indicating first the
length of the fiber, its aspect ratio and the shape of the fiber:
Straight (S) or Hooked (H). Fig. 4 shows the fiber types tested in
this research.

2.2. Tests methods

The mortar mixer used for every mortar/paste probe was a


Ibertest IB32-040 C2000, the mixing steps for every test follows
the standard procedure defined on UNE 196-1. All mixes were pre-
pared following the same shear-history procedures, previous to be
incorporated into the rheometer vessel.
To measure the induced torque T ðxÞ a rotational rheometer
suitable for fine-grained building materials (Model: ViskomatTM
NT) was used. This rheometer can realize operative measurements
on mortars up to a maximum particle size (Dmax ) of 2 mm. Every
test was executed filling the 370 ml rheometer vessel volume with
Fig. 2. Particle Size distribution of CEM I 52.5R used. fresh mortar/paste to introduce the system fiber-rheometer probe
inside. The rotational rheometer has an accuracy able to resolve an

Table 2
angle of 104 degrees, it allows also ramping from 0.001 rpm to
Chemical composition (wt%) of sand. maximum 400 rpm in a speed-controlled mode. The measurement
of torque induced over the rheometer probe can range between
Oxide wt%
250 to +250 Nmm, measured by a transducer. The torque resolu-
SiO2 96.80 tion measurement is 0.05 Nmm, the accuracy is 2 Nmm.
Al2 O3 1.51
The rheometer probe (Probe model-V0011) was modified dril-
K2O 0.56
Fe2 O3 0.43 ling a hole of 1 mm diameter to attach a steel fiber perpendicular
CaO 0.10 oriented to the rotation axis (See Fig. 6), the fiber was perpendicu-
LOI* 0.61 lar to the probe. Every experiment was executed using first the ref-
erence probe (values obtained are shown in Table 4) and after with
each fiber mechanically fixed to the rheometer probe. The fibers
used are shown by Table 5. Every fiber type is used to conduct a
sequence of rheological tests immersed into the fresh mortar/-
paste. The mixed mortars and paste was filled into the rheometer
vessel resting for five minutes prior to execute the two rheometer
tests (as indicated by Fig. 5).
Two different tests were sequentially conducted with the
rheometer for every mortar/paste and steel fiber aspect ratio (See
Fig. 5). Every test was repeated at least three times set up, the com-
puted mean are taken to be the representative value. The standard
deviation was taken, in every executed test as a value of experi-
mental uncertainty. The sampling rate to measure the induced tor-
que, by the rheometer probe, was set to 0.1 s. The first test is called
a stress growth test (SGT) and the second one a flow control test
(FCT). Five minutes of rest after mixing and two minutes between
Fig. 3. Particle size distribution (PSD) of sand aggregates used (cumulative finer the two rheological tests were always applied (Fig. 5 shows the
fraction). sequence).
The rheometer in the SGT mode operates with an angular speed
control, measuring the torque induced by the fresh mortar/paste
Table 3 (T ðxÞ) on the probe/fiber system from rest. Induced torque over
Quantitative mineralogical compo-
a defined angular speed profile is measured starting with a con-
sition of sand (wt%).
trolled signal of rotation speed of 1.5 rpm (0.025 rps) during 70 s
Mineralogical phase wt% (short period), measuring the change of the induced torque. Plot-
Quarz 98.3 ting the recorded torques from the SGT test vs time submitted to
Microcline 1.7 a rotational value, the maximum torque value can be taken as a
T ðosÞ (static yield torque), one of the three rheological parameters
Four fiber types were straight with aspect ratios ranging assessed in the present study. This yield torque is associated to a
between 40 to 65 and three fibers were hookend-end (DRAMIXÓ state before the fresh cementitious structure is broken down, so
3D series from BekaertTMCompany) with aspect ratios between T ðosÞ is the torque necessary to initiate flow, corresponding to a pre-
552 V.P. Villar et al. / Construction and Building Materials 207 (2019) 548–562

Table 4
Table with mortar compositions used during rheological experiments. Three parameters considered here: cement/aggregates (c/a), w/c ratio and maximum aggregate size (Dmax ).
The rheological parameters T ðodÞ ; T ðodÞ and S are considered as reference values of the paste and mortars without fibers.

Composite Code c/a (%) w/c Dmax (mm) T ðodÞ Ref (Nmm) T ðosÞ Ref (Nmm) SRef (Nmmmin)
Paste 0 (0%) 0.45 0.063 7.990 8.778 0.139
MOR-12-2MM-050 1/2 (66%) 0.50 2.0 10.878 21.171 0.298
MOR-13-2MM-060 1/3 (75%) 0.60 2.0 11.730 22.320 0.268
MOR-12-1MM-050 1/2 (66%) 0.50 1.0 14.360 35.457 0.351
MOR-11-2MM-050 1/1 (50%) 0.50 2.0 5.170 10.220 0.110
MOR-12-05MM-070 1/2 (66%) 0.70 0.5 2.020 11.138 0.062

Table 5
Table with different steel fiber geometries used for the experiments (S - Straight and
H Hooked-End). d – Diameter of steel fiber in mm and ‘ is the length of steel fiber in
mm.

Fibers (Cod.) ‘ (mm) d (mm) ‘/d


1F50-09S 59.00 0.90 65.56
1F40-09S 35.21 0.70 50.30
1F30-09S 40.98 0.90 45.53
1F40-11S 37.26 0.90 41.40
1F60-09H 60.00 0.90 66.67
1F35-07H 51.38 0.90 57.09
1F50-11H 40.98 1.10 37.25

Fig. 6. Rheometer probe with a steel fiber mechanically fixed to the main axis.

vious well-connected undisturbed internal micro-structure [36]. In


case of initially static fibers, this viscous torque T ðosÞ represents the
threshold to be overcome by an external torque to initiate rotation,
which is of interest to understand the fiber dynamics in aligning
processes.
The FCT test is also a angular speed-controlled test with a speed
profile defined as a sequence of constant angular speeds during a
fixed time interval, called patches: starting at 100 rpm during a
30 s interval, 90 rpm during five seconds, 80, 70 and so forth
decreasing until the test is stopped. A total of ten patches using
the same set of rotation speeds (xi ), per test. At every patch of con-
trolled speed the FCT test it takes the mean torque measurement
during an interval of five seconds, a set of T ðxi Þ values are
Fig. 4. Seven steel fibers used in the tests. Codes are related with Table 5. obtained. The FCT test give us a set of tuples is recorded

Fig. 5. Sequence of rheological tests executed per fiber and paste/mortar.


V.P. Villar et al. / Construction and Building Materials 207 (2019) 548–562 553

(xi ; T ðxi Þ) as result, these values are represented as straight line with the probe alone and with the probe and a fiber. As explained
(following the Bingham law) using a previous least square approx- before, T is related to the shear stress, s and S with the plastic vis-
imation, following Eq. (2) (One example can be seen in Fig. 7). All cosity [6] as expressed in Bingham Eq. (2). The viscosity and the
the results from FCT experiments have a coefficient of determina- dynamic yield stress are obtained for each mix with the ViskomatTM
tion R2 value with an average value of 0.97 and standard deviation NT probe. Considering these initial ideas, it is possible to affirm in
of 0.05, which is acceptable for a linear relationship, such as: every rheological test that the viscous torque T can be breakdown
depending on their dynamical state in:
T ðxÞ ¼ T ðodÞ þ S x if T > T o ð2Þ
 A single fiber starting from a static position, or zero angular
The relationship between the torque and angular velocity is velocity (x ¼ 0 rpm), immersed in pastes and mortars, must
plotted and the intercept at zero-torque rate considered is the
overcome first the static yield torque given by T ðosÞ (Nmm), mea-
dynamic yield torque T ðodÞ (Nmm), while the slope S (Nmmmin) sured by the SGT rheological test.
is the viscoplastic torque. Both are parameters corresponding to  A single fiber in rotation, from 0-100 r.p.m and immersed in
Bingham’s yield stress and plastic viscosity. The yield torque mea- cementitious composites (paste and/or mortars) within
sured through flow curve is regarded as the dynamic yield shear rheometer vessel has a viscous torque following Eq. (2). The
stress T ðodÞ when shear rate is zero, so this is the minimum stress parameters values are given by: the viscoplastic torque S
to sustain or terminate the flow of the material. The established (Nmmmin) and dynamic yield torque T ðodÞ (Nmm).
relationship 2 quite is similar to expresión 1 (Bingham formula),
what other researchers already previously presented [6] & 31.
The values obtained of dynamical yield torque T ðodÞ , and the vis-
The torque needed to rotate the fiber is considered from its
coplastic torque S contributions, due to only the fiber are the differ-
edges to its center of gravity (CG), so the CG is the pivot point. Sta-
ence between T ðodÞ Ref and the SRef of the reference probe (without
tic yield torque T ðosÞ is the macroscopic result of momentum of
fiber as included into Table 4) in each suspension and those
inter-granular friction with the steel fiber during initial paste/mor-
obtained with the reference probe with each fiber. The equation
tar shear, and must not be the value for the SGT and FCT tests.
obtained from the tests of a suspension with the is rheometer
Regarding viscoplastic torque S, this rheological value is considered
probe as follows, according to Eq. (2) is:
as the macroscopic effect of dynamic resistive torque caused onto
steel fiber by flow around, like water, passing through the contour
of the fiber [13]. T Ref ¼ T ðodÞ Ref þ SRef x if T Ref > T ðodÞ Ref ð3Þ
A laminar flow regime around the steel fiber is considered, The values obtained from the FCT experiments, according to Eq.
because the computed Reynolds number is still low even at greater 2 consider the rheometer measurements with the probe and a fiber
angular velocities (100 rpm) in the rheological experiments [6]
together. The corresponding viscous torque due only the fiber (T f )
§7.1. This situation permits to consider the drag proportional to
can be obtained as the difference between Eqs. (2) and (3). This dif-
the velocity without turbulence around the system probe-fiber.
ference can depicted algebraically as:
The cross-section geometry of blades are also streamlined enough
to avoid flow separation during the fluid rotation around the blade.    
The insertion of fibers is orthogonal to the plane that contains the T f ¼ T ðodÞ  T ðodÞ Ref þ S  SRef x ð4Þ
blades, minimizing the possible interference between fiber and
blades.
where T f is the viscous torque contribution of one fiber due rotation
in alignment process. In Fig. 7 the aforementioned process can be
2.3. Torque assessment for a single fiber observed. Once the dynamical yield torque due a single fiber T ðodÞf
is understood as a difference between dynamical yield torques:
The dynamical yield torque (T ðodÞ ) and the viscoplastic torque of T ðodÞ  T ðodÞ Ref measured, and the viscoplastic S f as: S  SRef for each
a fiber from its center of gravity were determined for every batch fiber in the different suspensions are determined, dynamics of
rotation to align fiber can be formulated accordingly. Similarly,
using the differences between values obtained in the SGT rheologi-
cal test, in such way that contribution of fiber to static yield torque
ðsÞ
is just the difference between observed values of T Ref (probe with-
ðsÞ
out fiber attached) and T k (probe with fiber innmersed in a specific
mortar k).
As the different suspensions present a different viscosity and
dynamical and static yield stress, the effort of the same fiber in dif-
ferent suspensions can not be directly compared. Therefore, a lin-
eal factor is applied for every batch as the suspensions follow the
Bingham model, which attends to a lineal equation. To compare
the results recorded in FCT rheological experiments, a procedure
for data homogenization was established. Taking the FCT rheolog-
ical value of cement paste (without fiber) as a reference for T ðdÞ Paste
equals to 7.990 Nmm) and for SPaste the value of 0.139 Nmm min.
On the other hand, the five mortars has a dynamic yield torque rep-
resented as T ðodÞ k and a viscoplastic torque Sk , where k is an index
number from 1 to 5. A five adjustment constants fkT has been

Fig. 7. Comparison between torque flow curves measured from reference probe,
defined for dynamic yield torques as a ratio T ðodÞ k =T ðdÞ Paste , and sim-
and (taken as example) three fibers in MOR-11-2MM-050 mortar. ilarly the adjustment ratio for viscoplastic fkS defined as a ratio
554 V.P. Villar et al. / Construction and Building Materials 207 (2019) 548–562

Sk =SPaste , where k is equal to 1,2,3,4,5 mortars included in Table 4. data processing algorithm was used to filter the noise in measured
The homogenized torques can be defined as: torque signals prior to take the maximum value. The algorithm
called Tikhonov-Phillips regularization was applied to SGT recorded
Tb k ¼ fkT T k  T kref ð5Þ torques with a standard prior deviation of 0.1 Nmm for pastes and
bk
S ¼ fkS Sk  Skref ð6Þ 0.16 Nmm for mortars.
The Fig. 9a shows the recorded static yield torque versus the
where T kref and Skref are the measured FCT torques without fiber per fiber aspect ratio for the straight fibers. It is possible to observe a
every five mortars (k = 1,2,3,4,5) indicated in Table 4. Eqs. (5) and transition of static yield torque up to 42 fiber aspect ratio. The
(6) are used to homogenize the FCT recorded data from torques to Fig. 9b shows the static yield torque versus the fiber aspect ratio
compare sand concentration and maximum particle size (Dmax ) for the hooked-end fibers. The straight fibers have greater values
effects. Therefore, the results obtained of induced fiber torques have of T ðosÞ than hooked-end reaching a difference mean value of 5
been analyzed and compared with mixtures with same viscosity Nmm approximately between both.
and shear stress.

3.2. Dynamic: viscoplastic results


3. Results
Viscoplastic torques S (Nmmmin) for steel fibers within a
Three rheological factors were considered to be measured by
range of angular rotations x between 0 and 100 rpm are depicted
the experiments, two of them affecting the Bingham Eq. (2):
considering all the tested paste/mortar and can be seen as a set of
dynamical yield (T ðodÞ ) and viscoplastic torque (S), and the third is plots in Fig. 10a (straight fibers) and b (hooked-end). These results
the static yield torque T ðosÞ . The following figures show the torque are given by fiber aspect ratio and the viscoplastic in rheometer
needed to rotate a steel fiber surrounded by the fresh cement units (Nmm min) for both type of fibers. Measured mean error
suspensions. due dispersion of experimental data falls in 0:01 Nmm min in
case of straight fibers, while the measured dispersion in case of
3.1. Static results hooked-end fibers give a 0:016 Nmm min.
Viscoplastic torque values are increasing aspect ratio from 37 to
The stress growth test (SGT) is commonly implemented to mea- 47 fiber as pointed [28], but up to that point the values remain con-
sure static yield torques T ðesÞ [36], where a linearly increasing shear stant. Therefore, it can be observed that viscoplastic torque S
stress due a rotating vessel at constant speed (x ¼ 1:5 rpm) was needed to rotate a steel fiber, has approximately the same value
applied, and the induced torque T ðxÞ on fiber is recorded. The dif- when the aspect ratio ‘=d is 37 or 57, at both extremes of the curve
ference between recorded torques, with and without attached fiber here shown. Using the difference between measured torques with-
to rheometer probe can be shown in Fig. 8, taken as an illustrative out fiber and the same with fiber in rheometer probe can be seen:
example for a cement paste. all the values of viscoplastic torque for one fiber are in the domain
Two series of experiments using fibers types (straight and range of 0.02–0.15 Nmmmin. The curves plotted in Fig. 10a, about
hooked-end) attached to the rheometer probe were made using the viscoplastic torque S studied with straight fibers, shown com-
the mortars and paste described in Table 4. Same experiments parable trends when the aspect ratios were higher than 50, but not
without fiber, taken as reference value for static yield torque were lower than it.
recorded in the Table 4 as a reference values for dynamic yield tor- In Fig. 11, the effect caused by the concentration of sand aggre-
que T ðodÞ Ref (4th column), static yield torque T ðosÞ Ref (5th column) and gates, for straight fiber is shown. Curves in this Fig. 11 represent
the homogenized viscoplastic torque for every straight fiber type
viscoplastic SRef the last one. The uncertainty due the experimental
considered in Table 5. The curves in this figure present seems to
SGT test procedure shows a dispersion greater in mortars than
show an initial plateau at low sand concentrations (0.0–0.4), and
paste, the signal obtained from probe was noisy, and an a suitable
a progressive decrease of the viscoplastic torque needed for rotat-
ing the fiber at the increasing aggregate concentration. However,
although fiber 1F40-09S(50.3) shows a decrease of S as the other
fibers, the trend is different as it is more continuous. Nevertheless
the range between 0% and 50% can be object of further experimen-
tation to determine the fiber behavior more precisely. It should be
mentioned that the lower the aspect ratio of fiber the lower the
viscoplastic torque necessary for the fiber to initiate rotation
(Fig. 11). Comparing 1F40-11S(41.4) and 1F40-09S(50.3) in
Fig. 11 (both with 40 mm length), it can be noticed that the first
with 1.1 mm diameter can rotate more easily than the latter with
0.9 mm diameter.
The set of plots presented in Fig. 11 seems to have constant
slope in all the fibers aspect ratios at low sand concentration, but
it is necessary to determine values near to the 0.2 sand ratio in
future experiments. It can be observed that viscoplastic torque
decreases when the fine aggregate concentration is more than
0.5 ratio. Fiber rotates more easily in concentrated cementitious
composites when aggregates are 50% of the volume fraction.
Regarding to Fig. 12, the evaluation of S for hooked-end fibers in
relation with the aggregate concentration has been studied. As in
Fig. 11, hooked-end fibers seems also to have a similar plateau
Fig. 8. Plot of samples to compare the results recorded from SGT rheological test response in the viscoplastic torque diagram (See Fig. 12) consider-
between measurements with fiber (1F40-11S) and without. ing constant value at low aggregate concentration below to 0.5
V.P. Villar et al. / Construction and Building Materials 207 (2019) 548–562 555

Fig. 9. Measured static yield torques T ðosÞ from the SGT rheological test according with two different type of fibers.

Fig. 10. Measured viscoplastic torque S versus steel fiber aspect ratio, from the FCT rheological test according with two different type of fibers.

Fig. 11. Homogenized viscoplastic torque b


S versus sand concentration. Considering Fig. 12. Homogenized viscoplastic torque b
S versus sand concentration. Considering
only straight fibers. only hooked-end fibers.
556 V.P. Villar et al. / Construction and Building Materials 207 (2019) 548–562

ratio cement/aggregate. Similar viscoplastic torque behaviour with


hooked-end fibers can be noticed showing a general tendency to
decrease the viscoplastic torque over the 0.5 ratio cement/aggre-
gate. It can be observed a different trend in the homogenized vis-
coplastic torque when 1F50-11H fiber is tested. At sand ratios
over 0.6, the values are quite similar for all hooked-end fibers
studied.
On other hand, the variation of viscoplastic torque S for straight
fibers depending on the maximum aggregate size is shown in
Fig. 13. The lower values obtained can be observed when the max-
imum aggregate size is 0.5 mm. However, higher values are pre-
sented with lower and higher grain sizes than 0.5 mm. The
higher viscoplastic torques were observed in straight fibers
immersed in mixtures with lower grain size than 0.5 mm, except
for 1F40-11S(41.4), which presents a different trend. When aggre-
gate diameter increased up to 0.5 mm the viscoplatic torque to
rotate a straight fiber increased also, except for 1F40-11S(41.4).
Considering the maximum size aggregate of the cement-based
composite mixture with hooked-end fibers Fig. 14 is plotted. Sim-
ilar increasing tendency of viscoplastic torque is observed in vis- Fig. 14. Homogenized viscoplastic torque b
S versus maximum particle size (Dmax ).
coplastic torque Figs. (13 and 14) for both types of fibers. Considering only hooked-end fibers.
However, the hooked-end fibers show higher S maximum values
to rotate at 0.12 Nmmmin.
for mortar 1/2 and maximum aggregate diameter 1 mm. The trends
are similar also for every mixture studied, although mortar1/2D 1
3.3. Dynamic: yield results mm presents different behaviour depending of the aspect ratio of
the fiber studied.
Considering dynamic yield torque (T ðodÞ ) values, obtained The dynamic yield torque measurements obtained for straight
through FCT tests, a set of plots is presented. Computed mean error fibers versus the aggregate concentration are represented in
due dispersion measurement of experimental data falls in 0.2 Fig. 16. All straight fibers seems to have same shape (inverted
Nmm considering the case of straight fibers, while the computed bathtub), with exception for fiber code 1F40-09S (aspect ratio
dispersion in case of hooked-end fibers give a 0.3 Nmm. 50.3).
The static yield torque T ðosÞ is expected to be higher than The dynamic yield torque (T ðodÞ ) needed to stop turning a single
dynamic yield stress T ðodÞ considering the corresponding internal fibre seems to be constant for aggregate concentrations within a
range 0.2 to 0.5 ratios, as shown before for cementitious pastes
structural states of fresh paste/mortars [39]. The values T ðodÞ versus
under dynamic conditions (viscoplastic torque). Fig. 16 shows also
fiber aspect ratio (‘=d) for straight fibers is represented in the
a descent of dynamic yield torque value at values larger than 0.5
Fig. 15a. This figure reveals a peak value close to an aspect ratio
ratio of sand concentration where a maximum T o is observed.
of 50. Viscoplastic torque S shown in Fig. 10a seems to have a sim-
It has been also observed that the fiber with higher diameter
ilar qualitative behaviour than dynamic yield torque (T ðodÞ ) at this start rotating easily, confirming the asseveration commented
aspect ratio of 50, showing a change of tendency close to this value. before: the lower the aspect ratio the lower the torque required
Values of dynamic yield torque T ðodÞ for a hooked-end fibers for stop rotating a single straight fiber. For a given aspect ratio
shown in Fig. 10b are in the domain range of 1 to 15 Nmm, except and fiber volume concentration, an increase in diameter means
the increase in fiber length and hence subsequent the increase in
effective mechanical interlocking. Some authors, like Laskar and
Talukdar [29] point a range between 50 and 100 of aspect ratio
to be affected the rheological behaviour of mortars and pastes.
Using dynamic yield torque measurements obtained for
hooked-end fiber at different sand concentrations, the Fig. 17 is
plotted. This Figure shows different behaviours of dynamical yield
torque T ðodÞ have been observed. However, yield torque what seems
to increase when the aggregate concentration is increased. At 0.7
ratio of sand concentration seems to decrease quickly. The fiber
with the lower aspect ratio present the lower yield torque values.
Nowadays in Fig. 18 the T ðodÞ variation for straight fibers with the
maximum grain size of the cementitious composites has been
shown. Yield torque of straight fibers has a maximum value
between 0.3 and 0.35 ratio of sand concentration, this effect does
not appears in Fig. 17 for hooked-end fibers. In both cases, the yield
torque T ðodÞ necessary to stop rotating the hooked-end, and straight
fibers, seems to increase more pronounced with sand concentra-
tion, but this increase is greater with long fibers (up to 50 aspect
ratio) than with shorter ones.
The dynamic yield torque increases with the maximum size of
Fig. 13. Homogenized viscoplastic torque b
S versus maximum particle size (Dmax ).
Considering only straight fibers. the aggregates (Dmax ). However, the value of T ðodÞ is nearly constant
V.P. Villar et al. / Construction and Building Materials 207 (2019) 548–562 557

Fig. 15. Measured dynamic yield torque T ðodÞ versus fiber aspect ratio from the FCT rheological test according with two different type of fibers.

Fig. 16. Homogenized dynamic yield torque T b ðodÞ versus sand concentration. b ðodÞ versus sand concentration.
Fig. 17. Homogenized dynamic yield torque T
Considering only the straight fibers. Viscoplastic torque S can be seen in Fig. 11. Considering only hooked-end fibers.

for mixtures with an aggregate maximum size under 0.5 mm. The
increase of maximum aggregate size from 1 mm to 2 mm in inequality in the 5th and 6th columns of Table 4 measurements of
cement-based composites also increased T ðodÞ ,
but pronounced than reference probe without fiber.
from 0.5 mm to 1 mm. Regarding the different values found of static/dynamic yield
Fig. 19 considers the maximum grain size (Dmax ) for hooked-end torque in Fig. 9a and b (static yield torque) and Fig. 15a and b
fibers. This figure is quite similar to the equivalent for straight (dynamic yield torque), can be seen the influence of particle size
fibers (See Fig. 18). distribution (PSD) of aggregates (showed in Fig. 3) on rheological
properties, pointed also by other authors like Bentz et al. [9].
The fiber geometry has a strong effect on the viscoplastic torque
4. Analysis & discussion response as expected [7]. Straight fibers (cylindrical geometry)
have a more linear behaviour against sand concentration than
The static yield torque is expected to be higher than dynamic hooked-end. However, when the maximum size particle is consid-
yield torque, as other authors pointed [36]. Hence the results ered the geometry seems to be not so relevant because the beha-
shown agree on this inequality:T ðosÞ > T ðodÞ , in the case of paste and viour to rotate is similar attending Figs. 13 and 14.
mortars analyzed here. The values per fiber type are always higher It has been also noticed that hooked fibers increase dynamical
in Fig. 9a for static yield stresses compared with the dynamic tor- yield torque values when the aspect ratio is reduced (ranging
ques represented in Fig. 15a, same result can be observed in between 40 and 45). This behaviour differs from that pointed out
Figs. 9b and 15b. In terms of fiber alignment, that means one fiber for straight fibers, because of the differences in fiber geometry.
need more external torque to overcome the static yield torque than Hooked-end geometry of fibers can increase the area or volume
to maintain rotating a certain speed. It can be also observed this of fluid that the fiber has to slice when it rotates. This fact is
558 V.P. Villar et al. / Construction and Building Materials 207 (2019) 548–562

amount of mixtures here studied is wide and their behaviours cor-


responded to others from the literature, a study with different
cements or type of aggregates can be also developed to increase
the knowledge of the design parameters of a cementitious compos-
ite reinforced with fibers to be align.
However, it has been observed in other research, that plastic
viscosity of cement based suspension increases with the volume
fraction of inclusions [30]. In the present case, the fiber torque val-
ues were obtained in mixtures with same viscosity and shear
stress, indicating that higher inclusion of rigid aggregates facili-
tates the alignment. In other words, the cement paste volume hin-
ders the fiber alignment.
Moreover, the volume of cement paste in a mixture must be
studied as a parameter in terms of mixture design, to increase fiber
alignment. Concrete with a higher cementitious paste content,
such SCC, may need a lower viscosity to achieve same fiber orien-
tation than other with higher aggregate volume fraction. In the
Fig. 13 it can be also observed that the torque necessary to rotate
dynamically the fiber S in cementitious composites is lower in
those batches containing larger aggregates than cement pastes
b ðodÞ versus maximum grain size in mm.
Fig. 18. Homogenized dynamic yield torque T
[22]. The S and T ðodÞ values are modified with the Dmax of cement-
Considering only straight fibers.
based composite. However, the results are promising for fiber ori-
entation through magnetic fields or casting methods for concrete,
as the maximum aggregate size (Dmax ) is around 8 mm even in
SCC with a low T ðosÞ , although more test must be done. On the other
hand, conventional concrete with higher Dmax , but also higher vis-
cosity will decrease the possibilities of fiber alignment.
Viscoplastic torque can be considered as a macroscopic drag
causing on fiber rotation due to the friction between small particles
assembling in cement-based suspension that contains more inter-
particle contacts than a large particle packing. Thus, the friction
generated is higher, for a given maximum packing fraction (MPF)
[30]. In order to predict the viscoplastic torque of fresh concrete,
it’s necessary to add the contributions of the various grain frac-
tions, which depend on their partial compaction index, weighed
by a coefficient [30,13]. This drag torque increases when the parti-
cle size decreases as in Figs. 13 and 14.
The behaviour shown in paste, with the lowest Dmax in Fig. 13
can be considered as a granular suspension in which small sand
grains assemblies result in more inter-particle contacts than large
particles packing. This situation can increase the opposite torque
needed to rotate the fiber, as can be contrasted also in Fig. 14.
Taking into account the results shown in the Figs. 13 and 14, it
Fig. 19. Homogenized dynamic yield torque T b o versus maximum grain size
ðdÞ
can observed that incorporated sand to the composite reduces the
expressed in mm. Considering only hooked-end fibers.
torque in a first moment with Dmax 0.5 mm. However, this beha-
viour varies with other volumetric fractions as can be observed.
The packing fraction obtained with several sizes is higher than
interesting because the amount of oriented fibers can be lower with two sizes of aggregate, and the S also increases again [43].
when hooked-end fibers are used instead of straight ones. To avoid The mortar with cement and sand, up to Dmax 0.5 mm which are
this, FRCC with lower shear stress and lower viscosity must be besides of very different are mixtures where there is clearly a
designed when hooked-end fibers are used [34,26]. domaining fraction [6,34].
It can be concluded that the geometry clearly modifies the flow The parameters regarding cementitious mixture rheology, like
around the fiber in the fresh cement mass. This fact requires a dif- yield torque seems to correlate with packing density. The packing
ferent model of stress distribution in the fiber depending on the density is increased with the maximum size of the aggregate and
geometry. A research considering different geometries immersed with the concentration or volume fraction of aggregates [12]. The
into viscoplastic fluids is reported [4]. It is known from the litera- cementitious mixtures studied, pastes and mortars, can be viewed
ture that yield stress of a mixture is increased with the increase of as a dry packing of aggregate particles, filled up with cement paste.
the solid concentration [9] or when the sand is finer [6], although Increasing the packing density reduces the ability to move initially
the fibers have presented a lower torque to rotate or the values the fiber, which leaves more initial resistance torque needed to
were quite similar. If we observe from the results those mortars rotate the fiber.
with bigger Dmax of aggregate, the yield torque both static and The increase of the packing density of the mixtures increase the
dynamic, and S are lower according to literature. For instance, torque necessary to align the fibers, as the strength of flocculated
MOR-12-2MM-050 and MOR-12-1MM-0.50 with same w/c ratio, network is increased with the number of particles in contact
[25,35]. As packing fraction is increased, when finer fractions are
present a 25% reduction of T ðosÞ , a 41% reduction in T ðdÞo and a 15%
used, the yield torque and the viscoplastic are also increased, and
of S when the Dmax passes from 1 mm to 2 mm. Although the
V.P. Villar et al. / Construction and Building Materials 207 (2019) 548–562 559

hence it is also higher the torque necessary to align successfully is known as T ðodÞ [36], hence is also the stress of the fiber during
the fiber. The finer aggregates also are able to pack densely the rotation, as shown in the Fig. 21.
fiber whereas the larger aggregates disturb this packing. We can This rheological behaviour of the fresh mass can show several
observe from the results, that MOR-12-2MM-050 and MOR-12- load patterns that can be different depending on the angular veloc-
1MM-050 with same w/c ratio and sand concentration but lower ity of the fiber during rotation, which are drawn in Fig. 21. When a
Dmax . Shows this behavior, in Table 4 yield torque and viscoplastic static fiber initiates the rotation, it must overcome the T ðosÞ consid-
of the mixture from Fig. 15a and b, where it can observed the plot ering velocities near to zero, and as its velocity is increased from
of MOR-12-2MM-050 located under of MOR-12-1MM-050 with
the axis to the outermost edge (plot 1 in the Fig. 21)). Viscosity
lower T ðodÞ f and Sf . The volume of fibers reduces the packing density increases the load due to shearing with the velocity, and according
of a fiber reinforced composite [35,25] as it disturbs the granular to this the stress of the fiber will be increased along its length, from
skeleton, although this could not be studied in this work it could its centroid to the edge.
be a topic for further research of fiber alignment. On the other hand, when the fiber is rotating, is possible
Dynamic yield torque (T ðodÞ ) needed to rotate a fiber is decreased observe in plot 2 in Fig. 21, that in the axis the torque is T ðodÞ due
with aggregate concentration, as shown with the same fibers under to thixotropy and is increased with rotation velocity due to S along
dynamic load (Fig. 11). This Figure shows how an increment of the its length. At very low velocity, the fresh cementitious composite
torque happens from 0 to 0.5 mm of Dmax . can recover the initial network and the values can be next to T ðosÞ
Although an increase of fiber aspect ratio increases the torque [36]. Along the fiber the linear speed is increased, and the values
necessary for fiber rotation, a change it has been observed in trend
can be reduced near T ðodÞ . When the speed is even fastest,
when ‘=d ratio was higher than 45. This behaviour can be
approaching to the edge, the mass presents a stress to overcome
explained because some elastic deformation causes a flexion of
the fiber. The fiber inserted perpendicular to the probe could T ðodÞ þ Sðv =xÞ. (plot 3 in the figure) Therefore, when a fiber rotates
absorb some strain energy due to elastic bending deformation. This from static (for instance: magnetic torque) the load due to shearing
effect can be seen amplified into yield torque figures (like Fig. 15a) is the highest as the fiber has to overcome T ðosÞ and S  x in each sec-
because this elastic deformation could be performed firstly during tion of the fiber. On the other, the torque necessary to rotate a fiber
the initial yield stages and increasing later the torque to initiate the has been obtained in this study with the rheometer. This is the
induced rotation. maximum moment according to the situations of load during rota-
Fiber alignment in FRC can be obtained in different ways, and to tion. The fibers here used have circular sections, and the diameter
reach it each fiber must shear the fresh mass where it is immersed. have been measured. Using the torque obtained from the tests we
This shear generates also a load causing the fiber to bend. From the can determine the deflection distance d of the fiber as it can be con-
STG and FCT tests, the torque necessary to rotate a fiber have been sidered as a cantilever beam according to the Euler-Bernoulli beam
obtained, which is the total momentum of the load caused during theory:
shearing. To understand the load chart along the fiber several facts Z ‘=2
Tf
have to be considered, and discussed as follows. d¼  x dx ð7Þ
A steel fiber during rotation x has a different linear speed v(x) 0 E Iz
along its own length ‘ according to equation v ðxÞ ¼ x  x. Where x
Where T f is the torque obtained in the rheological test, E is the elas-
is the rotational speed, v is the linear speed from x = 0 to ‘/2, the
tic modulus of the fiber, Iz is the moment of inertia of the steel fiber.
fiber outermost extreme. This rotation generates a different shear
The expression T f x dx can be obtained from the moment diagram
load in each section of the fiber, from the V = 0 in the rotation axis
(Fig. 22), although the centroid of the load plotted in the diagram
(in the center of mass or centroid of the fiber) to maximum speed
can be displaced as shown in the figure, depending on the speed
in its edge.
and thixotropy of the mixture.
Moreover, this stress chart along the fiber can be modified
depending on thixotropy. During a FCT test with a rotational
rheometer, the microstructure of particle-particle network is
affected [36]. When this happens T ðosÞ is reduced, coming into what

Fig. 20. Angular speed vs. linear speed in a fiber during alignment. Fig. 21. Load diagram in a fiber depending on rheological properties of the mixture.
560 V.P. Villar et al. / Construction and Building Materials 207 (2019) 548–562

Fig. 22. Moment diagram (first grade) and deflection of the fiber.

In order to discuss the behavior of the fiber during rotation, the


deflections (mm) of the fibers from the axis to the edge during
rotation in cement mixture MOR-11-2MM-050 (See Table 4) have
Fig. 23. Moment diagram (second grade) and deflection of the fiber.
been summarized. This mixture has been selected as it shows
f f
higher values of T and S considering the load of a fiber from sta- Where d is the deflection in the edge, q is the load due to shear
tic, corresponding to plot 1 from Fig. 21. The calculations have fol- according Fig. 20, ‘ is the length of the fiber, E is the elastic modulus,
lowed the previously shown equations considering the fiber as a and Iz is the inertia of steel fibers. Considering fibers mentioned
beam. above, the only factor changing is the length, but according to this
It can be observed from the results shown in Table 6 that some the deflection should increase. If the torque is reduced it can be
fibers can have a maximum deflection that can modify also the caused to a higher deflection that reduce the load on the fiber,
load chart estimated. As a high fraction of the span can be which under high deformations reduces the area of shearing. The
observed, over 1/5 in some cases, this deflection in many cases shortest fibers and with highest diameters and indeed highest iner-
can produce second grade efforts and even larger deformations. tia moment, are more rigid and they are submitted to less deforma-
All these results shown a higher energy absorption in the fiber tion when shearing the fresh suspension. Hence, they rotate more
when is deflected. (Fig. 23)) This point is important because it indi- effectively and the process to align them is easier, especially when
cates that those fibers, which are able to keep a relation of defor- the T ðosÞ and S of the composite is higher. However, longer fibers, if
mation according to elastic behavior the values, are predictable. are flexible,can also reduce their torque to be aligned when they
However up to this point, those fibers with lengths that allow them overdue a certain aspect ratio. Although this geometric ratio has
to deflect extremely, can reduce the torque necessary as shown in not been determined here it can be studied.
fiber 1F50-09S. The elastic deformation of steel fibers, and their effect into the
This change of trend can been observed in Fig. 15, where over yield torque and viscoplastic torque will be developed in further
the value of aspect ratio 50 the fibers reduce their torque. This studies and tests. The study be can also be extended to other steel
behavior can be only explained according to the aforementioned, fiber geometries like crimped fibers [40]. Moreover, statistical
as if we compare the fibers 1F50-09S and 1F40-09S with same studies of fiber alignment of reinforcing concrete and mortar with
diameter, shape but different length, the shorter has higher deflec- fibers should be developed. Fiber elastic deformation facilitates the
tion under same load conditions, 4.40 mm and 3.32 mm respec- alignment, even thought the fibers here tested are made of steel
tively (Table 6). The deflection for a cantilever beam with and considered rigid. As the fiber is deformed during the yield
constant load along its length view can be simplified as: stage, the friction load is not perpendicular to the fiber axis and
q ‘4 the fiber rotates with less resistance. Moreover, the area or volume
d¼ ð8Þ of fresh cement-based composite to move is lower. This means that
8 E Iz

Table 6
Table of computed fiber deflections d (mm).

Deflection d (mm) Fiber x ¼ 0 rpm x ¼ 20 rpm x ¼ 40 rpm x ¼ 60 rpm x ¼ 80 rpm x ¼ 100 rpm
1F50-09S 1.32 1.72 2.12 2.52 2.92 3.32
1F40-09S 2.00 2.48 2.96 3.44 3.92 4.40
1F30-09S 0.74 0.94 1.14 1.34 1.54 1.74
1F40-11S 0.58 0.73 0.87 1.02 1.17 1.31
1F60-09H 1.48 1.86 2.24 2.61 2.99 3.37
1F35-07H 1.08 1.38 1.67 1.97 2.26 2.56
1F50-11H 0.42 0.50 0.58 0.67 0.75 0.83
V.P. Villar et al. / Construction and Building Materials 207 (2019) 548–562 561

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