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Construction and Building Materials 282 (2021) 122706

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Construction and Building Materials


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The influence of fiber type and length on the cracking resistance,


durability and pore structure of face slab concrete
Lei Wang a,b,c,⇑, Tingshu He a, Yongxiang Zhou c,⇑, Shengwen Tang d,⇑, Jianjun Tan e, Zhentao Liu a,
Jianwen Su a
a
College of Materials Science and Engineering, Xi’an University of Architecture and Technology, Xi’an, China
b
College of Urban Construction, Wuchang University of Technology, Wuhan, China
c
State Key Laboratory of Building Safety and Built Environment, China Academy of Building Research, Beijing, China
d
State Key Laboratory of Water Resources and Hydropower Engineering Science, Wuhan, China
e
China Power Construction Group Guiyang Engineering Corporation Limited, Guiyang, China

h i g h l i g h t s

 The drying and autogenous shrinkage reduction effect is greatest for PVA fiber.
 The efficiency in improving the cracking resistance follows the order of PVA > PAN > PP.
 PAN fibers produce a low porosity, a low hardened air content and a high impermeability.
 Durability differences caused by fiber can be interpreted by the pore structure and air void.

a r t i c l e i n f o a b s t r a c t

Article history: The crack resistance and durability of face slab concrete are two important factors determining the nor-
Received 24 November 2020 mal operation and safety of concrete face rockfill dams (CFRDs). This paper investigates the influence of
Received in revised form 20 January 2021 polypropylene (PP), polyvinyl alcohol (PVA) and polyacrylonitrile (PAN) fiber with two lengths (10 mm
Accepted 11 February 2021
and 20 mm) on workability, strength, shrinkage behavior, cracking resistance and durability performance
Available online 26 February 2021
of face slab concrete. Besides, the parameters of the pores at multi-scales were investigated by a linear
traverse method and the mercury intrusion porosimetry (MIP), respectively. The results in this study
Keywords:
demonstrate that: (1) the efficiency in reducing the shrinkage and in enhancing the cracking resistance
Face slab concrete
Fibers
of face slab concrete follows the order of PVA > PAN > PP. In addition, both the impermeability and frost
Cracking resistance resistance of concrete can be improved by adding fibers, the efficiency is in the sequence: PAN > PVA > PP
Frost resistance and PVA > PAN > PP, respectively. (2) increasing fiber length from 10 mm to 20 mm reduces the shrinkage
Permeability by about 5.1%7.0%, enhances the tensile strength (r) by about 7.9%9.2% and declines the cracking tem-
Temperature stress testing machine (TSTM) perature (Tc) by about 5.6–6.5℃, all of which could significantly improve the cracking resistance.
Air void Moreover, the increase in fiber length improves the frost resistance, but increases the relative permeabil-
Pore structure ity coefficient (Kr) by about 28%47%. (3) The correlation analyses reveal that, the addition of PAN fibers
produces a lower porosity, a lower fraction of large capillary pores as well as a lower hardened air content
than the PVA and PP fibers at 28 days, thereby resulting in better impermeability of concrete. PVA fiber
enhanced concrete gives the smallest spacing factor and the largest total number of air voids among all
the fiber enhanced concretes, thus exhibiting the best frost resistance.
Ó 2021 Elsevier Ltd. All rights reserved.

1. Introduction face slabs as the primary anti-seepage structure [1]. Due to its
excellent seismic resistance, high adaptability, short construction
The concrete face rockfill dam (CFRD) is one kind of rockfill dam period and low cost, CFRD has become one of the most widely used
with a rockfill body as the main supporting structure and concrete dam types in the world [2,3]. Concrete face slab is a typical thin
structural member with highly exposed surfaces. As shown in
⇑ Corresponding authors. Table 1, the thickness of concrete face slab usually ranges from
E-mail addresses: 535250684@qq.com (L. Wang), xiangzizhou2006@126.com about 0.3 m at the top of the dam to about 0.6–1.1 m at the bottom,
(Y. Zhou), tangsw@whu.edu.cn (S. Tang).

https://doi.org/10.1016/j.conbuildmat.2021.122706
0950-0618/Ó 2021 Elsevier Ltd. All rights reserved.
L. Wang, T. He, Y. Zhou et al. Construction and Building Materials 282 (2021) 122706

Table 1
Parameters of concrete face slabs of some typical CFRDs in China.

Project Dam height Parameters of concrete face slabs of CFRDs Location in Construction
(m) China completed
Maximum length Slab width at side/middle Thickness at the top/ Number of
(m) parts (m) bottom (m) slabs
Fengning 120.3 207.5 10/12 0.3/0.6 54 North 2022
Aertash 164.8 >120 6/12 0.4/0.96 76 Northwest 2021
Jiyin 124.5 139.22 6/12 0.3/0.6 54 Northwest 2017
Pushihe 78.5 128.5 14 0.3/0.56 50 North 2012
Shuibuya 233 162 8/16 0.3/1.1 58 Central 2008
Gongbaxia 132.2 218 6/12 0.3/0.7 38 Northwest 2007

whereas its width is between 6 and 14 m and its length normally a weaker workability compared with that PP fiber enhanced one,
ranges from dozens to more than100 m. Due to the internal stress but presented better frost resistance. In a study by Yousefieh
caused by the drying conditions and external temperature fluctua- et al. [6], it was found that the polyolefin fibers at a content of
tions, the thin and quasi-brittle concrete face slabs are easy to 0.2% by volume of concrete could increase the adherence between
crack, especially at early age when the tensile strength of face slab fibers and cement matrix as well as the tensile strength of normal
concrete is relatively low [2,4]. In the case of Gongboxia CFCD concrete to a greater extent than the PP fibers.
located in northwestern China, 594 temperature-induced cracks In addition to the fiber type, fiber length also plays an important
formed in the face slabs before impoundment [1,2]. The cracks in role in influencing the cracking resistance of concrete. Banthia et al.
concrete face slabs can destroy the structural integrity of the con- [8] investigated the influence of PP fiber length on plastic shrink-
crete slabs, favor the ingress of moisture and cause severe leakage, age cracking in high strength concrete (about 89 MPa) and con-
all of which are detrimental to the durability of face slab concrete cluded that at three volume fractions of 0.1%, 0.2% and 0.3%,
and the normal operation of CFRDs [5]. Therefore, how to improve longer PP fiber (12.5 mm) was more effective in reducing crack
the cracking resistance and durability of face slab concrete are areas and crack widths than the shorter PP one (6.35 mm). Similar
important issues in CFRD design and construction. results were obtained by Nathalie et al. [15], who observed that at
An efficient method to improve the crack resistance of concrete different fiber dosages (0.3% and 0.6% by mass of binder), the effect
is by using fibers. The short and randomly distributed fibers with of longer flax fiber (50 mm) was more apparent in reducing the
high elastic modulus in concrete act as micro-steel bars to transfer stress concentration and the number of cracks in high-clay content
stresses and absorb energy under tensile stress, thus improving the concrete than the shorter one (12 mm). Shen et al. [20] reported
tensile strength and cracking resistance of concrete [6–8]. There that the cracking resistance of internally cured concrete added
are many types of fiber, including mainly the steel fibers, natural with 8.0 kg/m3 Barchip fibers increased first and then decreased
fibers such as flax fibers and polymeric fibers such as polypropy- as the fiber length increased from 42 mm to 60 mm. According
lene (PP), polyolefin, polyacrylonitrile (PAN) and polyvinyl alcohol to Shen et al.’ another study [21], increasing fiber length of PP plas-
(PVA) fibers. These fibers vary in component, chemical property, tic fibers from 42 mm to 60 mm reduced the cracking resistance of
tensile strength, and elastic modulus, which may affect the crack- high-strength concrete at a constant fiber content of 8.0 kg/m3. The
ing resistance and other important properties of concrete [6,9–11]. different influence of fiber length on concrete cracking resistance
Numerous studies have been carried out on the effects of fiber may be due to the differences in fiber type and concrete properties
type on concrete properties. Compared with the polymeric fibers, in different studies.
steel fibers could reduce the shrinkage and improve the cracking Overall, fiber reinforced concretes commonly have excellent
resistance of concrete more efficiently due to their much higher properties including the high ductility, high tensile strength,
strength and elastic modulus [6,11,12]. However, the high-rigid load-bearing capacity, and cracking resistance, which have great
steel fiber could increase the shear resistance of fresh concrete potential for various engineering applications, including the face
and hence lead to a significant reduction in concrete workability slab concrete in CFCDs. The face slab concrete is featured by a mod-
[12–14]. This drawback limits the application of steel fiber in face erate workability (commonly 50–70 mm in slump) and a relatively
slab concrete in China. The natural fiber has good tensile properties low cement content in order to reduce the source of shrinkage and
due to its high cellulose content, whereas its high-water absorp- hydration heat. To achieve satisfactory workability and cracking
tion ability could significantly weaken the workability of concrete resistance, PAN fiber at a dosage of 0.8 kg/m3 has been applied in
[15]. The polymeric fibers have some perfect characteristics such all face slabs in Shuibuya CFRD located in central China, which is
as small density, small filament diameter, suitable price, acid and the highest CFCD in the world by far [2]. In Hongjiadu CFCD in
alkali resistance, easy dispersion and so on [16]. Consequently, southern China, the combination of PP fibers with a content of
the polymeric fibers have been increasingly used in engineering 0.8 kg/m3 and MgO expansive agent at a dosage of 2.4% by mass
applications. PP fiber is inert in high pH environment and easy to of binder was used to improve the cracking resistance of face slab
disperse in concrete mixtures [8]. It has been reported that PP fiber concrete [2,22]. According to Woo et al. [23], PVA fiber with a con-
could reduce the final drying shrinkage of concrete remarkably [6] tent of 0.1% by volume was suggested to produce face slab concrete
but increase the ion permeability of concrete [17]. A comparative in South Korea to achieve desirable workability and durability.
study conducted by Chen et al. [16] revealed that the PAN fiber From the detailed review of existing literatures above, some
enhanced concrete exhibited better resistance to ion permeability investigations are found to be related with the effects of fibers
than the PP enhanced one. They also suggested an optimal PAN on the performance of face slab concrete, but there is still a lack
fiber volume fraction of 0.10%–0.14% for airport pavement con- of systematical study on the effects of fibers with different types
crete. PVA fiber contains hydroxyl group (OH) in its molecular and lengths on the cracking resistance and durability of face slab
chains, which could form strong chemical bonding with cement concrete. Therefore, the objective of this study is to investigate
matrix. For this reason, the tensile strength and frost resistance the impact of fiber type and length on cracking resistance and
of concrete can be improved by adding PVA fibers [7,18]. Nam durability of face slab concrete. For this purpose, the influences
et al. [19] verified that the PVA fiber enhanced mortar exhibited of PP, PVA and PAN fibers with different lengths (about 10 mm

2
L. Wang, T. He, Y. Zhou et al. Construction and Building Materials 282 (2021) 122706

and 20 mm) on the cracking resistance and durability including the air-entraining composition. The air-entraining agent (AEA) was
permeability and frost resistance of face slab concrete were used to keep the air content of the concrete at about 5%.
accessed and compared. Then, the parameters of the pores with The fiber reinforced concrete should be carefully prepared since
sizes at micro-, sub micro- and nanoscales were investigated by a it generally involves the balling of fibers and the difficulty of mix-
linear traverse method and the mercury intrusion porosimetry ing the mixture uniformly. The fiber addition in excess of 0.2% by
(MIP), respectively. After that the relationship between the con- volume would make it difficult to mix [6]. In the practical applica-
crete durability and the pore structure parameters were discussed tion of fibers in CFCDs [22,23], the fiber content below or equal to
and revealed. Moreover, the workability, strength development, 1.2 kg/m3 by mass or 0.1% by volume was commonly recom-
shrinkage behavior of the fiber enhanced face slab concrete were mended to prevent the reduction in workability. The recom-
studied and compared. The findings in this study should help to mended dosages above are not conflicting because the mass
better understand the impact of fibers on the cracking resistance content 1.2 kg/m3 can be converted into a volume faction about
and durability of face slab concrete and to select proper fibers in 0.1% based on the fiber density of 0.91–1.30 g/cm3, as shown in
designing face slabs in CFCDs. Table 3. Therefore, the fiber content in this study was kept constant
at 1.2 kg/m3. The sand volume fraction of each concrete mixture
was 33%. The proportions of face slab concrete mixtures as deter-
2. Materials and analytical methods mined by the volume method and their notations are shown in
Table 4. For instance, ‘‘C0” denotes a control concrete mixture
2.1. Raw materials without fiber, ‘‘CPP10” corresponds to a concrete mixture contain-
ing PP fiber with a length about 10 mm. Sufficient mixing is needed
In this study, PI Portland cement with a 28-day strength to achieve a homogeneous dispersion of fibers in concrete mixture.
48.6 MPa and ASTM Type F fly ash were used. Their chemical com- The solid components, i.e., the cement, fibers, and aggregates, were
positions and physical properties were shown in Table 2. Coarse mixed in the rotary mixer for about 5 min firstly, then the pre-
and fine aggregates were sourced from crushed limestone. The mixed water and the superplasticizer were poured in and the con-
density of coarse aggregate and fine aggregate is 2.68 g/cm3 and crete mixture was stirred for another 3 min. The mixing procedure
2.67 g/cm3, respectively. The coarse aggregate is a blend of large above is determined based on lots of preliminary trials, which can
aggregate with a particle size of 20–40 mm and middle aggregate ensure the uniform dispersion of fibers in concrete.
with a size between 5 and 20 mm at a ratio of 4:6. The relatively
small proportion of large aggregate is usually adopted to prevent 2.3. Experimental methods
segregation during the placement of face slab, during which the
chute method is normally adopted. According to this method, the 2.3.1. Compressive strength and splitting tensile strength
fresh concrete slides down through an adjustable steel chute from The compressive and splitting tensile strength of concrete tests
the top of the dam to where the concrete was placed. All coarse and were performed in accordance with DL/T 5150 (test code for
fine aggregates at a saturated surface dry (SSD) condition were pre- hydraulic concrete) [26]. The cubic specimens sized
pared before mixing. Three types of fibers, namely, PVA, PP and 150 mm  150 mm  150 mm were de-molded after 24 h and
PAN, were used in this study. The geometry and properties of fibers cured in a curing room at 20 ± 2 ℃ and relative humidity
were shown in Table 3. (RH) >95%. The compressive strength and splitting tensile were
measured at 7, 28 and 180 days after casting. Three cubic speci-
2.2. Mix proportion design mens were tested to get an average strength result.

The face slab concrete is commonly characterized by an 2.3.2. Volume deformation


extreme high surface, which is easy to crack and usually suffers The thin concrete face slabs with an extreme high surface are
from huge water pressure. The face slab concrete with a C30 generally susceptible to drying shrinkage, which is the main source
strength grade was prepared by using a 0.37 W/B ratio and a 20% of cracking of them. The autogenous shrinkage is also one of the
fly ash replacement ratio based on Chinese standard DL/T 5016 primary forms of volume deformation which can cause cracking.
(Design code for concrete faced rockfill dams) [24] and some pre- Drying shrinkage and autogenous shrinkage of concrete were
liminary trials. DL/T 5016 specified in detail about the ranges of determined using test methods specified in DL/T 5150 [26]. Drying
W/B ratio, fly ash dosage and air content used in face slab concrete shrinkage was performed on concrete specimens with a size of
[25]. To achieve a target slump value of 50–70 mm, a polycarboxy- 515 mm  100 mm  100 mm. Three specimens were prepared
late based superplasticizer at a dosage range of 0.6%–1.0% by for each concrete mixture. The specimens were cured under labo-
weight of binder was used. Notice this superplasticizer has no ratory conditions for 24 h before demolding, after that they were
placed in a drying room (20 ± 2 °C and 50 ± 5% RH) until tested.
The initial length and length changes of the concrete specimens
Table 2 under drying conditions at various ages up to 180 days were
Physical properties, chemical compositions of PI cement and fly ash.
recorded and calculated to determine the drying shrinkage value.
Parameters PI cement Fly ash The average value of measurements for three specimens was
Chemicals reported.
CaO 61.3 2.9 During the autogenous shrinkage test, for each concrete mix-
SiO2 19.3 54.5 ture, the fresh concrete was casted into three cylindrical steel bar-
Fe2O3 4.3 10.2 rels with a size of U 200 mm  500 mm. Before casting, a strain
MgO 3.7 2.9
SO3 2.6 0.4
meter was placed in the center of the barrel. Then, the steel barrels
Al2O3 4.7 24.8 filled with fresh concrete were welded and sealed to stop any
Loss on ignition (wt%) 1.2 2.2 moisture exchange between the concrete sample and external
Physical properties environment. After that, the sealed specimens were stored in a
Blaine specific surface area (m2/kg) 326 386 room and maintained at 20 ± 2 °C. The data measured by the strain
Fineness (retain in 45 mm sieve) 8.4 6.8 meter were recorded up to 180 days and used to calculate the
Specific gravity 3.19 2.32
autogenous shrinkage of concrete. The calculation processes and
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L. Wang, T. He, Y. Zhou et al. Construction and Building Materials 282 (2021) 122706

Table 3
Geometry and properties of PP, PVA and PAN fibers used in this study.

Fiber type Length (mm) Diameter (lm) Aspect ratio* Density (g/cm3) Tensile strength (MPa) Elastic modulus (GPa)
PP10 11.5 40 288 0.91 425 4.8
PP20 20 40 500 0.91 425 4.8
PVA10 12 30 400 1.30 1538 36
PVA20 20 30 667 1.30 1538 36
PAN10 11 24 458 1.18 570 16
PAN20 21 24 875 1.18 570 16

*Aspect ratio is the length to diameter ratio of fibers

Table 4
Mix proportions of face slab concrete.

Notation Mix proportions (kg/m3) Air content Slump


water cement fly ash sand coarseaggregate fiber plasticizer AEA
C0 120 259 65 635 1294 0 1.95 0.08 4.3 69
CPP10 120 259 65 635 1294 1.2 2.59 0.08 6.3 64
CPP20 120 259 65 635 1294 1.2 3.24 0.08 6.8 58
CPVA10 120 259 65 635 1294 1.2 2.59 0.08 5.6 57
CPVA20 120 259 65 635 1294 1.2 3.24 0.08 6.0 51
CPAN10 120 259 65 635 1294 1.2 2.59 0.08 5.1 52
CPAN20 120 259 65 635 1294 1.2 3.24 0.08 5.4 46

equations have been descripted in detail in our previous studies was also recorded. The average result of three specimens was
[27,28]. A mean value of three measurements was used as a result reported for each concrete mixture.
for each concrete.

2.3.3.2. The temperature stress testing machine (TSTM) test. The tem-
2.3.3. Crack resistance perature stress testing machine (TSTM, produced by ‘‘Walter + Bai”
The concrete face slabs are generally restrained by the rockfill, company, Switzerland), was another means in this work to study
foundations, or other structural members during operation. In the early-age cracking resistance of concrete, as shown in Fig. 2.
addition, the concrete face slabs in northern and northwestern The TSTM provides different restraint degrees and an adiabatic
China frequently suffer from severe moisture loss and large tem- condition to concrete specimens for better simulating the actual
perature fluctuations during the day and night. The synergetic working conditions of the mass concrete, which can be used to test
effects of restraint action, temperature drop and moisture loss will the resistance of concrete to the temperature stress-induced crack-
evidently induce large tensile stresses or even cause cracking of ing [20,32–34]. The cracking time and rate of stress development of
concrete. Therefore, the cracking risk of face slab concrete is very samples in the TSTM test depend on a variety of factors, including
high especially at early age when the tensile strength of concrete the thermal expansion coefficient of both the concrete and the
is relatively low. The assessment of the cracking resistance of face restraining instrument, mechanical property of concrete, and cool-
slab concrete at early age is essential in CFCDs design and con- ing rate, etc. The cooling rate of 1–5 °C/hour was recommended by
struction. In this study, the resistance of face slab concrete to RILEM TC 119 [35] and was widely adopted in many relative stud-
restrained shrinkage-induced and the temperature stress-induced ies [20,32–34]. If the cooling rate is higher than 8 °C/hour, temper-
cracking is evaluated based on the restrained shrinkage ring test ature difference may develop between the center and surface of
and the temperature stress testing machine (TSTM) test, the specimen, which could lead to a thermal stress gradient
respectively. through the concrete cross section [36]. The main procedure of
TSTM test conforming to RILEM TC 119 [35] and Refs. [32–34]
was as follows. Firstly, the fresh concrete was cast into the machine
2.3.3.1. The restrained shrinkage ring test. The restrained shrinkage chamber to form a specimen sized 15 cm  15 cm  150 cm. Before
ring test based on ASTM C 1581 is an effective means to evaluate casting, a plastic film was paved in the chamber to eliminate the
the risk of shrinkage-induced cracking of concrete at early age frictional restraint of the chamber wall on the specimen and to pre-
[29,30]. According to ASTM C 1581 [31], the thickness, outer diam- vent water exchange, as shown in Fig. 2(b). Then the temperature
eter and inner diameter of the concrete rings are 152 mm, 406 mm and restraint stress developments of the specimen in a completely
and 330 mm, respectively. Three ring specimens were prepared for constrained and semi-adiabatic conditions were recorded. In order
each concrete mix. During the test, the fresh concrete with large to provide a completely constrained condition, the ends of the
aggregate (greater than 20 mm in size) sieved out were cast into specimens were clamped to prevent any length change during
the molds, then the outer steel ring of the mold was removed after the test. The semi-adiabatic condition can be achieved by adjusting
24 h of standard curing. Thereafter, the top surfaces of the speci- the temperature of the circulating medium through pipes within
mens were sealed with a layer of sealant, in order to make sure the chamber side wall to an equivalent temperature with that
the drying of specimens occurs solely from the outer circumferen- inside the concrete specimen. When the peak temperature of the
tial surface. Subsequently, the specimens were moved in a drying concrete specimen occurred and subsequently maintained for
room (20 ± 2 °C and RH 50 ± 5%), the inner steel rings were bonded 3 days, the specimen was cooled down at a rate of 5 °C/hour by cir-
with strain gauges to measure the strains under drying, as shown culating the cool medium in the pipes until the cracking occurred.
in Fig. 1. The strains of each specimen were recorded continuously Since the cooling period is usually within dozens of hours to sev-
until a sudden change in strain curve occurred, which corre- eral days depending on the cooling rate adopted, the concrete
sponded to the cracking of a ring specimen. The cracking time shrinkage caused by the cement hydration (i.e., autogenous shrink-
4
L. Wang, T. He, Y. Zhou et al. Construction and Building Materials 282 (2021) 122706

Fig. 1. The diagram of the restrained shrinkage ring test (a) the tested concrete rings and (b) cracking of the rings.

Table 5
Key parameters obtained from the TSTM test [35].

Parameters Definitions
1st Zero stress Under restrained condition, the temperature at
temperature TZ,1 which compressive stresses during the generation
of hydration heat first occur, which describes the
change of concrete from plastic to visco-elastic
behavior.
Maximum Maximum compressive stress under restrained
compressive stress conditions during the temperature rise.
rc,max
Maximum Maximum temperature of the concrete specimen
temperature Tmax during hardening under semi-adiabatic conditions.
2nd Zero stress During the cooling phase, temperature at which the
temperature TZ,2 compressive stresses decrease completely to zero
and tensile stresses start to generate.
Tensile strength r Tensile stress at time of cracking, which
corresponds to the peak point in the stress-time
curves during the cooling phase.
Cracking temperature Temperature at which the restrained specimen
Tc cracks, i.e., the tensile stresses exceed the tensile
strength, which characterizes the cracking tendency
of the concrete tested. The higher Tc, the higher
tendency to thermal cracking at early ages.

ter and bottom diameter of 150 mm, 175 mm and 185 mm, respec-
tively, were cured for 28 days in a standard curing room and tested
simultaneously for each concrete mix. During this test, the circular
surfaces of the cylindrical specimens were coated with a layer of
paraffin, then the specimens were placed in the instrument. Once
the test began, the water pressure was increased directly to
1.2 MPa and maintained for 24 h. After that the water pressure
was unloaded and the specimens were split into two parts longitu-
Fig. 2. The diagra of the temperature stress testing machine (TSTM) test (a) the
dinally. Finally, the average water seepage height (Dm) of each
apparatus and (b) specimen casting. group of concrete specimens was calculated based on the measure-
ments of ten points along the fracture surface for each specimen.
The relative permeability coefficient (Kr) of concrete can be
age) during the cooling period can be neglected. Besides, no mois- determined by Eq. 1 [26], which is shown below.
ture exchange occurs during the TSTM test, therefore the cracking
was primarily due to the temperature-induced stresses rather than Kr ¼ aD2m =2TH ð2Þ
the drying or autogenous shrinkage. The cracking temperature and
cracking time of the specimens were recorded. The cracking ten- where, Kr is the relative permeability coefficient, cm/h; T is the
dency of concretes can be estimated in terms of several key param- duration of the penetration test, which is 24 h in this study; H is
eters obtained from the TSTM test, which are shown in Table 5. the water head (cm) corresponding to a constant water pressure
of 1.2 MPa, herein it is 12 244 cm; a is the absorption ratio of con-
2.3.4. Durability performance crete, which is a constant value of 0.03.
2.3.4.1. Water permeability. Generally, concrete impermeability is
considered as an important property determining the durability 2.3.4.2. Frost resistance. The rapid freezing and thawing method
of concrete, particularly for concrete subjected to a high-water specified in DL/T 5150 was used to estimate the frost resistance
pressure [16,37]. The water permeability test of concrete was car- of concrete. The test procedure of this method is almost the same
ried out according to DL/T 5150, using a Hp-4.0 model concrete with Method A described in ASTM C666 [38]. For each concrete
permeability instrument. Six specimens with a height, top diame- mixture, three concrete prisms cured for 28 days with a size of
5
L. Wang, T. He, Y. Zhou et al. Construction and Building Materials 282 (2021) 122706

100 mm  100 mm  400 mm were used to get the average test dental errors, all the results in Figs. 3 and 4 are the average values
results. During the frost resistance test, the specimens subjected of measurements conducted on five individually mixed samples for
to 400 freezing-thawing cycles and each cycle lasted for 4 h, each concrete proportion. It should be noted that the standard
including a quick temperature decline down to 17 °C that lasted error in all cases are less than 5% compared with the corresponding
for 2.5 h, followed by a temperature rise from 17 °C to 8 °C with a average value.
duration of 1.5 h. During the freezing-thawing actions, concrete *The notation ‘‘C” in the figures refers to the concrete samples,
would suffer from both superficial and internal damage. Superficial the numbers ‘‘10” and ‘‘20” denote the fiber length
damage leads to gradual surface scaling and therefore the mass As shown in Table 4, to obtain the target slumps of 50–70 mm,
loss of specimens, whereas internal damage reduces the relative various superplasticizer dosages have been used. In general, the
dynamic modulus of elasticity [39]. Hence, mass loss and the rela- superplasticizer dosage increases from 0.6 wt% of binder for a con-
tive elastic modulus are two typical parameters to evaluate the trol mix C0 to 0.8 wt% and 1.0 wt% for concrete mixes containing
frost resistance of concrete. Air content is the main factor influenc- fibers with lengths of 10 mm and 20 mm, respectively. It is widely
ing the frost resistance of concrete [40]. To improve the frost resis- reported that the inclusion of fiber in concrete could reduce the
tance of concrete, AEA is generally added during concrete mixing. workability and slump of concrete, because the evenly distributed
Besides, the air void structure of concrete, such as the air void spac- fibers with high specific surface and small diameter may create a
ing, air void number and size are believed to affect the frost resis- close network between fiber and cement matrix due to the fiber
tance significantly [40–44]. The changes in weight loss and the bridging effect, which inevitably inhibits the flowability of fresh
relative elastic modulus of the specimens were recorded per 50 concrete mixture [12].
freezing-thawing cycles. Comparison of the results in Fig. 3 indicates that the fiber aspect
ratio and length affect the workability of concrete. For instance,
PAN20 fiber with the largest fiber aspect ratio (8 7 5) in this study
2.3.5. Pore structure and air void parameters
gives the smallest concrete slump of 46 mm. By contrast, CPP10
The porosity and pore size distribution of concrete were ana-
fiber, which has the smallest aspect ratio of 288, produces the lar-
lyzed by using a mercury porosimeter (Micrometrics AutoPore IV
gest slump of 64 mm. As shown in Table 3, the diameter of PAN is
9510, U.S.A.) with a maximum intrusion pressure of 414 MPa.
only 60% and 80% of that of PVA and PP fiber, respectively. At a
The cubic samples sized about 5 mm  5 mm  5 mm were sawed
given fiber content and length, a finer fiber provides a higher num-
from the center of the concrete specimens at 3, 28 and 180 days.
ber of fibers in per unit volume of concrete, resulting in a stronger
The limestone coarse aggregates, which are light-grey in color
fiber bridging effect and hence a smaller slump, and vice versa.
and can be easily identified, should be stripped out. Three cubic
Besides, the fiber bridging effect becomes more significant with
samples were placed in a sealed glass sample container with a vol-
the increase in fiber length, which would produce an increase in
ume about 5 mL for each MIP test. Three MIP measurements were
viscosity of fresh concrete and hence a further decrease in slump
performed on each concrete mixture and the average result was
value, as shown in Fig. 3. The same trend has been reported by
reported. These measures could effectively minimize the MIP test
others who investigated the effects of flax fiber on workability of
errors caused by the variations in sample preparation and dimen-
high-clay content concrete [15] and PVA fiber on the flowability
sion, or in instrument operations.
of cement mortars [19].
The air void parameters including total number of air voids,
Fig. 4 reveals that the air content of concrete increases with the
hardened air content, average air void diameter and spacing factor
addition of fibers. Noted that the AEA dosage in all the concrete
of concrete cured for 28 days were determined by the linear tra-
mixtures are the same, the increase in air content was due to the
verse method according to ASTM C 457 [45]. This method can be
air-entraining effect of fibers. The fibers added in concrete could
used to estimate the likelihood of damage due to freezing and
increase the viscosity of the fresh matrix, which tends to prevent
thawing cycles or to explain why it has occurred [45]. The air void
some air bubbles from escaping during vibration and mixing and
analyses were carried out on a Rapid air 457 automatic air void
hence increases the amount of the entrapped air voids inside the
analyzer, which could characterize the pores with the diameter
concrete [16,18].
ranging from about 10 lm to 2000 lm. The diagram of the air void
A comparison between Fig. 4(a) and Fig. 4(b) shows that this
analyzer and the testing procedure of this method are described in
fiber air-entraining effect enhances with the fiber length. This cor-
detail in our previous study [25]. The concrete hydrated at 28 days
responds well with the findings reported by Nathalie et al.[15] who
was sawed up into slices sized 15 cm  15 cm  1 cm for air void
conducted experiments on flax fibers. Additionally, Fig. 4 indicates
parameter tests. The surfaces of the slices were ground and pol-
the PP fibers produce the highest air content in this study, followed
ished sufficiently to produce a smooth surface for the tests. Then
by the PVA fiber and PAN fiber. As Söylev and Özturan [46]
the surfaces of samples were painted with a layer of fluorescer
reported, the entrapped air content varied with the fiber type. In
carefully, so that the air voids on the surfaces can be identified
the previous study performed by Nam et al. [19], the addition of
and tested by the air void analyzer under the ultraviolet irradia-
PP fibers generated a higher flowability and air content than the
tion. For each concrete mix, the average air void parameter values
PVA fiber under the same experimental conditions including the
were obtained from three specimens, two slices were prepared for
fiber length. The differences in air content caused by the fiber type
each specimen and 7 linear traverses were evenly arranged on the
may be associated with the physical and chemical property differ-
surface of each slice, therefore the total length of linear traverses
ences of fibers, which will be investigated in the future work.
was 6 300 mm.
Fig. 3(c) and Fig. 4(c) indicate that there are significant losses in
both slump and air content with time for all concrete mixtures. At
3. Results and discussion first 0.5 h, all the concretes exhibit air content and slump losses
about 19%–24%, while at 1 h, these values increase to about 40%–
3.1. Properties of fresh face slab concrete 46%. Nevertheless, only slight differences in slump and air content
losses can be observed among different concretes, indicating the
The slump and air content of fresh concretes containing PP, PVA effects of fiber type and geometry on slump and air content losses
and PAN fibers with different lengths as well as their losses with appear to be insignificant. These losses are probably attributed to
time are shown in Figs. 3 and 4, respectively. In order to avoid acci- the continuous loss in superplasticizer efficiency with time.

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L. Wang, T. He, Y. Zhou et al. Construction and Building Materials 282 (2021) 122706

Fig. 3. Slump of concretes containing fibers with a length about (a) 10 mm and (b) 20 mm and the slump loss with time.

Fig. 4. Air content of concretes containing fibers with a length about (a) 10 mm and (b) 20 mm and the air content loss with time.

3.2. Compressive and splitting tensile strength of face slab concrete higher than the compressive strength enhancements due to fiber
addition. Similar results of tensile strength and compressive
The compressive and splitting tensile strengths of control con- strength enhancements by fibers have been reported elsewhere
crete and concretes containing PP, PVA and PAN fibers with differ- [6,7]. The enhancement of fibers on splitting tensile strength is
ent lengths are measured and plotted in Fig. 5. The error bars in because the evenly distributed fibers in the matrix can act as
Fig. 5 correspond to the standard deviation of three concrete sam- stitches between two cracked sections to transfer the tensile stres-
ples tested for each concrete proportion at each hydration time. It ses and improve the tensile capacity [6,48].
is clearly seen from Fig. 5 that the compressive and splitting tensile Fig. 5(c) and (d) also show that varying fiber type and length
strengths of all concretes increase with the curing time. could significantly affect the splitting tensile strength. Generally,
From Fig. 5(a) and (b), it can be found the incorporation of fibers the concrete added with PVA fiber exhibits larger splitting tensile
raises the compressive strength slightly, and the increments are strengths than the concrete with PP fiber and PAN fiber. For
within 3.1%–7.3% at various hydration time. These slight incre- instance, the inclusion of PVA with a length about 10 mm increases
ments are reported to result from the absorption of energy by the splitting tensile strength of C0 concrete by about 11.5%–12.5%
fibers, which could transfer the stresses through them to prevent at different ages, whereas the increments are 5.4%–5.8% and 8.8%–
the concrete from rupture [6]. Prior studies demonstrated that 9.5% for PP fiber and PAN fiber, respectively. The same phe-
the addition of fibers in a proper range (usually below a volume nomenon can be also found for the fibers with a length about
fraction of 0.25%) was beneficial to improve the compressive 20 mm. This is partly because the PVA fiber is higher in elastic
strength of concrete, whereas fibers exceed this dosage range could modulus value than the PP and PAN fibers, as shown in Table 3.
decline the compressive strength obviously [7,19,47]. It is notice- It is widely reported that fibers with a higher elastic modulus could
able that the fiber content in this study is within this optimal inhibit the generation and development of micro-cracks and conse-
range. In addition, it is hard to clearly distinguish the effects of quently improve the tensile strength of concrete [6]. Another pos-
fiber type and length on the compressive strength because the sible reason is that PVA fiber tends to generate a strong chemical
strength differences are within the error range of 5%. For example, bonding with cement matrix due to the presence of the hydroxyl
Fig. 5 shows that at various hydration ages, the compressive group in its molecular chains [18]. The smallest splitting tensile
strength of concrete added with PVA, PAV and PP fiber is reduced strength of PP fiber enhanced concrete among all the fiber
by 1.1%2.4%, 1.6%–0.9% and 1.5–2.2%, respectively, as the fiber enhanced ones could be also explained in part by the low elastic
length increases from 10 mm to 20 mm. These results are consis- modulus of PP fibers. Besides, it has been proved that PP fiber
tent with those reported by Nathalie et al. [15], who summarized had a smooth surface and was inert in high pH environment, thus
the length of fibers did not show a significant effect on the com- it was hard to form strong bonding strength with cement matrix
pressive strength. [8].
Fig. 5(c) and (d) indicate that the addition of fibers enhances the Moreover, an increase in fiber length from about 10 mm to
splitting tensile strength by about 5.5%–15.6% at 3 days, 5.4%– 20 mm may further increase the splitting tensile strength of con-
16.8% at 28 days and 5.8%–17.2% at 180 days, which are noticeably crete, regardless of the fiber type. This can be attributed to the

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L. Wang, T. He, Y. Zhou et al. Construction and Building Materials 282 (2021) 122706

Fig. 5. Compressive strength and splitting tensile strength of concretes containing PP, PVA and PAN fibers with lengths about (a) and (c) 10 mm; (b) and (d) 20 mm.

enhanced adherence between the fibers and matrix when longer 3.3. Volume deformation of face slab concrete
fibers are used [21,49]. The trend is consistent with previous inves-
tigations on glass fibers by wang et al. [49] and PP plastic fibers by 3.3.1. Drying shrinkage
Shen et al. [21]. For instance, at a fiber content of 8 kg/m3, the The drying shrinkage of control concrete and concretes contain-
increase in PP plastic fiber length from 16 mm to 60 mm could ing PP, PVA and PAN fibers with different lengths is shown in Fig. 6.
increase the splitting tensile strength of high strength concrete Fig. 6 indicates that more than 60% of the drying shrinkage of all
from 5.02 MPa to 8.15 MPa [21]. The slightly lower splitting tensile the concretes is generated during the first 14 days of drying, there-
strengths of fiber-enhanced concrete in this study than those in after the shrinkage develops slowly up to 180 days. The results in
Ref. [21] are mainly due to the differences in W/C ratios of concrete Fig. 6 show that the utilization of fibers tends to reduce the 180-
and fiber type. day drying shrinkage of concretes by about 5.5%-18.5%, depending
on the fiber type and length. It is widely reported that the bridging

Fig. 6. Drying shrinkage of concretes containing PP, PVA and PAN fibers with a length about (a) 10 mm (b) 20 mm.

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L. Wang, T. He, Y. Zhou et al. Construction and Building Materials 282 (2021) 122706

forces between fibers and matrix could restrain the shrinkage Fig. 7(a) also indicates that the inclusion of PP, PVA and PAN
development of concrete, since the randomly well-distributed fiber with a length about 10 mm reduces the autogenous shrinkage
fibers could provide a three-dimensional reinforcement for the of C0 concrete by about 5.6%, 13.5% and 9.0% at 14 days and 5.3%,
structure to resist the inner tensile force [6,15,47]. 11.4% and 8.3% at 180 days, respectively. The better performance of
For the 10 mm-level fibers, the data in Fig. 6(a) reveals that the PVA fibers than PP and PAN fibers in reducing the autogenous
drying shrinkage reduction effect was greatest for PVA fiber among shrinkage can be also observed for the concrete added with
all the fibers used in this study, followed by the PAN fiber and PP 20 mm-level fibers.
fiber. Specifically, PVA fiber reduces the drying shrinkage of C0 Additionally, the results in Fig. 7 show that the fibers with a
concrete by about 13.0% at 14 days and 12.4% at 180 days, followed length about 20 mm is more efficient in reducing the autogenous
by the PAN fiber and PP fiber, which lower the drying shrinkage of shrinkage than the 10 mm-level fibers. For instance, the 20 mm-
C0 concrete by about 9.5% and 5.8% at 14 days, 8.6% and 5.5% at level PVA fiber reduces the autogenous shrinkage strains by about
180 days, respectively. The same trend could be also found for 5.5%6.6% % at 14 days and 5.1%6.2% at 180 days, compared with
the 20 mm-level fibers in Fig. 6(b). The better performance of the the concrete added with 10 mm-level PVA fibers. These results are
PVA fiber than other types of fiber in reducing the shrinkage is in good agreement with those reported by others. For example,
probably due to its higher tensile strength and higher adherence Shen et al. [21] found increasing Barchip fiber length from
with cement matrix. Although the number of PAN fibers per unit 42 mm to 60 mm reduced the autogenous shrinkage of concrete
concrete volume is larger due to its smaller diameter than PVA by about 15%28%. The obviously higher efficiency of fibers in
fiber, the tensile strength of PAN fiber is only about 37% of that reducing the autogenous shrinkage in Ref. [21] could be attributed
of PVA, hence the PAN fiber may not provide bridging force as to the much higher fiber content (i.e., 8.0 kg/m3) than in this study
strong as the PVA fiber. The PP fiber exhibits the weakest tensile (i.e., 1.2 kg/m3). Similarly, Nathalie et al. [15] observed that the
strength, which may explain its weakest ability to resist the drying shrinkage decreased with the increase in flax fiber length from
shrinkage development among the three fiber types used in this 12 mm to 50 mm at various fiber contents. As mentioned above,
study. longer fibers could produce a better adherence with cement matrix
As for the fiber length effect, it can be observed that the 20 mm- than the shorter ones. However, the optimum fiber length selected
level fibers are more effective than the 10 mm-level ones in reduc- in practical use should be comprehensively evaluated combing the
ing the shrinkage strains. For instance, the drying shrinkage of con- workability, strength, and durability factors. One basic principle is
crete with 20 mm-level PVA fiber is reduced by 5.7%6.6% at that the longer fibers should be used without compromising other
14 days and 5.3%7.0% at 180 days, compared with the concrete important concrete properties.
added with 10 mm-level PVA fibers. This is due to the fact that
increasing fiber length generally enhances the adherence between
fibers and matrix and provides a sufficient stress transfer, which 3.4. Crack resistance of face slab concrete
could reduce the concrete shrinkage efficiently [6,15,21].
3.4.1. Concrete ring test results
In the concrete ring test, the shrinkage of concrete caused by
3.3.2. Autogenous shrinkage the drying and cement hydration is restrained by the steel rings,
The autogenous shrinkage of control concrete and concretes which inevitably generates tensile stress in the specimens [6,52].
containing PP, PVA and PAN fibers with different lengths is shown The cracking will occur when the tensile stress exceeds the tensile
in Fig. 7. strength of concrete. The restrained shrinkage strain and initial
Alike the effects of fibers on drying shrinkage, Fig. 7 displays the cracking time of concretes containing PP, PVA and PAN fibers with
addition of fibers inhabits the autogenous shrinkage development. different lengths are presented in Fig. 8. The maximal restrained
The phenomenon could be explained by the following two reasons. shrinkage strain, which is also called cracking strain, corresponds
Firstly, the fiber addition may generate a complex three- to the shrinkage strain when cracking occurs. The initial cracking
dimensional fiber–matrix system, a water film may also form on time is the time when cracking occurs. These two parameters are
the surface of fibers, both of which slow down the water flow closely related with the cracking resistance of concrete and there-
and water loss, thus reducing the self-desiccation and autogenous fore can be adopted to estimate the cracking potential of concrete
shrinkage. Secondly, the autogenous shrinkage development could [53]. Generally, the high cracking strain and the long initial crack-
be effectively restrained by the bridging forces between fibers and ing time of the concrete rings imply a high stress bearing capacity
cement matrix [50,51]. and a high ductility of concrete. Fig. 8(a) indicates that the

Fig. 7. Autogenous shrinkage of concretes containing PP, PVA and PAN fibers with a length about (a) 10 mm (b) 20 mm.

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L. Wang, T. He, Y. Zhou et al. Construction and Building Materials 282 (2021) 122706

Fig. 8. The concrete ring test results of concretes containing PP, PVA and PAN fibers (a) restrained shrinkage strain with time and (b) initial cracking time.

restrained shrinkage of all concretes increases with time until a 3.4.2. TSTM test results
sudden drop occurs, which corresponds to the cracking of concrete, In addition to the stresses caused by the drying shrinkage and
and thereafter it declines to about zero due to the release of tensile autogenous shrinkage, the face slab concrete frequently suffers
stress in concrete. This trend is in good agreement with previous from the temperature-induced stress, which is also the main cause
ring test findings [6,30,52,53]. of cracking. Therefore, it is necessary to investigate the effects of
It is clear from Fig. 8 that the fibers can improve the resistance fibers on the resistance of face slab concrete to the thermal stres-
of concrete to drying shrinkage-induced cracking by increasing the ses. The key temperature stress parameters obtained from the
cracking strain and prolonging the initial cracking time, irrespec- TSTM test conducted on control concrete and concretes containing
tive of the fiber type. Similar ring test results were obtained by PP, PVA and PAN fibers with different lengths are given in Table 6.
Yousefieh et al. [6], they found that the fibers such as steel fiber, Fig. 9 is a typical example of TSTM curves of control concrete (C0),
PP and polyolefin fiber could act as micro steel bars to increase concretes containing 10 mm-level PVA (CPVA10) and 20 mm level-
the cracking strain and provide more time for stress bearing before PVA (CPVA20). From Fig. 9, all the concrete samples exhibit similar
cracking. Also, Fig. 8 illustrates that the cracking resistance is temperature stress development, i.e., the compressive stresses of
affected notably by the fiber type and length. concrete increase with the internal temperature rising until the
Concerning the fiber type, Fig. 8 clearly shows that the PVA peak temperature is reached. Subsequently the compressive stress
fiber-enhanced concrete exhibits the best cracking resistance to is somewhat reduced even though the peak temperature of con-
restrained shrinkage, followed by the PAN one and PP one. For crete is kept constant. The same phenomenon of decreasing stress
instance, the cracking strain of concrete with 10 mm-level PVA in concrete subjected to a constant deformation during the TSTM
fibers is equal to 58.6  106, which is about 20.3% and 9.2% larger test has been reported by others, who referred to this phenomenon
than that of concrete containing PP and PAN with the same length. as stress relaxation [33]. As the temperature is cooled down, the
Correspondingly, the initial cracking time of CPVA10 is about 15 h tensile stress gradually develops until the cracking occurs, which
and 9 h longer than that of the CPP10 and CPAN10, respectively. corresponds to the peak point in Fig. 9(b).
The similar observation can be also found for the 20 mm-level It can be figured out from Table 6 and Fig. 9 that, the tempera-
fibers. The best cracking resistance of PVA fiber-enhanced concrete ture stress parameters such as the TZ,1, TZ,2, rc,max and Tmax are
in this study can be partly explained by the highest elastic modulus almost the same for all the concretes in this study. It was suggested
and tensile strength of PVA fiber among all the fibers used in this that TZ,1, TZ,2, rc,max and Tmax depend mainly on the binder amount
study. It was suggested that the addition of fibers with higher elas- used in concrete [54]. Herein, the binder amount is almost the
tic modulus and tensile strength could more effectively reduce the same for all the concrete samples, as shown in Table 4. Conse-
concrete shrinkage and improve the cracking resistance of concrete quently, the fibers would not affect the TZ,1, TZ,2, rc,max and Tmax val-
[6]. Therefore, the PVA fibers enhanced concrete could resist higher ues in this study, leading to the highly overlapping of the
cracking tendency and bear larger tensile stresses than concrete temperature stress curves of various concretes before the cooling
added with other fibers. The second possible reason could be the period in Fig. 9.
high hydrophilic property of the PVA fiber, which could result in It is interesting to note that the fiber type and length have an
better adherence between fibers and cement matrix, and finally obvious impact on tensile strength r and cracking temperature
prevent crack development far better [7,19]. Tc of concrete. According to RILEM TC119 [35], Tc and r are critical
Regarding the fiber length, Fig. 8 shows that increasing fiber parameters characterizing the anti-cracking performance of con-
length further increases the cracking strain and initial cracking crete. The higher Tc and r values provide a higher capacity of con-
time. To be specific, a prolongation in initial cracking time about crete to surfer from the tensile stress development caused by the
11.0–15.0 h and an increase in cracking strain about 15.5%–20.7% temperature decline.
can be observed for concretes with 20 mm-level fibers compared The results in Table 6 indicate that, PVA fiber exhibits the best
with those of concretes with 10 mm-level ones. As discussed efficiency in improving the resistance of concrete to temperature
above, the longer fibers tend to provide higher degrees of stress stress-induced cracking, followed by the PAN fiber and PP fiber.
transfer and stronger bridging forces to prevent the crack develop- To be specific, the 10-mm PVA fibers increase the r value of C0
ment and propagation, resulting in a stronger stress bearing capac- concrete by about 18% at the time of cracking, while the incre-
ity and finally a better cracking resistance [6,15]. Additionally, ments of r due to the addition of PP fiber and PAN fiber with the
increasing fiber length could enhance the bonding network same length are about 7% and 13%, respectively. The best perfor-
between the matrix and fibers, leading to enhanced bonding mance of PVA fibers among all the fibers in raising r can be also
strength and cracking resistance of concrete [20]. found for the 20 mm-level ones, followed by the PAN fiber and

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Table 6
The key temperature stress parameters of concretes containing PP, PVA and PAN fibers.

Notation 1st Zero stress Maximum compressive stress Maximum 2nd Zero stress Tensile strength Cracking
temperature TZ,1 (°C) rc,max (MPa) temperature Tmax(°C) temperature TZ,2 (°C) r (MPa) temperature Tc (°C)
C0 25.6 0.23 59.6 51.4 0.83 12.68
CPP10 25.4 0.23 59.4 51.9 0.89 9.8
CPP20 25.1 0.24 59.3 52.1 0.96 4.2
CPVA10 25.3 0.23 59.7 52.5 0.98 3.8
CPVA20 25.9 0.24 59.4 52.3 1.07 2.7
CPAN10 25.3 0.22 59.5 52.1 0.94 7.1
CPAN20 24.9 0.23 59.2 51.8 1.02 1.5

the PVA fibers with a length about 20 mm present the best perfor-
mance to reduce the thermal cracking risk of concrete in this study,
which is consistent with the concrete ring test results above and
the findings reported by others. Based on a series of TSTM tests,
Shen et al. [20] proposed that increasing Barchip fiber length from
42 mm to 54 mm improved the concrete resistance to the temper-
ature decline. It is also interesting to note that increasing fiber
length may appreciably weaken the workability of concrete, as evi-
dent in Section 3.1. It was reported that when the Barchip fiber
length exceeded 54 mm, the poor dispersion of fibers may lead
to the decrease in early age behavior and cracking resistance
[20]. Additionally, a weakening trend of cracking resistance of
high-strength concrete due to the increase in fiber length has been
reported for PP plastic fibers [21]. These seemingly conflicting
effects of fiber length on concrete cracking resistance above may
be caused by the significant difference in fiber type and concrete
properties. Therefore, the proper fiber type and length should be
examined before engineering applications.
It should be noted that only one cooling rate was selected in this
study. Further study will be conducted to understand the cooling
rates on the stress development during the TSTM test, which is
beyond the scope of the present paper.

3.5. Durability of face slab concrete

3.5.1. Permeability
The permeability of concrete is generally characterized by two
indexes, i.e., water seepage height (Dm) and relative permeability
coefficient (Kr). The permeability results of concrete containing
PP, PVA and PAN fibers with different lengths are shown in Table 7.
The results in Table 7 are the average values of six specimens mea-
Fig. 9. An example of the TSTM curves of C0, CPVA10 and CPVA20 concretes.
sured for each concrete mix hydrated at 28 days.
As presented in Table 7, the inclusion of fibers with a content of
PP fiber. Moreover, Table 6 shows that the PVA fibers lower the Tc
1.2 kg/m3 could increase the Dm and Kr values of concrete, irre-
value of C0 concrete by about 8.9 ℃, whereas the PP and PAN fibers spective of the fiber type. For instance, the average Dm and Kr val-
reduce the Tc by only 2.9 ℃ and 5.6 ℃ on average, respectively,
ues of CPAN10 concrete are about 22% and 48% larger compared
demonstrating that PVA fibers have the greatest impact on improv- with those of C0 one, respectively. Similar results of the adverse
ing the cracking resistance to thermal stresses.
effect of fibers on concrete impermeability have been reported
In addition, Table 6 shows that the increase in fiber length is by Toutanji [17] and Cao et al. [13], who ascribed the increased
also beneficial for the improvement of the cracking resistance.
chloride ion permeability to the increase in air content due to PP
For example, increasing the fiber length from 10 mm to 20 mm
increases the r values by about 7.9%  9.2%. This observed trend
is in agreement with the splitting tensile results in Section 3.2 Table 7
and the ring test results in Section 3.4.1 as well as the findings The 28-day permeability results of concretes containing PP, PVA and PAN fibers with
different lengths.
by Ref. [21]. Table 6 also displays the beneficial effect on Tc
becomes more obvious as the fiber length increases, irrespective Notation Water seepage height Relative permeability coefficient Kr
of the fiber type. For example, the 20 mm-level PP, PVA and PAN Dm(cm) (107 cm/h)
fibers could reduce the Tc by about 5.6 ℃, 6.5 ℃ and 5.6 ℃, respec- C0 2.3 ± 0.11 2.70 ± 0.25
tively, compared with the concretes with the 10 mm-level fibers. CPP10 3.8 ± 0.12 7.37 ± 0.46
CPP20 4.3 ± 0.15 9.44 ± 0.61
As discussed above, the longer fibers could transfer the tensile
CPVA10 3.3 ± 0.13 5.56 ± 0.43
stress better and provide stronger bridging forces, which endows CPVA20 3.9 ± 0.12 7.76 ± 0.39
the concrete better stress bearing capacity and resistance to tem- CPAN10 2.8 ± 0.13 4.00 ± 0.40
perature decline. Based on Tc and r values, it can be concluded that CPAN20 3.4 ± 0.14 5.90 ± 0.45

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L. Wang, T. He, Y. Zhou et al. Construction and Building Materials 282 (2021) 122706

fiber addition. As Zhang et al. [40] revealed, the chloride ion per- fibers in terms of the frost resistance. Some researchers [16] have
meability of concrete increased with increasing air content when studied the effects of various fibers fractions (0.10%, 0.12%, 0.15%
the air contents varied within the range of 2%-6 %. In this study, and 0.20% by volume) and found that the fiber fraction greater than
the lowered resistance to water permeability may be also attribu- 0.12% could adversely affect the frost resistance of concrete since
ted to the relatively high air content entrained by the fibers, which the fibers beyond this fraction tend to agglomerate together. In this
will be further evidenced in terms of air void parameter in study, the fiber fraction about 0.1% by volume is close to the sug-
Section 3.7. gested reasonable dosages above. There are two reasons responsi-
Moreover, the increase in fiber length may further worsen the ble for this beneficial effect of fibers on frost resistance. On the one
impermeability of concrete, as shown in Table 7. For example, hand, this is in part due to the air-entraining properties of the
the average Dm and Kr values of CPAN 20 are 3.4 cm and fibers [59]. It is known that air content is considered as the main
5.90  107 cm/h, which are about 21% and 47% larger than those factor affecting the frost resistance of concrete [18,58]. The
of CPAN10, respectively. The same trend can be observed for PP entrained air voids could provide empty spaces for accommodating
and PVA fibers. This phenomenon can be also partly explained by the ice expansion, thus relieving the hydrostatic pressure and
the increase in air content due to the fiber length increase. osmotic pressure during the low temperature cycle [16,58]. On
In addition to the fiber length, Table 7 shows that the fiber type the other hand, the ice expansion could cause severe heaving
has an obvious impact on impermeability of concretes, and the effi- cracking stress inside the concrete. The fibers could effectively
ciency in improving the impermeability is in the sequence of improve the stress bearing capacity and restrain the heaving crack-
PAN > PVA > PP. Specifically, from Table 7, among all the fibers ing of concrete, as evidenced above, which consequently slow
enhanced concretes, the PAN fiber enhanced concrete exhibits down the surface scaling rate and decrease the mass loss caused
the lowest Dm and Kr values, that is, the best impermeability, fol- by the freeze–thaw action [13,16,59].
lowed by the PVA fiber enhanced one and PP fiber enhanced one. In addition, the fiber type has significant effects on the frost
The impermeability differences among concretes added with dif- resistance of concrete. As evident from Fig. 10, the frost resistance
ferent fibers could be partly interpreted in terms of their air con- improvement effect is greatest for PVA fiber, followed by the PAN
tent differences. Apart from the air content, many studies [55,56] fiber and PP fiber. For instance, the mass loss of CPVA10 concrete
demonstrated that the volume fraction and micro-geometry of is about 33% smaller than that of the C0 one, while the reductions
the entire pore structure within the cement matrix have a signifi- in mass loss are about 25% and 17% for CPAN10 and CPP10, respec-
cant impact on the concrete permeability. Many pore-structural tively. The same trend can be found when comparing the relative
studies found that the PVA and PP fiber addition would affect the dynamic elastic modulus values. These results can be explained
pore structure of engineered cementitious composites (ECC) [18], by two possible reasons. Differences in air void parameters such
cement mortar [19] and geopolymer concrete [57] remarkably. as the air content may be the first reason for this trend. In addition
Therefore, the impermeability differences of face slab concrete to the air content, it is well demonstrated that other air void
caused by the fiber type and length in this study, which will be dis- parameter such as the air void spacing factor (the average distance
cussed from the viewpoint of pore structure in Section 3.6. between air void centers) and the number of air voids could affect
Although the fibers could raise the concrete permeability, there the frost resistance of concrete [18,40,44]. Further air void analyses
is another important role played by fibers with respect to perme- will be conducted to elucidate the effect the fiber type on frost
ability that must be highlighted is their ability to resist the crack- resistance of concrete in Subsections 3.7. The second possible rea-
ing of concrete. In the practical projects, the permeability of son could be the differences in the stress bearing capacity and
concrete is significantly exacerbated by the cracks in concrete. It cracking resistance of concretes containing different fibers. As
was reported that the permeability of high strength concrete with revealed by the splitting tensile test, ring test and TSTM test in pre-
micro cracks is up to ten times higher in intensity than that of the vious Sections, the PVA fiber is more notably in improving the ten-
concretes without micro cracks [6]. As discussed above, the fibers sile strength, cracking resistance, as well as the tensile stress-
are effective in reducing the shrinkage and the cracking risk of con- bearing capacity than other types of fiber in this study, which
crete. In this regard, fibers could inhabit the formation of cracks eventually enhances the resistance to the heaving cracking as well
and afford superior resistance to the water permeability, as as the surface scaling of concrete in the freezing and thawing
reported by Refs. [16,23]. cycles. The similar findings involving the influences of fiber type
(PVA and PP) have been reported by Nam et al. [19], who summa-
3.5.2. Frost resistance rized that the physical properties of the fibers have significantly
The freezing-thawing cycles may lead to a gradual decrease in influence on the frost resistance of cement mortar based on scan-
dynamic modulus of elasticity and an increase in surface scaling ning electron microscope (SEM) observations.
of concrete. Thus, the weight loss and the relative dynamic modu- Additionally, Fig. 10 shows that the improvement effect of
lus of elasticity are two important parameters to evaluate the frost fibers on frost resistance becomes more notably as the fiber length
resistance of concrete [42]. The mass loss and relative dynamic increase, which may be attributed to the better resistance to ten-
modulus of elasticity results of concretes containing PP, PVA and sile stress and cracking tendency when longer fibers are incorpo-
PAN fibers with different lengths are shown in Fig. 10. The error rated, as demonstrated above. This fiber length effect will be also
bars in Fig. 10 exhibit the standard deviations among the three revealed from the viewpoints of air void parameters in the next
concrete samples tested for each concrete proportion. The errors Section.
shown in Fig. 10 are minor, indicating that the experimental data
are reliable. It can be found from Fig. 10 that all the concrete spec- 3.6. Pore structures and their correlations with durability
imens exhibit mass losses smaller than 5% and relative dynamic
modulus of elasticity larger than 60%, demonstrating that all the The pore structure parameters including the porosity, the criti-
concretes have a frost resistance level as high as F400 according cal pore diameter and the pore size distribution of concretes con-
to DL/T 5150 [26]. taining PP, PVA and PAN fibers with different lengths hydrated at
Fig. 10 indicates the fiber addition is conductive to improve the 3, 28 and 180 days obtained from the MIP tests are given in Table 8.
frost resistance of concrete. Similar results of frost resistance Notice each result in Table 8 is an average of three MIP measure-
improvement by fibers have been reported elsewhere ments with a variation coefficient less than 5%, the results can
[13,16,58,59]. Nevertheless, there exists a reasonable dosage of therefore relatively reliably present the general trend of pore struc-
12
L. Wang, T. He, Y. Zhou et al. Construction and Building Materials 282 (2021) 122706

Fig. 10. The 28-day frost resistance results of concrete containing PP, PVA and PAN fibers: mass loss of concrete with (a) 10 mm fiber and (b) 20 mm fiber; relative dynamic
elastic modulus of concrete with (c) 10 mm fiber and (d) 20 mm fiber.

Table 8
Pore structure parameters of concretes obtained by MIP.

Notation Curing time(days) Critical porediameter (nm) Porosity(%) Pore size distribution
<10 nm (%) 10–50 nm (%) 50 nm–10 lm (%)
C0 3 128 26.5 7.2 29.6 61.3
28 73 21.8 13.6 46.7 38.4
180 38 17.3 16.1 53.8 28.5
CPP10 3 238 33.6 4.3 19.2 72.7
28 155 27.2 10.4 35.3 50.6
180 76 22.4 13.6 42.8 40.2
CPP20 3 267 36.8 3.5 14.5 77.9
28 171 29.8 7.6 31.7 56.2
180 91 23.6 11.9 38.9 46.1
CPVA10 3 203 31.4 6.5 22.2 68.1
28 132 25.1 12.3 38.5 46.3
180 64 20.3 14.4 46.3 35.6
CPVA20 3 231 34.5 5.2 18.5 72.8
28 156 28.1 9.8 35.1 50.6
180 77 22.2 13.2 42.9 41.4
CPAN10 3 144 29.8 7.7 25.8 63.2
28 109 23.3 14.7 41.1 41.8
180 52 18.1 15.3 50.2 31.1
CPAN20 3 176 32.3 6.4 21.5 68.7
28 133 26.4 11.3 39.5 46.3
180 65 20.6 14.2 46.5 36.9

ture development. An example of MIP curves is given in Fig. 11, shown in Fig. 11(b). In this study, the classification method pro-
which clearly shows the cumulative pore volume and the critical posed by Mindess et al. [60] has been adopted. According to this
pore diameter of 3-day concretes containing various fibers are dif- method, pores with diameter ranging from 2.5 nm to 10 nm,
ferent. The critical pore diameter is the size of pores corresponding 10 nm to 50 nm, 50 nm to 10 lm and over 10 lm, are classified
to the peak point of the differential pore size distribution curve
13
L. Wang, T. He, Y. Zhou et al. Construction and Building Materials 282 (2021) 122706

Fig. 11. An example of MIP curve of concrete containing 10-mm level fiber hydrated at 3 days: (a) the cumulative pore volume curve and (b) differential pore size distribution
curve.

as small capillary (gel) pores, medium capillary pores, large capil- Kr values. By contrast, the PAN fibers could make a finer pore struc-
lary pores, and air voids, respectively. ture and a denser cement matrix compared with PVA and PP fibers,
It can be seen from Table 8 that the fibers increase the critical resulting in a lower degree of permeability of concrete.
pore diameter and porosity of concrete. In the case of CPP10 However, a careful analysis of the data in Fig. 10 and Table 8
hydrated at 28 days, the critical pore diameter and porosity are found there is no definite relationship between the frost resistance
155 nm and 27.2%, which are 82 nm and 5.4% higher than those and pore structure of concrete. The PP fiber enhanced concrete
of C0 concrete, respectively. In addition, Table 8 shows the fibers with the highest porosity does not exhibit the best frost resistance.
raise the fraction of large capillary pores and reduce the fractions Similarly, the frost resistance of PAN fiber enhanced concrete is not
of the medium capillary pores as well as the gel pores to some the best even through it has the lowest porosity and fraction of
extent, regardless of the fiber type. These results indicate that large capillary pores. The mechanism beneath is that the porosity
the fiber addition could produce slightly coarser pore structures is not a good indicator of frost durability, the fine pores and poros-
in concrete at various hydration ages, which are consistent with ity obtained by MIP technique would not contribute to the increase
those found in previous studies [18,19]. Sßahmaran et al. [18] in frost resistance [18]. As stated by many previous studies, the
reported the volumes of pores with sizes between 0.30 and 2 lm frost resistance of concrete was greatly affected by pores with a
and the total intruded porosity in ECC increased considerably with diameter above 50 lm [41] or around 300 lm [42], all of which
the PVA fiber addition. Nam et al. [19] revealed the addition of PVA are within the pore size range of air voids. The analysis of the cor-
or PP fibers increased the pores in the range of 0.1–10 lm in relation between frost resistance and air void will be conducted in
cement mortars. The coarse pore structure in fiber enhanced con- Section 3.7.
crete in this study seems to be also related with the air entrapment From the comparison of data in Table 8, it can be found that
of fibers. Nevertheless, further study will be conducted to under- increasing the fiber length could further coarsen the pore structure
stand the mechanism of the increase in porosity due to the fiber of concrete. As for the PP fiber, an increase in fiber length from
addition, which is beyond the scope of the present paper. 10 mm to 20 mm may enlarge the critical pore diameter, porosity,
Furthermore, Fig. 11 and Table 8 clearly show that the pore and the fraction of large capillary pores concrete (CPP20) at 28 days
structure of concrete varies with the fiber type. The PP fiber to about 171 nm, 29.8% and 56.2%, which are about 16 nm, 2.6%
enhanced concrete seems to present the coarsest pore structure and 5.6% higher than those of CPP10 concrete, respectively. The
among all the fiber-enhanced concrete, followed by the PVA fiber same coarsening trend of pores with increasing fiber length could
enhanced one and the PAN fiber enhanced one. For instance, Table 8 be observed for the concretes added with PVA or PP fibers. As
presents that the porosity, the critical pore diameter, as well as the shown in Fig. 12, the high porosity and high volume of large capil-
fractions of large capillary pores of concrete containing fibers fol- lary pores favor the water permeation in concrete. Consequently,
low the order of CPP10 > CPVA10 > CPAN10 > C0 for 10-mm level concrete with longer fibers exhibits a weaker impermeability than
fibers, and CPP20 > CPVA20 > CPAN20 > C0 for 20-mm level fibers, the one with shorter ones.
which are in consistence with the orders of the air contents in
Fig. 4 and the impermeability in Table 7.
The correlations between relative permeability coefficient Kr
and pore structure parameters including the porosity and fraction 3.7. Air void parameters and their correlations with durability
of pores sized between 50 nm and 10 lm are shown in Fig. 12.
Fig. 12 clearly indicates that Kr is lineally corelated with porosity The air-void parameters of concretes containing PP, PVA and
as well as the fraction of large capillary pores. As Metha and Mon- PAN fibers with different lengths hydrated at 28 days are given
terio [56] clarified, the pores with a diameter of about 0.05–0.1 lm in Table 9. Notice that the hardened air content A values in Table 9
have a significant influence on the permeability of concrete. Some are nearly equivalent to the air contents in fresh concrete shown in
researchers [37,55] have pointed out that a high porosity and a Fig. 4. The same trend has been described by ASTM C 457 [45].
large amount of large capillary pores facilitated the formation of Apart from the air content A, Table 9 provides other air voids
channels for water penetration and ingress ions diffusion. Accord- parameters, including the total number of air voids N, the average
ingly, the impermeability differences caused by the fiber type can air void diameter D and the spacing factor L̄, which are believed to
be revealed in terms of the pore structure. The PP fibers produce a affect the frost resistance of concrete [40,43,44].
relatively coarse pore structure in concrete, leading to high Dm and Table 9 indicates that all the fibers (PP, PVA and PAN) increase
the values of N and A values and reduce the L̄ values, indicating the
14
L. Wang, T. He, Y. Zhou et al. Construction and Building Materials 282 (2021) 122706

Fig. 12. The correlations of relative permeability coefficient Kr with (a) fraction of pores sized between 50 nm and 10 lm (large capillary pores) and (b) porosity.

Table 9
Air void parameters of 28-day concretes determined by the linear traverse method.

Air void parameters C0 CPP10 CPP20 CPVA10 CPVA20 CPAN10 CPAN20


Total number of air voids N 1250 1589 1775 1952 2246 1723 1920
Traverse length through air Ta (mm) 264.6 396.9 422.1 346.5 378.0 321.3 333.9
Hardened air content A (%) 4.2 6.3 6.7 5.5 6.0 5.1 5.3
Average chord length l (lm) 212 250 238 178 168 186 174
Average air void diameter D (lm)D (lm) 318 375 357 266 252 280 261
Specific surface a (mm1) 18.9 16.0 16.8 22.5 23.8 21.5 23.0
Spacing factor¯L (lm) 252 227 200 182 161 206 185

fibers could entrap more air voids in concrete while at the same with the trend reported by others [40], the higher N and the smal-

time shorten the average distance among the air void centers. ler L, the better the frost resistance, and vice versa. In addition, it
The correlation of relative permeability coefficient Kr with A is can be seen from Table 9 that most of the fiber enhanced concretes
presented in Fig. 13. Fig. 13 clearly indicates that a linear e rela- 

tionship exists between Kr and A, with a relatively high coefficient exhibit L values below 250 lm or even below 200 lm. Based on the

R2 value of 0.925. The high R2 demonstrates that, in addition to the hypothesis of hydrostatic pressure reported by Powers [61], the L
pore structure parameters, the concrete permeability is signifi- value was supposed to be less than 250 lm to obtain a good frost

cantly determined by the hardened air content. resistance of concrete. Other study considered the L below 200 lm
Moreover, the correlations between frost resistance parameters to be critical for the durability of concrete in cold climates [18].
(i.e., mass loss and relative dynamic modulus of elasticity) and air 
 Obviously, the increased N and the decreased L down to around
void parameters of concrete (i.e., N, A, D and L) are shown in Figs. 14 200 lm caused by the fiber addition are beneficial to improve
and 15. From Figs. 14 and 15, the frost resistance of concrete is clo- the frost resistance of concrete.

sely related with the N and L with high coefficient R2 values above By comparing the data in Table 9, it can be found that under the
0.97, whereas the correlations of frost resistance with A and D are same fiber length, the fiber type affects the air void parameters

relatively weak, illustrating that N and L play more important roles obviously. PAN fiber generates the lowest hardened air content
than A and D in influencing the frost resistance. This is consistent (A) value while the PP fiber produces the largest. Based on the rela-
tionship between Kr and A revealed in Fig. 13, the low A can partly
explain the high impermeability of PAN fiber enhanced concrete.
Basd on the correlation between concrete frost resistance and
air void parameters, it can be conclued that PVA fiber enhanced

concrete gives the lowest spacing factor (L) value and largest total
number of air voids (N) value among all the fiber enhanced con-
cretes, thus exhibiting the best frost resistance. Similarly, the PP
fiber enhanced concrete has a higher A value than other types of
fiber enhanced ones, which may be beneficial for the concrete frost

resistance, but it has much higher L and lower N values, thus pre-
senting weaker frost resistance, as revealed in Figs. 14 and 15.
As for the fiber length, Table 9 shows that increasing fiber
length from 10 mm to about 20 mm could further decrease theL̄
values and increase the N values, thereby improving the frost resis-
tance of concrete. For instance, CPP20, CPVA20 and CPAN20 show
approximately 12%, 15% and 11% increases in N values, and about

12%, 11% and 10% reductions in L values compared with those of
Fig. 13. The correlation of relative permeability coefficient Kr with hardened air
content A. CPP10, CPVA10 and CPAN10, respectively. As revealed in Figs. 14

15
L. Wang, T. He, Y. Zhou et al. Construction and Building Materials 282 (2021) 122706


Fig. 14. The correlations of mass loss with (a) total number of air voids N, (b) air content A, (c) the average air void diameter D and (d) the spacing factor L.

Fig. 15. The correlations of relative dynamic modulus of elasticity with (a) total number of air voids N, (b) air content A, (c) the average air void diameter D and (d) the spacing
factor L.

16
L. Wang, T. He, Y. Zhou et al. Construction and Building Materials 282 (2021) 122706


and 15, the reduction in L values and increase in N values due to and National Engineering Research Center of Building Technology
the inclusion of longer fibers contributes much to the improve- (BSBE2020-2), The Belt and Road Special Foundation of the State
ment in frost resistance of concrete, while the increased A values Key Laboratory of Hydrology-Water Resources and Hydraulic Engi-
at the same time could compromise the impermeability of concrete neering (2020492311), Opening Project of State Key Laboratory of
to some degrees, as evident in Fig. 13. Green Building Materials (2020GBM07), Open funding of National
Dam Safety Research Center (CX2019B12), Natural Science
Research Project of Shaanxi Provincial Department of Education
4. Conclusion (20JK0722) and NSFC of China (51409016).

The following conclusions can be drawn in this work:


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