REFERENCE NO.

: MNLH24020144

APPLICANT: UNITED PULP AND PAPER CO., INC. JOB NO.: HRT12-00502
KM48 MCARTHUR HIGWAY, IBA ESTE, DATE: 20 FEBRUARY 2024
CALUMPIT, BULACAN
ATTN: ALLEN JAY CANO

SAMPLE DESCRIPTION:
ONE (1) SUBMITTED SAMPLE (10 PIECES) SAID TO BE UPPC LINER PAPER.

ITEM NO./PRODUCT CODE : UPPC TX

DATE SAMPLE RECEIVED : 30 JANUARY 2024

DATE OF ANALYSIS : 02 - 17 FEBRUARY 2024

TESTS CONDUCTED:
AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGES TWO TO EIGHT.

CHECKED AND APPROVED BY:

___________________________
MARIA NADYN E. LICLICAN
SENIOR SUPERVISOR – PHYSICAL & CHEMICAL LAB
CENTRAL LABORATORY – PRODUCTS
APPROVED SIGNATORY
rpu
Estimation of measurement uncertainty is available upon request .

PAGE 1 OF 8
This report (including any enclosures and attachments hereof) has been prepared for the exclusive use and benefit of the addressee(s) and solely for the purpose for
which it is intended. The analysis is based solely on the sample(s) submitted by the client. No part of this report should be reproduced, distributed or communicated to any
third party, unless Intertek Philippines provide or express prior written consent. We do not accept any liability if this report has been used maliciously or used for purpose
other than it was originally intended or stated, nor do we owe any duty of care to any third party in respect of this report.

Attention is drawn to the terms and conditions which was agreed and signed upon together with the proposal or test application form.

Intertek Testing Services Philippines, Inc.

Intertek Building, 2307 Chino Roces Ave. Extension, Makati City, 1231 Philippines
Tel +63 2 8195841 to 47 / +62 2 887 3320 to 23 / +63 2 894 4151 Fax +63 2 813 1850
intertek.com
 REFERENCE NO.: MNLH24020144
TESTS CONDUCTED:
(A) TEST RESULT SUMMARY:
Result
Test Item Unit Test Method Submitted sample RL
Heavy Metal
With reference to IEC 62321-5:
2013, by microwave or acid
Cadmium (Cd) Content ppm ND 5
digestion and determined by
ICP-OES.
With reference to IEC 62321-5:
2013, by microwave or acid
Lead (Pb) Content ppm ND 5
digestion and determined by
ICP-OES.
With reference to IEC 62321-
4: 2013+AMD1: 2017, by
Mercury (Hg) Content ppm ND 5
microwave or acid digestion
and determined by ICP-OES.
With reference to IEC 62321-
7-2: 2017, organic solvent
Chromium VI (Cr(VI)) Content ppm was used to dissolve or swell ND 5
sample matrix, followed by
alkaline digestion and
determined by UV-Vis
Spectrophotometer.
Polybrominated Biphenyls (PBBs)#
Monobrominated Biphenyls
ppm ND 5
(MonoBB)
Dibrominated Biphenyls
ppm ND 5
(DiBB)
Tribrominated Biphenyls
ppm ND 5
(TriBB)
Tetrabrominated Biphenyls
ppm ND 5
(TetraBB)
With reference to IEC 62321-6:
Pentabrominated Biphenyls
ppm 2015, by solvent extraction and ND 5
(PentaBB)
determined by GC-MS and
Hexabrominated Biphenyls
ppm further HPLC-DAD confirmation ND 5
(HexaBB)
when necessary.
Heptabrominated Biphenyls
ppm ND 5
(HeptaBB)
Octabrominated Biphenyls
ppm ND 5
(OctaBB)
Nonabrominated Biphenyls
ppm ND 5
(NonaBB)
Decabrominated Biphenyl
ppm ND 5
(DecaBB)

PAGE 2 OF 8
This report (including any enclosures and attachments hereof) has been prepared for the exclusive use and benefit of the addressee(s) and solely for the purpose for
which it is intended. The analysis is based solely on the sample(s) submitted by the client. No part of this report should be reproduced, distributed or communicated to any
third party, unless Intertek Philippines provide or express prior written consent. We do not accept any liability if this report has been used maliciously or used for purpose
other than it was originally intended or stated, nor do we owe any duty of care to any third party in respect of this report.

Attention is drawn to the terms and conditions which was agreed and signed upon together with the proposal or test application form.

Intertek Testing Services Philippines, Inc.

Intertek Building, 2307 Chino Roces Ave. Extension, Makati City, 1231 Philippines
Tel +63 2 8195841 to 47 / +62 2 887 3320 to 23 / +63 2 894 4151 Fax +63 2 813 1850
intertek.com
 REFERENCE NO.: MNLH24020144
Test Item Unit Test Method Result RL
Submitted sample
Polybrominated Diphenyl Ethers (PBDEs)#
Monobrominated Diphenyl Ethers ppm ND 5
(MonoBDE)
Dibrominated Diphenyl Ethers ppm ND 5
(DiBDE)
Tribrominated Diphenyl Ethers ppm ND 5
(TriBDE)
Tetrabrominated Diphenyl Ethers ppm With reference to IEC 62321-6: ND 5
(TetraBDE) 2015, by solvent extraction and
Pentabrominated Diphenyl Ethers determined by GC-MS and
ppm ND 5
(PentaBDE) further HPLC-DAD confirmation
when necessary.
Hexabrominated Diphenyl Ethers ppm ND 5
(HexaBDE)
Heptabrominated Diphenyl Ethers ppm ND 5
(HeptaBDE)
Octabrominated Diphenyl Ethers ppm ND 5
(OctaBDE)
Nonabrominated Diphenyl Ethers ppm ND 5
(NonaBDE)
Decabrominated Diphenyl Ether ppm ND 5
(DecaBDE)
Phthalates#
Di(2-ethylhexyl) Phthalate ppm ND 50
(DEHP)
With reference to IEC 62321-
Dibutyl Phthalate (DBP) ppm ND 50
8:2017, by solvent extraction
Benzyl Butyl Phthalate (BBP) ppm and determined by GC-MS. ND 50
Diisobutyl Phthalate (DIBP) ppm ND 50

Remarks: ND = Not Detected

RL = Reporting limit, quantitation limit of analyte in sample
# = Tests Conducted at Intertek Taiwan

PAGE 3 OF 8
This report (including any enclosures and attachments hereof) has been prepared for the exclusive use and benefit of the addressee(s) and solely for the purpose for
which it is intended. The analysis is based solely on the sample(s) submitted by the client. No part of this report should be reproduced, distributed or communicated to any
third party, unless Intertek Philippines provide or express prior written consent. We do not accept any liability if this report has been used maliciously or used for purpose
other than it was originally intended or stated, nor do we owe any duty of care to any third party in respect of this report.

Attention is drawn to the terms and conditions which was agreed and signed upon together with the proposal or test application form.

Intertek Testing Services Philippines, Inc.

Intertek Building, 2307 Chino Roces Ave. Extension, Makati City, 1231 Philippines
Tel +63 2 8195841 to 47 / +62 2 887 3320 to 23 / +63 2 894 4151 Fax +63 2 813 1850
intertek.com
 REFERENCE NO.: MNLH24020144
TESTED COMPONENT: UPPC LINER PAPER

ROHS LIMIT:
Restricted Substances Limits
Cadmium (Cd) content 0.01% (100ppm)
Lead (Pb) content 0.1% (1000ppm)
Mercury (Hg) content 0.1% (1000ppm)
Chromium VI (Cr6+) content 0.1% (1000ppm)
Polybrominated Biphenyls (PBBs) 0.1% (1000ppm)
Polybrominated Diphenyl Ethers (PBDEs) 0.1% (1000ppm)
Di(2-ethylhexyl) Phthalate (DEHP) 0.1% (1000ppm)
Dibutyl Phthalate (DBP) 0.1% (1000ppm)
Benzyl Butyl Phthalate (BBP) 0.1% (1000ppm)
Diisobutyl Phthalate (DIBP) 0.1% (1000ppm)
The limits were quoted from Annex II of 2011/65/EU and Amendment (EU) 2015/863 for homogeneous material.

PAGE 4 OF 8
This report (including any enclosures and attachments hereof) has been prepared for the exclusive use and benefit of the addressee(s) and solely for the purpose for
which it is intended. The analysis is based solely on the sample(s) submitted by the client. No part of this report should be reproduced, distributed or communicated to any
third party, unless Intertek Philippines provide or express prior written consent. We do not accept any liability if this report has been used maliciously or used for purpose
other than it was originally intended or stated, nor do we owe any duty of care to any third party in respect of this report.

Attention is drawn to the terms and conditions which was agreed and signed upon together with the proposal or test application form.

Intertek Testing Services Philippines, Inc.

Intertek Building, 2307 Chino Roces Ave. Extension, Makati City, 1231 Philippines
Tel +63 2 8195841 to 47 / +62 2 887 3320 to 23 / +63 2 894 4151 Fax +63 2 813 1850
intertek.com
 REFERENCE NO.: MNLH24020144

(D) MEASUREMENT FLOWCHART:

TEST FOR Cd / Pb / Hg / Chromium (VI) / PBBs / PBDEs CONTENTS
REFERENCE STANDARD: Cd/Pb: IEC 62321-5: 2013; Hg: IEC 62321-4:2013+AMD1:2017;
CHROMIUM (VI): IEC 62321-7-1:2015 (BOILING WATER EXTRACTION);
CHROMIUM (VI): IEC 62321-7-2:2017 (SOLVENT AND ALKALINE EXTRACTION);
PBBs/PBDEs: IEC 62321-6:2015

SAMPLING

Cd/Pb/Hg PBBs/PBDEs
Cr6+

METAL POLYMERS /
ELECTRONICS
FOR DIFFERENT MATERIAL,
DIGEST THE SAMPLE WITH WEIGH SAMPLE AND
APPROPRIATE ACID *1 ADD ORGANIC
50cm2 SAMPLE BOILING Insoluble/
unknown SOLVENT
WATER EXTRACTION WEIGH A SAMPLE
polymers
and
CONFIRM THE TESTED Soluble polymers electronics
BY SOLVENT
SAMPLES ARE TOTALLY
COOL AND FILTER THE EXTRACTION
DISSOLVED
EXTRACT
ADD NMP, ADD TOLUENE
ULTRASONIC AND DIGESTION
MAKE-UP WITH DEIONIZED EXTRACTION SOLUTION
CONCENTRATE THE
WATER MAKE UP WITH EXTRACT AND MAKE
DEIONIZED WATER UP WITH ORGANIC
AND ADD DIPHENYL- ALKALINE HEAT SAMPLE IN SOLVENT
CARBAZIDE SOLUTION DIGESTION A MICROWAVE
ANALYZED BY ICP-OES OVEN
METAL

Visual observation*2 ANALYZED BY GC-MS

REACTION WITH TAKE AQUEOUS

DCP PHASE FOR DCP
REACTION

MAKE UP WITH D.I. WATER

ANALYZED BY UV-VIS

PAGE 5 OF 8
This report (including any enclosures and attachments hereof) has been prepared for the exclusive use and benefit of the addressee(s) and solely for the purpose for
which it is intended. The analysis is based solely on the sample(s) submitted by the client. No part of this report should be reproduced, distributed or communicated to any
third party, unless Intertek Philippines provide or express prior written consent. We do not accept any liability if this report has been used maliciously or used for purpose
other than it was originally intended or stated, nor do we owe any duty of care to any third party in respect of this report.

Attention is drawn to the terms and conditions which was agreed and signed upon together with the proposal or test application form.

Intertek Testing Services Philippines, Inc.

Intertek Building, 2307 Chino Roces Ave. Extension, Makati City, 1231 Philippines
Tel +63 2 8195841 to 47 / +62 2 887 3320 to 23 / +63 2 894 4151 Fax +63 2 813 1850
intertek.com
 REFERENCE NO.: MNLH24020144

Remarks:

*1: List of Appropriate Acid:

Material Acid added for Digestion

Polymers HNO3, HCl, HF, H2O2, H3BO3
Metals HNO3, HCl, HF
Electronics HNO3, HCl, H2O2, HBF4

*2: If sample solution is significantly more intense than 0.13 µg/cm2 equivalent comparison standard, Chromium VI would be
determined as detected, the result of visual observation is positive.

PAGE 6 OF 8
This report (including any enclosures and attachments hereof) has been prepared for the exclusive use and benefit of the addressee(s) and solely for the purpose for
which it is intended. The analysis is based solely on the sample(s) submitted by the client. No part of this report should be reproduced, distributed or communicated to any
third party, unless Intertek Philippines provide or express prior written consent. We do not accept any liability if this report has been used maliciously or used for purpose
other than it was originally intended or stated, nor do we owe any duty of care to any third party in respect of this report.

Attention is drawn to the terms and conditions which was agreed and signed upon together with the proposal or test application form.

Intertek Testing Services Philippines, Inc.

Intertek Building, 2307 Chino Roces Ave. Extension, Makati City, 1231 Philippines
Tel +63 2 8195841 to 47 / +62 2 887 3320 to 23 / +63 2 894 4151 Fax +63 2 813 1850
intertek.com
 REFERENCE NO.: MNLH24020144

Measurement Flowchart:

Test for Phthalates Content

Reference Method: IEC 62321-8:2017

Sampling

Weigh sample and add organic solvent

By solvent extraction

ANALYZED BY GC-MS

PAGE 7 OF 8
This report (including any enclosures and attachments hereof) has been prepared for the exclusive use and benefit of the addressee(s) and solely for the purpose for
which it is intended. The analysis is based solely on the sample(s) submitted by the client. No part of this report should be reproduced, distributed or communicated to any
third party, unless Intertek Philippines provide or express prior written consent. We do not accept any liability if this report has been used maliciously or used for purpose
other than it was originally intended or stated, nor do we owe any duty of care to any third party in respect of this report.

Attention is drawn to the terms and conditions which was agreed and signed upon together with the proposal or test application form.

Intertek Testing Services Philippines, Inc.

Intertek Building, 2307 Chino Roces Ave. Extension, Makati City, 1231 Philippines
Tel +63 2 8195841 to 47 / +62 2 887 3320 to 23 / +63 2 894 4151 Fax +63 2 813 1850
intertek.com
 REFERENCE NO.: MNLH24020144

SUBMITTED SAMPLE PHOTO:

END OF REPORT

PAGE 8 OF 8
This report (including any enclosures and attachments hereof) has been prepared for the exclusive use and benefit of the addressee(s) and solely for the purpose for
which it is intended. The analysis is based solely on the sample(s) submitted by the client. No part of this report should be reproduced, distributed or communicated to any
third party, unless Intertek Philippines provide or express prior written consent. We do not accept any liability if this report has been used maliciously or used for purpose
other than it was originally intended or stated, nor do we owe any duty of care to any third party in respect of this report.

Attention is drawn to the terms and conditions which was agreed and signed upon together with the proposal or test application form.

Intertek Testing Services Philippines, Inc.

Intertek Building, 2307 Chino Roces Ave. Extension, Makati City, 1231 Philippines
Tel +63 2 8195841 to 47 / +62 2 887 3320 to 23 / +63 2 894 4151 Fax +63 2 813 1850
intertek.com