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Effect of the Number of Loading Cycles on the Behavior of

a Stabilized Fiber-Reinforced Soft Soil: Energy Evaluation


Ligia A. Martins 1; Antonio A. S. Correia 2; Paulo J. Venda Oliveira 3; and Luís J. L. Lemos 4

Abstract: When a material is subjected to cyclic loading, there are changes in the material’s geomechanical behavior that need to be known
and characterized for a safe design. To this end, a series of unconfined compressive strength (UCS) tests was performed, with and without
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the application of cyclic loading, to study the effect of the number of loading cycles on the behavior of a soft soil stabilized with different
binder contents, unreinforced and reinforced with polypropylene fibers. The results were analyzed in terms of the evolution of elastic and
plastic deformation energy, and it was observed that plastic energy prevailed in the first cycles, but decreased with the increase in the number
of loading cycles. The accumulated plastic deformation occurring during the cyclic loading induced a strain-hardening effect that was respon-
sible for the increase in the undrained resilient modulus and in the postcyclic unconfined compressive strength, regardless of the binder
content and fiber reinforcement. The addition of polypropylene fibers led to a reduction in the elastic deformation energy, which was more
noticeable in the first cycles, leading to an increase in the accumulated plastic axial strains and to a reduction in the undrained resilient
modulus during the cyclic loading. These facts are explained by the high compressibility of the fibers and by the weakening of the
stabilized matrix as a result of the physical presence of the fibers which may prevent the development of some cementitious bonds.
However, the addition of fibers led to an increase in the energy absorption capacity, explained by the fact that the deformations
occurring during the cyclic loading allow an earlier mobilization of the fibers as the UCS test proceeds. DOI: 10.1061/JMCEE7.
MTENG-15231. © 2023 American Society of Civil Engineers.
Author keywords: Stabilized soil; Reinforced soil; Cyclic loading; Energy; Unconfined compressive strength (UCS) test; Polypropylene
fibers.

Introduction tensile strength, change the behavior to being more ductile, and
reduce the loss of the postpeak strength (Abbaspour et al. 2020;
One of the techniques that has been successfully applied to improve Akbari et al. 2021; Consoli et al. 2009, 2011a, c, 2013a, b; Correia
the geomechanical behavior of soils is chemical stabilization, in et al. 2015, 2017, 2019; Falorca and Pinto 2011; Güllü and Khudir
which the natural soil is mixed in situ with chemical stabilizers such 2014; Kumar and Gupta 2016; Lemos et al. 2021; Olgun 2013;
as portland cement, quicklime, fly ash, and slag (Abdullah et al. Park 2011; Plé and Lê 2012; Soltani et al. 2018; Sukontasukkul
2020; Åhnberg 2006; Basha et al. 2005; Consoli et al. 2007, 2011b; and Jamsawang 2012; Tabassum and Bheemasetti 2022; Tang
Corrêa-Silva et al. 2020; Correia 2011; Correia et al. 2019, 2021; et al. 2007; Tinoco et al. 2016; Venda Oliveira et al. 2016; Yetimoglu
Horpibulsuk 2001; Horpibulsuk et al. 2003, 2005; Kamruzzaman and Salbas 2003; Yilmaz 2009; Zaimoglu and Yetimoglu 2012).
et al. 2009; Kitazume and Terashi 2013; Lorenzo and Bergado The cited studies have shown that the enhancement of the geome-
2004, 2006; Rios et al. 2016; Venda Oliveira et al. 2013, 2014). chanical behavior of fiber-reinforced stabilized soil depends on the
Despite the enhancement achieved, in general the composite soil type, the content and type of fiber and binder, and the temper-
material is characterized by brittle behavior and poor tensile ature and failure mechanism imposed.
strength. The inclusion of randomly distributed fibers (synthetic When a dynamic loading (induced by road and/or rail traffic,
or natural) to the stabilized soil has the potential to increase the industrial equipment, sea waves, wind loads, earthquakes, and
so forth) is applied to a fiber-reinforced stabilized soil, there are
1
Ph.D. Student, Dept. of Civil Engineering, Univ. of Coimbra, R. Luís changes in the material’s behavior that need to be characterized
Reis Santos, Coimbra 3030-788, Portugal. ORCID: https://orcid.org/0000 and understood. To date, the knowledge of such behavior still is
-0002-5232-5419. Email: uc2020142548@student.uc.pt limited (mainly focused on granular unreinforced materials), and
2
Assistant Professor, Chemical Process Engineering and Forest Products
sometimes the results are inconsistent. Dall’Aqua et al. (2010)
Research Centre, Dept. of Civil Engineering, Univ. of Coimbra, R. Luís Reis
Santos, Coimbra 3030-788, Portugal (corresponding author). ORCID:
and Venda Oliveira et al. (2017, 2018) observed an increase in the
https://orcid.org/0000-0002-3260-8729. Email: aalberto@dec.uc.pt plastic deformations induced by cyclic loading, with the most
3
Associated Professor with Aggregation, Institute for Sustainability and significant increase occurring during the first loading cycles. In
Innovation in Structural Engineering, Dept. of Civil Engineering, Univ. of contrast, Chauhan et al. (2008) found a sharp increase in the plastic
Coimbra, R. Luís Reis Santos, Coimbra 3030-788, Portugal. ORCID: deformations for a high number of loading cycles. Based on cyclic
https://orcid.org/0000-0001-8515-8664. Email: pjvo@dec.uc.pt tests, Ahmed and El Naggar (2018) and Narani et al. (2021) studied
4
Full Professor, CGeo, Dept. of Civil Engineering, Univ. of Coimbra, the effect of adding waste tire fibers to a stabilized soil, and
R. Luís Reis Santos, Coimbra 3030-788, Portugal. Email: llemos@dec.uc.pt
observed that the compressive strength decreased as the number
NOTE.This manuscript was submitted on July 15, 2022; approved on
March 1, 2023; published online on August 24, 2023. Discussion period of loading cycles increased, whereas Festugato et al. (2013),
open until January 24, 2024; separate discussions must be submitted for Khattak and Alrashidi (2006), and Venda Oliveira et al. (2018) re-
individual papers. This paper is part of the Journal of Materials in Civil ported an increase in the shear, compressive, and tensile strengths
Engineering, © ASCE, ISSN 0899-1561. when polypropylene (PP) fibers were added to stabilized soils.

© ASCE 04023392-1 J. Mater. Civ. Eng.

J. Mater. Civ. Eng., 2023, 35(11): 04023392


Although Narani et al. (2021) and Venda Oliveira et al. (2022) re- but may provide new insights on the subject. Thus, the aim of this
ported that the addition of fibers decreases the plastic strain and work was to add to the existing knowledge of the behavior of a
minimizes the compressive peak-strength loss under cyclic loading, stabilized fiber-reinforced soft soil under cyclic loading, thereby
Narani et al. observed that the stiffness decreases with the cyclic contributing to an effective future application of such composite
loading, whereas Venda Oliveira et al. noted the opposite. materials.
The energy concept has been applied to geotechnical problems This work analyzed the effect of the number of loading cycles
mainly to interpret the behavior of cohesionless soils (e.g., their on the compressive and postcyclic behavior of a stabilized soft soil,
densification and liquefaction) under dynamic loadings such as unreinforced and reinforced with polypropylene fibers. The con-
those imposed by earthquakes (Lenart 2008; Sas et al. 2017). The cept of elastic and plastic deformation energy was applied to better
energy concept states that a material under a load deforms, and this understand the effects of the cyclic loading and the reinforcement
deformation corresponds to a release or dissipation of energy with fibers on the accumulated plastic deformations and on the
(Lenart 2008; Sas et al. 2017; Xia et al. 2021). The energy dissi- stress–strain behavior of the composite material. These effects are
pated may be evaluated experimentally from the stress–strain the core subject and novelty of this study. To achieve these goals, an
experimental testing program was designed and complemented
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curve, and corresponds to the area below the curve (Choobbasti and
Kutanaei 2017; Lenart 2008; Narani et al. 2020, 2021; Sas et al. with an in-house algorithm developed to compute the deformation
2017). In a dynamic or cyclic loading, there are stress–strain hys- energy. The testing program was based on (1) monotonic uncon-
teresis loops from which it is possible to evaluate the dissipated fined compressive strength (UCS) tests performed with samples not
(plastic) energy, which is equal to the area inside the hysteresis subjected to cyclic loading; (2) unconfined compressive cyclic
loop, whereas the elastic (recovered) energy is equal to the area loading (Cyc) tests; and (3) and postcyclic UCS tests (UCSpc).
Table 1 briefly describes the experimental testing plan.
under the unloading curve (Sas et al. 2017). The energy concept
has been applied to a very small number of fiber-reinforced stabi-
lized soils under cyclic loading. Narani et al. (2021) performed
cyclic loading tests with displacement control to study the effect Materials
of the inclusion of tire fibers in a low-plasticity sandy-clay stabilized
with portland cement and found that: (1) the plastic energy was Characteristics of the Soil
higher for the first cycles, and decreased sharply with the increase
The soil selected for this study was an organic soft soil from the
in the number of loading cycles; (2) the plastic energy increased
Baixo Mondego region, near the city of Coimbra in the center of
with the cement content because cement stabilization leads to a more
Portugal, collected from a depth of 2–3 m (below the water table).
uniform and rigid solid skeleton with the ability to absorb more en- The soil was classified as soft soil in previous works performed at the
ergy; and (3) the addition of fibers promoted a decrease in plastic University of Coimbra (Coelho and Lemos 2017; Hindle 1994;
energy because part of the deformation applied to the samples was Lemos and Soares 1995; Phillipson 1994; Venda Oliveira et al.
absorbed by the fibers and less energy was transferred to the soil 2004, 2010). The soil was classified according to the Unified Soil
matrix, resulting in less degradation of the composite material. Classification System (ASTM 1998) as a high plasticity organic silt
Despite the research to date, the impact of the number of loading (OH) with an organic matter content of 9.5%. Its chemical compo-
cycles on the behavior of a stabilized soft soil reinforced with fibers sition revealed a high silica (SiO2 ) and alumina (Al2 O3 ) content
has not been studied properly. In addition, the analysis in terms of (59% and 17%, respectively), which means that the soil has signifi-
deformation energy is an important feature that is less discussed, cant pozzolanic properties (Janz and Johansson 2002). The physical
and chemical properties of the soil are presented in Tables 2 and 3.
Table 1. Experimental testing plan (UCS, Cyc, and UCSpc): number of
tests Characteristics of the Binder and the Fibers
Monotonic-stage Cyclic-stage The binder chosen for this research was portland cement Type I
binder quantity binder quantity
42.5 R [EN 197-1 (CEN 2000)], characterized by the chemical
(kg=m3 ) (kg=m3 )
Type composition presented in Table 4. It corresponds to a hydraulic
Type of fibers of test 100 175 250 325 100 175 250 325 binder, with fast strength development, exhibiting at 7 curing days
Unreinforced UCS 6 6 6 6 — — — — more than 80% of the strength developed at 28 days according to
Cyc — — — — 3 3 3 3
UCSpc — — — — 3 3 3 3
Table 3. Chemical characterization of soft soil
Polypropylene UCS 6 6 6 6 — — — —
Total
fibers Cyc — — — — 3 3 3 3
organic
(10 kg=m3 ) UCSpc — — — — 3 3 3 3
Loss on SiO2 Al2 O3 Fe2 O3 CaO MgO Na2 O K2 O carbon
Note: UCS = monotonic UCS test without a cyclic stage; Cyc = unconfined pH ignition (%) (%) (%) (%) (%) (%) (%) (TOC) (%)
compressive cyclic test; and UCSpc = monotonic UCS test carried out after
4.6 9 59 17 4.9 0.4 1.1 0.83 3.1 3.46
the cyclic stage.

Table 2. Physical characterization of soft soil


Organic matter
Mineralogical composition Gs (g=cm3 ) wnat (%) Grain size (%) Plasticity (%) content (OM) (%)
Quartz, muscovite, albite, microcline, 2.57 80.9 Clay ¼ 12 wP ¼ 44.9 9.5
smectite, ilite, kaolinite, and magnesium chlorite Silt ¼ 77 wL ¼ 72.2
Sand ¼ 11 PI ¼ 27.3

© ASCE 04023392-2 J. Mater. Civ. Eng.

J. Mater. Civ. Eng., 2023, 35(11): 04023392


Table 4. Main characteristics of binder portland cement type I 42.5 R 5. After the curing time had elapsed, the samples were removed
(manufacturer’s data) from the molds and the surfaces were trimmed to obtain samples
Property Value with a height of 76 mm.
6. The samples were weighed and positioned in a dynamic triaxial
CaO (%) 62.9
SiO2 (%) 19.0
apparatus for testing.
Al2 O3 (%) 5.2 The aim of the UCS tests was to define the mechanical charac-
Fe2 O3 (%) 3.2 teristics under monotonic conditions, and they were carried out at
SO2 (%) 3.1 a constant strain rate of 1%=min according to the standard BSI
MgO (%) 2.2 (1990). This strain rate is very fast, and thus the samples were
K2 O (%) 1.3 tested at close to an undrained condition. The UCS cyclic loading
Blaine specific surface (m2 =kg) 326.3 tests were carried out for a deviatoric stress level of 50% of the
maximum unconfined compressive strength (qu max ) defined in
the monotonic UCS test, with an amplitude of 10% of qu max
(inducing a safety factor ranging from 1.66 to 2.5), a frequency
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Table 5. Main characteristics of polypropylene fibers (manufacturer’s of 0.5 Hz [reproducing the passage of a car (Milliken et al. 1995)],
data)
and applying 5,000 loading cycles (CEN 2004). After the cyclic
Property Value loading stage, the samples were unloaded and a monotonic UCS
Length, L (mm) 12 test (postcyclic) was carried out to analyze the effect of the cyclic
Diameter, D (μm) 32 loading on the mechanical behavior of the samples. Both the UCS
Aspect ratio (L=D) 375 and cycling loading tests were carried out in a dynamic triaxial
Tensile strength 250 testing system.
Elasticity modulus 3.5–3.9 To guarantee the reliability of the study, six replicate samples
Surface texture roughnessa Lower were considered for the UCS tests and three replicate samples were
Biodegradability Not biodegradable considered for the UCS cyclic loading tests for each experimental
Density (g=cm3 ) 0.91 condition (with or without fibers; binder quantity of 100, 175, 250,
a
Data from Agboola et al. (2021). and 325 kg=m3 ) (Table 1). The requirement that each individual
unconfined compressive strength result must be within the range
10% of the average value was adopted as the conformity or com-
the manufacturer’s data. Due to the high organic matter content and pliance criterion, which is more demanding than that specified in
the acid pH of the soil, and the fact that the moisture content of the the standard (CEN 2007), i.e., 15%.
natural soil was higher than the liquidity limit (wnat ¼ 80.9% >
wL ¼ 72.2%) the portland cement was applied in quantities of 100,
Analysis of the Results
175, 250, and 325 kg=m3 (dry weight of cement per cubic meter of
soil), equivalent to binder contents of 12%, 21%, 30%, and 39% The experimental nature of the study implies the occurrence of
(dry weight ratio of binder to soil). some variability in the results, which should be characterized. In
For the reinforced samples, polypropylene fibers were selected terms of the unconfined compressive strength, the maximum vari-
as reinforcing elements. The fibers had a length of 12 mm and a ability observed between the individual strength values and the re-
diameter of 32 μm, presenting a very high aspect ratio but a lower spective average was 7.9% and 5.3% for the UCS and UCSpc
surface roughness (Table 5). The fibers were added to the chemi- tests, respectively. These values are not very significant, and are
cally stabilized soft soil in a quantity of 10 kg=m3 (dry weight of within the compliance criterion adopted (10%) and are consistent
fibers per cubic meter of soil), corresponding to a fiber content of with other studies focused on stabilized materials reinforced with
1.2% (weight ratio of dry fiber to dry soil). fibers (Consoli et al. 2010; Correia et al. 2015; Duong et al. 2021;
Huang et al. 2020; Khattak and Alrashidi 2006; Venda Oliveira
et al. 2016, 2018, 2022). The maximum variability of the maximum
Sample Preparation and Testing permanent axial strain measured during the cyclic stage was
9.0%, which is not significant. The results presented throughout
The samples of the chemically stabilized soft soil with or without this work refer to the test with the values closest to the average.
the inclusion of the polypropylene fibers were prepared based on
the laboratory procedure described by EuroSoilStab (2001) and
Cyclic Loading Stage: Permanent Axial Strain
Correia (2011), which is summarized as follows:
1. A specific amount of fibers was separated using compressed air. Fig. 1 shows the evolution of the accumulated permanent (plastic)
2. All the materials used (soil, cement, and/or fibers) were weighed axial strain (εa accum ) with the number of loading cycles for the
and mixed using a mechanical mixer at a speed of 142 rpm for different binder quantities studied and for both stabilized materi-
4 min to obtain a homogeneous paste and minimize the exper- als, i.e., unreinforced and fiber-reinforced. The analysis of the re-
imental variability. For the fiber-reinforced samples, the fibers sults shows a similar evolution of the accumulated permanent
were added gradually during the first minute of mixing. axial strain for a binder quantity in the range 175–325 kg=m3
3. The mixture was introduced into PVC molds (37-mm diameter, and independent of reinforcement with fibers, characterized by
85-mm height) and dynamically compacted in three layers. For a rapid increase in axial strain in the first 100 loading cycles, fol-
each layer, the mold was tapped (hit) 20 times by hand against a lowed by a smooth increase for a greater number of loading
wooden table (the conformity criterion was that the range of cycles, evolving asymptotically to a constant value. The samples
variation of the individual weights of the samples which should stabilized with the lowest binder quantity (100 kg=m3 ) had a
not exceed 1% of the mean value). distinct behavior characterized by a continuous increase in the ac-
4. The samples were cured under water for 28 days inside a room cumulated permanent axial strain during the cyclic stage. Further-
with temperature control (20°C  2°C). more, the addition of the fibers to the stabilized samples led to an

© ASCE 04023392-3 J. Mater. Civ. Eng.

J. Mater. Civ. Eng., 2023, 35(11): 04023392


Number of cycles
0 1000 2000 3000 4000 5000
0

0.5

qu (kPa)
εa accum. (%)

1 Plastic
Energy
325 kg/m³
1.5 Elastic
250 kg/m³
175 kg/m³ Energy
100 kg/m³
2 325 kg/m³ + PP
250 kg/m³ + PP
175 kg/m³ + PP
100 kg/m³ + PP εa (%)
2.5
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Fig. 3. Definition of deformation energy calculation for one cycle load-


Fig. 1. (Color) Evolution of the accumulated permanent axial strain
ing (stress–strain hysteresis loop).
with the number of loading cycles without and with fibers.

2.50 deformation energy was analyzed. Therefore, the elastic and plastic
without fibers with fibers
10 cycles
deformation energies of each stress–strain hysteresis loop were
2.00 500 cycles evaluated. The plastic deformation energy is equal to the area
1000 cycles (density) inside the hysteresis loop, whereas the elastic deformation
5000 cycles energy is equal to the area (density) under the unloading curve
εa accum. (%)

1.50
(Choobbasti and Kutanaei 2017; Narani et al. 2021; Ostadan et al.
1996; Sas et al. 2017) (Fig. 3). These calculations were made using
1.00 numerical integration and trapezoidal rule integration [the latter as
suggested by Lenart (2008)] in MATLAB version R2019a software
0.50
with an in-house algorithm. The results using each of the integra-
tion techniques were very close to each other, with a time advantage
for the trapezoidal rule integration. The expression used to calculate
0.00 both energies based on the trapezoidal rule integration of both sec-
100 175 250 325
tions of the hysteresis loop is (Azeiteiro et al. 2017)
Cement Quantity (kg/m³)

Fig. 2. Effect of binder quantity and reinforcement with polypropylene Z Z X


k−1
1 ðiþ1Þ ðiÞ
fibers on the accumulated permanent axial strain for a different number δW ¼ σdε ¼ qdεa ≈ ðqðiÞ þ qðiþ1Þ Þðεa − εa Þ
of loading cycles. k i¼1
2
ð1Þ

increase in the accumulated permanent axial strain, an effect that This methodology was carried out for any number of cycles.
The results are presented in Figs. 4–6.
tended to be attenuated with the increase in the number of loading
Fig. 4 presents the evolution of the deformation energy density
cycles (Fig. 2). As expected, the accumulated permanent axial
with the number of loading cycles for the unreinforced and fiber-
strain decreased as the binder quantity increased (Figs. 1 and 2),
reinforced stabilized materials. In both materials, plastic deforma-
reflecting the fact that a larger amount of binder promotes the
tion energy prevailed in the first cycles, but decreased with the
production of cementitious products from the physicochemical
increase in the number of loading cycles. In contrast, the elastic
reactions, leading to a stronger and stiffer stabilized matrix, in
deformation energy increased with the number of loading cycles,
accordance with other works (Correia et al. 2015; Kaniraj and increasing sharply during the first 10 cycles. This behavior is more
Havanagi 2001; Kumar et al. 2007; Olgun 2013). Moreover, the easily perceptible when analyzing the evolution of the plastic and
results seem to indicate that the addition of the fibers may prevent elastic deformation energies with the number of loading cycles
the development of some cementitious bonds within the stabi- (Figs. 5 and 6, respectively). In the first loading cycles, the energy
lized matrix, thereby producing a composite material with lower applied by the external cyclic load mostly dissipated as plastic
strength and stiffness, and therefore the fiber-reinforced stabilized energy, and whatever remained was absorbed by the composite
material will experience more axial strains during the cyclic load- material as elastic energy, a trend that quickly reversed as the num-
ing. The resulting effect of the addition of fibers decreased as the ber of cycles increased. The plastic energy is associated with several
amount of binder increased because the amount of fibers added dissipation mechanisms related to the frictional sliding at particles
was constant in all fiber-reinforced stabilized samples, i.e., the contacts, a viscous volumetric change induced by pore fluid move-
relative fiber importance decreased. ment, particle breakage (Johnson et al. 2021; Lenart 2008; Narani
et al. 2020; Okur and Ansal 2011; Sas et al. 2017; Xia et al. 2021),
and the breaking of interparticle (cementitious) bonds. For the
Cyclic Loading Stage: Deformation Energy Evaluation
stabilized materials studied here, the breakage of the cementitious
As stated previously, to bring new insights into the cyclic loading bonds seems to have been the dominant dissipation mechanism,
behavior of stabilized unreinforced and fiber-reinforced soils, which induced irrecoverable deformations of the solid skeleton,

© ASCE 04023392-4 J. Mater. Civ. Eng.

J. Mater. Civ. Eng., 2023, 35(11): 04023392


100 100
Energy density (kPa)

10 10

elastic plastic
1 1

0.1 0.1

0.01 0.01
0 1000 2000 3000 4000 5000 0 10 20 30 40 50
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Number of cycles Number of cycles


(a) (b)

100 100
Energy density (kPa)

10 10

elastic plastic
1 1

0.1 0.1

0.01 0.01
0 1000 2000 3000 4000 5000 0 10 20 30 40 50
Number of cycles Number of cycles
(c) (d)

Fig. 4. (Color) Evolution of deformation energy density (elastic and plastic) with the number of loading cycles: (a) without fibers; (b) without fibers—
magnification of first 50 loading cycles; (c) with fibers; and (d) with fibers—magnification of first 50 loading cycles.

i.e., permanent axial strains (Figs. 1 and 2). For the cyclic load prevent the development of some cementitious bonds, producing
applied (50%  10% of qu max ), this dissipation mechanism was a composite material with lower strength and stiffness.
more intense the smaller the binder content was, meaning that a For both of the stabilized materials, i.e., unreinforced and fiber-
sample stabilized with a lower quantity of binder (less stiff) dissi- reinforced, the transference of energy from plastic to elastic oc-
pated more energy [higher relative plastic deformation energy curred more markedly in the first cycles, evolving rapidly (after
(Fig. 5)] during the breakage of the cementitious bonds, leading 10–100 cycles) to a quasi steady-state level. Thus, for the materials
to greater permanent axial strains. As the number of loading cycles and testing conditions studied here, 100 loading cycles seemed to
increased, and as a result of the changes in the fabric induced by the be sufficient to study the influence of the cyclic loading. Moreover,
breakage of the cementitious bonds, the material was able to absorb except for the samples stabilized with the lowest binder content, as
more elastic energy in relative terms (Fig. 6). After some number of the number of loading cycles increased, the increment of the plastic
deformation caused by each cycle decreased gradually, i.e., the rate
cycles (10–100), the stabilized material achieved a quasi-steady
of the plastic deformation decreased during the cyclic loading,
hysteretic response, with a relative plastic deformation energy on
which seems to be in agreement with the plastic shakedown or plas-
the order of 10%–20% and a relative elastic deformation energy tic creep shakedown concept developed for unbound granular soils
ranging between 90% and 80% (Figs. 4–6). under cyclic loading (Lenart 2008; Narani et al. 2020; Sas et al.
Analysis of the results also shows that the addition of the fibers 2017; Werkmeister 2006). However, more research is required to
led to an increase in the plastic deformation energy (or a reduction verify such concepts and to set the thresholds of the shakedown
in the elastic deformation energy), which was more noticeable in theory for stabilized (or bounded) materials.
the first cycles, leading to the increase in the accumulated plastic
deformations (axial strains) during the cyclic loading for the fiber-
reinforced stabilized soil, in agreement with Figs. 1 and 2. This Cyclic Loading Stage: Evolution of the Resilient
increase in plastic deformation energy can be explained by two Modulus
cumulative effects: the high compressibility of the polypropylene The cyclic loading behavior of the stabilized unreinforced and
fibers (Narani et al. 2020); and the weakening of the stabilized ma- fiber-reinforced samples was analyzed in terms of the evolution
trix as a result of the physical presence of the fibers, which may of the resilient modulus. The undrained resilient modulus was

© ASCE 04023392-5 J. Mater. Civ. Eng.

J. Mater. Civ. Eng., 2023, 35(11): 04023392


100 100

90 90

80 80
100 kg/m³
70 70
Plastic Energy (%)

Plastic Energy (%)


175 kg/m³ 100 kg/m³ + PP
60 250 kg/m³ 60 175 kg/m³ + PP
325 kg/m³ 250 kg/m³ + PP
50 50
325 kg/m³ + PP
40 40

30 30

20 20

10 10

0 0
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1 10 100 1000 1 10 100 1000


(a) Number of cycles (b) Number of cycles

(c)

Fig. 5. (Color) Evolution of the plastic deformation energy (expressed in relative terms) with the number of loading cycles: (a) without fibers; (b) with
fibers; and (c) for cycles 2, 5, 500, and 5,000.

defined as the slope of the stress–strain hysteresis loop (Fig. 7), and Monotonic Stress–Strain Behavior
the results are presented in Fig. 8. The undrained resilient modulus
Figs. 9 and 10 show the stress–strain curves from the unconfined
increased (i.e., the inclination of the hysteresis loop toward the compressive strength tests performed before and immediately after
x-axis increased) with the number of loading cycles, independently the cyclic stage for different binder quantities for the stabilized
of the binder content and the presence of the fibers. Thus, the re- unreinforced and fiber-reinforced samples. The unconfined com-
sults suggest that the deformation that occurs during the cyclic pressive strength (qu max ) and stiffness increased with the binder
loading seems to promote a strain-hardening effect [similar to what quantity, and the behavior became more fragile, characterized by
occurs for unstabilized granular soils, Xia et al. (2021)] that is a clear peak failure and an abrupt loss of strength after peak (Fig. 9)
responsible for the increase in the resilient modulus. The strain- (Consoli et al. 2009; Correia et al. 2015, 2017; Horpibulsuk 2001;
hardening effect is compatible with the evolution of the plastic de- Narani et al. 2021; Olgun 2013; Sukontasukkul and Jamsawang
formation energy (Figs. 4 and 5), which decreased asymptotically 2012). The addition of polypropylene fibers (at 10 kg=m3 ) changed
as the cyclic loading test proceeded. The results also show that the the stress–strain behavior of the composite material, in agreement
undrained resilient modulus increased with the binder quantity, with the findings of Consoli et al. (2009), Correia et al. (2015), and
meaning that a composite material stabilized with a higher binder Olgun (2013). At the lower binder quantities (100 and 175 kg=m3 )
content had the ability to absorb a higher elastic deformation en- there was an increase in compressive strength, whereas the opposite
ergy (Figs. 4 and 6). occurred for larger binder quantities (250 and 325 kg=m3 ), Fig. 11.
The same trend was observed for the fiber-reinforced stabilized The postpeak strength loss was almost zero or was relatively small
samples, but the addition of the fibers led to a slight reduction in with lower binder quantities (100 and 175 kg=m3 ), whereas a sig-
the undrained resilient modulus compared with that of the corre- nificant postpeak strength loss occurred with higher (250 and
sponding unreinforced stabilized sample. This reduction was be- 325 kg=m3 ) binder quantities. There was a nonnegligible residual
cause the fiber-reinforced stabilized matrix is characterized by a strength, and the behavior was more ductile the lower the binder
lower stiffness induced by a higher compressibility of the fibers quantity was. Such behavior is explained by the fact that for lower
and because the fibers may prevent some cementitious bonds binder quantities (100 and 175 kg=m3 ), failure was associated with
between the soil particles. higher levels of strain allowing the mobilization of the fibers’

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J. Mater. Civ. Eng., 2023, 35(11): 04023392


100 100

90 90

80 80

70 70

Elastic Energy (%)


Elastic Energy (%)

60 60

50 50
325 kg/m³ 40 325 kg/m³ + PP
40
250 kg/m³ 250 kg/m³ + PP
30 30 175 kg/m³ + PP
175 kg/m³
20 100 kg/m³ 20 100 kg/m³ + PP

10 10

0 0
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1 10 100 1000 1 10 100 1000


(a) Number of cycles (b) Number of cycles

(c)

Fig. 6. (Color) Evolution of the elastic deformation energy (expressed in relative terms) with the number of loading cycles: (a) without fibers; (b) with
fibers; and (c) for cycles 2, 5, 500, and 5,000.

tensile strength, whereas for the higher binder quantities (250 and in monotonic stress up to a deviatoric stress level equal to 50% of
325 kg=m3 ), failure occurred before the effective mobilization of qu max , the cyclic loading stage, the unloading, and the postcyclic
the fibers. UCS test. Independently of the binder quantity and for both of
Fig. 10 presents the stress–strain changes experienced by the the stabilized materials, unreinforced and fiber-reinforced, the
samples under the UCS cyclic loading test, i.e., the initial increase cyclic loading led to an increase in the unconfined compressive
strength (Fig. 11). This increment was greater for the lower binder
quantities which had greater deformations during the cyclic stage
(Fig. 1), i.e., in which the strain hardening effect seemed to be more
Mu_2 Mu_10 Mu_100 pronounced. The addition of fibers led to the same changes as for
1 1 1
the UCS tests performed before the cyclic stage.
The stress–strain behavior of all samples was analyzed in terms of
energy absorption capacity (EAC), i.e., the energy required to induce
deformation in the composite material (Choobbasti and Kutanaei
qu (kPa)

2017; Patel and Singh 2017). The energy absorption capacity is


equal to the area below the stress–strain curve (Choobbasti and
Kutanaei 2017; Kafodya and Okonta 2021; Patel and Singh 2017),
and was computed for equal axial strain, considering the value of the
composite material with the highest axial strain at failure (εa failure ¼
6.55% for the fiber-reinforced sample stabilized with 100 kg=m3
portland cement and tested without cyclic loading). The EAC in-
εa (%) creased with the binder quantity (Fig. 12), reflecting the fact that
a greater binder quantity induces a stronger and stiffer solid matrix,
Fig. 7. Definition of undrained resilient modulus (Mu ).
in agreement with the increase in the undrained resilient modulus

© ASCE 04023392-7 J. Mater. Civ. Eng.

J. Mater. Civ. Eng., 2023, 35(11): 04023392


14000

12000
325 kg/m³

10000 325 kg/m³ + PP


250 kg/m³

Mu (kPa)
8000
250 kg/m³ + PP
6000 175 kg/m³
175 kg/m³ + PP
4000
100 kg/m³
2000
100 kg/m³ + PP
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0
0 1000 2000 3000 4000 5000
(a) Number of cycles

(b)
Fig. 8. (Color) (a) Evolution of the undrained resilient modulus with the number of loading cycles; and (b) evolution of the undrained resilient
modulus for cycles 2, 5, 500, and 5,000.

3500 3500

3000 3000 325 kg/m³ + PP


250 kg/m³ + PP
2500 2500
175 kg/m³ + PP
325 kg/m³
100 kg/m³ + PP
qu (kPa)

qu (kPa)

2000 250 kg/m³ 2000


175 kg/m³
1500 1500
100 kg/m³
1000 1000

500 500

0 0
0 2 4 6 8 10 12 14 16 18 20 0 2 4 6 8 10 12 14 16 18 20
(a) εa (%) (b) εa (%)

Fig. 9. Effect of binder quantity and reinforcement with polypropylene fibers on the stress–strain behavior of the UCS tests: (a) without fibers; and
(b) with fibers.

and greater elastic deformation energy. The deformation that oc- an increase in the EAC, because as the UCS test proceeded (i.e., as
curred during the cyclic loading stage (Fig. 1) promoted a strain- the axial strain increased) there was a progressive mobilization of the
hardening effect responsible for the increase in the energy absorption tensile strength of the fibers responsible for the ductile behavior, and
capacity of the composite materials. The addition of the fibers led to therefore failure occurred at higher levels of strains, allowing the

© ASCE 04023392-8 J. Mater. Civ. Eng.

J. Mater. Civ. Eng., 2023, 35(11): 04023392


3500 3500

3000 3000 325 kg/m³ + PP Cyc.


325 kg/m³ Cyc.
250 kg/m³ Cyc. 250 kg/m³ + PP Cyc.
2500 2500
175 kg/m³ Cyc. 175 kg/m³ + PP Cyc.
qu (kPa)

qu (kPa)
2000 2000 100 kg/m³ + PP Cyc.
100 kg/m³ Cyc.
1500 1500

1000 1000

500 500

0 0
0 2 4 6 8 10 12 14 16 18 20 0 2 4 6 8 10 12 14 16 18 20
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(a) εa (%) (b) εa (%)

Fig. 10. Effect of binder quantity and reinforcement with polypropylene fibers on the stress–strain behavior of the UCS tests after the cyclic stage:
(a) without fibers; and (b) with fibers.

composite material to absorb more energy, in agreement with the because the deformations that occurred during the cyclic loading
findings of Choobbasti and Kutanaei (2017), Maher and Ho (Fig. 1) allowed earlier mobilization of the fibers, in addition to
(1993), and Patel and Singh (2017). This effect was more pro- the strain-hardening effect.
nounced in the samples submitted to a prior cyclic loading stage
Conclusions
4000
The results of the unconfined compressive strength tests performed
3500 on stabilized unreinforced and fiber-reinforced samples subjected
3000
or not to a prior cyclic loading stage (50%  10% of qu max , applied
with a frequency of 0.5 Hz and during 5,000 loading cycles), al-
Max
qu máx (kPa)

2500 Average lowed the authors to reach the following conclusions:


Min 1. During cyclic loading, the accumulated permanent axial strain
2000
decreases as the binder quantity increases because a larger
1500 amount of binder leads to a stronger and stiffer stabilized matrix.
1000 2. The energy applied by the external cyclic load in the first load-
ing cycles mostly is dissipated as plastic energy, and the remain-
500 ing energy is absorbed by the composite material as elastic
0 energy, a trend that quickly reverses as the number of cycles
100 175 250 325 increases. After a low number of cycles (10–100) the stabilized
Cement quantity (kg/m³) material achieves a quasi-steady hysteretic response, with the
relative elastic deformation energy ranging between 90% and
Fig. 11. Effect of binder quantity and reinforcement with polypropy- 80%. The breakage of the cementitious bonds seems to be
lene fibers on the unconfined compressive strength of tests carried out the dominant dissipation mechanism inducing irrecoverable
before (UCS) and after (UCSpc) the cyclic stage. (plastic) deformations of the solid skeleton, which are more in-
tense the lower the binder content.
3. The deformation occurring during the cyclic loading seems to
promote a strain-hardening effect which is responsible for the
increase in the resilient modulus. The undrained resilient modu-
lus increases with the binder quantity, meaning that a composite
material stabilized with a higher binder content has the ability to
absorb a higher elastic deformation energy.
4. The addition of fibers leads to an increase in the plastic defor-
mation energy, which is more noticeable in the first cycles, lead-
ing to an increase in the accumulated plastic axial strains and to
a reduction of the undrained resilient modulus during the cyclic
loading, which is explained by two cumulative effects: the high
compressibility of the polypropylene fibers; and the weakening
of the stabilized matrix as a result of the physical presence of the
fibers, which may prevent the development of some cementi-
tious bonds, producing a composite material with lower strength
Fig. 12. Effect of binder quantity on the energy absorption capacity
and stiffness.
evaluated in the tests carried out before (UCS) and after (UCSpc)
5. The cyclic loading stage introduces changes in the postcyclic
the cyclic stage for the unreinforced and fiber-reinforced stabilized
stress–strain behavior characterized by an increase in the postcy-
samples.
clic unconfined compressive strength and the energy absorption

© ASCE 04023392-9 J. Mater. Civ. Eng.

J. Mater. Civ. Eng., 2023, 35(11): 04023392


capacity of the composite materials. The increase in the postcyclic considering temperatures of 20 and 40°C.” Bull. Eng. Geol. Environ.
unconfined compressive strength is more significant with lower 80 (2): 1841–1855. https://doi.org/10.1007/s10064-020-02028-x.
binder quantities that have greater deformations during the cyclic ASTM. 1998. Standard practice for classification of soils for en-
stage, i.e., in which the strain-hardening effect seems to be more gineering purposes (unified soil classification). ASTM D2487. West
pronounced. The addition of fibers leads to an increase in the en- Conshohocken, PA: ASTM.
Azeiteiro, R. J. N., P. A. L. F. Coelho, D. M. G. Taborda, and J. C. D.
ergy absorption capacity, which may be explained by the fact that
Grazina. 2017. “Energy-based evaluation of liquefaction potential
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under non-uniform cyclic loading.” Soil Dyn. Earthquake Eng. 92 (Jul):
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Data Availability Statement London: BSI.


CEN (European Committee for Standardization). 2000. Cement—Part 1:
Some or all data, models, or code generated or used during the Composition, specifications and conformity criteria for common
cements. EN 197-1. Brussels, Belgium: CEN.
study are available from the corresponding author upon reasonable
CEN (European Committee for Standardization). 2004. Unbound and
request.
hydraulically bound mixtures—Part 7: Cyclic load triaxial test for
unbound mixtures. EN 13286-7. Brussels, Belgium: CEN.
CEN (European Committee for Standardization). 2007. Concrete—Part 1:
Acknowledgments
Specification, performance, production and conformity. EN 206-1.
The authors express their thanks to CIMPOR and Biu International Brussels, Belgium: CEN.
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financially supported the research: Individual Research Grant
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2021.05748.BD, Project Research Grant FCT (PTDC/ECI-CON/ .001.
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