Quantachrome?ASiQwin?

Automated Gas Sorption Data

Acquisition and Reduction
ⓒ 1994-2017, Quantachrome Instruments
version 5.2

Analysis Report
Operator: SSU Date:2024/04/08 Operator: a
Date:2024/04/10
Sample ID: b Filename: 240408_H2.qps
Sample Desc: Comment: N2- micro/mesopore analysis-
general
Sample Weight: 0.0854 g Instrument: Autosorb iQ Station 2
Outgas Time: 0.0 hrs Outgas Temp.: 0 캜
Analysis gas: Nitrogen Non-ideality: 6.58e-05 1/Torr CellType:
9mm w/o rod
Analysis Time: 10:00 hr:min Bath temp.: 77.35 K
Analysis Mode: Standard VoidVol
Remeasure:off
VoidVol. Mode: He Measure Cold Zone V: 6.03079 cc Warm Zone V:
16.474 cc
Data Reduction Parameters
Thermal Transpiration: onEff. mol. diameter (D): 3.54 휛 ff. cell
stem diam. (d): 4.0000 mm

t-Method Calc. method: de Boer

BJH/DH method Moving pt. avg.: off Ignoring P-tags below 0.35 P/Po
Adsorbate modelNitrogen Temperature 77.350K
Molec. Wt.: 28.013 Cross Section: 16.200 ?2 Liquid
Density: 0.808 g/cc

Diameter Pore Volume Pore Surf dV(d) dS(d) dV(logd)

dS(logd)
Area
nm cc/g m?g cc/nm/g m?nm/g cc/g
cc/g

3.0491 5.0733e-03 6.6555e+00 1.5672e-02 2.0560e+01

1.0993e-01 1.4421e+02
3.4056 7.6303e-03 9.6588e+00 6.5682e-03 7.7147e+00
5.1450e-02 6.0430e+01
3.8216 1.2952e-02 1.5229e+01 1.2023e-02 1.2585e+01
1.0568e-01 1.1061e+02
4.2998 1.8035e-02 1.9957e+01 9.8891e-03 9.1995e+00
9.7793e-02 9.0974e+01
4.8963 2.3574e-02 2.4482e+01 8.1577e-03 6.6644e+00
9.1824e-02 7.5015e+01
5.6129 2.6538e-02 2.6595e+01 3.9305e-03 2.8011e+00
5.0722e-02 3.6147e+01
6.5316 2.9803e-02 2.8594e+01 3.0137e-03 1.8456e+00
4.5221e-02 2.7693e+01
7.7905 3.4423e-02 3.0967e+01 3.2213e-03 1.6540e+00
5.7622e-02 2.9586e+01
9.5713 3.9312e-02 3.3010e+01 2.2980e-03 9.6039e-01
5.0437e-02 2.1078e+01
12.2064 4.3653e-02 3.4432e+01 1.3813e-03 4.5263e-01
3.8607e-02 1.2651e+01
17.2431 4.5864e-02 3.4945e+01 3.1897e-04 7.3993e-02
1.2492e-02 2.8978e+00
 27.5969 5.2473e-02 3.5903e+01 4.7971e-04 6.9530e-02
2.9839e-02 4.3249e+00
166.5247 8.6489e-02 3.6720e+01 1.2881e-04 3.0941e-03
3.6288e-02 8.7165e-01

BJH desorption summary

Surface Area = 36.720 m?g

Pore Volume = 0.086 cc/g
Pore Diameter Dv(d) = 3.049 nm