W4700162 V1.5 EN - AlkaliCAU Installation

kajaaniALKALi™
- for Causticizing
Installation manual
W4700162 V1.5 EN
Table of Contents
Safety Information 4. Sample, Water & Air Connections
Caution / Warning 4.A. Analysis Water ........................................... 4.1
4.B. Flushing Water ........................................... 4.1
4.C. Instrument Air Connections ......................... 4.3
1. Introduction
4.D. Discharge & Overflow Connections .............. 4.3
1.A. Measurements ............................................ 1.1 4.E. Titration Vapor Outlet .................................. 4.4
1.B. Sampling ..................................................... 1.1 4.F. Water Purifier (option) ................................. 4.4
1.C. Sample Preparation .................................... 1.1
1.D. Analyzing .................................................... 1.1 5. Installation of Samplers
5.A. Sample Lines .............................................. 5.1
2. Installing the Analyzer
5.B. Mounting Cone ............................................ 5.1
2.A. Analyzer Models ......................................... 2.1 5.C. Sampler SD-701 .......................................... 5.2
2.B. Cabinet Model ............................................. 2.2 5.D. Installing SD-701 to a Tank ......................... 5.3
2.C. Compartment Model .................................... 2.2 5.E. Mounting & Removing SD-701 ..................... 5.4
5.F. Adjusting the Piston Stroke ........................ 5.4
3. Electric Connections 5.G. Sampler SD-702 .......................................... 5.5
3.A. Electronics unit ........................................... 3.1
3.B. Operating Voltage ....................................... 3.1
3.C. Signal Connections ..................................... 3.2 App. 1 - Technical Specifications
3.D. Analog Connections .................................... 3.3 App. 2 - Contents of Delivery
3.E. Binary Connections ..................................... 3.4
App. 3 - Chemical Safety Information
3.F. Serial Communication ................................. 3.5
3.F.1. DCS, Modbus ................................. 3.5 App. 4 - ModBus Specifications
3.F.2. Modem connection ......................... 3.5
App. 5 - Installation Drawings
3.F.3. PC connections .............................. 3.5
3.G. Communicator-i Remote Connection ........... 3.6
3.H. Communicator-i Extra Cable ....................... 3.7
kajaaniALKALi Installation - TOC - W4700162 V1.5 EN

Safety Information
Follow the applicable safety regulations

and always use appropriate protective equipment
during all installation, operating and service
operations to protect against injuries
caused by hazardous chemicals!
First Aid measures
Seek medical advice immediately if

- the patient has difficulty breathing,
- the patient has convulsions, or
- the patient is unconscious.
If no immediate symptoms are observed, give first aid
on the spot as instructed below:
F After ingestion of chemical

Do NOT induce vomiting! Find out if vomiting is
necessary, recommended, or harmful – this is depen-
dent on the chemical in question! In many cases taking
medicinal carbon is the primary cure, however NOT if
some corrosive chemical has been ingested.
After first aid measures
F After contact with skin seek medical advice!
Immediately rinse the contaminated area thoroughly
with plenty of lukewarm running water.
Then wash with soap, rinse with water.
F After contact with eyes

Immediately rinse the eye thoroughly with plenty of
water, e.g. by pouring water from a glass into the eye.
Continue rinsing for about 10 minutes. Do not use a
strong hard shower that may damage the eye.
If the chemical is corrosive, continue rinsing for 10–30
minutes and seek medical advice.
F After inhaling a chemical

Allow the patient to rest in fresh air.
kajaaniALKALi SAFETY
Caution / Warning
During installation, maintenance and service operations,
! remember that the sample line may contain hot sample

or water – be careful!
The chemical vapors released during titration are
! hazardous when inhaled!

Make sure to lead the vapors out of the working area!
Never run the pump unit dry –

! this will damage the pump!
When installing or servicing the sample lines,
! always wear appropriate protective clothing to

prevent injuries caused by hot liquor!
Always check that the incoming voltage & frequency

are correct before making any electric connections.
Incorrect connections will damage the equipment!
The applicable electrical safety regulations must be
closely followed in all installation work!
kajaaniALKALi CAUTION / WARNING

1. Introduction
1.A. Measurements
The kajaaniALKALi is an automatic titrator for causti-
cizing processes. Following the SCAN 30:85 standard,
it analyzers the following values from liquor samples: SD-701
• sodium hydroxide (NaOH),
• sodium sulphide (Na2S),
• sodium carbonate (Na2CO3), SD-702
• effective alkali (EA),
• total titratable alkali (TTA),
• active alkali (AA),
• causticizing degree (CE %),
• sulphidity (S%).
The results are reported as Na2O or NaOH.
The system consists of 1–8 samplers, a sample unit,
and a measurement unit. One sample unit may contain
one or two sample preparation units, with 4 sample line
connectors each. Sample titration takes place in the
titration modules located in the measurement unit.
1.B. Sampling
Samples are extracted from the selected sampling points,
using either pneumatically controlled valves or dedi-
cated samplers, and led to the analyzer through sample
lines made of PTFE.
1.C. Sample Preparation

The sample flows into the sample preparation unit
where lime mud is separated by sedimentation. After
this the liquor sample is led to the measurement unit for
titration. Fig. 1.1. kajaaniALKALi analyzer and samplers.
1.D. Analyzing
In the measurement unit, the titration modules (1 or 2)
perform ABC titration.
The titration curve and its three equivalence points
are determined by adding 1 N hydrochloric acid to the
sample.
kajaaniALKALi – Installation - 1.1 - W4700162 V1.5 EN

2. Installing the Analyzer
2.A. Analyzer Models
The kajaaniALKALi consists of a sample unit and a sample preparation unit has 4 sample line connections
measurement unit. These can be either assembled in a and a sedimentation tank.
steel cabinet or in a protective compartment. The measurement unit contains a titration frame
One sample unit contains one or two sample prepa- with 1 or 2 titration modules.
ration units, a waste tank, and a waste pump. Each
790 (31
)
)
(31 790 (31
)
790 Sample
prep. unit 2
Electronics
unit
Sample
preparation unit 1
1900 (75")
Titration frame
Analysis water tank
Hydrochloric acid tank

Waste tank
Sample unit Measurement unit
Fig. 2.1. Dimensions and main parts of the kajaaniALKALi analyzer (shown here with all side doors removed).
The configuration illustrated here contains 2 sample preparation units (in sample unit) and 2 titration modules.
kajaaniALKALi Installation - 2.1 - W4700162 V1.5 EN

2.B. Cabinet Model 2.C. Compartment Model
The cabinet model is designed for operating environ- In very demanding process environments the analyzer
ments where the ambient temperature is +5..+50°C can be installed in a separate compartment (Fig. 2.4)
(+41...122°F). Enclosure classification (Fig. 2.1): where the operating conditions, e.g. temperature, can
• IP54 (NEMA 3S) better be stabilized.
• dimensions: height 1900 mm (75”), width 790 mm Mounting bolts for compartment installation are
(31”), depth 790 mm (31”) included in delivery.
• weight: 210 kg (463 lbs) NOTE: If the protective compartment is purchased from
The cabinet model analyzer must be fastened to the another supplier, make sure to verify with a Metso Auto-
floor or to a mounting stand with bolts. Select bolt mation specialist that its dimensions are correct before
material and dimensions according to the installation placing the order!
site. The bolt locations are shown in Fig. 2.2. The
analyzer’s installation space requirement is illustrated
in Fig. 2.3.
Sample unit Measurement unit

ø13 (33/64")
18 mm 56
0
(2 )
Similar mounting stand
2
1/ 9/16"
16 (27
under each unit
") 700
Fig. 2.2. Location of the fastening bolts, for cabinet model.
1 m (3.3 ft)
) )
8 8
(2 (2
m m
0m 00m
0
~7 ~7
~
70
0
m
m
1 m (3.3 ft) (2
790 x 790 mm 790 x 790 mm 8
)
(31 x 31) (31 x 31)
1 m (3.3 ft)
~ ~
70 70
0 0
m m
m m
(2 (2
8 8
) )
1 m (3.3 ft)
Fig. 2.3. Installation space required for the cabinet model.

Communicator-i, extra cable connector
Measurement unit
2430 (96")
Sample
preparation
- unit 1
- unit 2
Discharge pump
Waste tank
2440 (96")
400 (16") About 0.5 m (~ 2 ft)
free space above
the compartment
Titration
frame
Measurement unit
Electronics Sample
unit preparation unit 2
2800 (110")
Sample
preparation unit 1
10
00
(3
9
)
Fig. 2.4. kajaaniALKALi analyzer in a protective compartment. The configuration illustrated here contains 2 sample
preparation units and a titration frame with two titration modules.

3. Electric Connections
3.A. Electronics unit
The door mechanism of the electronics unit can be

opened e.g. with a screwdriver.
Electronic board racks:

Analyzer Server
Modem
Terminal strips Mains terminal Power switch
Fig. 3.1. Electronics unit, with front door opened.
3.B. Operating Voltage
Lead the operating power cables into the analyzer

through the bushings on its rear wall, and connect them
to the mains terminal strip (Fig. 3.2). This terminal strip
is located in the bottom right part of the electronics unit,
under a protective cover.
Specifications:
• 85–132 / 170–264 VAC (automatic selection)
• 60 / 50 Hz
• power intake 150 W
The analyzer’s power feed must be secured with a
fuse that meets the applicable mill specifications.
NOTE: Always check that the incoming voltage & fre-
quency are correct before making any electric connec-
tions. Incorrect connections will damage the equipment!
The applicable electrical safety regulations must be close-
ly followed in all installation work!
Fig. 3.2. Operating power connection.

3.C. Signal Connections
The analyzer’s electronics boards are installed in two Terminals BO1, BI1, BO2 & BI2 are reserved for
board racks (“Analyzer” and “Server”, Fig. 3.1) located internal control signals (sample preparation unit con-
in the upper part of the electronics unit. trol).
All connections to the sample unit and to customer All external signals (analog inputs/outputs, binary
systems are made using the terminal strips. These are inputs/outputs, DCS-signals) are connected to termi-
located in the lower part of the electronics unit (Fig. 3.1 nals ANAL./BIO/DCS.
& 3.3).
17 51 ANAL./BIO/DCS 248
1 69 101 117 151 169 201
18 34 70 88 118 134 170 188 249 296

-output signals -input signals -output signals -input signals Analog inputs & Outputs,
BO1 BI1 BO2 BI2 Binary input & outputs
Sample preparation unit 1 Sample preparation unit 2 DCS connection
Fig. 3.3. Connections at the terminal strip.
Table 3.1. Sample preparation unit 1, output signals. Table 3.3. Sample preparation unit 2, output signals.
Terminal strip Sample preparation unit Name Terminal strip Sample preparation unit Name
1 Valve 1A, sample line 1 S1 101 Valve 1B, sample line 1 S2
5 Valve 5A, sampling device 1 S1 105 Valve 5B, sampling device 1 S2
9 Valve 9A, sample back to process S1 110 Valve 10B, ejector S2
10 Valve 10A, ejector S1 111 Valve 11B, water in S2
11 Valve 11A, water in S1 112 Valve 12B, acid wash S2
12 Valve 12A, acid wash S1 113 Valve 13B, waste tank S2
13 Valve 13A, waste tank S1 114 Valve 14B, sedimentation inlet S2
14 Valve 14A, sedimentation inlet S1 116 Valve 16B, sample to titration S2
15 Valve 15A, valve betw. SPUs S1 133 +24V
16 Valve 16A, sample to titration S1 134 +24V
17 Waste pump control valve S1
33 +24V
34 +24V
Table 3.2. Sample preparation unit 1, input signals. Table 3.4. Sample preparation unit 2, input signals.
Terminal strip Sample preparation unit Name Terminal strip Sample preparation unit Name
55 Water pressure S1 156 Air pressure, SPU 2 S2
56 Air pressure, SPU 1 S1 161 Water valve position sensor S2
61 Water valve ( 11A) position sensor S1 163 Waste tank valve (13B ) position sensor S2
63 Waste tank valve (13A) position sensor S1 164 Sedim. vessel valve (14A ) position sensor S2
64 Sedim. vessel valve (14A ) position sensor S1 185 +24V
69 Waste tank level sensor S1 186 +24V
85 +24V 187 +24VGND
86 +24V 188 +24VGND
87 +24VGND
88 +24VGND

3.D. Analog Connections
Depending on the system, the “Server” board rack may

contain 0–2 analog boards. The number of available
analog inputs and outputs is dependent on the number
of boards present, as follows:
• no analog board
=> no analog inputs/outputs;
• one analog board
=> 7 analog inputs, 8 analog outputs;
• two analog boards
=> 14 analog inputs, 16 analog outputs.
Analog inputs: Analog outputs:

0–5 VDC / 0–20 mA / 4–20 mA, isolated. 0–5 VDC / 0–20 mA / 4–20 mA, common isolation.
The analog inputs are connected to the lower termi- Max. load RL = 600Ω.
nals of the ANAL./BIO/DCS terminal strip (Table 3.5). The analog outputs are connected to the upper
Signal type (voltage/current) for the analog inputs is terminals of the ANAL./BIO/DCS terminal strip (Table
set with a jumper: 3.6).
• jumper 1->2: voltage signal 0–5 VDC The measurement results (EA, AA, TTA, CE%, S%,
• jumper 2->3: current signal, software-selectable NaOH, Na2S, Na2CO3, V1…V3, pH1…pH3) can be
current range. Default: 4–20 mA. freely configured to any of the analog outputs 1…16.
External Analyzer Analog Unit External Analyzer

connections connections Terminal Analog
Terminal
Aout1 Unit
Ain 1
- 250 250W -
4-20 mA 202
3 2 1 4-20 mA Rmax =
4-20 mA
+ 600W + 201
249 0-5 VDC
NOTE terminal polarity! NOTE terminal polarity!
Fig. 3.4. Connection of analog inputs. Fig. 3.5. Connection of analog outputs.
Table 3.5. Connection of analog inputs to the terminal strip. Table 3.6. Connection of analog outputs to the terminal strip.
Analog Board 1 Analog Board 2 Analog Board 1 Analog Board 2

Signal Terminal Signal Terminal Signal Terminal Signal Terminal
Ain1+ 249 Ain1+ 263 Aout1+ 201 Aout1+ 217
Ain1- 250 Ain1- 264 Aout1- 202 Aout1- 218
Ain2+ 251 Ain2+ 265 Aout2+ 203 Aout2+ 219
Ain2- 252 Ain2- 266 Aout2- 204 Aout2- 220
Ain3+ 253 Ain3+ 267 Aout3+ 205 Aout3+ 221
Ain3- 254 Ain3- 268 Aout3- 206 Aout3- 222
Ain4+ 255 Ain4+ 269 Aout4+ 207 Aout4+ 223
Ain4- 256 Ain4- 270 Aout4- 208 Aout4- 224
Ain5+ 257 Ain5+ 271 Aout5+ 209 Aout5+ 225
Ain5- 258 Ain5- 272 Aout5- 210 Aout5- 226
Ain6+ 259 Ain6+ 273 Aout6+ 211 Aout6+ 227
Ain6- 260 Ain6- 274 Aout6- 212 Aout6- 228
Ain7+ 261 Ain7+ 275 Aout7+ 213 Aout7+ 229
Ain7- 262 Ain7- 276 Aout7- 214 Aout7- 230
Aout8+ 215 Aout8+ 231
Aout8- 216 Aout8- 232

3.E. Binary Connections
Binary inputs:
8 opto-isolated inputs, 24–48 VDC. External Analyzer
connections Bin1
Measuring permit to analyzer’s channels 1…8: Bin1
= permit to channel 1; Bin2 = permit to channel 2, etc.
24…48 – 278
NOTE: Signal 1 = NO measuring permit (=off), signal 0 = VDC + 277
measuring permit (=on)!
NOTE terminal polarity!
Bout1
Binary outputs: max. 48 VDC/30W
8 relay outputs (1 alarm), opening/closing contact. 24 or 233
VDC/1A, 48 VDC/0.5A, or 125VAC/0.5A. 125 VAC/0.5A 234
• Bout1 = alarm (closing contact, control = 0).
• Bout2 = error (opening contact, control = 1)
Fig. 3.6. Connection of binary inputs/outputs.
– remains on for 25 seconds.
• Bout3 = Service (opening contact, control = 1).
• Bout4 = “Analysis ready” (opening contact, Table 3.7. Connection of binary inputs/outputs to the terminal
control = 1). strip.
• Bout5...8 = address of meas. result
Binary outputs Binary inputs
(opening contact, control = 1).
Signal Terminal Signal Terminal
1111 = channel 1 1011 = channel 5 Bout1+ 233 Bin1+ 277
0111 = channel 2 0101 = channel 6 Bout1- 234 Bin1- 278
1011 = channel 3 1001 = channel 7 Bout2+ 235 Bin2+ 279
0011 = channel 4 0001 = channel 8 Bout2- 236 Bin2- 280
Bout3+ 237 Bin3+ 281
When a new measurement result is ready, Bout4 Bout3- 238 Bin3- 282
opens (control = 0) and Bout5...8 indicate the result Bout4+ 239 Bin4+ 283
address. Bout4 remains open for 60 seconds, then Bout4- 240 Bin4- 284
Bout5+ 241 Bin5+ 285
closes again and remains closed until the next result is
Bout5- 242 Bin5- 286
ready – however at least for 60 seconds. The measure- Bout6+ 243 Bin6+ 287
ment result address changes only when Bout4 opens Bout6- 244 Bin6- 288
again. In other words, there is at least 120 seconds time Bout7+ 245 Bin7+ 289
to read each measurement result from the analog out- Bout7- 246 Bin7- 290
puts. Bout8+ 247 Bin8+ 291
Bout8- 248 Bin8- 292

3.F. Serial Communication
Serial communication cabling must be made using

shielded instrumentation cable. Maximum cable length
is 300 m (984 ft).
3.F.1. DCS, Modbus

DCS-communication is connected to the terminal strip
in the bottom of the electronics unit.
Protocol: RS-485, 4-wire. Modbus protocols 3 and PC Modem
4 are available.
Communi-
cator-i
Signal Terminal
TxD_A 293 Analyzer Server
TxD_B 294
RxD_A 295
RxD_B 296 Fig. 3.7. Location of serial ports in the electronics unit.
GND yellow/green
3.F.2. Modem connection

The modem is factory-connected to D9 connector “Mo-
dem” on the “Server” motherboard. Protocol: RS-232.
Connect the telephone line to the modem’s connector
“LINE”. The receiving end must have a PC + modem
and the AlkaliTool software installed.
Set the “Modbus Float” protocol for the analyzer’s
modem port.
Using the AlkaliTool software, select Communica- PC Modem
tion -> Stop communication. Then select Communica-
tion -> “Check and set serial port and modem”, and a Communi-
cator-i
Setup window will appear on the screen. Choose the
correct modem port (= the port where the PC’s modem Server
is connected). Activate “Modem”, and then type the PC-connection
D9; female whi blu D9; female
phone number for communication. Click OK to accept RxD 2 2
blu whi
the settings. Then select Communication -> Start com- TxD 3 bro bro 3
GND 5 5
munciation. RTS 7
CTS 8 NOT IN USE
3.F.3. PC connections D25; female whi whi D25; male
The PC can be connected directly to the connector TxD 2 blu blu 2
RxD 3 bro bro 3
located in the analyzer’s “Server” board rack. A stan- GND 7 7
dard KAJAANI PC-cable can be used for connection RTS 4
CTS 5
(order code A4500382 V1.0); see Fig. 3.8.
3m
Signal connections of the PC-connector:

Pin Signal
1 NC
2 RxD
3 TxD
4 NC
A4500382 V1.0
RS232 CABLE
5 GND
6 NC
7 NC
8 NC
9 NC
Fig. 3.8. Connecting a PC to analyzer.

Fig. 3.9 shows the PC connection to the DCS-port;
in this case the DCS-port is not available for other
communications.
ANAL./BIO/DCS 248
169 201
188 249 296
(A) = RS-485/RS-232 converter

Westermo MA-42
Positions of DIP switches in RS-485/232
converter (Westermo MA-42)
2-pair cable 1 S3 6 1 S2 6
(max. 1200 m)
On (1)
Off (0)
RS-485 cable RS-485/232
1 0 11 0 0 0 0 1 0 0 0
(251801, option) converter
(251723, option)
RXD 2 2 2 R- 293 TxD_A

PC TXD 3 3 1 R+ 294 TxD_B Analyzer
D9 conn. GND 5 7 4 T- 295 RxD_A terminal strip
3 T+ 296 RxD_B
(A)
Fig. 3.9. Connecting a PC to analyzers DCS-connection with RS-converter.
3.G. Communicator-i Remote Connection (option)

The analyzer is normally operated using a Communicator-
i terminal. For operation, the terminal is plugged to the
connector on the rear wall of the electronics unit (Fig. 3.10).
If required, remote connection cabling can be used, and
in this case the Communicator-i can be placed for example
in the control room. For connection, see Fig. 3.11.
Server
Communicator-i
Connector for Communicator-i
A4700503 V1.0
max.
Electronics 350 m
unit (1148 ft)
Connection cable
- not included in delivery.
Use for example
JAMAK 4 x (2+1) x 0.5 mm2
Connection:
Fig. 3.10. Location of the Communicator-i connector.
1 +24V
2 GND
3 Tx+
4 Tx–
5 Rx+
6 Rx–
Fig. 3.11. Communicator-i remote connection.

3.H. Communicator-i Extra Cable
The compartment model analyzer also includes an extra

connection for the Communicator-i. This extra connec- 6000 mm
tion is located next to the sample preparation units, 50 mm
outside the compartment.
If the compartment will not be purchased from Neles
Field Controls, the Communicator-i extra cable can be
ordered as an option; order code A4700680 V1.0. The
installation is illustrated in Fig. 3.12 & 3.13.
Communicator-i
extra cable
Measurement unit connector
Sample
preparation Johdotus:
- unit 1 P23 P29 Schaltbau- Merkintä Johtimen
- unit 2 pin pin liittimen pinni (avoin pää) väri
1 1 1 1 musta
2 2 2 2 musta
3 3 3 3 musta
4 4 4 4 musta
5 5 5 5 musta
6 6 6 6 musta
7 7 ground ground ke/vi
Fig. 3.12. Location of the extra cable connector. Fig. 3.13. Communicator-i extra cable.

4. Sample, Water & Air Connections
Fig. 4.1–4.3 show all connections of the kajaaniALKA- Table 4.1. Tube sizes.
Li analyzer. More detailed information is given in the
Outside diameter Inside diameter Wall thickness
following sections. DN10 17.2mm 14.0mm 1.6mm
The recommended pipe sizes (DNxx) are specified [11/16”] [35/64”] [1/16”]
in Table 4.1. DN15 21.3mm 18.1mm 1.6mm
[27/32”] [23/32”] [1/16”]
DN20 26.9mm 23.7mm 1.6mm
NOTE: To ensure continuous and undisturbed operation, [1 1/16”] [15/16”] [1/16”]
the analysis water supply and flushing water supply must DN25 33.7mm 30.5mm 1.6mm
[1 21/64”] [1 13/64”] [1/16”]
be STEADY and UNINTERRUPTED!
4.A. Analysis Water 4.B. Flushing Water
NOTE: Ensure steady, uninterrupted water supply! NOTE: Ensure steady, uninterrupted water supply!
The analysis water is led into the analysis water tank, Specifications:
located in the lower part of the measurement unit. • chemically purified, acceptable for return to process
Specifications: • pressure 4–8 bar (58–116 psi), at least 2 bar (29 psi)
• distilled or deionized water higher than highest process pressure at the sampling
• pressure < 4 bar (< 58 psi) points
• temperature +10–40°C (50–104°F) • temperature +5–50°C (41–122°F)
• conductivity < 30 µS/m. NOTE: The hottest flushing water must be at least 20°C
• pH = 6–8 (36°F) cooler than the coolest process samples!
• consumption 2.5 liters (0.7 US gal) / h / titr. module
• connection ISO 7/1–Rp 1/2" or NPT 1/2" • filter 100 µm
• recommended inlet pipe DN10 • consumption 150 liters (40 US gal) / hour / sample
unit (= 4 sample lines)
• connection ISO 7/1–Rp 1/2" or NPT 1/2"
• recommended inlet pipe DN20
700 (27 1/2")
350
(13 3/4")
285
(11 1/4")
180
(7 1/8")
130
Discharge (5 1/8") 1090 (43")
Compressed air in
Flushing water in, 937 (37")
sample prep. unit 1 840 (33")
Flushing water in, 737 (29")
sample prep. unit 2
625 (24 1/2")
Analysis water in 540 (21 1/4")
Discharge from 460 (18")
titration modules
Analysis water overflow
Waste tank overflow
80–130 (~ 3–5")
Fig. 4.1. Connections of sample unit, cabinet model.

Flushing water in Titration Analysis water in
Instrument air in vapors
Sample & waters Flushing water in

back to process
B5 B6
A5 A6 A7 A8 B7 B8
Sampler valve controls:

1…4 = A5,A6,A7,A8 / 5…8 = B5,B6,B7,B8
Sample lines 1–4 Sample lines 5–8

Sample and water
back to process
DN25 Rp1/2" or NPT 1/2”
Instrument air in
DN15 Rp1/2" or NPT 1/2”
Flushing water in Flushing water in
DN20 Rp1/2" or NPT 1/2” DN20 Rp1/2" or NPT 1/2”
Washing gun
(water/air)
Overflow, d=2" Waste tank

(3 alternative outlets;
one in use,
2 closed with plugs)
Fig. 4.2. Connections of sample unit, analyzer installed in a KAJAANI protective compartment.
Sampler Sampler
SD-701 / SD-702 SD-701 / SD-702
Sample preparation unit 1 Sample preparation unit 2
5A 6A 7A 8A 8B 7B 6B 5B
Sample line 1
Sample line 2
Sample line 6
Sample line 5
16A 16B
Sample line 4
Sample line 8
Sample line 7
Sample line 3
1A 2A 3A 4A 4B 3B 2B 1B
14A 14B
11A 12B
12A 13A 15A 13B 11B
Outlet DN20 Waste tank Waste tank

9A
Rp 1/2” or NPT 1/2”
10A Ejector Ejector 10B
From waste pump Analysis
water Analysis
DN10, Rp 1/2" Flushing water DN20
Flushing water DN20 cups Rp 1/2" or NPT 1/2”
Rp 1/2" or NPT 1/2” or NPT 1/2”
Fig. 4.3. Valve diagram of sample preparation units.

4.C. Instrument Air Connections 4.D. Discharge & Overflow Connections
Instrument air is needed for the waste pump, and for the Analysis waste (used samples, flushing water, etc.) is
control of sample unit and sampler valves. drained from the waste tank by a pump.
Specifications: Discharge outlet connection ISO 7/1–Rp1/2" or
• filtered, water-free, oil-free instrument air NPT 1/2", recommended pipe size DN20, max. length
• pressure 4–6 bar (63–94 psi) 30 m (98 ft), max. delivery height 10 m (33 ft).
• flow min. 1,000 liters (35.5 ft3) / minute
• connection ISO 7/1–Rp 1/2" or NPT 1/2" Overflow connections:
• recommended inlet pipe DN15 Waste tank overflow: tube diameter 2", plastic hose or
corresponding. Connect the hose to one of the three
Instrument air to samplers: overflow outlet connectors with an acid-proof hose
Two air supply lines (6/4) are connected from the clamp, and lead the other end to an acceptable drain.
sample unit to samplers SD-701 and SD-702. Also see Make sure to close the other outlet connectors with
Fig. 4.2 & 4.4. plugs.
• valves A5, A6, A7, A8 => lines 1–4 Analysis water overflow: tube diameter 19mm, lead
• valves B5, B6, B7, B8 => lines 5–8 the outlet end to an acceptable drain.
Titration module overflow: tube DN10, lead the
outlet end to an acceptable drain.
4 valves on the right

in the upper solenoid block
are used for sampler control
1 2 3 4 5 6 7 8
Open SD-701
SD-702 Open Closed

Closed
Fig. 4.4. Location of air valves for sampler control, and connection of air tubes.

4.E. Titration Vapor Outlet 4.F. Water Purifier (option)
Chemical vapors released during titration must be led The reverse-osmosis-based water purifier generates
from the titration modules to a suitable ventilation deionized water, and it must always be installed if the
conduit. mill does not have an own boiler.
In the cabinet model, the titration vapors are led with The water purifier is installed inside the protective
a hose from the titration frame to an outlet opening compartment (compartment model) or on the analyz-
located on top of the cabinet (Fig. 4.5). ers side wall (cabinet model); Fig. 4.6. Also connect
Fig. 4.2 shows the location of the vapor outlet in the the control cable delivered with the water purifier (Fig.
protective compartment supplied by Neles Field Con- 4.7).
trols. Make the water connections as instructed in the
manual supplied with the water purifier. Connect the
water supply line to the analyzers analysis water inlet
Vapor out connector (Fig. 4.1).
Titration
frame
Measurement unit
Electronics Sample
unit preparation
unit 2
Sample
preparation
unit 1
Fig. 4.5. Location of titration vapor outlet, cabinet model.
Water purifier (option)
Fig. 4.6. Installation of water purifier inside a protective

compartment.
21
14
Relay
A2 A1
Water purifier kajaaniALKALi
AB C
Connection of plug wires:
A: Not in use
B & C: Connect relay pins to these, one to each.
Install plug to the connector on the water purifier.
Fig. 4.7. Connections of the water purifier.

5. Installation of Samplers
5.A. Sample Lines
Up to 4 sample lines can be connected to each sample R1/2"
preparation unit; thus, an analyzer with two sample FEP 3/4"
70101352
preparation units is able to handle max. 8 sample lines.
Specifications for the sample lines:
• material Teflon FEP or PFA
Hmin = 0.1 x L min. 300 (~12")
• outside diameter 19.1 mm (3/4")
• wall thickness 1.575 mm (1/16")
• minimum bending radius 300 mm (~12")
• length:
- for gravity-feed samples max. 35 m (115 ft)
- for pressurized samples max. 100 m (330 ft)
For gravity-feed samples the sample line must be
sufficiently inclined to ensure good sample flow: con- L
tinuous fall at least 10% (Hmin in Fig. 5.1). Threaded sleeve
1. Push the Tool H4700692
If process pressure at the sampling point is > 4 bar connector’s threaded
(58 psi) and sample temperature is > 95°C (203°F), the sleeve on the
sample line must be made of AISI 316L, outside diam- sample tube.
eter 16 mm (5/8"). Sample
2. Push the tool
Connect the sample line at both ends using 1/2" into the tube. tube Hot air blower
Teflon FEP/PFA connectors. Fig. 5.1 illustrates the
installation of a sample line connector with the special 3. Heat the tube
tool. The tool is included in delivery. evenly from all sides,
and push the tube
NOTE: Apply thread sealing tape and silicone grease end until the tool
(e.g. Molykote 111) on the screw-on sample line connec- collar.
Connector
tions!
4. Remove the tool
and push the tube
properly on the
connector.
5. Tighten with the

threaded sleeve.
Fig. 5.1. Sample line connections.

5.B. Mounting Cone
Samplers SD-701 and SD-702 are installed to the pro- 49 (1 15/16")
cess using a mounting cone that is welded to the process
pipeline or tank wall (Fig. 5.2).
Mounting to a pipeline: use the straight mounting
cone (code H4700324). 45
Mounting to tank wall: use the bevelled mounting
cone (code H4700328) which allows sampler installa-
80 (3 5/32")
tion at a 45° angle.

NOTE: Apply thread sealing tape and silicone grease
(e.g. Molykote 111) on the screw-on sample line connec-
tions!
22 (7/8")
H4700324 V1.1 H4700328 V 1.1
Fig. 5.2. Mounting cones.

5.C. Sampler SD-701
The SD-701 sampler is used for sampling from causti- example when installing through a thick tank wall, to
cizing vessels. ensure that the sampler tip is properly in the process.
The sampler is installed to process using a 3/4” ball See section 5.D for more information.
valve (70100038), tightening assembly (70100944),
and a mouting cone welded to the process pipe or tank Other specifications:
wall. • material AISI 316 L
The analyzer controls the sampler’s actuator pneu- • ambient temperature +5–60°C (41–140°F)
matically. • humidity 10–100%
Sampler SD-701 is available in four versions that • process temperature max. +110°C (230°F)
differ from each other as regards the length of the probe • process pressure max. 6 bar (87 psi)
tube; Fig. 5.3. A longer sampler may be needed for
SD-701/450 = A4700325 V1.1

SD-701/650 = A4700300 V1.1
SD-701/850 = A4700326 V1.1
SD-701/1200 = A4700327 V1.1
240 (9 1/2")
256768 H4700324 V1.0
A4700525 V1.0
ø48
120 (4 3/4") 142 (5 19/32") (57/64")
R1/2"
SD-701/450 (A4700325): 650 (25 5/8")

SD-701/650 (A4700300): 850 (33 1/2")
SD-701/850 (A4700326): 1050 (41 3/8")
SD-701/1200 (A4700327): 1400 (55 1/8”)
Fig. 5.3. Sampler SD-701, installed to process.
Total space required for pulling sampler out:

SD-701/450: ~ 995 (39”)
SD-701/650: ~ 1420 (56”)
SD-701/850: ~ 1620 (64”)
SD-701/1200: ~ 1950 (77”)
Total length:
SD-701/45: ~ 650 (26")
SD-701/65: ~ 850 (34")
+ extra space SD-701/85: ~ 1050 (41 1/2")
~ 250 (10") SD-701/1200: ~ 1400 (55”) ~ 320 (12 1/2")
Sufficient free space below sampler (no pipelines, racks, etc.)

to allow unhindered sample line installation
- minimum bend radius of sample line is 300mm (11 13/16")
Fig. 5.4. Installation space required for SD-701.

5.D. Installing SD-701 to a Tank
When installing the sampler to a tank, use the bevelled
mounting cone (code H4700328) which allows sampler
installation at a 45° angle. See Fig. 5.5.
Security chains or cables are not needed when
installing the mounting cone, as the cone is always
installed when the process is not pressurized (= not
operating).
NOTE: To ensure sufficient sample flow, the sample line
connector must not be more than 1 m (3.3 ft) higher than
H < 1 m (3.3 ft)
the sampler tip!
Choosing sampler length:

In order to obtain a sufficient sample flow, the sampler 45•
tip must not remain inside the tank wall. Choose the
sampler length so that when installed, its tip protrudes
into the interior of the tank.
Sampler SD-701 is available in four versions that differ
from each other as regards the length of the probe Fig. 5.5. Sampler SD-701, installation to tank.
tube:
• SD-701/450, probe length 450mm (~17 3/4")
- order code A4700325 V1.1
• SD-701/1200, probe length 1,200mm (~47 1/4")
The required sampler length is dependent on the
thickness of the tank wall: the thicker the wall, the 45• x x = 1.4 x d
longer section of the probe tube will remain inside the
wall structure. Fig. 5.6 illustrates how the length of this d
probe section is calculated. When this length has been
calculated, add to it the length of the probe section that
must be reserved to accommodate the installation parts
(Fig. 5.3). d
Example:Wall thickness d = 15cm (~6"). From Fig. = tank wall thickness
5.6 we get the length of the probe section that will
remain inside the wall when the sampler is installed at
a 45° angle: Fig. 5.6. Calculating the required sampler length: how
x = 1.4 x 15cm = 21cm (8 1/4") much of the probe tube will remain inside the tank wall
In addition, about 32 cm (12 5/8") of the probe will when installing at a 45° angle.
be inside the installatino parts. Thus, when the sampler
is installed to process, about 53 cm (~21") of the total
probe length will be hidden inside the installation parts
and the tank wall; therefore we need model SD-701/650
or longer.

5.E. Mounting & Removing SD-701 5.F. Adjusting the Piston Stroke
NOTE: When mounting or removing samplers, always

The stroke length of the sampler’s piston (SD-701) is
wear appropriate protective clothing and safety equip- adjusted by a nut located on the valve axis. The required
ment to prevent injuries caused by hot liquor! stroke length is dependent on the sampling point:
• Pressurized samples – the piston should open only
1–2 mm (up to 5/64").
Installing: • Gravity-feed samples (causticizing tank) – adjust
1. Make sure that the instrument air supply to the the stroke length to maximum.
sampler is closed (pneumatic valve control).
NOTE: Make sure to lock the adjustment nut in position
2. Connect the sample line to its connector on the
every time its setting is changed!
sampler.
3. Push the air tubes through the bushings, and connect
them to the sampler’s valve.
4. Make sure that the sampler’s piston is closed. Push Packing
the sampler through the tightening assembly until it Open Closed
touches the closed ball valve. Fasten the security
chain so that it is tight.
Adjustment of
piston stroke length
Sample line
5. Open the ball valve and push the sampler into the
process stream. Screw nut A to the tightening assem- Fig. 5.7. Actuator of sampler SD-701.
bly.
Removing:
1. Make sure that the instrument air supply to the
sampler is closed (pneumatic valve control).
2. Loosen nut A from the tightening assembly.
3. Pull the sampler out of the ball valve until the
security chain is fully stretched.
4. Close the ball valve properly.
5. Detach the security chain.
6. Pull the sampler completely out of the tightening
assembly.
7. Disconnect the air tubes from the sampler.
8. Disconnect the sample line from sampler.

5.G. Sampler SD-702
The SD-702 sampler is used for white liquor and green The analyzer controls the sampler’s actuator pneu-
liquor. matically.
It can also be used for causticized liquor in sampling Other specifications:
points with very high process pressure (> 6 bar, 87 psi) • material AISI 316 L
or strong abrasion (e.g. after a pump), or when installa- • ambient temperature +5–60°C (41–140°F)
tion space is so limited that the SD-701 sampler is • humidity 10–100%
impossible to install. • process temperature max. +110°C (230°F)
This sampler consists of a 1/2" ball valve and a • process pressure max. 10 bar (145 psi)
pneumatic actuator. It is installed to process using a 3/
4” ball valve and a mounting cone welded to the process
pipeline.
1. Mounting cone 3/4" H4700324 V1.0

2. Ball valve 3/4" 256768 Open
3. Adapter 1/2"–3/4" 70102189
4. Ball valve Fujikin 70100215
Closed
185 (7 1/4")
1
R1/2"
4
2 3
150 (~6")
Fig. 5.8. Sampler SD-702 (70103527).
At least ~ 130 (5") of free space

around sampler in all directions,
i.e. the sampler must have space
to rotate freely around its axis
- the sampler is installed by
screwing it to the mounting cone!
Sufficient free space

to allow unhindered
sample line installation
- minimum bend radius
of sample line is
300mm (11 13/16")
~ 230 (9")
Fig. 5.9. Installation space required for SD-702.

App. 1 - Technical Specifications
• kajaaniALKALi - for causticizing
• KAJAANI protective compartment
• Water purifier (option)
• Communicator-i
• kajaaniALKALi Tool Windows software
kajaaniALKALi – Installation - A1 - W4700162 V1.5 EN

06. Jul. 2009 Page 1 (2)
kajaaniALKALi – for Causticizing Technical Specifications

Measurement Unit
Titration module with 1 or 2 titration arms. Relative humidity .................... 10…90%, no condensation
Ambient temperature ..............+5…+50 C (+41…+122 F)
Measurement results: Power intake.................................................... max. 150 W
Measurement based on standard SCAN 30:85. Operating voltage ..................... 85…132 / 170…264 VAC,
Sodium hydroxide, NaOH 60/50 Hz
Sodium carbonate, Na2CO3
Sodium sulphide, Na2S Connections:
Effective Alkali (EA) = NaOH + 1/2 Na2S
Active Alkali (AA) = NaOH + Na2S Analog connections
Total Titratable Alkali (TTA) Analog board ................................ 8 outputs + 7 inputs
= NaOH + Na2S + Na2CO3 (calculated as g NaOH/l, g Max. 2 analog boards
Na2O/l, lb/ft3, lb/gal, or ml HCl) Signals ........................................ 0 - 20 mA, 4 - 20 mA
Causticizing Degree (CD%) or 0 - 5 VDC
= NaOH * 100 / (NaOH + Na2CO3) Analog outputs.................................. 0 / 8 / 16 outputs,
Sulphidity (S%) = Na2S * 100 / (NaOH + Na2S) max. 1 k (isolated)
Analog inputs ....................... 0 / 7 / 14 inputs (isolated)
Analysis time ..................... 8 - 10 min / sample
Binary connections
pH-measurement Binary outputs....................8 outputs, relay (3 alarms),
Measuring range ......... pH 0–14 changeover contact,
Sensor type ................. CPS11-1BA2GSA 24 VDC/1A, 48 VDC/0.5A
or 125 VAC/0.5A
Measurement repeatability: Binary inputs .............. 8 inputs (isolated), 24 - 48 VDC
Determined by analyzing the same white liquor sample
10 times (n) and calculating the standard error of Serial communication
estimate (s) as follows: DCS, Modbus ........................................ RS-485 4-wire
Communicator-i ................................................ RS-485
PC ..................................................................... RS-232
n Modem .............................................................. RS-232
( xi – x )2
s= –––––––––––
Analysis water ..................................................... deionized
n–1
i=1 Conductivity ........................................... max. 30µS/cm
pH ............................................................................. 6–8
where: Temperature ....................+10…+40 C (+50…+104 F)
x mean of measurements Pressure................................................ < 4 bar (58 psi)
xi measurement results x1...x10 Consumption ..................................... 2.5 l / h / titr. unit
(0.7 US gal / h / titr. unit)
Standard error (s) < 0.5 g/l (< 0.03 lb/ft3) for NaOH, Na2CO3 Connection.......................... ISO 7/1 - Rp ½" (NPT ½")
and Na2S Recommended inlet pipe .....................................DN10
Analysis chemical............................ Hydrochloric acid HCl

(1.0 0.05N,measurement accuracy 0.001N)
Consumption ............................8 l / week / titr. module
(2.1 US gal / week / titr. module)
Dimensions (h x w x d)........................... 1900 x 790 x 790

(74 13/16" x 31 1/8" x 31 1/8")
Weight ....................................................... 210 kg (463 lbs)
© Metso Manufacturer reserves the right to changes without prior notice. CAU_SPECIFICATION_EN.doc
Page 2 (2)
kajaaniALKALi – for Causticizing Technical Specifications

Sample Unit Samplers
1 or 2 sample processing units, SD-701
each with max. 4 sample lines. Available in three versions that differ from each other as
to the length of sampler probe; alternatives 450mm (17
Sample lines 3/4”), 650mm (25 5/8”), 850mm (33 1/2”) and 1200mm
Lines ..................... 1 - 4 lines / sample processing unit (47 1/4")
Material ........................................... Teflon FEP or PFA Sampling .....................................from green liquor and
Size .......................................................................... 3/4” causticizing vessels
Ext. diameter ......................................... 19.1 mm (3/4”) Type .................................... Flow-type, valve with seat
Wall thickness ................................... 1.575 mm (1/16”) Installation.................................. With a ball valve 3/4”,
Minimum bend radius ........................... 300 mm (~12") tightening assembly and a cone
NOTE: If process pressure at the sampling point is welded to process pipeline
> 4 bar (58 psi) and sample temperature is Compressed air ..................................... from analyzer
> 95 C (203 F), then sample line material must be AISI Material .........................................................AISI 316 L
316L, ext. diameter 16 mm (5/8”). Ambient temperature.........+5…+60 C (+41…+140 F)
Length: Relative humidity ..........................................10…100%
gravity feed samples ...................... max. 35 m (115 ft), Process temperature................max. +110 C (+230 F)
(causticizing vessels) fall 10% Process pressure ........................... max. 6 bar (87 psi)
pressurized samples ..................... max. 100 m (328 ft)
(green/white liquor) SD-702
Sampling ............................. primarily from white liquor
Outlet pipe for analyzed samples: Type ................................................ 1/2” ball valve with
Connection ........................... ISO 7/1 - Rp½" (NPT ½") pneumatic actuator
Recommended pipe size .................................... DN20 Installation................ With a ball valve 3/4” and a cone
Length............................................. max. 30 m (98.4 ft) welded to the process pipeline
Delivery height ............................... max. 10 m (32.8 ft) Compressed air ...................................... from analyzer
Material .........................................................AISI 316 L
Relative humidity ....................10…90%, no condensation Ambient temperature.........+5…+60 C (+41…+140 F)
Ambient temperature .............. +5…+50 C (+41…+122 F) Relative humidity ..........................................10…100%
Process temperature................max. +110 C (+230 F)
Flushing water Acceptable for return to process Process pressure ....................... max. 10 bar (145 psi)
Pressure ..................... 4 - 8 bar (58 - 116 psi), at least
2 bar (29 psi) higher than highest
process pressure at sampling point
Consumption .................... 150 - 300 l / h / sample unit
(40–79 US gal / h / sample unit)
Temperature...................... +5…+50 C (+41…+122 F)
NOTE: Hottest flushing water must be at least 20 C
(36 F) cooler than the coolest liquor sample!
Connection .......................... ISO 7/1 - Rp ½" (NPT ½")
Recommended inlet pipe..................................... DN20
Ext. diameter Int. diameter Wall thickn.
Compressed air: DN10 17.2mm 14.0mm 1.6mm
Pressure ......................................4 - 6 bar (58 - 87 psi) [11/16”] [35/64”] [1/16”]
Consumption ...................... min. 1000 l / min (35.5 ft3), DN15 21.3mm 18.1mm 1.6mm
intermittent
[27/32”] [23/32”] [1/16”]
Connection .......................... ISO 7/1 - Rp ½" (NPT ½")
Recommended inlet pipe..................................... DN15 DN20 26.9mm 23.7mm 1.6mm
[1 1/16”] [15/16”] [1/16”]
Enclosure class of cabinet ..................... IP 54 (NEMA 3S)
Dimensions (h x w x d) ........................... 1900 x 790 x 790

(74 13/16” x 31 1/8” x 31 1/8”)
Weight ....................................................... 200 kg (441 lbs)
© Metso Automation Manufacturer reserves the right to changes without prior notice. CAU_SPECIFICATION_EN.doc
20.Jan.2000 1 2
kajaaniALKALi for Causticizing Technical Specifications

Protective Compartment
Base structure Dividing wall
• KYV U-120 mm steel • Reinforced plastic coating, glass fiber mat
2
300 g/m
• Painted • Plywood board 12 mm
• With hoisting supports • Supporting ribs
• Plywood board 12 mm
Floor • Mounting points of equipment reinforced with plywood
• Reinforced plastic coating, glass fiber mat 300 g/m2 board
• Plywood board 9 mm • Reinforced plastic coating, glass fiber mat 300 g/m2
• Polyurethane insulation 70 mm
• Plywood board 12 mm Ventilation
• Reinforced plastic coating, glass fiber mat 450 g/m2 • Air inlet and outlet ducts (2 + 2)
• 2 floor drains, decline towards drains
Electricity
Ceiling • Branch distribution center, enclosure class IP55
• Reinforced plastic coating, glass fiber mat 450 g/m2 • 2 fluorescent tubes, splash-proof
• Molded fiber board • 2 power outlets, each with 2 sockets
• Molded fiber board 4 hoisting slings
• Reinforced plastic coating, glass fiber mat 300 g/m2
Color: Neste Polyester 2450 gray
Outer wall
• Reinforced plastic coating, glass fiber mat
2
450 g/m
(external surface)
• Molded fiber board
• Molded fiber board
• Reinforced plastic coating, glass fiber mat 300 g/m2
© Metso Automation Manufacturer reserves the right to changes without prior notice. Compartment_specs.doc
20.Jan.2000 Page 2 (2)
kajaaniALKALi for Causticizing Technical Specifications

Protective Compartment
2430 (96")
NOTE: Shown here
with ceiling removed!
2440 (96")
400 (16")
Titration
module
2800 (110")
Electronics
unit
10
00
(39
”)
© Metso Automation Manufacturer reserves the right to changes without prior notice. Compartment_specs.doc
18.Jan.2000 Page 1 (1)
Communicator-i Technical Specifications

Voltage .... 18…72 VDC/5W, power supplied from analyzer
Serial Communication .........................RS-485 (fullduplex)
Ambient Temperature............... 0…+50°C (+32°…+131°F)
Enclosure Class .......................................................IP 64
Display Operating..................1/4 VGA, LCD with backlight
Keypad ................................................Membrane keypad
Dimensions (h x w x d) .....................180 x 198 x 40 mm

(6 5/16” x 7 51/64” x 1 37/64”)
Weigth ...................................................... 1.4 kg (3.1 lbs)
© Metso Automation Manufacturer reserves the right to changes without prior notice. Communicator _specs
18.Jan.2000 Page 1 (1)
kajaaniALKALi Tool Technical Specifications

KajaaniALKALi Tool is a Windows software for Minimum system requirements:
kajaaniALKALi analyzers. With the kajaaniALKALi Tool • Personal computer with Pentium processor
software you can perform the same functions as with the • Processor speed:133 MHz
analyzer’s operating terminal, Communicator. • Memory: 32MB RAM; 64MB recommended
• Serial port: RS-232
You can • (Color) monitor: resolution 800 x 600
• monitor the analyzer, • Microsoft Windows 95/98/NT
• control the analyzer’s operations, • Free hard disk space:
• configure the analyzer’s parameters. - software 25MB
- database 75 MB
With the Windows software you can also
• collect result data (trends) on a PC,
• save analyzer/mill results in a separate database,
• keep backups of configuration parameters,
• get reports of all data on paper and in Excel or HTML
format (for Internet use),
• print the reports automatically on paper,
• convert analyzer data into Excel format for further
analysis,
• use a modem connection to transfer data between the
analyzer and a PC.
© Metso Automation Manufacturer reserves the right to changes without prior notice. AlkaliTool_e
App. 2 - Contents of Delivery
• kajaaniALKALi, cabinet model
• kajaaniALKALi, compartment model
• SD-701 sampler
• SD-701 mounting cone for tank installation (option)
• SD-702 sampler

07.Jun.2001 Page 1 (2)
kajaaniALKALi – for CausticizingDelivery – Cabinet Model
C
F A
G E
H 1
2
3
I 5
4
O B 6
J 7
8
O
K R
O P
L
M Q
N
'
The following connection tubes between the units are included in delivery:
• Sediment tank to Sample cup; PTFE 8/6, length 1.2 m (3.9 ft)
• Flushing water to Measurement unit; PA 8/6, length 0.6 m (2 ft)
• Sample cup to Waste tank; rubber hose, diam. 13mm, 1/2" length 0.6 m (2 ft)
• Suction tube, Analysis cup -> Ejector; PTFE 6/4, length 1.4 m (4.6 ft)
• Air to Measurement unit; PA 8/6, length 0.9 m (3 ft)
• Analysis water to Measurement unit; rubber hose, diam. 13mm, 1/2" length 0.8 m (2.6 ft)
• Titration module owerflow;Tricoclair, diam. 13mm, 1/2" length 1.4 m (4.6 ft), lead to drain
• Analysis water overflow; Tricoclair, diam. 19mm, 3/4"length 1.4 m (4.6 ft), lead to drain
© Metso Automation Manufacturer reserves the right to changes without prior notice. 070_DELCABIN_070601_EN
07.Jun.2001 Page 2 (2)
kajaaniALKALi – for Causticizing Delivery – Cabinet Model
Code Item Qty Symbol Metso Customer Select
A4700108 V2.0 Alkali Measuring Unit 1 (1 titration arm) OR 1 A x

A4700109 V2.0 Alkali Measuring Unit 2 (2 titration arms) 1 A x
A4700110 V1.1 Sample Unit 4 Cabinet Model ( 4 sample lines) OR 1 B x
A4700111 V1.1 Sample Unit 8 Cabinet Model ( 8 sample lines) 1 B x
A4310082 V1.2 Communicator-i 1 C x
A4310014 V1.6 Server-i Analog Board 0/1/2 E option
Sample overflow outlet 1 F x
Deionized water overflow outlet 1 G x
Washing water discharge 1 H x
Vapor outlet 1 I x
Deionized water inlet 1 J x
Cold water inlet 1/2 K x
Instrument air inlet 1/2 L x
Sample discharge tube 1 M x
Sample line from Sampler *) 4/8 N x
Shut-off valves for inlets 3 O x
P4700652 V1.0 kajaaniALKALi Tool Windows-program 1 x
A4500382 V1.0 RS-232 cable (PC) 1 P x
Remote PC connection 1 option
251801 - cable 1
251723 - RS485/232 converter 1
P4700414 V1.3 Alkali Document CD 1 Q x
Manuals 1 Q x
Filter to cold water inlet line 1 R x
Mains power cabling 1 1 x
Analog input cabling 0/7/14 2 x
Binary input cabling 8 3 x
Analog output cabling 0/8/16 4 x
Binary output cabling 8 5 x
Serial interface cabling; Modbus 1 6 x
Phone cabling; Modem 1 7 x
Serial interface cabling; PC 1 8 x
256040 4” flexible hose (for disharge) 1m x
168575 Hose clamp for disharge hose 2 x
256354 Extra tank for HCl 1 x
H4700692 V1.0 Sample tube installation tool 1 x
70103857 Triton X-100 100ml x
216032 Water purifier Millipore Rios16/230 VAC/50 Hz option
A4700646 V1.0 Millipore cable option
A4700503 V1.0 Communicator remote connection 1 option
*) Sample line tubes are also available from Metso as option. Order codes: FEP-tube 3/4” (252593) OR PFA-tube 3/4” (70101355).
Connectors are included in the delivery.
© Metso Automation Manufacturer reserves the right to changes without prior notice. 070_DELCABIN_070601_EN
07.Jun.2001 Page 1 (2)
kajaaniALKALi – for Causticizing Delivery-Compartment Model
The following connection tubes between

the units are included in delivery:
• Sediment tank to Sample cup; PTFE
8/6, length 1.2 m (3.9 ft)
• Flushing water to Measurement unit;
PA 8/6, length 0.6 m (2 ft)
• Sample cup to Waste tank; rubber
hose, diam. 13mm, 1/2" length 0.6 m (2
ft)
• Suction tube, Analysis cup ->
Ejector; PTFE 6/4, length 1.4 m (4.6 ft)
• Air to Measurement unit; PA 8/6,
length 0.9 m (3 ft)
• Analysis water to Measurement unit;
rubber hose, diam. 13mm, 1/2" length
0.8 m (2.6 ft)
P • Titration module owerflow;Tricoclair,
diam. 13mm, 1/2" length 1.4 m (4.6 ft),
lead to drain
Q • Analysis water overflow; Tricoclair,
diam. 19mm, 3/4"length 1.4 m (4.6 ft),
lead to drain
D F
C G
H
1
2 I
3 O J
4
5 A
6
7
E R O K
8
O
L
Measuring Unit 2 B
Sample Unit 8
M
N
070_DELCOMPARTMENT_070601
© Metso Automation Manufacturer reserves the right to changes without prior notice.
_EN
07.Jun.2001 Page 2 (2)
kajaaniALKALi – for Causticizing Delivery-Compartment Model

Item Select Qty Symbol Metso Customer
Code
A4700108 V2.0 Alkali Measuring Unit 1 (1 titration arm) OR 1 A x
A4700109 V2.0 Alkali Measuring Unit 2 (2 titration arms) 1 A x
A4700112 V1.1 Sample Unit 4 comp. model (4 sample lines) OR 1 B x
A4700113 V1.1 Sample Unit 8 comp. model (8 sample lines) 1 B x
A4310082 V1.2 Communicator-i 1 C x
H3700018 V1.0 Protective Compartment 1 D option
A4310014 V1.6 Server-i Analog Board 0/1/2 E option
Sample overflow outlet 1 F x
Deionized water overflow outlet 1 G x
Washing water discharge 1 H x
Vapor outlet 1 I x
Deionized water inlet 1 J x
Cold water inlet 1/2 K x
Instrument air inlet 1/2 L x
Sample discharge 1 M x
Sample line from sampler *) 4/8 N x
Shut-off valves for inlets 3 O x
P4700652 V1.0 kajaaniALKALi Tool Windows-program 1 x
A4500382 V1.0 RS-232 cable (PC) 1 P x
Remote PC connection 1 option
251801 - cable 1
251723 - RS485/232 converter 1
P4700414 V1.3 Alkali Document CD 1 Q x
Manuals 1 Q x
Filter for cold water inlet line 1 R x
Mains power cabling 1 1 x
Analog input cabling 0/7/14 2 x
Binary input cabling 8 3 x
Analog output cabling 0/8/16 4 x
Binary output cabling 8 5 x
Serial interface cabling; Modbus 1 6 x
Serial interface cabling; Modem 1 7 x
Serial interface cabling; PC 1 8 x
256040 4” flexible hose (for disharge) 1m x
168575 Hose clamp (for disharge hose) 2 x
256354 Extra tank for HCl 1 1
H4700692 V1.0 Sample tube installation tool 1 1
70103857 Triton X-100 100ml x
A4700680 V1.0 Communicator-i extra cable option
A4700646 V1.0 Millipore cable option
*) Sample line tubes are also available from Metso as option: FEP-tube 3/4” (252593) OR PFA-tube 3/4” (70101355).
Connectors are included in the delivery.
070_DELCOMPARTMENT_070601
© Metso Automation Manufacturer reserves the right to changes without prior notice.
_EN
3.Feb.2000 Page 1 (1)
kajaaniALKALi – for Causticizing Delivery – SD-701

d
F
A B C D
E
G
Sampler for sampling from causticizing vessels.
Code Item Qty Symbol Kajaani Customer

A4700325 V1.1 Sampler SD-701/450 (d = 450 mm, 17 3/4")
Sampler SD-701/450 1 A x
OR
A4700300 V1.1 Sampler SD-701/650 (d = 650 mm, 25 5/8")
OR
A4700326 V1.1 Sampler SD-701/850 (d = 850 mm, 33 1/2")
OR
A4700327 V1.1 Sampler SD-701/1200 (d = 1200 mm, 47 1/4")
Common parts for all SD-701 models:

A4700525 V1.0 Packing assembly 1 B x
256768 Ball valve 1 C x
H4700324 V1.0 Mounting cone 1 D x
255448 Sample line coupling FEP 1/2" / 3/4" 2 E x
Instr. air inlet from analyzer 2 F x
Sample line (see kajaaniALKALi delivery) 1 G x
© Metso Automation Manufacturer reserves the right to changes without prior notice. Delivery_sd701.doc
3.Feb.2000 Page 1 (1)
kajaaniALKALi for Causticizing Mounting Cone for Tank

SD-701 Sampler Installation (option)
Order code: H4700328 V1.0
45°
© Metso Automation Manufacturer reserves the right to changes without prior notice. Mounting_cone.doc
3.Feb.2000 Page 1 (1)
kajaaniALKALi – for Causticizing Delivery – SD-702
H E
H E
A F
D C B G
Sampler for sampling from pressurized process (white liquor and green liquor).

A4700334 V1.0 Sampler SD-702
70100215 Ball valve Fujikin 1 A x
70102189 Adapter 1 B x
256768 Ball valve 3/4“ 1 C x
H4700324 V 1.0 Mounting cone 1 D x
239418 Angle coupling 1541-6/4-1/8 AVS 2 E x
255448 Sample line coupling FEP 1/2" / 3/4" 2 F x
Sample line (see Alkali Analyzer delivery) 1 G x
Instrument air inlet from analyzer 2 H x
© Metso Automation Manufacturer reserves the right to changes without prior notice. Delivery_sd702.doc
App. 3 - Chemical Safety Information

kajaaniALKALi – Chemical Safety Information
The following chemicals are used in connection with the kajaaniALKALi analyzer:
Analysis chemical: hydrochloric acid (HCl) The local chemicals supplier

Cleaning chemical: sulphamic acid (NH2SO3H) (manufacturer / importer)
Triton X-100
is required to provide complete
Hydrochloric acid:
• Corrosive, sensitizer.
• Causes eye and skin burns.
• May cause severe respiratory and digestive tract
irritation with possible burns.
• May be FATAL if inhaled or swallowed. SAFETY INFORMATION
• Vapor extremely irritating. for all chemicals they supply,
stating the safety precautions
Sulphamic acid:
required when handling or storing
• Causes eye burns and skin irritation. the chemical, and also any
• Prolonged contact may cause skin burns.
protective equipment needed!
Triton X-100
• Harmful if swallowed.
• Causes eye irritation.
kajaaniALKALi CHEMICAL SAFETY INFORMATION

App. 4 - ModBus Specifications
S4700531 - Floating point
S4700532 - Integer

S4700531 V1.4
28.12.1999
Modbus specification for the Alkali Analyzer
(Floating point number version, protocol = 3)
Created : Ilkka Pyykkönen / 28.10.1997
Checked : Lauri Keränen / 28.10.1997
Approved : Lauri Keränen / 28.10.1997

S4700531
28.12.1999
CONTENTS
1. INTRODUCTION ..................................................................................................................................3
2. MODBUS FUNCTIONS ........................................................................................................................4

2.1. READ HOLDING REGISTERS ..................................................................................................................4
2.2. PRESET MULTIPLE REGISTERS ..............................................................................................................5
3. THE DATA TO BE TRANSFERRED .................................................................................................7
3.1. DATE, TIME AND SOFTWARE VERSION...................................................................................................8
3.2. MEASURING PERMISSION AND SAMPLER TIMING ...................................................................................9
3.3. SAMPLER STARTUP MODES .................................................................................................................10
3.4. ANALYSIS DATA .................................................................................................................................11
3.5. ANALYSIS RESULTS ............................................................................................................................15
3.6. ANALYSIS PARAMETERS .....................................................................................................................18
3.7. ANALOG OUTPUTS ..............................................................................................................................20
3.8. STATUS INFO .......................................................................................................................................21
3.9. TEMPERATURE SENSORS .....................................................................................................................26
3.10. MODBUS REMAPPING TABLE ..........................................................................................................27
3.11. SAMPLE LINES ................................................................................................................................28
3.12. SAMPLE ORDER ..............................................................................................................................32
3.13. ERROR LOG ....................................................................................................................................33
3.13.1. Error and service codes ...........................................................................................................38
3.14. SERVICE COUNTERS .......................................................................................................................39
3.15. ANALYZER CONTROL .....................................................................................................................40
3.16. SERVICE PARAMETERS ...................................................................................................................41
3.17. ERROR PARAMETERS ......................................................................................................................42
3.18. ANALYZER VARIABLE PARAMETERS ..............................................................................................43
3.19. BINARY-I/O DESCRIPTIONS ............................................................................................................44
3.20. BINARY-I/O STATES.......................................................................................................................45
3.21. RESULT ADJUSTMENT ....................................................................................................................46
3.22. TITRATOR CONTROL REGISTERS .....................................................................................................47
3.23. SAMPLER CONTROL REGISTERS ......................................................................................................48
3.24. CONTROLLED SHUTDOWN ..............................................................................................................49
4. REGISTER REMAPPING TABLE ...................................................................................................50
5. MODIFICATION HISTORY .............................................................................................................51
2
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28.12.1999
1. INTRODUCTION
The document specifies the operation of the MODBUS interface in the Alkali Analyzer.
3
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28.12.1999
2. MODBUS FUNCTIONS
The Modbus operates only in the RTU-mode. The ASCII-mode is not available.
The default serial communication parameters are: 9600 baud, 1 start bit, 8 data bits, no
parity, 2 stop bits.
The following functions are supported: Read Holding Registers (03), Preset Single Holding
Register (06) and Preset Multiple Registers (16).
The register range in the Modbus-messages is 0-65535. I.e. in the messages the 1st register
is accessed as 0, the 2nd register as 1 etc.
2.1. Read Holding Registers
The form of the message is:
Field Meaning
ADDRESS (0-255) The address of the slave
FUNCTION (3) The function code
Starting Address Hi 8 MSB (most significant bits) of the 1st register to read
Starting Address Lo 8 LSB (least significant bits) of the 1st register to read
No. of registers Hi 8 MSB of the number of the registers to read
No. of registers Lo 8 LSB of the number of the registers to read
CRC Hi 8 MSB of the CRC
CRC Lo 8 LSB of the CRC
The return message is:
Field Meaning
ADDRESS (0-255) Address of the slave
FUNCTION (3) Function code
Byte Count Number of data bytes is the message
Data Hi 8 MSB of the 1st register read
Data Lo 8 LSB of the 1st register read
...
Data Hi 8 MSB of the last register read
Data Lo 8 LSB of the last register read
If the read command addresses a reserved register within the defined register range the
returned register value is 0 and no error is reported.
If only one register of the two registers holding a float value is accessed the data is not read
and an error message is returned.
4
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2.2. Preset Multiple Registers
Field Meaning
Starting Address Hi 8 MSB of the address of the first register to write
Starting Address Lo 8 LSB of the address of the first register to write
No. of registers Hi 8 MSB of the number of the registers to write
No. of registers Lo 8 LSB of the number of the registers to write
Byte Count The number of data bytes in the message
Data Hi 8 MSB of the 1st register to write
Data Lo 8 LSB of the 1st register to write
...
Data Hi 8 MSB of the last register to write
Data Lo 8 LSB of the last register to write
Field Meaning
Starting Address Hi 8 MSB (most significant bits) of the 1st register written
Starting Address Lo 8 LSB (least significant bits) of the 1st register written
No. of registers Hi 8 MSB of the number of the registers written
No. of registers Lo 8 LSB of the number of the registers written
If the read command addresses a reserved or read only register within the defined register
range the data is not stored and no error is reported.
If only one register of the two registers holding a float value is accessed the data is not
written and an error message is returned. However, the registers prior to the erroneous
register are written correctly.
5
S4700531
28.12.1999
Exception messages
The exception message is of form:

Field Meaning
FUNCTION The function code ored with 80H
Exception code Information of the error
An exception message is returned under some of the following conditions.
Illegal function
The function code received is not supported. The exception code is 1.
Illegal data address
The register address received is out of the defined register range. The exception code is 2.
Illegal data value
Only one of the two registers holding a float value is accessed. The exception code is 3.
6
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28.12.1999
3. THE DATA TO BE TRANSFERRED
The indexes of the data are in the following tables. The type field is either RW (i.e. the
register can be read and written) or R (i.e. the register can only be read).
The data to be transferred can have one some of the following forms:
ASCII-character:
(8-bit) ASCII character, 2 characters/one register
Unsigned integer:
16-bits: 0-65535
Unsigned long integer:

32-bits: 0-4294967295, uses two successive registers
Signed long integer:

32-bits: uses two successive registers
Floating point number:

32-bits: single precision floating point number (32 bit IEEE-format), uses two
successive registers for each value.
16 1
Register address : SEEEEEEEEFFFFFFF
Register address + 1: FFFFFFFFFFFFFFFFF
32-bit float:
32 1
S EEEEEEEE FFFFFFFFFFFFFFFFFFFFFFF
S = sign field (+/-)
E = exponent field (including bias 127)
F = fraction field (negative powers of 2)
Float value = <Sign> 1.<Fraction> * 2(<Exponent> -127)
Example:
Reg. addr : 1011111110110000
Reg addr. + 1: 0000000000000000
S Exp. Fraction
= 1 01111111 01100000000000000000000
= -(1.0 + 2-2 + 2-3) * 2(127-127) = - (1.0 + 0.25 + 0.125) = -1.375
A register holds an unsigned integer value if not otherwise defined. The allowed value
range may be presented in parenthesis on the usage-field. The floating point values are
presented with the MSB-register.
7
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28.12.1999
3.1. Date, time and software version
Register Usage Type

1 Year RW
2 Month RW
3 Day of the month RW
4 Hour RW
5 Minute RW
6 Seconds R
7 Software version, MSB of the float R
8 Software version, LSB of the float R
9 Date mode * RW
* This determines how the date is shown in the display of the communicator.
0 = day-month-year, 1 = month-day-year.
8
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28.12.1999
3.2. Measuring permission and sampler timing
- by the measuring permissions the user is able to disable measurements from certain sample lines
- in the timed sampling mode the sampler will start the sampling at the certain time. In the
continous mode the sampling is done as soon as the titrator is ready .
Register Usage Type

10 Get permission from modbus * RW
11 Sample line 1 measuring permission ** RW
12 Sample line 2 measuring permission RW
19
20 Sampler 1 timing mode *** RW
21 Sampler 2 timing mode RW
* The measuring permissions can be set either via the binary inputs or modbus. In order to set the
permissions from modbus, you need to set the value of this register to ”1” first.
- 0 = measuring permissions are read from the binary inputs
- 1 = measuring permissions are read from modbus
** If the value in the register nr. 10 Get permission from modbus is”0”, reading these registers will
give the states of the binary inputs. Writing operation to these registers will have an effect to the
analyzer’s operation only if the value in the register nr. 10 is ”1”.
- 0 = line enabled
- 1 = line disabled
*** - 0 = continuous sampling mode

- 1 = timed sampling mode
9
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28.12.1999
3.3. Sampler startup modes
- if the sample from the sample line is cold, the analyzer will give an error message No warm
sample. Startup mode enables the sampler to collect also cold samples.
Note: this mode will go automatically off, when the sampler has observed three times warm sample
from the line.
Register Usage Type

30 Line 1 startup mode off/on ( 0 / 1 ) RW
10
S4700531
28.12.1999
3.4. Analysis data
- the current analysis data shows the values of the current analysis:
- analysis loop index starts from 0 and increases by 1 after each HCl adding,
in other words it tells how many addings are done in the analysis. Maximum value is
56.
- pH shows the pH value at loop index, values vary from 0 – 14.
- derivate 1 shows how fast the pH curve is changing at loop index. Typical value
is between 0 – 10 000, in some error situations it can also have a negative value.
- derivate 2 shows how fast the derivate 1 is changing at loop index. Derivate 2
is used to notify the equivalence point. Typical value is –50 000- + 50 000.
- HCl volume is the total amount of acid which has been used in analysis at loop
index. Volume is represented in microlitres, typical value is 0 – 15 000.
- next adding is the amount of acid which will be added, typical value is 30 – 2000.
- analysis duration shows how long the analyzer has analyzed the sample, typical
value is 0 – 1200.
- analysis start time: hh:mm:ss
- HCl volume 1,2 and 3 are the volumes in each equivalence point, typical value is
500 – 15 000.
- pH 1, 2 and 3 are the pH values of each equivalence point, typically values are
between 2 and 12.
- sample line shows the line where the sample is from (1 – 8 in automatic mode, 9 –
16 in analyzer 1 manual samples, 17 – 24 in analyzer 2 manual samples )
- this data can be used to create graphical presentation of the analysis as is done in the analysis
trend page in the communicator. The curve can be drawn using the pH values and HCl volumes at
each loop index, and the equivalence points can be drawn using the HCl volume 1,2 and 3 values
and pH 1, 2 and 3 values.
- for more exact monitoring of the analysis it is useful create numerical presentation as is done in
the analysis trend page in communicator. In this presentation should also derivate values be
included.
- with the analysis data by loop index registers it is possible to read the data from the previous
loops
- in the analysis data history there are max 5 analyses saved per sample line, so it is possible to
inspect the previous analyses. This can be used for troubleshooting purposes, because even the
failed analyses are also saved.
11
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28.12.1999
The current analysis data from titrator 1:
Register Usage Type

50 Analysis loop index R
51 pH, MSB of the float R
52 pH, LSB of the float R
53 Derivate 1, MSB of the float R
54 Derivate 1, LSB of the float R
57 HCl volume R
58 Next adding R
59 Analysis duration R
60 Analysis start time (1st and 2nd character) R
61 Analysis start time (3rd and 4th character) R
62 Analysis start time (5th and 6th character) R
66 HCl volume 1 R
67 HCl volume 2 R
68 HCl volume 3 R
69 pH 1, MSB of the float R
70 pH 1, LSB of the float R
75 Sample line R
Analysis data from titrator 1 by analysis loop index:
Register Usage Type

90 Analysis loop index (Note) RW
97 HCl volume R
98 Next adding R
Note: Set the Analysis loop index (register 90) before read analysis data.
12
S4700531
28.12.1999
The current analysis data from titrator 2:
Register Usage Type

110 Analysis loop index R
117 HCl volume R
118 Next adding R
126 HCl volume 1 R
127 HCl volume 2 R
128 HCl volume 3 R
135 Sample line R
Analysis data from titrator 2 by analysis loop index:

155 HCl volume R
156 Next adding R
Note: Set the Analysis loop index (register 150) before read analysis data.
13
S4700531
28.12.1999
The analysis data history:
Register Usage Type

160 Sample line number ( 0 - 9 * ) (Note) RW
161 Block number ( 0 - 4 ) (Note) RW
162 Analysis loop index (Note) RW
163 Current block index ** R
170 HCl volume R
171 Next adding R
172 Analysis number, MSB of the long integer *** R
173 Analysis number, LSB of the long integer R
174 HCl volume 1 R
175 HCl volume 2 R
176 HCl volume 3 R
189 Analysis start date (1st and 2nd character) R
190 Analysis start date (3rd and 4th character) R
191 Analysis start date (5th and 6th character) R
193 Analysis duration *** R
194 Start pH, MSB of the float R
195 Start pH, LSB of the float R
* sample line number 8 is titrator 1 manual sample
sample line number 9 is titrator 2 manual sample
** Current block index indicates the index (0 – 4) that is in use with the selected sample line
*** Analysis number and analysis duration can be 0 in following three cases:
- block contains no data
- current analysis data is written to this block
- analysis has not been successful, e.g. third inflection has not been found
Note: Set the sample line number, block number and analysis loop index before reading
14
S4700531
28.12.1999
3.5. Analysis results
- block number increases from 0 to 1999 and after that it starts over from 0
- the analysis type informs which analysis parameter table is used for this analysis (0 – 7)
- sample line shows the line where the sample is from (1 – 8 in automatic mode, 9 – 16 in analyzer
1 manual samples, 17 – 24 in analyzer 2 manual samples )
- HCl volume 1,2 and 3 are the volumes in each equivalence point, typical value is 500 – 15 000.
- pH 1, 2 and 3 are the pH values of each equivalence point, typically values are between 2 and 12.
- analysis start date: dd-mm-yy
- result type show the units of the result and if the results are calculated in Na2O or NaOH
- result type is displayed in 8 lowest bits:
- MSB: 0 = Na20, 1 = NaOH
- next 3 bits, alkaline units: 0 = g/l, 1 = lb in cubical feet, 2 = lb in
gallon, 3 = ml HCl
- 4 LSBs, carbonate units: 0 = g/l, 1 = lb in cubical feet, 2 = lb in
gallon, 3 = ml HCl
- start pH shows the pH in the beginning of the analysis, i.e. sample pH
- in the analysis results by block number it is possible to read previous results
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S4700531
28.12.1999
The last results from analyzer:
Register Usage Type

200 Block number R
201 Analysis number, MSB of the long integer R
203 Analysis type R
204 Sample line R
205 HCl volume 1 R
206 HCl volume 2 R
207 HCl volume 3 R
214 EA, MSB of the float R
215 EA, LSB of the float R
216 AA, MSB of the float R
217 AA, LSB of the float R
218 TTA, MSB of the float R
219 TTA, LSB of the float R
220 CE%, MSB of the float R
221 CE%, LSB of the float R
222 S%, MSB of the float R
223 S%, LSB of the float R
224 Na2CO3, MSB of the float R
225 Na2CO3, LSB of the float R
226 NaOH, MSB of the float R
227 NaOH, LSB of the float R
228 Na2S, MSB of the float R
229 Na2S, LSB of the float R
241 Result type info * R
* Result type is displayed in 8 lowest bits:
- MSB: 0 = Na20, 1 = NaOH
- next 3 bits, alkaline units: 0 = g/l, 1 = lb in cubical feet, 2 = lb in gallon, 3 = ml HCl
- 4 LSBs, carbonate units: 0 = g/l, 1 = lb in cubical feet, 2 = lb in gallon, 3 = ml HCl
16
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The results from analyzer by block number:
Register Usage Type

250 Block number (Note) RW
253 Analysis type R
254 Sample line R
255 HCl volume 1 R
256 HCl volume 2 R
257 HCl volume 3 R
264 EA, MSB of the float R
265 EA, LSB of the float R
266 AA, MSB of the float R
267 AA, LSB of the float R
268 TTA, MSB of the float R
269 TTA, LSB of the float R
270 CE%, MSB of the float R
271 CE%, LSB of the float R
272 S%, MSB of the float R
273 S%, LSB of the float R
274 Na2CO3, MSB of the float R
275 Na2CO3, LSB of the float R
276 NaOH, MSB of the float R
277 NaOH, LSB of the float R
278 Na2S, MSB of the float R
279 Na2S, LSB of the float R
- MSB: 0 = Na20, 1 = NaOH
Note: Set the block number (register 250) before read the history results.
17
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3.6. Analysis parameters
- index for analysis type is the number of the analysis parameter table ( 0 – 7)
- sample volume typical values 2.0 – 2.5 ml
- T1 is the first acid additions (for each equivalence point)
- T2 is the second acid additions (for each equivalence point)
- Dmin is the limit value for derivate 1. Derivate 1 must be over this value in equivalence point,
otherwise the point is not accepted.
- FA, FB and FC form the formula how the additions are calculated, i.e. how the additions will follow
the changes in pH curve
- minimum adding is the limit for HCl addings
Analysis parameters by index:
18
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Register Usage Type

300 Index for analysis type ( 0 - 7 ) RW
301 Description (1st and 2nd character) RW
302 Description (3rd and 4th character) RW
303 Description (5th and 6th character) RW
317 Sample volume, MSB of the float RW
318 Sample volume, LSB of the float RW
319 Reserved
320 T1 point 1 RW
321 T2 point 1 RW
322 Dmin point 1 RW
323 FA point 1 RW
324 FB point 1 RW
325 Minimum adding 1 RW
326 FC point 1, MSB of the float RW
327 FC point 1, LSB of the float RW
328 T1 point 2 RW
329 T2 point 2 RW
330 Dmin point 2 RW
331 FA point 2 RW
332 FB point 2 RW
336 T1 point 3 RW
337 T2 point 3 RW
338 Dmin point 3 RW
339 FA point 3 RW
340 FB point 3 RW
Note: Set index (register 300) before reading parameters (range 0..7)
19
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3.7. Analog outputs
- output index tells the output line, 0 –15

- channel informs the result which is sent from this output:
- 0 = output is not used
- 1 = EA
- 2 = AA
- 3 = TTA
- 4 = CE%
- 5 = S%
- 6 = Na2CO3
- 7 = NaOH
- 8 = Na2S
- 9 = V1 (HCl volume in 1st equivalence point)
- 10 = V2 (HCl volume in 2nd equivalence point)
- 11 = V3 (HCl volume in 3rd equivalence point)
- 12 = pH 1 (pH value in 1st equivalence point)
- 13 = pH 2 (pH value in 2nd equivalence point)
- 14 = pH 3 (pH value in 3rd equivalence point)
- minimum and maximum values and currents will set the scaling for the results
- sample line sets the line where result is taken from. If sample line is set to 0, the output is
multiplexed, so the result is taken from all the sample lines, and the binary outputs will tell the line
where the result is from.
- current value is the result which is currently set to the output
- current current tells the current which is currently at the output
- with the test mode it is possible to set certain current to the output. The other outputs will be 0 mA
and the results will not be updated into the outputs.
- test current is the desired current in the test mode
Register Usage Type

400 Output index RW
401 Channel RW
402 Minimum value, MSB of the float RW
403 Minimum value, LSB of the float RW
404 Maximum value, MSB of the float RW
405 Maximum value, LSB of the float RW
406 Minimum current, MSB of the float RW
407 Minimum current, LSB of the float RW
408 Maximum current, MSB of the float RW
409 Maximum current, LSB of the float RW
410 Sample line RW
411 Current value, MSB of the float R
412 Current value, LSB of the float R
413 Current current, MSB of the value R
414 Current current, LSB of the value R
415 Test mode on/off RW
416 Test current, MSB of the float * W
417 Test current, LSB of the float * W
* set test mode on before setting test current. Current must be between 4 – 20 mA (4080 0000 –
41A0 0000). Write operation to register 417 will activate the analog outputs.
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3.8. Status info
- status info includes the text which can be read from the main page of the communicator. It
informs what the device is doing.
- sample line tells the name of the sample line where the current sample is coming from
- queue number, queue index and macro line number tells the location where the sequence is
currently running in the macro structure
- sample line number is the same information as sample line, but in numerical form
- number of manual analyses tells which manual sample is currently analyzed and the amount of
ordered manual analyses tell how many analyses the user has set.
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Titrator 1:
Register Usage Type

600 Status info (1st and 2nd character) R
601 Status info (3rd and 4th character) R
602 Status info (5th and 6th character) R
620 Sample line (1st and 2nd character) R
621 Sample line (3rd and 4th character) R
622 Sample line (5th and 6th character) R
640 Queue number R
641 Queue index R
642 Macro line number R
643 Sample line number R
644 Number of manual analysis R
645 Amount of ordered manual analysis R
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Sampler 1:
Register Usage Type

640 Queue number R
641 Queue index R
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Titrator 2:
Register Usage Type

740 Queue number R
741 Queue index R
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Sampler 2:
Register Usage Type

790 Queue number R
791 Queue index R
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3.9. Temperature sensors
- temperature sensor 1 measures the temperature in sampler 1

- electronics temperature sensor is located in the amplifier board
Register Usage Type

794 Temperature sensor 1, MSB of the float R
795 Temperature sensor 1, LSB of the float R
796 Temperature sensor 2, MSB of the float R
797 Temperature sensor 2, LSB of the float R
798 Electronics temperature, MSB of the float R
799 Electronics temperature, LSB of the float R
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3.10. Modbus remapping table
- the user can set separate registers into consecutive registers in the remapping table, so there is
no need to do several read/write operations for the required registers. See section 4. Register
remapping table for further information.
Register Usage Type

1500 Register index (1 - 1000)* RW
1501 Remapped register RW
1502 Modem port remapping ON/OFF RW
1503 DCS port remapping ON/OFF RW
1504 PC port remapping ON/OFF RW
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3.11. Sample lines
- in this section the user is able to set descriptions for sample lines and set the formula for
calculating the sulfidity
Sample line 1:
Register Usage Type

2017 Sample type RW
2018 Sulfidity formula (0=Na2s/AA, 1=Na2S/TTA) RW
Sample line 2:
Register Usage Type

2117 Sample type RW
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Sample line 3:
Register Usage Type

2217 Sample type RW
Sample line 4:
Register Usage Type

2317 Sample type RW
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Sample line 5:
Register Usage Type

2417 Sample type RW
Sample line 6:
Register Usage Type

2517 Sample type RW
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Sample line 7:
Register Usage Type

2617 Sample type RW
Sample line 8:
Register Usage Type

2717 Sample type RW
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3.12. Sample order
- sample order tells the sampler in which order the samples should be taken. Use only characters
(not numbers) from ’1’ to ’8’, the last mark must be NULL mark to tell the analyzer that the order
string has ended. The analyzer will not read any characters after the NULL mark.
Note: One register has two ASCII-characters from the sample order table. Add NULL
mark (hex 0) to the end of the character string !
Titrator 1:
Register Usage Type
3500 Sample order index RW
3501 Sample line order (1st and 2nd character) RW
3502 Sample line order (3rd and 4th character) RW
...3550 Sample line order (99th and 100th character) RW
Titrator 2:
Register Usage Type
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3.13. Error log
- when the analyzer detects an error, it sets a certain error flag on (depending on the severity of the
error), and writes the error code into the error log
- in the error log the sample line is also shown if the error is related to sample line
- the error log index is from 0 to 99 and is increased when new error. The index starts over from 0
after each 100 errors.
- the error codes are shown in this manual after this section, in section 3.12.1 Error and service
codes
Error flag:
Register Usage Type
4000 General error flag RW
4001 Fatal error flag RW
4002 Service flag RW
4003 Last general error device* R
4004 Last fatal error device* R
*these registers show, which device had the last error: 0 = titrator 1, 1 = titrator 2, 2 = sampler 1, 3
= sampler 2
The last error from titrator 1:

Register Usage Type
4010 Error log index R
4011 Date and time (1st and 2nd character) R
4012 Date and time (3rd and 4th character) R
4013 Date and time (5th and 6th character) R
4021 Error code R
4022 Sampleline (0 = no sampleline related to error) R
The error from titrator 1 by error log index:

Register Usage Type
4050 Error log index (Note) RW
4061 Error code R
Note: Set the error log index (register 4050) before read date, time and error code.
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Register Usage Type

4121 Error code R
Register Usage Type

4161 Error code R
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The last error from sampler 1:
Register Usage Type

4221 Error code R
The error from sampler 1 by error log index:
Register Usage Type

4261 Error code R
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Register Usage Type

4321 Error code R
Register Usage Type

4361 Error code R
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The last service message:
4410 Service log index R

4421 Service code R
The service message by index:
4550 Service log index (Note) RW

4561 Service code R
Note: Set the service log index (register 4550) before read date, time and service code.
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3.13.1. Error and service codes
Titrator error codes:

1 = Arm up sensor error
2 = Arm down sensor error
3 = Arm out sensor error
4 = Arm in sensor error
5 = No sample ready from sampler
6 = pH too low
7 = Too much HCl
8 = Analysis duration too long
9 = Analysis water tank empty
10 = Analysis cabinet overflow
11 = Sample cup cabinet overflow
12 = Analyzer room temp. too high
13 = Burette timeout
14 = Analysis water tank not filled
15 = A-point not found
16 = B-point not found
17 = No water pressure
18 = No air pressure
Sampler error codes:

1 = No water pressure
2 = No air pressure
3 = Sample not collected
4 = Temp. too high after rinse
5 = Sedim. tank not empty
6 = No warm sample
7 = Sedim. tank not full
8 = Sample line index error
9 = Analysis duration too long
10 = Sample line order error
Service codes:
1 = Test submodule reset
2 = System Reset
3 = Loss of Clock Reset
4 = Stop Monitor Reset
5 = Software Watchdog Reset
6 = Power-Up Reset
7 = External Reset
8 = Unknown Reset
9 = HCl tank level low
10 = Service time exceeded
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3.14. Service counters
- with these counters the user is able to know how much acid there is left in the containers and get
a warning message to the service log when the volume has dropped below a certain level. The
service alarm will remind the user about the regular services that has to be done
for the analyzer.
- Titrator x HCl alarm ON/OFF: when this variable is on, the analyzer will calculate the current
volumes and will give the warning message if the volume is less than the alarm limit.
- Titrator x HCl current volume: this variable shows how much acid there is left in container. After
refilling the container the user must enter the correct volume in these variables.
- Titrator x HCl alarm limit: this is the limit value for the warning message.
- Titrator x HCl strength: this is the normality of the acid currently in use, default 1.000 N
- Service alarm ON/OFF: this sets the service reminder on/off use
- Hours to service: the service interval in hours. When this interval is passed, the analyzer sends
”Service time exceeded” message to the user as a reminder.
Register Usage Type

4700 Titrator 1 HCl alarm ON/OFF RW
4701 Titrator 1 current HCl volume, MSB of the float RW
4702 Titrator 1 current HCl volume, LSB of the float RW
4703 Titrator 1 HCl alarm limit, MSB of the float RW
4704 Titrator 1 HCl alarm limit, LSB of the float RW
4705 Titrator 1 HCl strength, MSB of the float RW
4706 Titrator 1 HCl strength, LSB of the float RW
4708 Titrator 2 current HCl volume, MSB of the float RW
4709 Titrator 2 current HCl volume, LSB of the float RW
4710 Titrator 2 HCl alarm limit, MSB of the float RW
4711 Titrator 2 HCl alarm limit, LSB of the float RW
4712 Titrator 2 HCl strength, MSB of the float RW
4713 Titrator 2 HCl strength, LSB of the float RW
4714 Service alarm ON/OFF RW
4715 Hours to service RW
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3.15. Analyzer control
- with these registers the user is able to change the descriptions of the virtual machines
(analyzers)
- the analyzers can be started and stopped via modbus from registers in section 3.21. Titrator
control registers
- analyzer index: 0 = Analyzer 1 + Sampler 1
1 = Analyzer 2 + Sampler 2
2 = Analyzer 1 + Sampler 1 + Sampler 2
4 = Analysis water tank control
5 = Waste tank control
- titrator start and stop queue: the macroqueue the titrator uses in start and stop situations
- titrator start mode: sets the mode in which the titrator is in start.
- 0 = IDLE
- 1 = AUTOMATIC
- 2 = MANUAL
- sampler start and stop queue: the macroqueue the sampler uses in start and stop situations
- sampler start mode: sets the mode in which the sampler is in start.
- 0 = IDLE
- 1 = AUTOMATIC
- 2 = MANUAL
- run from start: if set active, the analyzer will start automatically after a power failure
0 = NOT ACTIVE
1 = ACTIVE
- group start: if set active, the analyzer will start using the RUN ANALYZER –command in control
page of the communicator.
0 = NOT ACTIVE
1 = ACTIVE
Register Usage Type

5000 Analyzer index RW
5016 Titrator start queue RW
5017 Titrator stop queue RW
5018 Titrator start mode RW
5019 Sampler start queue RW
5020 Sampler stop queue RW
5021 Sampler start mode RW
5022 Run from start RW
5023 Group start RW
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3.16. Service parameters
- these registers define which macroqueue and analyzers the service programs use. The service
programs are run from the control page, Services TI/SA menu in the communicator. The services
include e.g. burette services, manual analyses and rinsing programs.
Titrator services:
Register Usage Type
5080 Service index RW
5081 Queue number RW
5082 Analyzer ID RW
Sampler services:
Register Usage Type
5092 Analyzer ID RW
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3.17. Error parameters
- with these registers the user is able to change the errors shown in section 3.12.1 Error codes
- error index = error code
- severity: 1 = fatal error, the analyzer will stop
2 = general error, the analyzer continues operation
3 = service error, informative message
Titrator error:
Register Usage Type
5100 Error index RW
5101 Error description (1st and 2nd character) RW
5102 Error description (3rd and 4th character) RW
5103 Error description (5th and 6th character) RW
5116 Severity RW
Sampler error:
Register Usage Type
5120 Error index RW
5136 Severity RW
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3.18. Analyzer variable parameters
- variable index (0 –190) is the variable number shown in the parameter configuration pages in the
communicator (e.g. Sample Lines -> 11 L1 Rinse time)
- unit: - 0 = none
- 1 = time in seconds
- 2 = temperature (°C or °F)
- 3 = acid volume in microlitres
Register Usage Type

5140 Variable index RW
5141 Description (1st and 2nd character) R
5142 Description (3rd and 4th character) R
5143 Description (5th and 6th character) R
5150 Value RW
5151 Unit R
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3.19. Binary-I/O descriptions
- with these registers the user is able to rename the binary inputs and outputs
Register Usage Type

5220 Card index (0=Titrator 1, 1=Titrator 2, 2=Sampler 1, 3=Sampler 2) RW
5221 I/O-index RW
5222 Output description (1st and 2nd character) RW
5223 Output description (3rd and 4th character) RW
5224 Output description (5th and 6th character) RW
5230 Input description (1st and 2nd character) RW
5231 Input description (3rd and 4th character) RW
5232 Input description (5th and 6th character) RW
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3.20. Binary-I/O states
- with these registers the user is able to read the states of the binary inputs and outputs. The states
are shown in blocks of 8 inputs/outputs in 8 LSBs of the register.
Register Usage Type

5300 Titrator 1 inputs 1-8 R
5308 Sampler 1 inputs 1-8 R
5316 Titrator 1 outputs 1-8 R
5324 Sampler 1 outputs 1-8 R
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3.21. Result adjustment
- with these registers the user is able to adjust the results to the laboratory results.
Register Usage Type

7000 Sample line RW
7001 EA offset, MSB of the float RW
7002 EA offset, LSB of the float RW
7003 EA gain, MSB of the float RW
7004 EA gain, LSB of the float RW
7005 AA offset, MSB of the float RW
7006 AA offset, LSB of the float RW
7007 AA gain, MSB of the float RW
7008 AA gain, LSB of the float RW
7009 TTA offset, MSB of the float RW
7010 TTA offset, LSB of the float RW
7011 TTA gain, MSB of the float RW
7012 TTA gain, LSB of the float RW
7013 CE% offset, MSB of the float RW
7014 CE% offset, LSB of the float RW
7015 CE% gain, MSB of the float RW
7016 CE% gain, LSB of the float RW
7017 S% offset, MSB of the float RW
7018 S% offset, LSB of the float RW
7019 S% gain, MSB of the float RW
7020 S% gain, LSB of the float RW
7021 Na2CO3 offset, MSB of the float RW
7022 Na2CO3 offset, LSB of the float RW
7023 Na2CO3 gain, MSB of the float RW
7024 Na2CO3 gain, LSB of the float RW
7025 NaOH offset, MSB of the float RW
7026 NaOH offset, LSB of the float RW
7027 NaOH gain, MSB of the float RW
7028 NaOH gain, LSB of the float RW
7029 Na2S offset, MSB of the float RW
7030 Na2S offset, LSB of the float RW
7031 Na2S gain, MSB of the float RW
7032 Na2S gain, LSB of the float RW
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3.22. Titrator control registers
- with these registers it is possible to start/stop titrators of the virtual machines (=analyzers)
Register Usage Type

10000 Titrator 1 control request RW
10006 Titrator 1 operating mode R
10012 Titrator 1 current sampleline R
R
10000.. request : 71H = start, 72H = stop
10005 reply : 4H = processing, 85H = request failed
10006.. mode : 0H = IDLE, 1H = AUTOMATIC, 2H = MANUAL

10011
Titrator control by index
Register Usage Type

10050 Titrator index * RW
10051 Titrator control request RW
10052 Titrator operation mode R
10053 Titrator current sampleline R
10054 Titrator queue number R
10055 Titrator queue index R
10056 Titrator macro line number R
10051 request : 71H = start, 72H = stop

reply : 4H = processing, 85H = request failed
10052 mode : 0H = IDLE, 1H = AUTOMATIC, 2H = MANUAL

* set the titrator index before reading
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3.23. Sampler control registers
- with these registers it is possible to start/stop samplers of the virtual machines (=analyzers)
Register Usage Type

10100 Sampler 1 control request RW
10106 Sampler 1 operating mode R
10112 Sampler 1 current sampleline R
10100.. request : 71H = start, 72H = stop

10106.. mode : 0H = IDLE, 1H = AUTOMATIC, 2H = MANUAL

10111
Sampler control by index
Register Usage Type

10150 Sampler index * RW
10151 Sampler control request RW
10152 Sampler operation mode R
10153 Sampler current sampleline R
10154 Sampler queue number R
10155 Sampler queue index R
10156 Sampler macro line number R

reply : 4H = processing, 85H = request failed

* set the sampler index before reading
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3.24. Controlled shutdown
- in the controlled shutdown the analyzer will not stop immediately. The sequence will go on until a
stop flag is set on, usually after rinsing programs. The controlled shutdown can be set by writing ”1”
to the desired register.
Register Usage Type

10200 Analyzer 1 controlled shutdown RW
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4. REGISTER REMAPPING TABLE
Depending on the application a number of access holding registers commands are needed
to access the registers defined in the previous chapter.
To reduce the number of needed commands a register remapping table has been
implemented. The register numbers used in the modbus messages are converted to Alkali
modbus register numbers according this table.
The remapping table usage and table contents are selected on the configuration pages of
the analyzer user interface.
When the table usage has been selected the table occupies the registers 1-1000. The
registers beginning from the register 1001 can also be accessed directly.
An example of the usage of the register remapping table: The error flags and EA, AA and
TTA results and sample line information are desired. The register remapping table contents
are:
Table index Register number
1 4000
2 4001
3 4002
4 204
5 214
6 215
7 216
8 217
9 218
10 219
Now the data can be read by using a single read holding registers -command which
accesses the registers 1-10 instead of three separate read holding registers -commands
(4000-4002, 204, 214-219).
ATTENTION. When defining the register remapping table care must be taken to keep
together the two registers holding a floating point number.
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5. MODIFICATION HISTORY
Rev. Comments Author / Date

Vt.a Document created JHa / 28.10.1997
Vt.b Measuring permission and parameters (5000-5999) added JHa / 30.12.1997
V1.0 Updates for K A A v1.0 JPuu / 23.03.1998
V1.1 Updates for K A A v1.1 IPy / 05.03.1999
V1.2 Updates for K A A v1.2 IPy / 28.12.1999
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Modicon/Gateway specification for the kajaaniALKALi
(Integer version, protocol = 4)
Created : Ilkka Pyykkönen / 29.10.1997

Checked : Lauri Keränen / 29.10.1997
Approved : Lauri Keränen / 29.10.1997
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Contents:
1. INTRODUCTION...................................................................................................................................... 3
2. MODBUS FUNCTIONS ........................................................................................................................... 3
2.1. Read Holding Registers ................................................................................................................. 3
2.2. Preset Multiple Registers ............................................................................................................... 4
3. THE DATA TO BE TRANSFERRED........................................................................................................ 5
3.1. Date, time and software version .................................................................................................... 5
3.2. Measuring permission and sampler timing .................................................................................... 6
3.3. Sampler startup modes.................................................................................................................. 6
3.4. Analysis results .............................................................................................................................. 7
3.5. Analysis parameters ...................................................................................................................... 8
3.6. Status info ...................................................................................................................................... 9
3.7. Temperature sensors................................................................................................................... 14
3.8. Modbus remapping table ............................................................................................................. 14
3.9. Sample lines ................................................................................................................................ 14
3.10. Sample order ............................................................................................................................... 18
3.11. Error log ....................................................................................................................................... 19
3.11.1. Error and service codes................................................................................................ 22
3.12. Service counters .......................................................................................................................... 23
3.13. Analyzer control ........................................................................................................................... 23
3.14. Service parameters...................................................................................................................... 24
3.15. Error parameters.......................................................................................................................... 25
3.16. Analyzer variable parameters ...................................................................................................... 26
3.17. Binary-I/O descriptions................................................................................................................. 26
3.18. Binary I/O states........................................................................................................................... 27
3.19. Titrator control registers ............................................................................................................... 28
3.20. Sampler control registers ............................................................................................................. 29
3.21. Controlled shutdown .................................................................................................................... 29
3.22. Result adjustment ........................................................................................................................ 30
4. REGISTER REMAPPING TABLE.......................................................................................................... 31
5. MODIFICATION HISTORY .................................................................................................................... 31
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1. INTRODUCTION
The document specifies the operation of the MODBUS interface in the kajaaniALKALi when using a Modicon
gateway.
2. MODBUS FUNCTIONS
The Modbus operates only in the RTU-mode. The ASCII-mode is not available.
The default serial communication parameters are: 9600 baud, 1 start bit, 8 data bits, no parity, 2 stop bits.
The following functions are supported: Read Holding Registers (03), Preset Single Holding Register (06) and
Preset Multiple Registers (16).
The register range in the Modbus-messages is 0-65535. I.e. in the messages the 1st register is accessed as
0, the 2nd register as 1 etc.
2.1. Read Holding Registers

Field Meaning
Starting Address Hi 8 MSB (most significant bits) of the 1st register to read
Starting Address Lo 8 LSB (least significant bits) of the 1st register to read
No. of registers Hi 8 MSB of the number of the registers to read
No. of registers Lo 8 LSB of the number of the registers to read

Field Meaning
ADDRESS (0-255) Address of the slave
FUNCTION (3) Function code
Byte Count Number of data bytes is the message
Data Hi 8 MSB of the 1st register read
Data Lo 8 LSB of the 1st register read
...
Data Hi 8 MSB of the last register read
Data Lo 8 LSB of the last register read
If the read command addresses a reserved register within the defined register range the returned register
value is 0 and no error is reported.
If only one register of the two registers holding a float value is accessed, the data will not be read and an
error message will be returned.
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2.2. Preset Multiple Registers

Field Meaning
Starting Address Hi 8 MSB of the address of the first register to write
Starting Address Lo 8 LSB of the address of the first register to write
No. of registers Hi 8 MSB of the number of the registers to write
No. of registers Lo 8 LSB of the number of the registers to write
Byte Count The number of data bytes in the message
Data Hi 8 MSB of the 1st register to write
Data Lo 8 LSB of the 1st register to write
...
Data Hi 8 MSB of the last register to write
Data Lo 8 LSB of the last register to write

Field Meaning
Starting Address Hi 8 MSB (most significant bits) of the 1st register written
Starting Address Lo 8 LSB (least significant bits) of the 1st register written
No. of registers Hi 8 MSB of the number of the registers written
No. of registers Lo 8 LSB of the number of the registers written
If the read command addresses a reserved or read only register within the defined register range the data is
not stored and no error is reported.
If only one register of the two registers holding a float value is accessed the data is not written and an error
message is returned. However, the registers prior to the erroneous register are written correctly.
Exception messages
The exception message is of form:

Field Meaning
FUNCTION The function code ored with 80H
Exception code Information of the error
An exception message is returned under some of the following conditions.
• Illegal function
The function code received is not supported. The exception code is 1.
• Illegal data address
The register address received is out of the defined register range. The exception code is 2.
• Illegal data value
Only one of the two registers holding a float value is accessed. The exception code is 3.
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3. THE DATA TO BE TRANSFERRED
The indexes of the data are in the following tables. The type field is either RW (i.e. the register can be read
and written) or R (i.e. the register can only be read).
The range field is used when the server the internally used value needs scaling. The range field specifies the
server internally used value range. If no range is given the server value range is 0-32767. In this case the
allowed values can be specified in the usage field.
The values are scaled using the following formulas:
When reading a register value from the server:
R = ROUND( (32767 / (FH - FL) )* (FL - F) )
and when writing a register value to the server:
F = FL + ( (FH - FL) / 32767) * R
where
R = the holding register value
FL and FH = the lower and upper limit for the value in the server
F = the value in the server
and ROUND denotes a funtion thet rounds its input to an integer value.
3.1. Date, time and software version
Register Usage Type Range

1 Year RW
2 Month RW
3 Day of the month RW
4 Hour RW
5 Minute RW
6 Seconds R
7 Software version R 0 - 10
8 Date mode * RW
* This determines how the date is shown in the display of the communicator.
0 = day-month-year, 1 = month-day-year.
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3.2. Measuring permission and sampler timing
- by the measuring permissions the user is able to disable measurements from certain sample lines
- in the timed sampling mode the sampler will start the sampling at the certain time. In the continous mode
the sampling is done as soon as the titrator is ready .
Register Usage Type

10 Get permission from modbus * RW
11 Sample line 1 measuring permission ** RW
19
20 Sampler 1 timing mode *** RW
21 Sampler 2 timing mode RW
* The measuring permissions can be set either via the binary inputs or modbus. In order to set the
permissions from modbus, you need to set the value of this register to ”1” first.
- 0 = measuring permissions are read from the binary inputs
- 1 = measuring permissions are read from modbus
** If the value in the register nr. 10 Get permission from modbus is”0”, reading these registers will give the
states of the binary inputs. Writing operation to these registers will have an effect to the analyzer’s operation
only if the value in the register nr. 10 is ”1”.
- 0 = line enabled
- 1 = line disabled
*** - 0 = continuous sampling mode
- 1 = timed sampling mode
3.3. Sampler startup modes
- if the sample from the sample line is cold, the analyzer will give an error message No warm sample.
Startup mode enables the sampler to collect also cold samples.
Note: this mode will go automatically off, when the sampler has observed three times warm sample from the
line.
Register Usage Type

30 Sampler startup mode off/on ( 0 / 1 )* RW
31 Line 1 startup mode off/on ( 0 / 1 ) R
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3.4. Analysis results
- block number increases from 0 to 1999 and after that it starts over from 0
- the analysis type informs which analysis parameter table is used for this analysis (0 – 7)
- - sample line shows the line where the sample is from (1 – 8 in automatic mode, 9 – 16 in analyzer 1
manual samples, 17 – 24 in analyzer 2 manual samples )
- HCl volume 1,2 and 3 are the volumes in each equivalence point, typical value is 500 – 15,000.
- pH 1, 2 and 3 are the pH values of each equivalence point, typically values are between 2 and 12.
- analysis start date: dd-mm-yy
- result type show the units of the result and if the results are calculated in Na2O or NaOH
- result type is displayed in 8 lowest bits:
- MSB: 0 = Na20, 1 = NaOH
- next 3 bits, alkali units: 0 = g/l, 1 = lb in cubic feet, 2 = lb in gallon, 3 = ml HCl
- 4 LSBs, carbonate units: 0 = g/l, 1 = lb in cubic feet, 2 = lb in gallon, 3 = ml HCl
- start pH shows the pH in the beginning of the analysis, i.e. sample pH
- in the analysis results by block number it is possible to read previous results
The last results from analyzer:

200 Block number R
203 Analysis type R
204 Sample line R
205 HCl volume 1 R
206 HCl volume 2 R
207 HCl volume 3 R
208 pH 1 R 0.0 - 14.0
209 pH 2 R 0.0 - 14.0
210 pH 3 R 0.0 - 14.0
211 EA R 0.0 - 200.0
212 AA R 0.0 - 200.0
213 TTA R 0.0 - 200.0
214 CE% R 0.0 - 200.0
215 S% R 0.0 - 200.0
216 Na2CO3 R 0.0 - 200.0
217 NaOH R 0.0 - 200.0
218 Na2S R 0.0 - 200.0
230 Result type info (note !) R

- MSB: 0 = Na20, 1 = NaOH
- next 3 bits, alkali units: 0 = g/l, 1 = lb in cubic feet, 2 = lb in gallon, 3 = ml HCl
- 4 LSBs, carbonate units: 0 = g/l, 1 = lb in cubic foot, 2 = lb in gallon, 3 = ml HCl
7
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The results from analyzer by block number:

250 Block number RW
253 Analysis type R
254 Sample line R
255 HCl volume 1 R
256 HCl volume 2 R
257 HCl volume 3 R
258 pH 1 R 0.0 - 14.0
259 pH 2 R 0.0 - 14.0
260 pH 3 R 0.0 - 14.0
261 EA R 0.0 - 200.0
262 AA R 0.0 - 200.0
263 TTA R 0.0 - 200.0
264 CE% R 0.0 - 200.0
265 S% R 0.0 - 200.0
266 Na2CO3 R 0.0 - 200.0
267 NaOH R 0.0 - 200.0
268 Na2S R 0.0 - 200.0
281 Start pH R 0.0 - 14.0

- MSB: 0 = Na20, 1 = NaOH
Note: Set the block number (register 250) before read the history results.
3.5. Analysis parameters
- index for analysis type is the number of the analysis parameter table ( 0 – 7)
- sample volume typical values 2.0 – 2.5 ml
- T1 is the first acid additions (for each equivalence point)
- T2 is the second acid additions (for each equivalence point)
- Dmin is the limit value for derivate 1. Derivate 1 must be over this value in equivalence point, otherwise
the point is not accepted.
- FA, FB and FC form the formula how the additions are calculated, i.e. how the additions will follow the
changes in pH curve
8
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Analysis parameters by index:

300 Index for analysis type RW
317 Sample volume RW 0.0 - 10.0
318 Reserved
319 T1 point 1 RW
320 T2 point 1 RW
321 Dmin point 1 RW
322 FA point 1 RW
323 FB point 1 RW
324 FC point 1 RW
325 FD point 1 RW 0.0 - 10.0
326 T1 point 2 RW
327 T2 point 2 RW
328 Dmin point 2 RW
329 FA point 2 RW
330 FB point 2 RW
331 FC point 2 RW
332 FD point 2 RW 0.0 - 10.0
333 T1 point 3 RW
334 T2 point 3 RW
335 Dmin point 3 RW
336 FA point 3 RW
337 FB point 3 RW
338 FC point 3 RW
339 FD point 3 RW 0.0 - 10.0
Note: Set index (register 300) before reading parameters (index = 0..7)
3.6. Status info
- status info includes the text which can be read from the main page of the communicator. It informs what
the device is doing.
- sample line tells the name of the sample line where the current sample is coming from
- queue number, queue index and macro line number tells the location where the sequence is currently
running in the macro structure
- sample line number is the same information as sample line, but in numerical form
- number of manual analyses tells which manual sample is currently analyzed and the amount of ordered
manual analyses tell how many analyses the user has set.
9
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Titrator 1:
Register Usage Type

640 Queue number R
641 Queue index R
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Sampler 1:
Register Usage Type

640 Queue number R
641 Queue index R
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Titrator 2:
Register Usage Type

740 Queue number R
741 Queue index R
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Sampler 2:
Register Usage Type

790 Queue number R
791 Queue index R
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3.7. Temperature sensors

- electronics temperature sensor is located in the amplifier board
794 Temperature sensor 1 R *
795 Temperature sensor 2 R *
796 Electronics temperature R *
* if temperatures are presented in Celsius, range –25.0 – +125.0,

if temperatures are presented in Fahrenheit, range –13.0 – +257.0
3.8. Modbus remapping table
- the user can set separate registers into consecutive registers in the remapping table, so there is no need
to do several read/write operations for the required registers. See section 4. Register remapping table for
further information.
Register Usage Type

1500 Register index (1 - 1000)* RW
1501 Remapped register RW
1502 Modem port remapping ON/OFF RW
1503 DCS port remapping ON/OFF RW
1504 PC port remapping ON/OFF RW
3.9. Sample lines
- in this section the user is able to set descriptions for sample lines and set the formula for calculating the
sulfidity
Sample line 1:
Register Usage Type

2017 Sample type RW
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Sample line 2:
Register Usage Type

2117 Sample type RW
Sample line 3:
Register Usage Type

2217 Sample type RW
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Sample line 4:
Register Usage Type

2317 Sample type RW
Sample line 5:
Register Usage Type

2417 Sample type RW
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Sample line 6:
Register Usage Type

2517 Sample type RW
Sample line 7:
Register Usage Type

2617 Sample type RW
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Sample line 8:
Register Usage Type

2717 Sample type RW
3.10. Sample order
- sample order tells the sampler in which order the samples should be taken. Use only characters (not
numbers) from ’1’ to ’8’, the last mark must be NULL mark to tell the analyzer that the order string has
ended. The analyzer will not read any characters after the NULL mark.
Note: One register has two ASCII-characters from the sample order table. Add NULL mark (hex 0) to the end
of the character string !
Titrator 1:
Register Usage Type
Titrator 2:
Register Usage Type
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3.11. Error log
- when the analyzer detects an error, it sets a certain error flag on (depending on the severity of the error),
and writes the error code into the error log
- in the error log the sample line is also shown if the error is related to sample line
- the error log index is from 0 to 99 and is increased when new error. The index starts over from 0 after
each 100 errors.
- the error codes are shown in this manual after this section, in section 3.12.1 Error and service codes
Error flag:
Register Usage Type
4000 General error flag R
4001 Fatal error flag R
4002 Service flag R

Register Usage Type
4021 Error code R

Register Usage Type
4061 Error code R
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Register Usage Type

4121 Error code R
Register Usage Type

4161 Error code R
Register Usage Type

4221 Error code R
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Register Usage Type

4261 Error code R
Register Usage Type

4321 Error code R
Register Usage Type

4361 Error code R
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The last service message:
Register Usage Type

4410 Service log index R
4421 Service code R
The service message by index:
Register Usage Type

4550 Service log index (Note) RW
3.11.1. Error and service codes
Titrator error codes: Sampler error codes:

1 = Arm up sensor error 1 = No water pressure
2 = Arm down sensor error 2 = No air pressure
3 = Arm out sensor error 3 = Sample not collected
4 = Arm in sensor error 4 = Temp. too high after rinse
5 = No sample ready from sampler 5 = Sedim. tank not empty
6 = pH too low 6 = No warm sample
7 = Too much HCl 7 = Sedim. tank not full
8 = Analysis duration too long 8 = Sample line index error
9 = Analysis water tank empty 9 = Analysis duration too long
10 = Analysis cabinet overflow 10 = Sample line order error
11 = Sample cup cabinet overflow Service codes:
12 = Analyzer room temp. too high 1 = Test submodule reset
13 = Burette timeout 2 = System Reset
14 = Analysis water tank not filled 3 = Loss of Clock Reset
15 = A-point not found 4 = Stop Monitor Reset
16 = B-point not found 5 = Software Watchdog Reset
17 = No water pressure 6 = Power-Up Reset
18 = No air pressure 7 = External Reset
8 = Unknown Reset
9 = HCl tank level low
10 = Service time exceeded
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3.12. Service counters
- with these counters the user is able to know how much acid there is left in the containers and get a
warning message to the service log when the volume has dropped below a certain level. The service
alarm will remind the user about the regular services that has to be done to the analyzer.
- Titrator x HCl alarm ON/OFF: when this variable is on, the analyzer will calculate the current volumes and
will give the warning message if the volume is less than the alarm limit.
- Titrator x HCl current volume: this variable shows how much acid there is left in container. After refilling
the container the user must enter the correct volume in these variables.
- Titrator x HCl alarm limit: this is the limit value for the warning message.
- Titrator x HCl strength: this is the normality of the acid currently in use, default 1.000 N
- Service alarm ON/OFF: this sets the service reminder on/off use
- Hours to service: the service interval in hours. When this interval is passed, the analyzer sends ”Service
time exceeded” message to the user as a reminder.

4701 Titrator 1 current HCl volume RW 0.0 - 30.0
4702 Titrator 1 HCl alarm limit RW 0.0 - 30.0
4703 Titrator 1 HCl strength RW 0.5 -1.5
4705 Titrator 2 current HCl volume RW 0.0 - 30.0
4706 Titrator 2 HCl alarm limit RW 0.0 - 30.0
4707 Titrator 2 HCl strength RW 0.5 -1.5
4708 Service alarm ON/OFF RW
4709 Hours to service RW
3.13. Analyzer control
- with these registers the user is able to change the descriptions of the virtual machines (analyzers)
- the analyzers can be started and stopped via Modbus from registers in section 3.21. Titrator control
registers
- titrator start and stop queue: the macroqueue the titrator uses in start and stop situations
- titrator start mode: sets the mode in which the titrator is in start.
- 0 = IDLE
- 1 = AUTOMATIC
- 2 = MANUAL
- sampler start and stop queue: the macroqueue the sampler uses in start and stop situations
- sampler start mode: sets the mode in which the sampler is in start.
- 0 = IDLE
- 1 = AUTOMATIC
- 2 = MANUAL
- run from start: if set active, the analyzer will start automatically after a power failure
0 = NOT ACTIVE
1 = ACTIVE
- group start: if set active, the analyzer will start using the RUN ANALYZER –command in control page of
the communicator.
0 = NOT ACTIVE
1 = ACTIVE
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Register Usage Type

5000 Analyzer index RW
5016 Titrator start queue RW
5017 Titrator stop queue RW
5018 Titrator start mode RW
5019 Sampler start queue RW
5020 Sampler stop queue RW
5021 Sampler start mode RW
5022 Run from start RW
5023 Group start RW
3.14. Service parameters
- these registers define which macroqueue and analyzers the service programs use. The service programs
are run from the control page, Services TI/SA menu in the communicator. The services include e.g.
burette services, manual analyses and rinsing programs.
Titrator services:
Register Usage Type
5082 Analyzer ID RW
Sampler services:
Register Usage Type
5092 Analyzer ID RW
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3.15. Error parameters
- with these registers the user is able to change the errors shown in section 3.12.1 Error codes
- error index = error code
- - severity: 1 = fatal error, the analyzer will stop
2 = general error, the analyzer continues operation
3 = service error, informative message
Titrator error:
Register Usage Type

5100 Error index RW
5116 Severity RW
Sampler error:
Register Usage Type
5120 Error index RW
5136 Severity RW
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3.16. Analyzer variable parameters
- variable index (0 –190) is the variable number shown in the parameter configuration pages in the
communicator (e.g. Sample Lines -> 11 L1 Rinse time)
- - unit: - 0 = none
- 1 = time in seconds
- 2 = temperature (°C or °F)
- 3 = acid volume in microlitres
Register Usage Type

5140 Variable index RW
5141 Description (1st and 2nd character) R
5142 Description (3rd and 4th character) R
5150 Value RW
5151 Units R
3.17. Binary-I/O descriptions
- with these registers the user is able to rename the binary inputs and outputs
Register Usage Type

5220 Card index (0=Titrator 1, 1=Titrator 2, 2=Sampler 1, 3=Sampler 2) RW
5221 I/O-index RW
5222 Output description (1st and 2nd character) RW
5223 Output description (3rd and 4th character) RW
5230 Input description (1st and 2nd character) RW
5231 Input description (3rd and 4th character) RW
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3.18. Binary I/O states
- with these registers the user is able to read the states of the binary inputs and outputs. The states are
shown in blocks of 8 inputs/outputs in 8 LSBs of the register.
Register Usage Type

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3.19. Titrator control registers
- with these registers it is possible to start/stop titrators of the virtual machines (=analyzers)
Register Usage Type

R

6011
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3.20. Sampler control registers
- with these registers it is possible to start/stop samplers of the virtual machines (=analyzers)
Register Usage Type



6111
3.21. Controlled shutdown
- in the controlled shutdown the analyzer will not stop immediately. The sequence will go on until a stop
flag is set on, usually after rinsing programs. The controlled shutdown can be set by writing ”1” to the
desired register.
Register Usage Type

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3.22. Result adjustment
- with these registers the user is able to adjust the results to the laboratory results.

7000 Sample line index RW
7001 EA offset RW -50 - 50
7002 EA gain RW -50 - 50
7003 AA offset RW -50 - 50
7004 AA gain RW -50 - 50
7005 TTA offset RW -50 - 50
7006 TTA gain RW -50 - 50
7007 CE% offset RW -50 - 50
7008 CE% gain RW -50 - 50
7009 S% offset RW -50 - 50
7010 S% gain RW -50 - 50
7011 Na2CO3 offset RW -50 - 50
7012 Na2CO3 gain RW -50 - 50
7013 NaOH offset RW -50 - 50
7014 NaOH gain RW -50 - 50
7015 Na2S offset RW -50 - 50
7016 Na2S gain RW -50 - 50
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4. REGISTER REMAPPING TABLE
Depending on the application a number of access holding registers commands are needed to access the
registers defined in the previous chapter.
To reduce the number of needed commands a register remapping table has been implemented. The register
numbers used in the modbus messages are converted to Alkali modbus register numbers according this
table.
The remapping table usage and table contents are selected on the configuration pages of the analyzer user
interface.
When the table usage has been selected the table occupies the registers 1-1000. The registers beginning
from the register 1001 can also be accessed directly.
An example of the usage of the register remapping table: The error flags and EA, AA and TTA results and
sample line information from the titrators are desired. The register remapping table contents are:
Table index Register number

1 4000
2 4001
3 4002
4 204
5 211
6 212
7 213
8 8
9 9
10 10
Now the data can be read by using a single read holding registers -command which accesses the registers 1-
7 instead of three separate read holding registers -commands
(4000-4002, 204, 211-213).
ATTENTION. When defining the register remapping table care must be taken to keep together the two
registers holding a floating point number.
5. MODIFICATION HISTORY
Rev. Comments Author / Date

Vt.a Document created JHa / 29.10.1997
Vt.b Measuring permission and parameters (5000-5999) added JHa / 31.12.1997
V1.0 Updates for K A A V1.0 JPuu/ 02.06.1998
V1.1 Updates for K A A V1.1 IPy/03.03.1999
V1.2 Updates for K A A V1.2 IPy/29.12.1999
31
App. 5 - Installation Drawings

kajaaniALKALi Tube connections (Cabinet model)
FEP 3/4" R1/2"

Sample Lines 70101352 Instrument Air to Samplers Installation Space Required for
Each sample preparation unit has connections for 14 sample lines, i.e. Two instrument air lines (6/4) are connected from Analyzer (cabinet model)
analyzer with two SPUs can handle up to 8 sample lines. Specifications: SD-701 the sample unit to samplers SD-701 and SD-702.
material Teflon FEP or PFA Hmin = 0.1 x L valves A5, A6, A7, A8 => lines 14
outside diameter 19.1 mm (3/4") min. 300 (~12") valves B5, B6, B7, B8 => lines 58
wall thickness 1.575 mm (1/16")
1 m (3.3 ft)
minimum bend radius 300 mm (12") SD-702
length: gravity-feed samples max. 35 m (115 ft); ) )
(28
SD-702
Open m (28
pressurized samples max. 100 m (328 ft). 0m m m
70 00
For gravity feed samples the sample line must have at least 10% continuous ~ ~7
fall to ensure proper sample flow. Closed
~
70
If process pressure at the sampling point is > 4 bar (58 psi) and sample temp. L 0
m
is > 95°C (203°F), sample line material must be AISI 316L, outside diam. 1 m (3.3 ft) m
(2
8
16 mm (5/8). Connect the sample line at both ends using 1/2" Teflon 790 x 790 mm 790 x 790 mm )
FEP/PFA sample line connectors. Use the special tool! 5 6 7 8 (31 x 31) (31 x 31)
NOTE: Apply thread sealing tape and silicone grease 1 m (3.3 ft)
(e.g. Molykote 111) on the screw-on sample line connections! ~ ~
70 70
0 0
m m
Flushing Water SD-701 m
(2
8
m
(2
8
NOTE: Ensure steady, uninterrupted water supply! Closed ) )
Open
Specifications: 1 m (3.3 ft)
chemically purified, acceptable for return to process
pressure 48 bar (58116 psi), at least 2 bar (29 psi) higher than
highest process pressure at the sampling point
temperature +5...+50°C (41122°F)
NOTE: The coolest liquor sample must be at least +20°C (36°F)
hotter than the hottest flushing water used! Measurement unit (1 or 2 titr. modules)
filtered to 100 µm Dimensions (h x w x d):
consumption 150 l (40 US gal) / hour / sample unit (= 4 lines) 1900 x 790 x 790 (75 x 31 x 31) 700 (27 1/2")
connection ISO 7/1Rp 1/2" or NPT 1/2 Weight: 210 kg (463 lbs)
recommended inlet pipe DN20 Relative humidity: 1090%, no condensation
Ambient temperature: +5...+50°C (+41..122°F) 350
Analysis Water Analysis chemical:
(13 3/4")
NOTE: Ensure steady, uninterrupted water supply! Hydrochlorid acid HCl (1.0 ± 0.05N, meas. accuracy ±0.001N)
Analysis water is led to the analysis water tank, located in the lower part 285
Consumption: 8 liters (2.1 US gal) / week / titr. module (11 1/4")
of measurement unit.
Specifications: 180
(7 1/8")
distilled or deionized water Water Purifier (option)
pressure < 4 bar (< 58 psi) The reverse-osmosis-based water purifier generates deionized 130
temperature +1040°C (50104°F) water. It must always be installed if the mill does not have an (5 1/8") 1090 (43")
conductivity < 30 µS/cm own boiler.
pH = 68 The water purifier can be installed e.g. on the analyzers side 937 (37")
consumption 2.5 l (0.7 US gal) / hour / titr. module wall (cabinet model). Also connect the control cable delivered
connection ISO 7/1Rp 1/2" or NPT 1/2 with the water purifier. Make water connections according to 840 (33")
recommended inlet pipe DN10 the manual supplied with the device. Connect inlet water to the 737 (29")
Instrument Air Connections analyzer's analysis water inlet connector.
625 (24 1/2")
Instrument air is needed for the waste pump (returning analysis waste to
process) and for the valve controls of sample unit and samplers. Titration Vapors 540 (21 1/4")
Specifications: Chemical vapors released during titration should be led 460 (18")
filtered, water-free, oil-free instrument air from the titration frame to a suitable ventilation conduit.
pressure 46 bar (6394 psi) In the cabinet model, the vapors are led with a hose from
minimum flow 1000 liters (35.5 ft3)/minute. titration frame to an opening on top of the cabinet.
connection ISO 7/1Rp 1/2" or NPT 1/2
recommended inlet pipe DN15
Discharge Connection 80130 (~ 35")

Waste pump removes analysis waste (used samples, flushing water, etc.)
from waste tank. Outlet connection ISO 7/1Rp1/2 or NPT 1/2, recomm.
pipe size DN25. Max. length 30 m (98 ft), max. delivery height 10 m (33 ft).
Overflow connections
Waste tank overflow: tube diam. 2", e.g. rubber hose. Connect the hose
to one of the three overflow connectors with an acid-proof hose clamp (close
other outlets with plugs), and lead the outlet end to an acceptable drain.
Analysis water tank overflow: tube diam. 19mm, lead the outlet to an The cabinet model analyzer is fastened to
acceptable drain. the floor or mounting stand with bolts. Select
Titration module overflow: tube DN10, lead the outlet to an acceptable bolt material and dimensions according to
drain. the installation point. The mounting stand is
similar for both units of the analyzer.
Pipe Sizes
Outside diameter Inside diameter Wall thickness
DN10 17.2mm 14.0mm 1.6mm 18 mm ø13 (33/64")
[11/16] [35/64] [1/16]
DN15 21.3mm 18.1mm 1.6mm When the cabinets are installed
[27/32] [23/32] [1/16] side by side, make sure to leave
DN20 26.9mm 23.7mm 1.6mm 18 mm (~3/4) between the 56
0
[1 1/16] [15/16] [1/16] mounting stands (2
2 ")
1/ 9/16
16 (27
") 700
kajaaniALKALi Installation - A5.1 - W4700162 V1.5 EN Manufacturer reserves the right to changes without prior notice.
kajaaniALKALi Tube connections (Compartment model)
FEP 3/4" R1/2" 2440 (96")

Sample Lines 70101352 Protective Compartment 400 (16")
Each sample preparation unit has connections for 14 sample lines, i.e. About 0.5 m (» 2 ft)
In very demanding process environments, the analyzer free space above
analyzer with two SPUs can handle up to 8 sample lines. Specifications: can be installed in a separate compartment. In this way the compartment
material Teflon FEP or PFA Hmin = 0.1 x L
min. 300 (~12") SD-701 the operating conditions, e.g. ambient temperature, can Titration
outside diameter 19.1 mm (3/4") better be stabilized. frame
wall thickness 1.575 mm (1/16") SD-702 Mounting bolts for compartment installation are included
minimum bend radius 300 mm (12") Measurement unit
in delivery.
length: gravity-feed samples max. 35 m (115 ft); NOTE: Prior to purchasing a compartment, check its
pressurized samples max. 100 m (328 ft). L dimensions with Neles Field Controls specialists! Electronics
For gravity feed samples the sample line must have at least 10% continuous unit
Sample
2800 (110")
preparation
fall to ensure proper sample flow. unit 2
If process pressure at the sampling point is > 4 bar (58 psi) and sample temp.
is > 95°C (203°F), sample line material must be AISI 316L, outside diam. Water Purifier (option)
16 mm (5/8). Connect the sample line at both ends using 1/2" Teflon The reverse-osmosis-based water purifier generates Sample
preparation
FEP/PFA sample line connectors. Use the special tool! deionized water. It must always be installed if the unit 1
NOTE: Apply thread sealing tape and silicone grease mill does not have an own boiler.
(e.g. Molykote 111) on the screw-on sample line connections! The water purifier is installed inside the protective
compartment. Also connect the control cable
Flushing Water Titration
delivered with the water purifier. Make water
NOTE: Ensure steady, uninterrupted water supply! Flushing water in vapors Analysis water in connections according to the manual supplied 10 Water purifier
Specifications: with the device. Connect inlet water to the analyzer's 00
Instrument air in (39
chemically purified, acceptable for return to process Sample & waters
analysis water inlet connector. )
pressure 48 bar (58116 psi), at least 2 bar (29 psi) higher than back to process Flushing water in
highest process pressure at the sampling point B5 B6
A5 A6
temperature +5...+50°C (41122°F) A7 A8 B7 B8
Compressed Air to Samplers:
NOTE: The coolest liquor sample must be at least +20°C (36°F) Two compressed air lines (6/4) are connected from
hotter than the hottest flushing water used! the sample unit to samplers SD-701 and SD-702.
filtered to 100 µm Sampler valve controls:
valves A5, A6, A7, A8 => lines 14 SD-702
consumption 150 l (40 US gal) / hour / sample unit (= 4 lines) 1 4 = A5,A6,A7,A8 / 5 8 = B5,B6,B7,B8
valves B5, B6, B7, B8 => lines 58
connection ISO 7/1Rp 1/2" or NPT 1/2 Open
recommended inlet pipe DN20
Closed
Titration Vapors
Chemical vapors released during titration should be led from the titration Sample lines 14
frame to a suitable ventilation conduit.
In the compartment model, the vapors are led with a hose from titration Sample and water
back to process 5 6 7 8
frame to an outlet on top of the compartment. DN25 Rp1/2" or NPT 1/2
Sample lines 58
Instrument air in
Analysis Water DN15 Rp1/2" or NPT 1/2
Flushing water in
NOTE: Ensure steady, uninterrupted water supply! Flushing water in
DN20 Rp1/2" or NPT 1/2
DN20 Rp1/2" or NPT 1/2
Analysis water is led to the analysis water tank, located in the lower part SD-701
of measurement unit. Washing gun
Specifications: (water/air) Open
Closed
distilled or deionized water
pressure < 4 bar (< 58 psi)
Overflow, d=2"
temperature +1040°C (50104°F) (3 alternative outlets; Waste tank
conductivity < 30 µS/cm one in use,
pH = 68 2 closed with plugs)
consumption 2.5 l (0.7 US gal) / hour / titr. module
connection ISO 7/1Rp 1/2" or NPT 1/2 Measurement unit (1 or 2 titr. modules)
recommended inlet pipe DN10 Dimensions (h x w x d):
1900 x 790 x 790 (75 x 31 x 31)
Instrument Air Connections Weight: 210 kg (463 lbs)
Instrument air is needed for the waste pump (returning analysis waste to Pipe Outside diameter Inside diameter Wall thickness Relative humidity: 1090%, no condensation
process) and for the valve controls of sample unit and samplers. Sizes DN10 17.2mm 14.0mm 1.6mm Ambient temperature: +5...+50°C (+41..122°F)
Specifications: [11/16] [35/64] [1/16] Analysis chemical: Hydrochlorid acid HCl
filtered, water-free, oil-free instrument air DN15 21.3mm 18.1mm 1.6mm (1.0 ± 0.05N, meas. accuracy ±0.001N)
pressure 46 bar (6394 psi) [27/32] [23/32] [1/16] Consumption: 8 liters (2.1 US gal) / week /
minimum flow 1000 liters (35.5 ft3)/minute. DN20 26.9mm 23.7mm 1.6mm titration module
connection ISO 7/1Rp 1/2" or NPT 1/2 [1 1/16] [15/16] [1/16]
recommended inlet pipe DN15 The analyzer cabinet is fastened to the floor
or mounting stand with bolts. Select bolt
Discharge Connection Information for installations in the USA: material and dimensions according to the
Waste pump removes analysis waste (used samples, flushing water, etc.) All the BEBCO-built compartments have a specific Bulk Head for all the connections. installation point. Mounting stand is similar in
from waste tank. Outlet connection ISO 7/1Rp1/2 or NPT 1/2, recomm. Instrument Air is divided in two; customer can choose which air supply will be used. both units.
pipe size DN25. Max. length 30 m (98 ft), max. delivery height 10 m (33 ft). a. Mill Air: (for ARO Waste Pump)
- Low quality, filtered, not dried; high volume, minimum 1000 liters (35.5 ft3)/minute.
Overflow connections - Connection 3/8 Tube Bulkhead Union.
Waste tank overflow: tube diam. 2", e.g. rubber hose. Connect the hose b. Instrument Air: ø13 (33/64")
to one of the three overflow connectors with an acid-proof hose clamp (close - High quality, filtered, water-free,oil-free; low volume, min. 10 liters (0.36 ft3)/minute.
- Connection 3/8 Tube Bulkhead Union.
other outlets with plugs), and lead the outlet end to an acceptable drain. c. Sample Return: 18 mm
Analysis water tank overflow: tube diam. 19mm, lead the outlet to an - Connection 3/4 Tube Bulkhead Union. When the cabinets are installed
acceptable drain. 56
d. High Pressure Rinsing Water: side by side, make sure to leave 0
(2
Titration module overflow: tube DN10, lead the outlet to an acceptable 18 mm (~3/4) between the 2 ")
- Connection 1 Female NPT. 1/ 9/16
drain. e. Potable Water: (for Analysis water or for RiOs water purifier system) mounting stands 16 (27
") 700
- Connection 3/4 Female NPT.
f. Sample Lines:
- Connection directly to the valve, R1/2.
kajaaniALKALi – Samplers
Technical specifications: Mounting Cone Technical specifications:

• material AISI 316 L Samplers SD-701 and SD-702 are connected to the process with • material AISI 316 L
• ambient temperature +5–60°C (41–140°F) a mounting cone that is welded to the process pipeline or tank wall. • ambient temperature +5–60°C (41–140°F)
• humidity 10–100% Mounting to pipe: straight mounting cone, code H4700324. • humidity 10–100%
• process temperature max. 110°C (230°F) Mounting to tank wall: bevelled mounting cone, code H4700328, • process temperature max.+ 110°C (230°F)
• process pressure max. 6 bar (87 psi) allows sampler installation at a 45° angle. • process pressure max. 10 bar (145 psi)
SD-701/450 = A4700325 V1.1 NOTE: Apply thread sealing tape and silicone grease (e.g. Part list:
SD-701/650 = A4700300 V1.1 Molykote 111) on the screw-on sample line connections! 1. Mounting cone 3/4" .........H4700324 V1.0
SD-701/850 = A4700326 V1.1 2. Ball valve 3/4" .................256768
SD-701/1200 = A4700327 V1.1 3. Adapter 1/2"–3/4"............70102189
4. Ball valve Fujikin .............70100215
240 (9 1/2")
49 (1 15/16")
256768 H4700324 V1.0
A4700525 V1.0 45•
185 (7 1/4")
1
120 (4 3/4") 142 (5 19/32") ø48
(57/64") R1/2"
R1/2" 4
80 (3 5/32")
2 3
SD-701/450 (A4700325): 650 (25 5/8")

SD-701/650 (A4700300): 850 (33 1/2")
SD-701/850 (A4700326): 1050 (41 3/8")
SD-701/1200 (A4700327): 1400 (55 1/8”)
22 (7/8") 150 (~6")
H4700324 V1.0 H4700328 V 1.0

Total space required for pulling sampler out:
SD-701/450: ~ 995 (39”) At least ~ 130 (5") of free space
SD-701/650: ~ 1420 (56”) around sampler in all directions:
SD-701/850: ~ 1620 (64”) the sampler is installed by
SD-701/1200: ~ 1950 (77”) screwing it to the mounting cone,
so there must be enough space
Total length: for the sampler to rotate freely
SD-701/45: ~ 650 (26") around its axis during installation!
SD-701/65: ~ 850 (34")
+ extra space SD-701/85: ~ 1050 (41 1/2")
~ 250 (10") SD-701/1200: ~ 1400 (55”) ~ 320 (12 1/2")
Sufficient free space below sampler (no pipelines, racks, etc.)

to allow unhindered sample line installation Sufficient free space for
sample line installation
- minimum bend radius of sample line is 300mm (12") -- minimum bend radius
of sample line is
300mm (12")
~ 230
kajaaniALKALi – Installation - A5.3 - W4700162 V1.5 EN Manufacturer reserves the right to changes without prior notice.
kajaaniALKALi – Electric connections
Analog Connections Binary Connections Electronic board racks:
Analyzer Server Connector for
• no analog board Binary inputs: 8 opto-isolated inputs, 24–48 VDC. Communicator-i remote Communicator-i
=> no analog inputs/outputs, Meas. permits to analyzer’s channels 1…8: Bin1 =
• one analog board permit to channel 1; Bin2 = permit to channel 2, etc. connection (option)
=> 7 analog inputs, 8 analog outputs, NOTE: Signal 1 = NO meas. permit (off), signal 0 The analyzer is normally opeated
• two analog boards = meas. permit ON! using a Communicator-i terminal
=> 14 analog inputs, 16 analog outputs. Binary outputs: 8 relay outputs (1 alarm), that is plugged to the connector
opening/closing contact. 24 VDC/1A, 48 VDC/0.5A, on the rear wall of the electronics unit.
Analogia inputs: or 125VAC/0,5A. If required, remote connection cabling Electronis
0–5 VDC / 0–20 mA / 4–20 mA, isolated. • Bout1 = Alarm (closing contact, control = 0). can be used so that the Communicator-i unit
Analog inputs are connected to the lower terminals • Bout2 = Error (opening contact, control = 1), can be placed e.g. in the control room.
of the ANAL./BIO/DCS terminal strip. remains on for 25 seconds.
Analog input signal type (voltage/current) is set with • Bout3 = Service (opening contact, control = 1).
a jumper: • Bout4 = "Analysis ready" (opening contact, Modem
• jumper 1->2: voltage signal 0–5 VDC control = 1).
• jumper 2->3: current signal, software-selectable • Bout5…8 = address of meas. result A4700503 V1.0
Server
current range, default: 4–20 mA. (opening contact, control = 1). max. Communicator-i
1111 = channel 1 1011 = channel 5 350 m

(1148 ft)
External Analyzer Analog Unit 0111 = channel 2 0101 = channel 6
connections Terminal 1011 = channel 3 1001 = channel 7
0011 = channel 4 0001 = channel 8
Ain 1 When a new measurement result is ready, Bout4 Connection cable
- 250 250W opens (control = 0) and Bout5…8 indicate the result - not included in delivery.
4-20 mA address. Bout4 remains open for 60 seconds, then Terminal strips Mains Power switch Use e.g. JAMAK 4 x (2+1) x 0.5 mm2
4-20 mA 3 2 1 terminal Connection:
+ closes again and remains closed until the next result
249 0-5 VDC is ready, however for at least 60 seconds. 1 +24V
2 GND
Measurement result address changes only when Terminal Sample preparation unit Name 3 Tx+
Bout4 opens again -- i.e. each result can be read 1 Valve 1A, sample line 1 S1
4 Tx–
NOTE terminal polarity! from the analog outputs for at least 120 seconds. 5 Rx+
2 Valve 2A, sample line 2 S1 6 Rx–
3 Valve 3A, sample line 3 S1
Connector for
Connection of analog inputs to terminal strip:
4 Valve 4A, sample line 4 S1
Communicator-i
External Analyzer Measurement unit extra cable
Analog Board 1 Analog Board 2 5 Valve 5A, sampling device 1 S1
Signal Terminal Signal Terminal connections Bin1 6 Valve 6A, sampling device 2 S1
Ain1+ 249 Ain1+ 263
Ain1- 250 Ain1- 264 24…48 – 278 7 Valve 7A, sampling device 3 S1
Ain2+ 251 Ain2+ 265 VDC + 8 Valve 8A, sampling device 4 S1
Ain2- 252 Ain2- 266 277 9 Valve 9A, sample back to process S1
Ain3+ 253 Ain3+ 267
NOTE terminal polarity! 10 Valve 10A, ejector S1
1
Ain3- 254 Ain3- 268
18
Ain4+ 255 Ain4+ 269 11 Valve 11A, water in S1
Sample preparation unit 1

Ain4- 256 Ain4- 270 Bout1 12 Valve 12A, acid wash S1
Ain5+ 257 Ain5+ 271 max. 48 VDC/30W
Ain5- 258 Ain5- 272 233 13 Valve 13A, waste tank S1
Ain6+ 259 Ain6+ 273 or
234 14 Valve 14A, sedimentation inlet S1 Output signals Sample
Ain6- 260 Ain6- 274 125 VAC/0.5A 15 Valve 15A, valve between SPUs S1 BO1 preparation
Ain7+ 261 Ain7+ 275
17
- unit 1
34
Ain7- 262 Ain7- 276 16 Valve 16A, sample to titration S1
- unit 2
51
70
Binary outputs Binary inputs 17 Waste pump control valve S1
Signal Terminal Signal Terminal 33 +24V
Analog outputs: Bout1+ 233 Bin1+ 277 34 +24V
0–5 VDC / 0–20 mA / 4–20 mA, common Bout1- 234 Bin1- 278
Bout2+ 235 Bin2+ 279 Terminal Sample preparation unit Name
isolation. Bout2- 236 Bin2- 280 Input signals
Max. load RL = 600 W. Bout3+ 237 Bin3+ 281
55 Water pressure S1
BI1
Bout3- 238 Bin3- 282 56 Air pressure, SPU 1 S1
Analog outputs are connected to the upper
69
Bout4+ 239 Bin4+ 283 Waste pump
88
61 Water valve (11A) position sensor S1
terminals of ANAL./BIO/DCS terminal strip. Bout4- 240 Bin4- 284
118
63 Waste tank valve (13A) position sensor S1
101
Measurement results (EA, AA, TTA, CD%, S%, Bout5+ 241 Bin5+ 285 Waste tank
64 Sedim. vessel valve (14A) posit. sensor S1
Sample preparation unit 2

NaOH, Na2S, Na2CO3, V1…V3, pH1…pH3) Bout5- 242 Bin5- 286
Bout6+ 243 Bin6+ 287 69 Waste tank level sensor S1
can be freely configured to any of the Bout6- 244 Bin6- 288 85 +24V
analog outputs 1…16. Bout7+ 245 Bin7+ 289 Output signals
Bout7- 246 Bin7- 290 86 +24V
BO2
External Analyzer Bout8+ 247 Bin8+ 291 87 +24VGND Communicator-i extra cable
134
117
Bout8- 248 Bin8- 292 88 +24VGND
connections Terminal Analog KAJAANI compartment also includes an
151
170
Aout1 Unit Terminal Sample preparation unit Name extra connection for Communicator-i, located
101 Valve 1B, sample line 1 S2 outside the compartment, next to sample
- 102 Valve 2B, sample line 2 S2 preparation units.
Rmax = 202 103 Valve 3B, sample line 3 S2 If the compartment will not be purchased from
4-20 mA Input signals
600W + 201 104 Valve 4B, sample line 4 S2 Neles Field Controls, the Communicator-i
105 Valve 5B, sampling device 1 S2 BI2 extra cable can be ordered as option;
169
188
106 Valve 6B, sampling device 2 S2 order code A4700680 V1.0.
107 Valve 7B, sampling device 3 S2
201
249
NOTE terminal polarity!
108 Valve 8B, sampling device 4 S2 6000 mm
Connection of analog outputs to terminal strip: 110 Valve 10B, ejector S2 50 mm
11 Valve 11B, water in S2
Analog Board 1 Analog Board 2 112 Valve 12B, acid wash S2
Signal Terminal Signal Terminal 1
113 Valve 13B, waste tank S2
Aout1+ 201 Aout1+ 217
Aout1- 202 Aout1- 218 114 Valve 14B, sedimentation inlet S2
ANAL./BIO/DCS
Aout2+ 203 Aout2+ 219 116 Valve 16B, sample to titration S2 Wire connections:
Aout2- 204 Aout2- 220 133 +24V Schaltbau Marking
Aout3+ 205 Aout3+ 221 P23 pin P29 pin conn. pin (open end) Wire color
Aout3- 206 Aout3- 222 134 +24V 1 1 1 1 black
Aout4+ 207 Aout4+ 223 Terminal Sample preparation unit Name 2 2 2 2 black
Aout4- 208 Aout4- 224 3 3 3 3 black
Aout5+ 209 Aout5+ 225 156 Air pressure, SPU 2 S2 Analog 4 4 4 4 black
Aout5- 210 Aout5- 226 161 Water valve position sensor S2 5 5 5 5 black
Aout6+ 211 Aout6+ 227
inputs/outputs; 6 6 6 6 black
163 Waste tank valve (13B) position sensor S2 Binary 7 7 ground ground yel/grn
Aout6- 212 Aout6- 228
Aout7+ 213 Aout7+ 229 164 Sedim. vessel valve (14A) posit. sensor S2 inputs/outputs;
Aout7- 214 Aout7- 230 185 +24V DCS-connection
Aout8+ 215 Aout8+ 231 186 +24V
248
296
Aout8- 216 Aout8- 232

187 +24VGND
188 +24VGND
kajaaniALKALi – Installation - A5.4 - W4700162 V1.5 EN Manufacturer reserves the right to changes without prior notice.
kajaaniALKALi Serial communication
Electronic board racks:

Analyzer Server PC-connection with RS-converters to the DCS-terminals
Serial Communication
ANAL./BIO/DCS
Serial communication cabling must be made using shielded instrumentation cable. Maximum 169 201 248
cable length is < 300 m (984 ft). Connect the PC and modem to the electronics unit (motherboards
"Analyzer" & "Server") as instructed below.
188 249 296
(A) = RS-485/RS-232 converter

Westermo MA-42
DCS, Modbus Positions of DIP switches in RS-485/232
DCS-communication is connected to the terminal strip in the bottom of the electronics unit. converter (Westermo MA-42)
Protocol: RS-485, 4-wire. Modbus protocols 3 and 4 are available. S3 S2
2-pair cable 1 6 1 6
(max. 1200 m)
Signal Terminal On (1)
Modem Off (0)
TxD_A 293
TxD_B 294 RS-485 cable RS-485/232
10 11 00 001 000
RxD_A 295 (251801, option) converter
RxD_B 296 (251723, option)
GND yel/grn
RXD 2 2 2 R- 293 TxD_A

Modem PC 1 R+
The modem is factory-connected to the D9-connector MODEM on Server motherboard. TXD 3 3 294 TxD_B
D9 conn. GND 5 7 4 T- 295 RxD_A
Protocol: RS-232. Connect the telephone line to modems connector LINE. 3 T+ Analyzer
The receiving end must have a PC + modem and the ALKALi Tool software installed. Terminal strips Mains Power switch 296 RxD_B terminal strip
Use Modbus Float protocol for the analyzers modem port. terminal (A)
Direct PC-connection
Connect a PC to the D9-connector PC
located on the "Server" motherboard.
Protocol: RS-232.
A standard KAJAANI PC-cable
(order code A4500382 V1.0)
can be used for the connection.
Signal connections of the PC-connector: PC Modem
Pin Signal Communi-

cator-i
1 NC Server
2 RxD PC-connection
3 TxD D9; female whi blu D9; female
4 NC RxD 2 blu whi 2
5 GND TxD 3 bro bro 3
GND 5 5
6 NC RTS 7
7 NC CTS 8 NOT IN USE
8 NC D25; female whi whi D25; male
9 NC TxD 2 blu blu 2
RxD 3 bro bro 3
GND 7 7
RTS 4
CTS 5
3m
A4500382 V1.0
RS232 CABLE
Metso Automation
Field Systems Division
Kehräämöntie 3, PO Box 177
FIN-87101 Kajaani, Finland
Tel. +358 (0)2048 3120
Fax +358 (0)2048 3121
www.metsoautomation.com
This document discloses subject matter in

which the manufacturer has proprietary
rights. Neither receipt nor possession
thereof confers or transfers any right to
reproduce or disclose the document, any
part thereof, any physical article or device,
except by written permission from the
manufacturer. Manufacturer reserves the
right to alter the contents of this document
without prior notice.
Modbus is the trademark of Modicon Inc.
Copyright © August 2000.

Metso Automation Inc., Field Systems Division.
Documentation: Päivi Häätylä.
Translation: Marjo Nygård.

W4700162 V1.5 EN - AlkaliCAU Installation

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W4700162 V1.5 EN - AlkaliCAU Installation

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kajaaniALKALi™

kajaaniALKALi  Installation - TOC - W4700162 V1.5 EN

Follow the applicable safety regulations

First Aid measures

Seek medical advice immediately if

F After ingestion of chemical

F After contact with eyes

F After inhaling a chemical

During installation, maintenance and service operations,

! remember that the sample line may contain hot sample

The chemical vapors released during titration are

! hazardous when inhaled!

Never run the pump unit dry –

When installing or servicing the sample lines,

! always wear appropriate protective clothing to

Always check that the incoming voltage & frequency

kajaaniALKALi CAUTION / WARNING

1.C. Sample Preparation

kajaaniALKALi – Installation - 1.1 - W4700162 V1.5 EN

Analysis water tank

Hydrochloric acid tank

Sample unit Measurement unit

kajaaniALKALi  Installation - 2.1 - W4700162 V1.5 EN

Sample unit Measurement unit

Fig. 2.2. Location of the fastening bolts, for cabinet model.

Fig. 2.3. Installation space required for the cabinet model.

kajaaniALKALi – Installation - 2.2 - W4700162 V1.5 EN

kajaaniALKALi – Installation - 2.3 - W4700162 V1.5 EN

The door mechanism of the electronics unit can be

Electronic board racks:

Terminal strips Mains terminal Power switch

Fig. 3.1. Electronics unit, with front door opened.

3.B. Operating Voltage

Lead the operating power cables into the analyzer

Fig. 3.2. Operating power connection.

kajaaniALKALi – Installation - 3.1 - W4700162 V1.5 EN

18 34 70 88 118 134 170 188 249 296

Fig. 3.3. Connections at the terminal strip.

kajaaniALKALi – Installation - 3.2 - W4700162 V1.5 EN

Depending on the system, the “Server” board rack may

Analog inputs: Analog outputs:

External Analyzer Analog Unit External Analyzer

NOTE terminal polarity! NOTE terminal polarity!

Analog Board 1 Analog Board 2 Analog Board 1 Analog Board 2

kajaaniALKALi – Installation - 3.3 - W4700162 V1.5 EN

kajaaniALKALi – Installation - 3.4 - W4700162 V1.5 EN

Serial communication cabling must be made using

3.F.1. DCS, Modbus

3.F.2. Modem connection

Signal connections of the PC-connector:

kajaaniALKALi – Installation - 3.5 - W4700162 V1.5 EN

188 249 296

(A) = RS-485/RS-232 converter

RXD 2 2 2 R- 293 TxD_A

Fig. 3.9. Connecting a PC to analyzers DCS-connection with RS-converter.

3.G. Communicator-i Remote Connection (option)

Fig. 3.11. Communicator-i remote connection.

kajaaniALKALi  Installation - 3.6 - W4700162 V1.5 EN

The compartment model analyzer also includes an extra

kajaaniALKALi  Installation - 3.7 - W4700162 V1.5 EN

4.A. Analysis Water 4.B. Flushing Water

700 (27 1/2")

Fig. 4.1. Connections of sample unit, cabinet model.

kajaaniALKALi Installation - TOC - W4700162 V1.5 EN

kajaaniALKALi Installation - 2.1 - W4700162 V1.5 EN

Fig. 3.9. Connecting a PC to analyzers DCS-connection with RS-converter.

kajaaniALKALi Installation - 3.6 - W4700162 V1.5 EN

kajaaniALKALi Installation - 3.7 - W4700162 V1.5 EN

kajaaniALKALi Installation - 4.4 - W4700162 V1.5 EN