05523SiteInvestigationSamsClub08 12 2014

Lim
mited
d Sitte Inv
vestigatio
on
Propose
ed Sam’s
s Club # 4
4062
Alc
coa Highw
way,
Alco
oa, Bloun
nt County
y, Tennes
ssee
A
August 12, 2
2014
Terraccon Project No.: E2137
7034
Prepared
d for:
Ca
arlson Con
nsulting E
Engineers, Inc.
Bartlettt, Tennesssee
Prepared
d by:
Terrracon Con
nsultants, Inc.
Chattanoogaa, Tennesssee
TABLE OF CONTENTS
1.0 INTRODUCTION ................................................................................................................. 1

1.1 Standard of Care ....................................................................................................... 1
1.2 Additional Scope Limitations ..................................................................................... 1
1.3 Reliance .................................................................................................................... 2
2.0 SAMPLE COLLECTION ..................................................................................................... 2
2.1 Soil Sample Collection .............................................................................................. 2
2.2 Temporary Groundwater Monitoring Wells ................................................................ 3
2.3 Soil-Gas Sampling Points.......................................................................................... 4
3.0 LABORATORY ANALYTICAL AND RESULTS ................................................................ 4
3.1 Laboratory Analytical Program .................................................................................. 4
3.2 Soil Analytical Results ............................................................................................... 5
3.3 Groundwater Analytical Results ................................................................................ 5
3.4 Soil Gas Analytical Results ....................................................................................... 5
4.0 CONCLUSIONS AND RECOMMENDATIONS .................................................................. 6
4.1 Conclusions ............................................................................................................... 6
4.2 Recommendations .................................................................................................... 6
LIST OF APPENDICES
Appendix A Exhibits
Appendix B Soil Boring Logs
Appendix C Tables and Laboratory Analytical Reports

LIMITED SITE INVESTIGATION
PROPOSED SAM’S CLUB #4062
ALCOA HIGHWAY
ALCOA, BLOUNT COUNTY, TENNESSEE
Terracon Project No. E2137034
1.0 INTRODUCTION
Terracon Consultants, Inc. (Terracon) has completed a Limited Site Investigation (LSI) at the
proposed Sam’s Club #4062 site located on the east side of Alcoa Highway US129/Route 155
and south of Mills Street in Alcoa, Blount County, Tennessee (site). The location of the site is
illustrated on Exhibit 1 in Appendix A. The general layout of the site and the soil boring
locations are illustrated on Exhibit 2 in Appendix A. Soil boring logs are presented in
Appendix B. Tables summarizing the analytical results and the laboratory analytical reports are
provided in Appendix C.
Terracon’s LSI activities were performed in accordance with our contractor services agreement
with Carlson Consulting Engineers and Terracon’s proposal dated June 12, 2014. The purpose
of the LSI activities was to evaluate subsurface conditions with respect to a recognized
environmental condition (REC) identified at the site during Terracon's Phase I Environmental
Site Assessment (ESA) dated June 4, 2013 (Terracon Project No. E2137034). The results of
the ESA reported the following REC associated with the site:
 The south-adjoining former Alcoa West Plant facility, particularly Landfill WPA which
adjoins the site to the immediate southeast corner.
1.1 Standard of Care
This LSI was performed in accordance with generally accepted practices of this profession,
undertaken in similar studies at the same time and in the same geographical area. We have
endeavored to meet this standard of care, but may be limited by conditions encountered during
performance, a client-driven scope of work, or inability to review information not received by the
report date. Where appropriate, these limitations are discussed in the text of the report, and an
evaluation of their significance with respect to our findings has been conducted.
1.2 Additional Scope Limitations
Findings, conclusions and recommendations resulting from these services are based upon
information derived from the on-site activities and other services performed under this scope of
work; such information is subject to change over time. Certain indicators of the presence of
hazardous substances, petroleum products, or other constituents may have been latent,
inaccessible, unobservable, nondetectable or not present during these services, and we cannot
represent that the site contains no hazardous substances, toxic materials, petroleum products,
or other latent conditions beyond those identified during this LSI. Subsurface conditions may
vary from those encountered at specific borings or wells or during other surveys, tests,
Responsive ■ Resourceful ■ Reliable 1

Limited Site Investigation
Proposed Sam’s Club #4062 ■ Alcooa Highway
Alcoa, Tennessee ■ Te
erracon Proje
ect No.: E2137
7034

assessm ments, investtigations or exploratory
e services;
s the
e data, interrpretations, findings, and our
recomme endations arre based solely upon datta obtained at the time a and within th
he scope of tthese
services.. The scope e of work was intended to determine e if constituents of conceern are preseent at
the locations sample ed and was not intended d to delineatte impacts identified or to develop costs
for correc
ctive action, if warranted
d.
1.3 Reliance
This repo ort can be re

elied upon by, b and has been
b preparred for the e exclusive usee of the follo
owing
entities: Carlson
C Connsulting Engineers, Inc., a Tennesse ee corporatio on, Wyatt, T
Tarrant & Co ombs,
LLP, a Kentucky
K limiited liability partnership,
p and Sam's Real Estate e Business TTrust, a Dela aware
statutory trust, and th
heir respective successo ors, assigns,, affiliates, a
and subsidiaries.
Any auth horization for use or reliance by an ny other partty (except a governmen ntal entity ha
aving
jurisdictio
on over the site) is proh
hibited without the expre
ess written a
authorization
n of these paarties
and Terrracon. Any
A unautho orized distrribution or reuse is at the client’s sole risk.
Notwithstanding the foregoing, reliance by y authorized
d parties will be subje ect to the teerms,
conditionns and limittations stateed in Terrac con's contra
actor services agreeme ent with Ca arlson
Consultin ng Engineerss.
2.0 SA
AMPLE COLLECTION
N
The obje ective of this

s LSI was to o evaluate on-site
o soils , soil gas, a
and groundw water for impacts
resulting from potential releases s associated d with the foormer operattion of the A Alcoa West Plant
facility, particularly
p Landfill WPAA which adjoins the site tto the imme ediate southeeast corner. The
LSI was conducted in conjunctio on with a ge eotechnical investigation that was ccompleted a at the
site. The e geotechnic cal investigattion is refere
enced as Te erracon Proje ect Number E2135031 a and is
submitted d as a sepa arate cover. The soil boring
b locatiions, monito oring well lo
ocations, and d soil
vapor sa ampling poin nts are illustrated on Ex xhibit 2 in Apppendix A. The soil bo oring logs fo
or the
geotechn nical investiggation are denoted
d as B-1
B thru B-5 57 and are p provided in the geotech hnical
report. The
T soil borin ng logs for th
he environm mental investtigation are d denoted as MMW-1 thru M MW-4
and B-15 5. The soil borings dem moted as MW W-1 thru MW W-4 are loccated in the proposed S Sam’s
Club building footprint. The so oil boring de enoted as B -15 is locate ed in the prroposed gassoline
service station
s and iss referencedd as a base line environ nmental borin ng location. The boring g logs
for MW-1 1 thru MW-4 and B-15 are provided in Appendixx B of this report.
2.1 Soil Sample Collection

C
Drilling was
w performed using sta andard drilling procedurres to advance each boring and ccollect
subsurfacce soil samples. Fifty-s
seven (57) geotechnica
g al soil boring
gs were advvanced within the
proposed d building an
nd parking lot
l areas. Four
F (4) envvironmental soil boringss were adva
anced
Responsive ■ Resourrceful ■ Relia

able 2
erracon Proje
ect No.: E2137
7034

within the
e proposed building
b foot print and aloong the nortthern bounda ary of Landffill WPA to deepths
ranging from
f 45 feet below groun nd surface (bgs) to 61 fe eet bgs. So oil boring B-115 was adva anced
within the
e proposed UST
U tank pit location for the propose
ed gasoline sservice statioon and termin nated
at 20 feeet bgs. Soil samples we ere collected at 2.5 feet iintervals in tthe upper ten 10 feet of each
boring and every fiv ve feet therreafter. Soil samples w were examiined by onssite personn nel to
documen nt soil types
s, color, rela
ative moisturre content, a and evidencce of chemiical or petro oleum
impact. In addition, each soil sa ample was split
s and a pportion of thhe soil samp ple was colleected
into a new, dedicatted containe er for heads space scree ening analyysis using a an organic vvapor
analyzer (OVA) photto ionization detector (PID) to detecct the presen nce of volatille organic va
apors
(VOVs).
The soil OVA screenning results for the environmental ssoil borings are provided d in the atta
ached
boring loogs (Appenddix B). The e soil OVA screening rresults for tthe geotech hnical boringg are
provided in the geottechnical rep port. In summmary, the highest OVA A concentraation (5 partts per
million [p
ppm]) was measured
m att 6 to 7.5 feet bgs at booring locatio
on MW-4. S Soil boring MMW-1
had a OVA concenttration of 2 ppm at 23.5 to 25 fee t bgs. VOV Vs were nott detected in the
remaining soil samplles from the soil borings s (B-1 thru B
B-57 and MW W-1 through MW-4). The soil
samples did not exhhibit obvious s indicationss of impact (odors, staiining, free p
product, elevvated
OVA readings) in any y of the geottechnical or environmen ntal soil samples.
Based on n the field screening

s res
sults, future development plans of the site, and d the most likely
environm mental impac ct of the forrmer Alcoa WPA Landfiill, four soil samples we ere submitte ed for
laboratorry analysis. The four sa amples subm mitted are iddentified as MW-1 (53.5 5' - 54.5'), M
MW-2
(28.5' - 30.0'),
3 MW-3 3 (38.5' - 40
0.0'), and MW W-4 (28.5' - 30.0'). MW W-1 is locatted in the ce entral
portion of
o the propos sed building, MW-2 is lo ocated in the e southern mmost cornerr of the prop posed
building, MW-3 is loc cated in the middle of the southern n rear wall o
of the propossed building, and
MW-4 is located in th he eastern most
m corner of the propoosed buildingg. The four ssoil samples were
submitted d for laboraatory analyssis of VOCs s, SVOCs, PCBs, and Metals (alu uminum, ba arium,
chromium m, copper, irron, lead, magnesium,
m mercury,
m nicckel, and zin
nc). In addition one sample,
identified as B-15 (18.5’
( - 20’)) was subm mitted for la
aboratory an nalysis of be enzene, toluuene,
ethylbenz zene, and xyylene (BTEX X).
The inve
estigation derived waste (IDW) was transferred into 55-gallo
on drums fo
or storage. T
These
drums weere then labe
eled and left on-site for proper
p dispossal.
2.2 Tem
mporary Grroundwater Monitoring
g Wells
Upon completion of the soil sam

mpling activitties, the fourr soil borings (denoted a as MW-1, M MW-2,
MW-3, and MW-4) were w converrted to temp
porary groun ndwater mon nitoring wells to facilitatte the
collection
n of groundwater sam mples. Th
he temporarry groundwa ater monitooring wells were
constructted as follows:

able 3
erracon Proje
ect No.: E2137
7034

 In
nstallation of 2-inch diameter, 0.010-inch machine e slotted PVC
C well screeen with a thre
eaded
bottom cap;
 nstallation of 2-inch diameter, threade
In ed, flush-joint PVC riser p
pipe to surfacce;
 Addition
A e-sieved 20//40 grade silica sand for a
of pre annular sandd pack aroun nd the well sccreen
frrom the botto
om of the borring to appro
oximately 2-fe eet above the top of the w
well screen; and
 Placement
P of an approxim
mate 2-feet thhick bentonitee seal.
The temp porary grounndwater mon nitoring wells were purged of approximately three e casing volu
umes.
A ground dwater samp ple was colle ected using a new dedicated disposable bailer. Samples were
placed directly into la
aboratory prrovided conttainers, were e immediate ely placed on ice in a co
ooler,
and ship pped to the e laboratory y using cha ain-of-custod
dy procedures. The p purge water was
transferre
ed into 55-ggallon drums s, then labeeled and leftt on-site forr proper disposal. Afteer the
groundwa ater samplinng activities was
w completted, the temporary moniitoring wells were aband doned
by comp pletely remooving the we ell casing and
a screen from the bo ore holes a
and finishing
g the
boreholee to match the surroundin ng surface.
2.3 Soil-Gas Sampling Points

s
Five soil--gas samplinng points (deenoted as SG-1,

S SG-2, SG-3, SG-4 4, and SG-5 5) were adva anced
within the
e proposed building
b footpprint to an appproximate ddepth of 3-feeet for purpooses of colle
ecting
soil gas samples.
s Upon advanc cement of the soil boring g a stainlesss steel scree
en was place ed on
the end of nylon tub bing and lowwered to witthin approxi mately 6-incches from th he bottom o of the
boring. Filter
F sand was
w placed around
a the stainless stee
el screens too within 1-fo
oot of the surrface.
The rema ainder of the
e boring wass backfilled with
w hydrate d bentonite.. The well sscreen and tu ubing
was then n purged of at e volumes of air prior to collecting soil gas samp
a least three ples in laborratory
provided summa canisters. Th he soil gas sampling
s po
oints were a abandoned by removing g the
tubing annd finishing the
t borehole e to match th he surroundi ng surface.
3.0 LA
ABORATOR
RY ANALY
YTICAL AND RESULT
TS
3.1 boratory An
Lab nalytical Pro
ogram
The fourr soil samples and the e four groun ndwater sam mples from MW-1 thro ough MW-4 were
submitted
d to Test Am merica Labo oratories in Nashville,
N T ennessee fo or analysis o
of VOCs by EPA
Method 8260B, SVO OCs by EP PA Method 8270C, PC Bs by EPA A Method 80 082, and m metals
m, barium, chromium,
(aluminum c co
opper, iron, lead, magne esium, mercury, nickel, aand zinc) byy EPA
Methods 6010B/7471A. In addition, one so oil sample ffrom B-15 w was submitteed for analyssis of
BTEX by y EPA Meth hod 8260B. The five soil gas sam mples within the propose ed building were
d to Eurofins – Air Toxics in Folsom, California
submitted a for analyssis of VOCs by EPA Me ethod
TO-15. Please
P referr to Appendix
x C for the la
aboratory an
nalytical repoorts and sum
mmary tabless.

able 4
erracon Proje
ect No.: E2137
7034

3.2 Soil Analytica
al Results
VOCs, SVOCs,
S and PCBs were e not detecteed at conce entrations ab bove the labboratory repoorting
limit in th
he soil sampples analyzeed from borings MW-1 thru MW-4. In addition n, BTEX wa as not
detected above the laboratory
l re
eporting limiit in the soil sample ana alyzed from boring B-15 5. As
summarized in Table e 1, aluminum, barium, chromium,
c coopper, iron, lead, magneesium, nickell, and
zinc were e detected in the four soil samples at concen ntrations above the laboratory repo orting
limit, butt below the EPA Industrial Soil RSLs. Mercurry was not d detected in the soil sam
mples
collectedd.
3.3 Gro
oundwater Analytical
A Results
R
Groundwwater contam
minant concentrations were
w compa red to the EEPA Maximum Contam minant
Levels (M
MCLs) where
e available. When MCL Ls are not a
available con
ntaminant co
oncentration
ns are
compared to the EPA
A Tap Waterr RSL Value.
With the exception of Tetrachloro

oethene, the
e groundwatter samples collected fro
om MW-1, MMW-2,
MW-3, anda MW-4 were below w laboratoryy detection levels for V
VOCs, SVO OCs, and PPCBs.
Tetrachlooroethene exceeded
e th
he May 201 14 EPA MC CL Value in
n the groun ndwater sam
mples
collected
d from boring
g locations MW-1,
M MW-2, and MW--4. Tetrachlloroethene w was not dete
ected
in the gro
oundwater sample colleccted from bo
oring location
n MW-3.
As indica
ated in Table
e 2, several metals were
e detected a
at concentraations above
e the MCL a
and/or
Tap Wateer RSL in ea
ach of the grroundwater samples
s colllected from MW-1 thru M
MW-4.
3.4 Soil Gas Analy

ytical Results
Soil gas analytical results were compared to the May 2014 Enviro onmental Protection Ag gency
(EPA) Re egional Scre eening Leveels (RSLs) foor indoor air in residential and indusstrial settings. In
order to simulate th he concentrrations of so oil gas insid de of the p proposed on nsite buildin
ng an
attenuation factor off 0.03 has been
b adoptedd by TDEC to present a conservattive evaluation of
potential soil vapor impacts to thhe indoor airr of the onsiite building. For examp ple, the EPAA RSL
3
(H.Q.-0.11) for aceton
ne concentra ations in industrial indooor air is 14,0
000 ug/m . If the attenuuation
factor of 0.03 is applied to the cu
urrent EPA RSLs
R for ind
door air, then
n the accepttable shalloww soil
gas conc centration for acetone would be 466 6,667 ug/m3. Terracon u used this meethod to estaablish
the approopriate screeening levels of the VOCs s detected inn the shalloww soil gas.
As indica
ated in Tablee 3, none off the soil gas
s sample va
alues exceed
ded the Mayy 2014 EPA
A RSL
for Resid
dential Indoo
or Air where established..

able 5
erracon Proje
ect No.: E2137
7034

4.0 CO
ONCLUSIONS AND RECOMMEN
R NDATIONS
S
4.1 Conclusions
Based on
o the findin ngs of this LSI, it appeears that su
ubsurface m media at thee site have been
impacted
d by release es from the former Alco oa West Plaant facility an
nd associateed Landfill W
WPA.
Several metals
m were e detected in
n the soil sa
amples at co
oncentrationss above the e residential RSL,
but below the Industrial RSL. Tetrachloro oethene wass detected in 3 of the e 4 groundw water
samples at concentrrations abov ve the MCL. Several m metals were detected in the groundw water
samples at concenttrations abo ove the MC CL and/or TTap Water RSL. Seve eral VOCs were
detected in the soil gas
g samples at concentrrations below w the EPA R RSL for residential indoor air.
4.2 Recommenda
ations
Based on n the scope of services and limitatio assessment, Terracon rrecommendss that
ons of this a
the site be entered into the Bro ownsfield prrogram and the propertty owner sh hould file a deed
he use of groundwater
restriction against th g for potablee purposes. In addition n, Terracon also
recomme ends that th
he eight 55-gallon drumms of soil cuttings and o one 55-gallo
on drum of ppurge
water generated duriing this LSI be properly disposed. F For construcction purposes, the soilss may
be managed on-site. Further inve estigation is needed if so
oils will be tra
ansported offf-site.

able 6


APPENDIX A
EXHIBITS
Site Location
This figure copied from USGS 7.5 minute Quadrangle

Maps: Maryville (1979), Tennessee
Project Manager: Project No.
TTS E2137034 Topographic Map Exhibit
Drawn By: Scale:
JIM 1” = 2,000’ Proposed Sam’s Club #4062
Checked By: File Name:
Approved By:
TTS N:\Projects\2013
Date: 51 Lost Mound Drive, Suite 135 Chattanooga, TN 37406
Alcoa Highway
Alcoa, Blount County, Tennessee 1
DEW 4/12/13 PH. (423) 499-6111 FAX. (423) 499-8099
Geotechnical Soil Boring
Temporary Monitoring Well
Soil-Gas Sampling Point
B-26 B-14
B-13
B-25
B-24 B-16
B-22 B-23 B-27
B-15
B-21 B-28
B-34 B-29 B-30
B-32 B-33
B-31
B-35
B-36 B-41 B-42 B-43

B-37 B-38 B-39 B-40
B-44
B-1 B-2 B-3 B-4
B-20
SG-1
B-45 B-46
SG-2 B-47
B-5
MW-1
B-8 B-48 B-49
B-6 B-7
B-19
B-50
B-51
B-53 B-52
SG-3 B-54
MW-2 MW-3 MW-4 B-55
B-9 SG-4 B-10 B-11 SG-5 B-12
B-18
B-56
Landfill WPA
B-17 B-57
BASE DRAWING PROVIDED BY CLIENT

DIAGRAM IS FOR GENERAL LOCATION ONLY, AND IS NOT
INTENDED FOR CONSTRUCTION PURPOSES
Project Manager: Project No.

BWW E2137034 Site Map Exhibit
Drawn By: Scale:
BWW 1” = 2,000’ Proposed Sam’s Club #4062
Checked By: File Name:
Approved By:
DEW N:\Projects\2013
Date: 51 Lost Mound Drive, Suite 135 Chattanooga, TN 37406
Alcoa Highway
Alcoa, Blount County, Tennessee
2
PH. (423) 499-6111 FAX. (423) 499-8099
DEW 07/01/14


APPENDIX B
BORING LOGS
WELL LOG NO. MW-1 Page 1 of 2
PROJECT: Sams Club Alcoa, TN CLIENT: Carlson Consulting Engineers
Bartlett, TN
SITE: Alcoa Highway Site
Alcoa, Tennessee
LOCATION See Exhibit A-2 INSTALLATION DETAILS
OBSERVATIONS
SAMPLE TYPE
RECOVERY (%)
SAMPLE SENT
GRAPHIC LOG
WATER LEVEL
(ID NUMBER)
DEPTH (ft)
TO LAB
OVA/PID
(ppm)
Well Completion:
DEPTH MATERIAL DESCRIPTION

0.3 TOPSOIL
SANDY LEAN CLAY (CL), brown, stiff to very stiff
75 0
3.0
FAT CLAY WITH SAND (CH), brown to yellow, very stiff to hard
50 0
THIS BORING LOG IS NOT VALID IF SEPARATED FROM ORIGINAL REPORT. ENVIRONMENTAL SMART LOG E2137034 SAMS CLUB ALCOA, TN.GPJ ENV STANDARD 2012.GDT 8/11/14
5
soft to medium stiff, at 6'
50 0
8.0
SANDY FAT CLAY (CH), yellow to reddish-brown, medium stiff to stiff
75 0
10
12.0
SANDY SILT (ML), medium brown, very stiff, weathered shale
100 0
15
17.0
SANDY SILT (ML), trace gravel, olive-brown, hard, weathered shale
50 0
20
2" diameter PVC.

Flush threaded
joints with 100 2
O-rings.
25
100 0
30
The stratification lines represent the approximate transition between differing soil types and/or rock types;
in-situ these transitions may be gradual or may occur at different depths than shown.
Advancement Method: Notes:

Hollow Stem Augers
See Report for description of field procedures.
See Report for description of laboratory procedures and additional
data (if any).
Abandonment Method:
Borings backfilled with cement-bentonite grout upon
completion.
WATER LEVEL OBSERVATIONS Well Started: 6/30/2014 Well Completed: 6/30/2014

Encountered groundwater at 54.5'
Drill Rig: DR009 Driller: J. Reinert
Groundwater rose to 51.05' after 22.5 hours
51 Lost Mound Drive, Suite 135
Chattanooga, Tennessee Project No.: E2137034
Bartlett, TN
Alcoa, Tennessee
LOCATION See Exhibit A-2
OBSERVATIONS
SAMPLE TYPE
RECOVERY (%)
SAMPLE SENT
GRAPHIC LOG
WATER LEVEL
(ID NUMBER)
DEPTH (ft)
TO LAB
OVA/PID
(ppm)
SANDY SILT (ML), trace gravel, olive-brown, hard, weathered shale (continued)
100 0
35
37.0
SANDY SILT (ML), trace gravel, brown, very stiff to hard, weathered shale
100 0
40
100 0
45
Sand
0 0
50
75 0 MW-1
(53.5'-54.5')
55
2" diameter PVC
wtih 0.010" slots
100 0
60
61.0
Auger Refusal at 61 Feet

Hollow Stem Augers
Abandonment Method:
completion.

Encountered groundwater at 54.5'
Groundwater rose to 51.05' after 22.5 hours
Bartlett, TN
Alcoa, Tennessee
OBSERVATIONS
SAMPLE TYPE
RECOVERY (%)
SAMPLE SENT
GRAPHIC LOG
WATER LEVEL
(ID NUMBER)
DEPTH (ft)
TO LAB
OVA/PID
(ppm)
Well Completion:

0.3 TOPSOIL
LEAN CLAY WITH SAND (CL), brown, stiff, with manganese noddles
75 0
3.0
FAT CLAY WITH SAND (CH), reddish-brown, very stiff to hard
75 0
5.0
SANDY LEAN CLAY (CL), yellow to reddish-brown, stiff to very stiff, weathered
5
shale
100 0
8.0
SANDY SILT (ML), yellow brown to reddish-brown, very stiff, weathered shale
100 0
10
12.0
SANDY SILT (ML), light brown to yellow, hard, weathered shale
100 0
15
17.0
SANDY LEAN CLAY (CL), light olive to dark brown, very stiff, weathered shale
2" diameter PVC.
Flush threaded
joints with 100 0
O-rings.2
20
22.0
SANDY SILT (ML), trace gravel, light olive, hard, weathered shale
100 0
25
100 0 MW-2 (
28.5'-30.0')
30
32.0
SANDY LEAN CLAY (CL), medium brown, very stiff, weathered shale

Hollow Stem Augers
data (if any).
Abandonment Method:
completion.

Encountered groundwater at 34'
Groundwater rose to 38.25' at 1:15pm on 7-1-14
Bartlett, TN
Alcoa, Tennessee
OBSERVATIONS
SAMPLE TYPE
RECOVERY (%)
SAMPLE SENT
GRAPHIC LOG
WATER LEVEL
(ID NUMBER)
DEPTH (ft)
TO LAB
OVA/PID
(ppm)
SANDY LEAN CLAY (CL), medium brown, very stiff, weathered shale (continued)
100 0
35
Sand
- trace gravel at 38.5'

0 0
40
2" diameter PVC 45

with 0.010" slots
50
53.0

Hollow Stem Augers
Abandonment Method:
completion.

Groundwater rose to 38.25' at 1:15pm on 7-1-14
Bartlett, TN
Alcoa, Tennessee
OBSERVATIONS
SAMPLE TYPE
RECOVERY (%)
SAMPLE SENT
GRAPHIC LOG
WATER LEVEL
(ID NUMBER)
DEPTH (ft)
TO LAB
OVA/PID
(ppm)
Well Completion:

SANDY SILT (ML), trace gravel, light brown to yellow, hard, weathered shale
50 0
100 0
5
reddish-brown to brown, at 6'
100 0
100 0
10
light olive, at 13.5'

75 0
15
2" diameter PVC.

Flush threaded
joints with 75 0
O-rings.
20
22.0
SANDY SILT WITH GRAVEL (ML), light olive, very stiff to hard, weathered shale
75 0
25
75 0
30

Hollow Stem Augers
data (if any).
Abandonment Method:
completion.

Groundwater rose to 42.2' at 1:40pm on 7/1/14
Bartlett, TN
Alcoa, Tennessee
OBSERVATIONS
SAMPLE TYPE
RECOVERY (%)
SAMPLE SENT
GRAPHIC LOG
WATER LEVEL
(ID NUMBER)
DEPTH (ft)
TO LAB
OVA/PID
(ppm)
SANDY SILT WITH GRAVEL (ML), light olive, very stiff to hard, weathered shale
(continued) 75 0
35
Sand
100 0 MW-3
(38.5'-40.0')
40
42.0
LEAN CLAY WITH SAND (CL), dark brown, medium stiff to stiff, weathered shale
100 0
45
2" diameter PVC

with 0.010" slots
50
55
56.0

Hollow Stem Augers
Abandonment Method:
completion.

Bartlett, TN
Alcoa, Tennessee
OBSERVATIONS
SAMPLE TYPE
RECOVERY (%)
SAMPLE SENT
GRAPHIC LOG
WATER LEVEL
(ID NUMBER)
DEPTH (ft)
TO LAB
OVA/PID
(ppm)
Well Completion:

0.3 TOPSOIL
SANDY LEAN CLAY (CL), brown, stiff to very stiff
75 0
3.0
FAT CLAY WITH SAND (CH), reddish-brown to yellow, very stiff to hard
50 0
5.0
5
SANDY SILT (ML), yellow brown to light brown, stiff to very stiff, weathered shale
100 5
75 0
10
2" diameter PVC.

Flush threaded
100 0
joints with 15
O-rings.
100 0
20
100 0
25
27.0
SANDY SILT (ML), trace gravel, light olive, hard, weathered shale
Sand
75 0 MW-4
(28.5'-30.0')
30
32.0
SANDY LEAN CLAY (CL), medium brown, stiff, weathered shale

Hollow Stem Augers
data (if any).
Abandonment Method:
completion.

Bartlett, TN
Alcoa, Tennessee
OBSERVATIONS
SAMPLE TYPE
RECOVERY (%)
SAMPLE SENT
GRAPHIC LOG
WATER LEVEL
(ID NUMBER)
DEPTH (ft)
TO LAB
OVA/PID
(ppm)
SANDY LEAN CLAY (CL), medium brown, stiff, weathered shale (continued)
100 0
35
37.0
SANDY LEAN CLAY (CL), trace gravel, light brown, weathered shale
2" diameter PVC

with 0.010" slots
40
45.0
45

Hollow Stem Augers
Abandonment Method:
completion.

BORING LOG NO. B-15 Page 1 of 1
Bartlett, TN
Alcoa, Tennessee
OBSERVATIONS
LOCATION
RECOVERY (%)
SAMPLE TYPE
See Exhibit A-2
SAMPLE SENT
GRAPHIC LOG
WATER LEVEL
(ID NUMBER)
DEPTH (ft)
OVA/PID
TO LAB
(ppm)
FAT CLAY (CH), reddish-brown, stiff to very stiff
100 0
100 0
5.0
FAT CLAY WITH SAND (CH), reddish-brown, stiff to very stiff
5
100 0
medium stiff to stiff, at 8.5'

100 0
10
75 0
15
17.0
SANDY LEAN CLAY (CL), yellow, soft to medium stiff, weathered shale
100 0 B-15
20.0
Boring Terminated at 20 Feet
20

Hollow Stem Augers
data (if any).
Abandonment Method:
Borings backfilled with soil cuttings upon completion.
WATER LEVEL OBSERVATIONS Boring Started: 6/1/2014 Boring Completed: 6/1/2014

No free water observed


APPENDIX C
TABLES
and
LABORATORY ANALYTICAL REPORTS
Table 1
Soil Analytical Summary
Project Number: E2137034
Proposed Sams Club #4062, Alcoa, TN
Sample ID MW‐1 MW‐2 MW‐3 MW‐4

Collect Date 6/30/14 6/30/14 6/30/14 6/30/14
Sample Depth 53.5' ‐ 54.5' 28.5' ‐ 30.0' 38.5' ‐ 40.0' 28.5' ‐ 30.0'
EPA RSL EPA RSL
2014 2014
Parameter Units Residential Industrial Value Value Value Value
Screening Screening
Levels Levels
Metals
Aluminum mg/kg 7,700 110,000 6,350 7,850 8,890 10,800
Barium mg/kg 1,500 22,000 34.0 42.6 41.1 30.5
Chromium mg/kg 12,000 180,000 16.7 11.2 16.6 7.46
Copper mg/kg 310 4,700 23.7 15.3 19.0 16.8
Iron mg/kg 5,500 82,000 14,300 16,300 16,000 23,100
Lead mg/kg 400 800 5.54 8.94 6.98 17.1
Magnesium mg/kg 180 2,600 2,400 1,570 2,260 474
Nickel mg/kg 150 2,200 22.6 22.7 23.1 16.5
Zinc mg/kg 2,300 35,000 18.5 30.1 29.8 15.7
Note: For clarity only detected analytes are shown.
EPA RSL- EPA Risk-Based Assessment Regional Screening Levels - HQ 0.1, last updated May 2014
Detected Value Exceeding EPA Residential RSL Values HQ - 0.1
Detected Value Exceeding EPA Industrial RSL Values - HQ 0.1
NE - Screening Levels Not Established
Page 1 of 1
Table 2
Groundwater Analytical Summary
Sample ID MW‐1 MW‐2 MW‐3 MW‐4

Collect Date 7/1/14 7/1/14 7/1/14 7/1/14
EPA RSL EPA RSL
Parameter Units 2014 Value Value Value Value
2014 Tap
MCL
Water
Volatile Organic Compounds
Tetrachloroethene ug/L 4.1 5 102 26.0 ND 21.3
Metals
Aluminum mg/L 2 NE 228 92.1 179 1580
Barium mg/L 0.38 2 1.94 1.48 1.37 40.1
Chromium (Total) mg/L NE 0.1 0.512 0.220 0.306 2.73
Chromium (VI) mg/L 0.000035 0.1 0.017 ND ND ND
Copper mg/L 0.08 1.3 0.641 0.183 0.345 3.81
Iron mg/L 1.4 NE 601 229 333 4390
Lead mg/L NE 0.015 0.901 0.120 0.197 3.39
Magnesium mg/L NE NE 116 40.6 50.3 364
Mercury mg/L 6.30E‐05 0.002 ND ND ND 0.00267
Nickel mg/L 0.039 NE 1.36 0.420 0.508 6.91
Zinc mg/L 0.6 NE 1.60 ND 0.550 5.47
Note: For Clarity only detected analytes are shown
EPA RSL- EPA Risk-Based Assessment Regional Screening Levels, last updated May 2014
Detected Value Exceeding EPA Maxmium Contaminant Level (MCL) Values
Detected Value Exceeding EPA Tap Water Values
Page 1 of 1
Table 3
Soil Vapor Analytical Summary
Sample ID SG‐1 SG‐2 SG‐3 SG‐4 SG‐5

Collect Date 7/1/14 7/1/14 7/1/14 7/1/14 7/1/14
Sample Depth 3' 3' 3' 3' 3'
EPA RSL EPA RSL

Parameter Units Residential Industrial Value Value Value Value Value
Indoor Air Indoor Air
Volatile Organic Compounds

Ethanol ug/m3 NE NE ND ND ND 9.6 ND
Acetone ug/m3 3,200 14,000 ND ND 34 51 29
2‐Propanol ug/m3 NE NE 27 27 25 28 18
4‐Methyl‐2‐pentanone ug/m3 310 1,300 9.3 10 7.6 5.2 ND
Note: For Clarity only detected analytes are shown
EPA RSL- EPA Risk-Based Assessment Regional Screening Levels, last updated May 2014
Detected Value Exceeding EPA Residential Indoor Air Values
Detected Value Exceeding EPA Industrial Indoor Air Values
Page 1 of 1
1
2
3
4
5
ANALYTICAL REPORT
6
TestAmerica Laboratories, Inc.
TestAmerica Nashville 7
2960 Foster Creighton Drive
Nashville, TN 37204 8
Tel: (615)726-0177
9
TestAmerica Job ID: 490-56655-1
TestAmerica Sample Delivery Group: Alcoa, TN 10
Client Project/Site: Proposed Sams Club #4062 E2137034
11
For:
Terracon Consulting Eng & Scientists 12
51 Lost Mound Suite 135
Chattanooga, Tennessee 37406 13
Attn: Mr. Travis Stamper
Authorized for release by:

7/22/2014 12:34:05 PM
Shali Brown, Project Manager II
(615)301-5031
shali.brown@testamericainc.com
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
Client: Terracon Consulting Eng & Scientists TestAmerica Job ID: 490-56655-1 1
Project/Site: Proposed Sams Club #4062 E2137034 SDG: Alcoa, TN
2
Table of Contents 3
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 4
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
5
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 7
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22
44
8
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47 9
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49
10
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51 11
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55 12
13
TestAmerica Nashville
Page 2 of 55 7/22/2014
Sample Summary 1
Client: Terracon Consulting Eng & Scientists TestAmerica Job ID: 490-56655-1
Project/Site: Proposed Sams Club #4062 E2137034 SDG: Alcoa, TN 2
3
Lab Sample ID Client Sample ID Matrix Collected Received
490-56655-1 MW-1 53.5 to 54.5 ft. Solid 06/30/14 13:48 07/02/14 08:15
490-56655-2 MW-2 28.5 to 30.0 ft. Solid 06/30/14 15:25 07/02/14 08:15
4
490-56655-3 MW-3 38.5 to 40.0 ft. Solid 07/01/14 07:50 07/02/14 08:15
490-56655-4 MW-4 28.5 to 30.0 ft. Solid 07/01/14 09:35 07/02/14 08:15
5
6
7
8
9
10
11
12
13
Page 3 of 55 7/22/2014
Case Narrative 1
Job ID: 490-56655-1 3
Laboratory: TestAmerica Nashville
4
Narrative
Job Narrative 5
490-56655-1
6
Comments
Reference attached email for changes made to analysis requested on the chain of custody. 7
Receipt
The samples were received on 7/2/2014 8:15 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
8
The temperature of the cooler at receipt was 5.0º C.
9
Except:
10
Soil Trip Blank received was in an empty 4oz jar. An empty jar cannot be used for a trip blank; therefore, analysis was not provided for "Trip
Blank".
11
GC/MS VOA
Method(s) 8260B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate 12
(MS/MSD/DUP) associated with batch 174623
13
Method(s) 8260B: The laboratory control sample (LCS) and / or laboratory control sample duplicate (LCSD) for batch 175076 recovered
outside control limits for the following analytes: bromoform. These analytes were biased high in the LCS and were not detected in the
associated samples; therefore, the data have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA

No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
GC Semi VOA
Metals
Organic Prep
VOA Prep
Page 4 of 55 7/22/2014
Definitions/Glossary 1
Qualifiers 3
GC/MS VOA
Qualifier Qualifier Description
4
* LCS or LCSD exceeds the control limits
F1 MS and/or MSD Recovery exceeds the control limits
5
GC/MS Semi VOA
6
F1 MS and/or MSD Recovery exceeds the control limits
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
7
Metals 8
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not 9
applicable.
E Result exceeded calibration range.
10
Glossary 11
Abbreviation These commonly used abbreviations may or may not be present in this report.
¤ Listed under the "D" column to designate that the result is reported on a dry weight basis 12
%R Percent Recovery
CFL Contains Free Liquid 13
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
Page 5 of 55 7/22/2014
Client Sample Results 1
Client Sample ID: MW-1 53.5 to 54.5 ft. Lab Sample ID: 490-56655-1 3
Date Collected: 06/30/14 13:48 Matrix: Solid
Date Received: 07/02/14 08:15
4
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 5
1,1,1,2-Tetrachloroethane ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
1,1,1-Trichloroethane ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1 6
1,1-Dichloroethane ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
1,1-Dichloroethene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1 8
1,1-Dichloropropene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
1,2,3-Trichlorobenzene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
1,2,3-Trichloropropane ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
9
1,2,4-Trimethylbenzene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
10
1,2-Dibromo-3-Chloropropane ND 0.00439 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
1,2-Dibromoethane (EDB) ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
11
1,2-Dichlorobenzene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
1,2-Dichloroethane ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1 12
1,2-Dichloropropane ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
1,3,5-Trimethylbenzene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1 13
2-Butanone (MEK) ND 0.0439 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
2-Chlorotoluene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
2-Hexanone ND 0.0439 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
4-Methyl-2-pentanone (MIBK) ND 0.0439 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Acetone ND 0.0439 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Benzene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Bromobenzene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Bromochloromethane ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Bromodichloromethane ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Bromoform ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Bromomethane ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Carbon disulfide ND 0.00439 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Carbon tetrachloride ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Chlorobenzene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Chlorodibromomethane ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Chloroethane ND 0.00439 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Chloroform ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Chloromethane ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
cis-1,2-Dichloroethene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
cis-1,3-Dichloropropene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Dibromomethane ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Dichlorodifluoromethane ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Ethylbenzene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Hexachlorobutadiene ND 0.00439 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Isopropylbenzene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Methyl tert-butyl ether ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Methylene Chloride ND 0.00877 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Page 6 of 55 7/22/2014
Client Sample ID: MW-1 53.5 to 54.5 ft. Lab Sample ID: 490-56655-1
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Naphthalene ND 0.00439 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
n-Butylbenzene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1 6
N-Propylbenzene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
p-Isopropyltoluene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
sec-Butylbenzene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
7
Styrene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
tert-Butylbenzene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
8
Tetrachloroethene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Toluene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
9
trans-1,2-Dichloroethene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
trans-1,3-Dichloropropene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1 10
Trichloroethene ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Trichlorofluoromethane ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1 11
Vinyl chloride ND 0.00175 mg/Kg 07/02/14 16:08 07/04/14 05:00 1
Xylenes, Total ND 0.00263 mg/Kg 07/02/14 16:08 07/04/14 05:00 1 12
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac
1,2-Dichloroethane-d4 (Surr) 100 70 - 130 07/02/14 16:08 07/04/14 05:00 1
13
4-Bromofluorobenzene (Surr) 99 70 - 130 07/02/14 16:08 07/04/14 05:00 1
Dibromofluoromethane (Surr) 102 70 - 130 07/02/14 16:08 07/04/14 05:00 1
Toluene-d8 (Surr) 102 70 - 130 07/02/14 16:08 07/04/14 05:00 1
Method: 8270C - Semivolatile Organic Compounds (GC/MS)

Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
1-Methylnaphthalene ND 0.0657 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
2,4,5-Trichlorophenol ND 0.817 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
2,4-Dichlorophenol ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
2,4-Dimethylphenol ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
2,4-Dinitrophenol ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
2,4-Dinitrotoluene ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
2-Chloronaphthalene ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
2-Chlorophenol ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
2-Methylphenol ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
2-Nitroaniline ND 0.817 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
2-Nitrophenol ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
3 & 4 Methylphenol ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
3,3'-Dichlorobenzidine ND 0.654 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
4,6-Dinitro-2-methylphenol ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
4-Chloro-3-methylphenol ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
4-Bromophenyl phenyl ether ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
4-Chloroaniline ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
4-Chlorophenyl phenyl ether ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Page 7 of 55 7/22/2014
3
4
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
4-Nitrophenol ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1 6
Acenaphthene ND 0.0657 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Acenaphthylene ND 0.0657 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Anthracene ND 0.0657 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
7
Benzo[a]anthracene ND 0.0657 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Benzo[a]pyrene ND 0.0657 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
8
Benzo[b]fluoranthene ND 0.0657 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Benzo[g,h,i]perylene ND 0.0657 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
9
Benzo[k]fluoranthene ND 0.0657 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
bis (2-chloroisopropyl) ether ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1 10
Carbazole ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Chrysene ND 0.0657 mg/Kg 07/03/14 10:13 07/03/14 23:09 1 11
Dibenz(a,h)anthracene ND 0.0657 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Dibenzofuran ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1 12
Dimethyl phthalate ND 1.64 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Diethyl phthalate ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1 13
Di-n-butyl phthalate ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Di-n-octyl phthalate ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Fluorene ND 0.0657 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Fluoranthene ND 0.0657 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Hexachlorobenzene ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Hexachlorocyclopentadiene ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Hexachloroethane ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Indeno[1,2,3-cd]pyrene ND 0.0657 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Isophorone ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Nitrobenzene ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
N-Nitrosodi-n-propylamine ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
n-Nitrosodiphenylamine(as ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
diphenylamine)
Pentachlorophenol ND 0.817 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Phenanthrene ND 0.0657 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Pyrene ND 0.0657 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Phenol ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Cresols ND 0.653 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Bis(2-chloroethoxy)methane ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Bis(2-chloroethyl)ether ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Bis(2-ethylhexyl) phthalate ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1
Butyl benzyl phthalate ND 0.326 mg/Kg 07/03/14 10:13 07/03/14 23:09 1

Nitrobenzene-d5 (Surr) 64 27 - 120 07/03/14 10:13 07/03/14 23:09 1
2-Fluorophenol (Surr) 60 10 - 120 07/03/14 10:13 07/03/14 23:09 1
2-Fluorobiphenyl (Surr) 62 29 - 120 07/03/14 10:13 07/03/14 23:09 1
2,4,6-Tribromophenol (Surr) 89 10 - 120 07/03/14 10:13 07/03/14 23:09 1
Phenol-d5 (Surr) 63 10 - 120 07/03/14 10:13 07/03/14 23:09 1
Terphenyl-d14 (Surr) 91 13 - 120 07/03/14 10:13 07/03/14 23:09 1
Page 8 of 55 7/22/2014
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4
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
PCB-1016 ND 0.0325 mg/Kg 07/03/14 11:34 07/09/14 01:29 1
PCB-1221 ND 0.0325 mg/Kg 07/03/14 11:34 07/09/14 01:29 1 6
PCB-1232 ND 0.0325 mg/Kg 07/03/14 11:34 07/09/14 01:29 1
PCB-1242 ND 0.0325 mg/Kg 07/03/14 11:34 07/09/14 01:29 1
PCB-1248 ND 0.0325 mg/Kg 07/03/14 11:34 07/09/14 01:29 1
7
PCB-1254 ND 0.0325 mg/Kg 07/03/14 11:34 07/09/14 01:29 1
PCB-1260 ND 0.0325 mg/Kg 07/03/14 11:34 07/09/14 01:29 1
8
Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 9
Tetrachloro-m-xylene 88 19 - 147 07/03/14 11:34 07/09/14 01:29 1
DCB Decachlorobiphenyl (Surr) 103 20 - 150 07/03/14 11:34 07/09/14 01:29 1 10
Method: 6010B - Metals (ICP)
11
Aluminum 6350 20.0 mg/Kg 07/11/14 11:11 07/15/14 22:42 1
Barium 34.0 2.00 mg/Kg 07/11/14 11:11 07/15/14 22:42 1
12
Chromium 16.7 1.00 mg/Kg 07/11/14 11:11 07/15/14 22:42 1
Copper 23.7 2.00 mg/Kg 07/11/14 11:11 07/15/14 22:42 1
13
Iron 14300 40.0 mg/Kg 07/11/14 11:11 07/15/14 22:42 1
Lead 5.54 1.00 mg/Kg 07/11/14 11:11 07/15/14 22:42 1
Magnesium 2400 200 mg/Kg 07/11/14 11:11 07/15/14 22:42 1
Nickel 22.6 2.00 mg/Kg 07/11/14 11:11 07/15/14 22:42 1
Zinc 18.5 10.0 mg/Kg 07/11/14 11:11 07/15/14 22:42 1
Method: 7471A - Mercury (CVAA)

Mercury ND 0.0960 mg/Kg 07/11/14 09:47 07/11/14 13:56 1
Page 9 of 55 7/22/2014
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9
10
11
2-Hexanone ND 0.0457 mg/Kg 07/02/14 16:08 07/04/14 05:31 1
Acetone ND 0.0457 mg/Kg 07/02/14 16:08 07/04/14 05:31 1
Benzene ND 0.00183 mg/Kg 07/02/14 16:08 07/04/14 05:31 1
Page 10 of 55 7/22/2014
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4
7
Styrene ND 0.00183 mg/Kg 07/02/14 16:08 07/04/14 05:31 1
8
Toluene ND 0.00183 mg/Kg 07/02/14 16:08 07/04/14 05:31 1
9
13
Toluene-d8 (Surr) 102 70 - 130 07/02/14 16:08 07/04/14 05:31 1

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4
7
8
9
Chrysene ND 0.0666 mg/Kg 07/03/14 10:13 07/03/14 23:32 1 11
Fluorene ND 0.0666 mg/Kg 07/03/14 10:13 07/03/14 23:32 1
diphenylamine)
Pyrene ND 0.0666 mg/Kg 07/03/14 10:13 07/03/14 23:32 1
Phenol ND 0.331 mg/Kg 07/03/14 10:13 07/03/14 23:32 1
Cresols ND 0.662 mg/Kg 07/03/14 10:13 07/03/14 23:32 1

Phenol-d5 (Surr) 65 10 - 120 07/03/14 10:13 07/03/14 23:32 1
Terphenyl-d14 (Surr) 95 13 - 120 07/03/14 10:13 07/03/14 23:32 1
Page 12 of 55 7/22/2014
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PCB-1016 ND 0.0332 mg/Kg 07/03/14 11:34 07/09/14 02:38 1
PCB-1221 ND 0.0332 mg/Kg 07/03/14 11:34 07/09/14 02:38 1 6
PCB-1232 ND 0.0332 mg/Kg 07/03/14 11:34 07/09/14 02:38 1
PCB-1242 ND 0.0332 mg/Kg 07/03/14 11:34 07/09/14 02:38 1
PCB-1248 ND 0.0332 mg/Kg 07/03/14 11:34 07/09/14 02:38 1
7
PCB-1254 ND 0.0332 mg/Kg 07/03/14 11:34 07/09/14 02:38 1
PCB-1260 ND 0.0332 mg/Kg 07/03/14 11:34 07/09/14 02:38 1
8
11
Aluminum 7850 20.0 mg/Kg 07/11/14 11:11 07/15/14 22:45 1
Barium 42.6 2.00 mg/Kg 07/11/14 11:11 07/15/14 22:45 1
12
Chromium 11.2 1.00 mg/Kg 07/11/14 11:11 07/15/14 22:45 1
Copper 15.3 2.00 mg/Kg 07/11/14 11:11 07/15/14 22:45 1
13
Iron 16300 40.0 mg/Kg 07/11/14 11:11 07/15/14 22:45 1
Lead 8.94 1.00 mg/Kg 07/11/14 11:11 07/15/14 22:45 1
Magnesium 1570 200 mg/Kg 07/11/14 11:11 07/15/14 22:45 1
Nickel 22.7 2.00 mg/Kg 07/11/14 11:11 07/15/14 22:45 1
Zinc 30.1 10.0 mg/Kg 07/11/14 11:11 07/15/14 22:45 1

Mercury ND 0.0966 mg/Kg 07/11/14 09:47 07/11/14 13:58 1
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9
10
11
2-Hexanone ND 0.0453 mg/Kg 07/02/14 16:08 07/04/14 06:01 1
Acetone ND 0.0453 mg/Kg 07/02/14 16:08 07/04/14 06:01 1
Benzene ND 0.00181 mg/Kg 07/02/14 16:08 07/04/14 06:01 1
Page 14 of 55 7/22/2014
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4
7
Styrene ND 0.00181 mg/Kg 07/02/14 16:08 07/04/14 06:01 1
8
Toluene ND 0.00181 mg/Kg 07/02/14 16:08 07/04/14 06:01 1
9
13
Toluene-d8 (Surr) 103 70 - 130 07/02/14 16:08 07/04/14 06:01 1

Page 15 of 55 7/22/2014
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4
7
8
9
Chrysene ND 0.0653 mg/Kg 07/03/14 10:13 07/03/14 23:55 1 11
Fluorene ND 0.0653 mg/Kg 07/03/14 10:13 07/03/14 23:55 1
diphenylamine)
Pyrene ND 0.0653 mg/Kg 07/03/14 10:13 07/03/14 23:55 1
Phenol ND 0.325 mg/Kg 07/03/14 10:13 07/03/14 23:55 1
Cresols ND 0.650 mg/Kg 07/03/14 10:13 07/03/14 23:55 1

Phenol-d5 (Surr) 71 10 - 120 07/03/14 10:13 07/03/14 23:55 1
Terphenyl-d14 (Surr) 92 13 - 120 07/03/14 10:13 07/03/14 23:55 1
Page 16 of 55 7/22/2014
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4
PCB-1016 ND 0.0329 mg/Kg 07/03/14 11:34 07/09/14 03:00 1
PCB-1221 ND 0.0329 mg/Kg 07/03/14 11:34 07/09/14 03:00 1 6
PCB-1232 ND 0.0329 mg/Kg 07/03/14 11:34 07/09/14 03:00 1
PCB-1242 ND 0.0329 mg/Kg 07/03/14 11:34 07/09/14 03:00 1
PCB-1248 ND 0.0329 mg/Kg 07/03/14 11:34 07/09/14 03:00 1
7
PCB-1254 ND 0.0329 mg/Kg 07/03/14 11:34 07/09/14 03:00 1
PCB-1260 ND 0.0329 mg/Kg 07/03/14 11:34 07/09/14 03:00 1
8
11
Aluminum 8890 19.6 mg/Kg 07/11/14 11:11 07/15/14 22:49 1
Barium 41.1 1.96 mg/Kg 07/11/14 11:11 07/15/14 22:49 1
12
Chromium 16.6 0.980 mg/Kg 07/11/14 11:11 07/15/14 22:49 1
Copper 19.0 1.96 mg/Kg 07/11/14 11:11 07/15/14 22:49 1
13
Iron 16000 39.2 mg/Kg 07/11/14 11:11 07/15/14 22:49 1
Lead 6.98 0.980 mg/Kg 07/11/14 11:11 07/15/14 22:49 1
Magnesium 2260 196 mg/Kg 07/11/14 11:11 07/15/14 22:49 1
Nickel 23.1 1.96 mg/Kg 07/11/14 11:11 07/15/14 22:49 1
Zinc 29.8 9.80 mg/Kg 07/11/14 11:11 07/15/14 22:49 1

Mercury ND 0.0997 mg/Kg 07/11/14 09:47 07/11/14 14:00 1
Page 17 of 55 7/22/2014
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9
10
11
2-Hexanone ND 0.0464 mg/Kg 07/02/14 16:08 07/08/14 14:39 1
Acetone 0.0490 0.0464 mg/Kg 07/02/14 16:08 07/08/14 14:39 1
Benzene ND 0.00186 mg/Kg 07/02/14 16:08 07/08/14 14:39 1
Bromoform ND * 0.00186 mg/Kg 07/02/14 16:08 07/08/14 14:39 1
Page 18 of 55 7/22/2014
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4
7
Styrene ND 0.00186 mg/Kg 07/02/14 16:08 07/08/14 14:39 1
8
Tetrachloroethene 0.00810 0.00186 mg/Kg 07/02/14 16:08 07/08/14 14:39 1
Toluene ND 0.00186 mg/Kg 07/02/14 16:08 07/08/14 14:39 1
9
13
Toluene-d8 (Surr) 99 70 - 130 07/02/14 16:08 07/08/14 14:39 1

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4
7
8
9
Chrysene ND 0.0654 mg/Kg 07/03/14 10:13 07/04/14 00:17 1 11
Fluorene ND 0.0654 mg/Kg 07/03/14 10:13 07/04/14 00:17 1
diphenylamine)
Pyrene ND 0.0654 mg/Kg 07/03/14 10:13 07/04/14 00:17 1
Phenol ND 0.325 mg/Kg 07/03/14 10:13 07/04/14 00:17 1
Cresols ND 0.650 mg/Kg 07/03/14 10:13 07/04/14 00:17 1

Phenol-d5 (Surr) 72 10 - 120 07/03/14 10:13 07/04/14 00:17 1
Terphenyl-d14 (Surr) 87 13 - 120 07/03/14 10:13 07/04/14 00:17 1
Page 20 of 55 7/22/2014
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4
PCB-1016 ND 0.0331 mg/Kg 07/03/14 11:34 07/09/14 03:23 1
PCB-1221 ND 0.0331 mg/Kg 07/03/14 11:34 07/09/14 03:23 1 6
PCB-1232 ND 0.0331 mg/Kg 07/03/14 11:34 07/09/14 03:23 1
PCB-1242 ND 0.0331 mg/Kg 07/03/14 11:34 07/09/14 03:23 1
PCB-1248 ND 0.0331 mg/Kg 07/03/14 11:34 07/09/14 03:23 1
7
PCB-1254 ND 0.0331 mg/Kg 07/03/14 11:34 07/09/14 03:23 1
PCB-1260 ND 0.0331 mg/Kg 07/03/14 11:34 07/09/14 03:23 1
8
11
Aluminum 10800 20.0 mg/Kg 07/11/14 11:11 07/15/14 22:52 1
Barium 30.5 2.00 mg/Kg 07/11/14 11:11 07/15/14 22:52 1
12
Chromium 7.46 1.00 mg/Kg 07/11/14 11:11 07/15/14 22:52 1
Copper 16.8 2.00 mg/Kg 07/11/14 11:11 07/15/14 22:52 1
13
Iron 23100 40.0 mg/Kg 07/11/14 11:11 07/15/14 22:52 1
Lead 17.1 1.00 mg/Kg 07/11/14 11:11 07/15/14 22:52 1
Magnesium 474 200 mg/Kg 07/11/14 11:11 07/15/14 22:52 1
Nickel 16.5 2.00 mg/Kg 07/11/14 11:11 07/15/14 22:52 1
Zinc 15.7 10.0 mg/Kg 07/11/14 11:11 07/15/14 22:52 1

Mercury ND 0.0992 mg/Kg 07/11/14 09:47 07/11/14 14:01 1
Page 21 of 55 7/22/2014
QC Sample Results 1
Method: 8260B - Volatile Organic Compounds (GC/MS) 3
Lab Sample ID: 490-56655-4 MS Client Sample ID: MW-4 28.5 to 30.0 ft. 4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 175076 Prep Batch: 174266
Sample Sample Spike MS MS %Rec.
5
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits
1,1,1,2-Tetrachloroethane ND 0.0440 0.06666 mg/Kg 151 19 - 158 6
1,1,1-Trichloroethane ND 0.0440 0.07697 F1 mg/Kg 175 35 - 149
1,1,2,2-Tetrachloroethane ND 0.0440 0.04354 mg/Kg 99 10 - 162 7
1,1,2-Trichloroethane ND 0.0440 0.04775 mg/Kg 108 19 - 157
1,1-Dichloroethane ND 0.0440 0.06660 F1 mg/Kg 151 42 - 136 8
1,1-Dichloroethene ND 0.0440 0.07979 F1 mg/Kg 181 41 - 143
1,1-Dichloropropene ND 0.0440 0.06603 F1 mg/Kg 150 38 - 145 9
1,2,3-Trichlorobenzene ND 0.0440 0.03001 mg/Kg 68 10 - 157
1,2,3-Trichloropropane ND 0.0440 0.03993 mg/Kg 91 10 - 157 10
1,2,4-Trimethylbenzene
1,2-Dibromo-3-Chloropropane
ND
ND
0.0440
0.0440
0.02857
0.04913
mg/Kg
mg/Kg
65
112
14 - 165
10 - 147
11
1,2-Dibromoethane (EDB) ND 0.0440 0.04512 mg/Kg 103 18 - 156
1,2-Dichlorobenzene ND 0.0440 0.04220 mg/Kg 96 10 - 160
12
1,2-Dichloroethane ND 0.0440 0.04791 mg/Kg 109 28 - 138
1,2-Dichloropropane ND 0.0440 0.05728 mg/Kg 130 20 - 146
13
1,3,5-Trimethylbenzene ND 0.0440 0.04193 mg/Kg 95 18 - 164
2-Butanone (MEK) ND 0.220 0.2326 mg/Kg 106 18 - 153
2-Chlorotoluene ND 0.0440 0.04256 mg/Kg 97 20 - 156
2-Hexanone ND 0.220 0.1963 mg/Kg 89 10 - 169
4-Chlorotoluene ND 0.0440 0.04250 mg/Kg 97 17 - 159
4-Methyl-2-pentanone (MIBK) ND 0.220 0.2110 mg/Kg 96 10 - 168
Acetone 0.0490 0.220 0.2746 mg/Kg 103 19 - 175
Benzene ND 0.0440 0.06420 F1 mg/Kg 146 31 - 143
Bromobenzene ND 0.0440 0.03897 mg/Kg 89 12 - 157
Bromochloromethane ND 0.0440 0.05962 mg/Kg 135 31 - 141
Bromodichloromethane ND 0.0440 0.06020 mg/Kg 137 19 - 148
Bromoform ND * 0.0440 0.06643 mg/Kg 151 10 - 165
Bromomethane ND 0.0440 0.05880 mg/Kg 134 10 - 164
Carbon disulfide ND 0.0440 0.07808 F1 mg/Kg 177 32 - 144
Carbon tetrachloride ND 0.0440 0.08854 F1 mg/Kg 201 31 - 149
Chlorobenzene ND 0.0440 0.05233 mg/Kg 119 25 - 152
Chlorodibromomethane ND 0.0440 0.05601 mg/Kg 127 14 - 146
Chloroethane ND 0.0440 0.06863 F1 mg/Kg 156 10 - 151
Chloroform ND 0.0440 0.06090 mg/Kg 138 34 - 160
Chloromethane ND 0.0440 0.05776 mg/Kg 131 10 - 156
cis-1,2-Dichloroethene ND 0.0440 0.05572 mg/Kg 127 36 - 139
cis-1,3-Dichloropropene ND 0.0440 0.04455 mg/Kg 101 15 - 166
Dibromomethane ND 0.0440 0.04955 mg/Kg 113 20 - 146
Dichlorodifluoromethane ND 0.0440 0.08605 F1 mg/Kg 196 10 - 143
Ethylbenzene ND 0.0440 0.05212 mg/Kg 118 23 - 161
Hexachlorobutadiene ND 0.0440 0.03818 mg/Kg 87 10 - 171
Isopropylbenzene ND 0.0440 0.05296 mg/Kg 120 23 - 181
Methyl tert-butyl ether ND 0.0440 0.03177 mg/Kg 72 28 - 141
Page 22 of 55 7/22/2014
QC Sample Results 1
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) 3
Lab Sample ID: 490-56655-4 MS Client Sample ID: MW-4 28.5 to 30.0 ft.
4
Sample Sample Spike MS MS %Rec. 5
Methylene Chloride ND 0.0440 0.06028 mg/Kg 131 24 - 182 6
Naphthalene ND 0.0440 0.009062 mg/Kg 21 10 - 176
n-Butylbenzene ND 0.0440 0.03759 mg/Kg 85 10 - 175 7
N-Propylbenzene ND 0.0440 0.04519 mg/Kg 103 19 - 162
p-Isopropyltoluene ND 0.0440 0.04176 mg/Kg 95 12 - 168 8
sec-Butylbenzene ND 0.0440 0.04619 mg/Kg 105 12 - 170
Styrene ND 0.0440 0.02391 mg/Kg 54 10 - 165
tert-Butylbenzene ND 0.0440 0.04782 mg/Kg 109 20 - 164
9
Tetrachloroethene 0.00810 0.0440 0.07320 mg/Kg 148 33 - 161
Toluene ND 0.0440 0.05564 mg/Kg 126 30 - 155
10
trans-1,2-Dichloroethene ND 0.0440 0.06476 F1 mg/Kg 147 39 - 140
trans-1,3-Dichloropropene ND 0.0440 0.04207 mg/Kg 96 10 - 157
11
Trichloroethene ND 0.0440 0.06573 mg/Kg 149 27 - 153
Trichlorofluoromethane ND 0.0440 0.08241 F1 mg/Kg 187 25 - 140 12
Vinyl chloride ND 0.0440 0.07500 F1 mg/Kg 170 20 - 141
Xylenes, Total ND 0.0880 0.09565 mg/Kg 109 25 - 162 13
MS MS
Surrogate %Recovery Qualifier Limits
1,2-Dichloroethane-d4 (Surr) 101 70 - 130
4-Bromofluorobenzene (Surr) 79 70 - 130
Dibromofluoromethane (Surr) 110 70 - 130
Toluene-d8 (Surr) 97 70 - 130
Lab Sample ID: 490-56655-4 MSD Client Sample ID: MW-4 28.5 to 30.0 ft.
Sample Sample Spike MSD MSD %Rec. RPD
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit
1,1,1,2-Tetrachloroethane ND 0.0419 0.07057 F1 mg/Kg 169 19 - 158 6 50
1,1,1-Trichloroethane ND 0.0419 0.08037 F1 mg/Kg 192 35 - 149 4 50
1,1,2,2-Tetrachloroethane ND 0.0419 0.05011 mg/Kg 120 10 - 162 14 50
1,1,2-Trichloroethane ND 0.0419 0.05322 mg/Kg 127 19 - 157 11 50
1,1-Dichloroethane ND 0.0419 0.07092 F1 mg/Kg 169 42 - 136 6 50
1,1-Dichloroethene ND 0.0419 0.08348 F1 mg/Kg 199 41 - 143 5 50
1,1-Dichloropropene ND 0.0419 0.06994 F1 mg/Kg 167 38 - 145 6 50
1,2,3-Trichlorobenzene ND 0.0419 0.03696 mg/Kg 88 10 - 157 21 50
1,2,3-Trichloropropane ND 0.0419 0.04613 mg/Kg 110 10 - 157 14 50
1,2,4-Trimethylbenzene ND 0.0419 0.03419 mg/Kg 82 14 - 165 18 50
1,2-Dibromo-3-Chloropropane ND 0.0419 0.05613 mg/Kg 134 10 - 147 13 50
1,2-Dibromoethane (EDB) ND 0.0419 0.05076 mg/Kg 121 18 - 156 12 50
1,2-Dichlorobenzene ND 0.0419 0.04685 mg/Kg 112 10 - 160 10 50
1,2-Dichloroethane ND 0.0419 0.05161 mg/Kg 123 28 - 138 7 50
1,2-Dichloropropane ND 0.0419 0.06104 mg/Kg 146 20 - 146 6 50
1,3,5-Trimethylbenzene ND 0.0419 0.04659 mg/Kg 111 18 - 164 11 50
1,3-Dichloropropane ND 0.0419 0.04997 mg/Kg 119 22 - 148 10 42
Page 23 of 55 7/22/2014
QC Sample Results 1
4
Sample Sample Spike MSD MSD %Rec. RPD 5
2,2-Dichloropropane ND 0.0419 0.07053 F1 mg/Kg 168 33 - 148 8 50 6
2-Butanone (MEK) ND 0.209 0.2749 mg/Kg 131 18 - 153 17 50
2-Chlorotoluene ND 0.0419 0.04558 mg/Kg 109 20 - 156 7 50 7
2-Hexanone ND 0.209 0.2438 mg/Kg 116 10 - 169 22 50
4-Chlorotoluene ND 0.0419 0.04666 mg/Kg 111 17 - 159 9 50 8
4-Methyl-2-pentanone (MIBK) ND 0.209 0.2592 mg/Kg 124 10 - 168 21 50
Acetone 0.0490 0.209 0.3232 mg/Kg 131 19 - 175 16 50
Benzene ND 0.0419 0.06785 F1 mg/Kg 162 31 - 143 6 50
9
Bromobenzene ND 0.0419 0.04424 mg/Kg 106 12 - 157 13 50
Bromochloromethane ND 0.0419 0.06304 F1 mg/Kg 151 31 - 141 6 50
10
Bromodichloromethane ND 0.0419 0.06450 F1 mg/Kg 154 19 - 148 7 50
Bromoform ND * 0.0419 0.07202 F1 mg/Kg 172 10 - 165 8 50
11
Bromomethane ND 0.0419 0.06737 mg/Kg 161 10 - 164 14 50
Carbon disulfide ND 0.0419 0.08286 F1 mg/Kg 198 32 - 144 6 50 12
Carbon tetrachloride ND 0.0419 0.09156 F1 mg/Kg 219 31 - 149 3 50
Chlorobenzene ND 0.0419 0.05505 mg/Kg 131 25 - 152 5 50 13
Chlorodibromomethane ND 0.0419 0.06172 F1 mg/Kg 147 14 - 146 10 50
Chloroethane ND 0.0419 0.07510 F1 mg/Kg 179 10 - 151 9 50
Chloroform ND 0.0419 0.06443 mg/Kg 154 34 - 160 6 49
Chloromethane ND 0.0419 0.05871 mg/Kg 140 10 - 156 2 50
cis-1,2-Dichloroethene ND 0.0419 0.05986 F1 mg/Kg 143 36 - 139 7 50
cis-1,3-Dichloropropene ND 0.0419 0.05053 mg/Kg 121 15 - 166 13 50
Dibromomethane ND 0.0419 0.05320 mg/Kg 127 20 - 146 7 50
Dichlorodifluoromethane ND 0.0419 0.08860 F1 mg/Kg 212 10 - 143 3 50
Ethylbenzene ND 0.0419 0.05478 mg/Kg 131 23 - 161 5 50
Hexachlorobutadiene ND 0.0419 0.04649 mg/Kg 111 10 - 171 20 50
Isopropylbenzene ND 0.0419 0.05644 mg/Kg 135 23 - 181 6 50
Methyl tert-butyl ether ND 0.0419 0.03692 mg/Kg 88 28 - 141 15 50
Methylene Chloride ND 0.0419 0.06522 mg/Kg 149 24 - 182 8 50
Naphthalene ND 0.0419 0.01202 mg/Kg 29 10 - 176 28 50
n-Butylbenzene ND 0.0419 0.04466 mg/Kg 107 10 - 175 17 50
N-Propylbenzene ND 0.0419 0.04966 mg/Kg 119 19 - 162 9 50
p-Isopropyltoluene ND 0.0419 0.04822 mg/Kg 115 12 - 168 14 50
sec-Butylbenzene ND 0.0419 0.05113 mg/Kg 122 12 - 170 10 50
Styrene ND 0.0419 0.02849 mg/Kg 68 10 - 165 17 50
tert-Butylbenzene ND 0.0419 0.05264 mg/Kg 126 20 - 164 10 50
Tetrachloroethene 0.00810 0.0419 0.07222 mg/Kg 153 33 - 161 1 50
Toluene ND 0.0419 0.05865 mg/Kg 140 30 - 155 5 50
trans-1,2-Dichloroethene ND 0.0419 0.06952 F1 mg/Kg 166 39 - 140 7 50
trans-1,3-Dichloropropene ND 0.0419 0.04751 mg/Kg 113 10 - 157 12 50
Trichloroethene ND 0.0419 0.06767 F1 mg/Kg 162 27 - 153 3 50
Trichlorofluoromethane ND 0.0419 0.08313 F1 mg/Kg 199 25 - 140 1 50
Vinyl chloride ND 0.0419 0.08110 F1 mg/Kg 194 20 - 141 8 50
Xylenes, Total ND 0.0838 0.1020 mg/Kg 122 25 - 162 6 50
MSD MSD
Page 24 of 55 7/22/2014
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4
MSD MSD
5
6
7
Lab Sample ID: MB 490-174623/9 Client Sample ID: Method Blank
Matrix: Solid Prep Type: Total/NA 8
Analysis Batch: 174623
MB MB 9
1,1,1,2-Tetrachloroethane ND 0.00200 mg/Kg 07/04/14 03:30 1 10
1,1,1-Trichloroethane ND 0.00200 mg/Kg 07/04/14 03:30 1
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
ND
ND
0.00200
0.00500
mg/Kg
mg/Kg
07/04/14 03:30
07/04/14 03:30
1
1
11
1,1-Dichloroethane ND 0.00200 mg/Kg 07/04/14 03:30 1
1,1-Dichloroethene ND 0.00200 mg/Kg 07/04/14 03:30 1
12
1,1-Dichloropropene ND 0.00200 mg/Kg 07/04/14 03:30 1
1,2,3-Trichlorobenzene ND 0.00200 mg/Kg 07/04/14 03:30 1
13
1,2,3-Trichloropropane ND 0.00200 mg/Kg 07/04/14 03:30 1
1,2,4-Trimethylbenzene ND 0.00200 mg/Kg 07/04/14 03:30 1
1,2-Dibromo-3-Chloropropane ND 0.00500 mg/Kg 07/04/14 03:30 1
1,2-Dibromoethane (EDB) ND 0.00200 mg/Kg 07/04/14 03:30 1
1,2-Dichlorobenzene ND 0.00200 mg/Kg 07/04/14 03:30 1
1,2-Dichloropropane ND 0.00200 mg/Kg 07/04/14 03:30 1
2-Butanone (MEK) ND 0.0500 mg/Kg 07/04/14 03:30 1
2-Chlorotoluene ND 0.00200 mg/Kg 07/04/14 03:30 1
2-Hexanone ND 0.0500 mg/Kg 07/04/14 03:30 1
4-Methyl-2-pentanone (MIBK) ND 0.0500 mg/Kg 07/04/14 03:30 1
Acetone ND 0.0500 mg/Kg 07/04/14 03:30 1
Benzene ND 0.00200 mg/Kg 07/04/14 03:30 1
Bromobenzene ND 0.00200 mg/Kg 07/04/14 03:30 1
Bromochloromethane ND 0.00200 mg/Kg 07/04/14 03:30 1
Bromodichloromethane ND 0.00200 mg/Kg 07/04/14 03:30 1
Bromoform ND 0.00200 mg/Kg 07/04/14 03:30 1
Bromomethane ND 0.00200 mg/Kg 07/04/14 03:30 1
Carbon disulfide ND 0.00500 mg/Kg 07/04/14 03:30 1
Carbon tetrachloride ND 0.00200 mg/Kg 07/04/14 03:30 1
Chlorobenzene ND 0.00200 mg/Kg 07/04/14 03:30 1
Chlorodibromomethane ND 0.00200 mg/Kg 07/04/14 03:30 1
Chloroethane ND 0.00500 mg/Kg 07/04/14 03:30 1
Chloroform ND 0.00200 mg/Kg 07/04/14 03:30 1
Chloromethane ND 0.00200 mg/Kg 07/04/14 03:30 1
Page 25 of 55 7/22/2014
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MB MB 5
cis-1,2-Dichloroethene ND 0.00200 mg/Kg 07/04/14 03:30 1 6
cis-1,3-Dichloropropene ND 0.00200 mg/Kg 07/04/14 03:30 1
Dibromomethane ND 0.00200 mg/Kg 07/04/14 03:30 1 7
Dichlorodifluoromethane ND 0.00200 mg/Kg 07/04/14 03:30 1
Ethylbenzene ND 0.00200 mg/Kg 07/04/14 03:30 1 8
Hexachlorobutadiene ND 0.00500 mg/Kg 07/04/14 03:30 1
Isopropylbenzene ND 0.00200 mg/Kg 07/04/14 03:30 1
Methyl tert-butyl ether ND 0.00200 mg/Kg 07/04/14 03:30 1
9
Methylene Chloride ND 0.0100 mg/Kg 07/04/14 03:30 1
Naphthalene ND 0.00500 mg/Kg 07/04/14 03:30 1
10
n-Butylbenzene ND 0.00200 mg/Kg 07/04/14 03:30 1
N-Propylbenzene ND 0.00200 mg/Kg 07/04/14 03:30 1
11
p-Isopropyltoluene ND 0.00200 mg/Kg 07/04/14 03:30 1
sec-Butylbenzene ND 0.00200 mg/Kg 07/04/14 03:30 1 12
Styrene ND 0.00200 mg/Kg 07/04/14 03:30 1
tert-Butylbenzene ND 0.00200 mg/Kg 07/04/14 03:30 1 13
Tetrachloroethene ND 0.00200 mg/Kg 07/04/14 03:30 1
Toluene ND 0.00200 mg/Kg 07/04/14 03:30 1
trans-1,2-Dichloroethene ND 0.00200 mg/Kg 07/04/14 03:30 1
trans-1,3-Dichloropropene ND 0.00200 mg/Kg 07/04/14 03:30 1
Trichloroethene ND 0.00200 mg/Kg 07/04/14 03:30 1
Trichlorofluoromethane ND 0.00200 mg/Kg 07/04/14 03:30 1
Vinyl chloride ND 0.00200 mg/Kg 07/04/14 03:30 1
Xylenes, Total ND 0.00300 mg/Kg 07/04/14 03:30 1
MB MB
1,2-Dichloroethane-d4 (Surr) 100 70 - 130 07/04/14 03:30 1
4-Bromofluorobenzene (Surr) 101 70 - 130 07/04/14 03:30 1
Dibromofluoromethane (Surr) 103 70 - 130 07/04/14 03:30 1
Toluene-d8 (Surr) 102 70 - 130 07/04/14 03:30 1
Lab Sample ID: LCS 490-174623/5 Client Sample ID: Lab Control Sample
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
1,1,1,2-Tetrachloroethane 0.0500 0.05135 mg/Kg 103 80 - 136
1,1,1-Trichloroethane 0.0500 0.04642 mg/Kg 93 72 - 140
1,1-Dichloroethane 0.0500 0.04456 mg/Kg 89 75 - 124
1,1-Dichloroethene 0.0500 0.04934 mg/Kg 99 75 - 131
1,1-Dichloropropene 0.0500 0.04746 mg/Kg 95 79 - 127
1,2,3-Trichlorobenzene 0.0500 0.04503 mg/Kg 90 70 - 150
1,2,3-Trichloropropane 0.0500 0.05087 mg/Kg 102 65 - 139
1,2,4-Trimethylbenzene 0.0500 0.04205 mg/Kg 84 77 - 139
1,2-Dibromo-3-Chloropropane 0.0500 0.04879 mg/Kg 98 49 - 142
Page 26 of 55 7/22/2014
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4
Spike LCS LCS %Rec. 5
1,2-Dibromoethane (EDB) 0.0500 0.05330 mg/Kg 107 80 - 135 6
1,2-Dichlorobenzene 0.0500 0.04630 mg/Kg 93 80 - 134
1,2-Dichloroethane 0.0500 0.04807 mg/Kg 96 65 - 134 7
1,2-Dichloropropane 0.0500 0.04918 mg/Kg 98 69 - 120
1,3,5-Trimethylbenzene 0.0500 0.04577 mg/Kg 92 78 - 138 8
9
2-Butanone (MEK) 0.250 0.2877 mg/Kg 115 61 - 132
10
2-Chlorotoluene 0.0500 0.04577 mg/Kg 92 78 - 132
2-Hexanone 0.250 0.2731 mg/Kg 109 57 - 148
11
4-Methyl-2-pentanone (MIBK) 0.250 0.2780 mg/Kg 111 59 - 138 12
Acetone 0.250 0.2711 mg/Kg 108 51 - 149
Benzene 0.0500 0.04831 mg/Kg 97 75 - 127 13
Bromobenzene 0.0500 0.04722 mg/Kg 94 75 - 130
Bromochloromethane 0.0500 0.04947 mg/Kg 99 70 - 132
Bromodichloromethane 0.0500 0.04979 mg/Kg 100 68 - 135
Bromoform 0.0500 0.04259 mg/Kg 85 36 - 150
Bromomethane 0.0500 0.05219 mg/Kg 104 43 - 142
Carbon disulfide 0.0500 0.04675 mg/Kg 93 74 - 135
Carbon tetrachloride 0.0500 0.04726 mg/Kg 95 70 - 141
Chlorobenzene 0.0500 0.04720 mg/Kg 94 84 - 125
Chlorodibromomethane 0.0500 0.04417 mg/Kg 88 66 - 134
Chloroethane 0.0500 0.05129 mg/Kg 103 53 - 144
Chloroform 0.0500 0.04521 mg/Kg 90 76 - 130
Chloromethane 0.0500 0.04703 mg/Kg 94 23 - 150
cis-1,2-Dichloroethene 0.0500 0.04400 mg/Kg 88 75 - 125
cis-1,3-Dichloropropene 0.0500 0.05053 mg/Kg 101 73 - 148
Dibromomethane 0.0500 0.05107 mg/Kg 102 71 - 130
Dichlorodifluoromethane 0.0500 0.05760 mg/Kg 115 12 - 144
Ethylbenzene 0.0500 0.04697 mg/Kg 94 80 - 134
Hexachlorobutadiene 0.0500 0.04352 mg/Kg 87 65 - 148
Isopropylbenzene 0.0500 0.04698 mg/Kg 94 80 - 150
Methyl tert-butyl ether 0.0500 0.04956 mg/Kg 99 70 - 136
Methylene Chloride 0.0500 0.04704 mg/Kg 94 68 - 144
Naphthalene 0.0500 0.05010 mg/Kg 100 69 - 150
n-Butylbenzene 0.0500 0.04309 mg/Kg 86 72 - 152
N-Propylbenzene 0.0500 0.04243 mg/Kg 85 75 - 137
p-Isopropyltoluene 0.0500 0.04483 mg/Kg 90 77 - 141
sec-Butylbenzene 0.0500 0.04358 mg/Kg 87 79 - 141
Styrene 0.0500 0.04762 mg/Kg 95 82 - 137
tert-Butylbenzene 0.0500 0.04669 mg/Kg 93 80 - 132
Tetrachloroethene 0.0500 0.04712 mg/Kg 94 78 - 140
Toluene 0.0500 0.04803 mg/Kg 96 80 - 132
trans-1,2-Dichloroethene 0.0500 0.04465 mg/Kg 89 76 - 128
trans-1,3-Dichloropropene 0.0500 0.04806 mg/Kg 96 62 - 139
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QC Sample Results 1
4
Trichloroethene 0.0500 0.04800 mg/Kg 96 77 - 127 6
Trichlorofluoromethane 0.0500 0.04908 mg/Kg 98 50 - 140
Vinyl chloride 0.0500 0.05338 mg/Kg 107 47 - 136 7
Xylenes, Total 0.100 0.09269 mg/Kg 93 80 - 137
LCS LCS 8
1,2-Dichloroethane-d4 (Surr) 95 70 - 130 9
Dibromofluoromethane (Surr) 95 70 - 130 10
11
Lab Sample ID: LCSD 490-174623/6 Client Sample ID: Lab Control Sample Dup
Spike LCSD LCSD %Rec. RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
13
1,1,1,2-Tetrachloroethane 0.0500 0.05487 mg/Kg 110 80 - 136 7 50
1,1,1-Trichloroethane 0.0500 0.04910 mg/Kg 98 72 - 140 6 50
1,1,2,2-Tetrachloroethane 0.0500 0.05073 mg/Kg 101 66 - 134 3 50
1,1-Dichloroethane 0.0500 0.04862 mg/Kg 97 75 - 124 9 50
1,1-Dichloroethene 0.0500 0.05055 mg/Kg 101 75 - 131 2 50
1,1-Dichloropropene 0.0500 0.05061 mg/Kg 101 79 - 127 6 50
1,2,3-Trichlorobenzene 0.0500 0.04703 mg/Kg 94 70 - 150 4 50
1,2,3-Trichloropropane 0.0500 0.04926 mg/Kg 99 65 - 139 3 50
1,2,4-Trimethylbenzene 0.0500 0.04478 mg/Kg 90 77 - 139 6 50
1,2-Dibromo-3-Chloropropane 0.0500 0.04620 mg/Kg 92 49 - 142 5 50
1,2-Dibromoethane (EDB) 0.0500 0.05502 mg/Kg 110 80 - 135 3 50
1,2-Dichlorobenzene 0.0500 0.04923 mg/Kg 98 80 - 134 6 50
1,2-Dichloropropane 0.0500 0.05236 mg/Kg 105 69 - 120 6 50
2-Butanone (MEK) 0.250 0.2738 mg/Kg 110 61 - 132 5 50
2-Chlorotoluene 0.0500 0.04949 mg/Kg 99 78 - 132 8 50
2-Hexanone 0.250 0.2555 mg/Kg 102 57 - 148 7 50
4-Methyl-2-pentanone (MIBK) 0.250 0.2738 mg/Kg 110 59 - 138 2 50
Acetone 0.250 0.2408 mg/Kg 96 51 - 149 12 50
Benzene 0.0500 0.05087 mg/Kg 102 75 - 127 5 50
Bromobenzene 0.0500 0.04903 mg/Kg 98 75 - 130 4 50
Bromochloromethane 0.0500 0.05228 mg/Kg 105 70 - 132 6 50
Bromodichloromethane 0.0500 0.05287 mg/Kg 106 68 - 135 6 50
Bromoform 0.0500 0.04286 mg/Kg 86 36 - 150 1 50
Page 28 of 55 7/22/2014
QC Sample Results 1
4
Spike LCSD LCSD %Rec. RPD 5
Bromomethane 0.0500 0.05503 mg/Kg 110 43 - 142 5 50 6
Carbon disulfide 0.0500 0.04859 mg/Kg 97 74 - 135 4 50
Carbon tetrachloride 0.0500 0.04957 mg/Kg 99 70 - 141 5 50 7
Chlorobenzene 0.0500 0.05076 mg/Kg 102 84 - 125 7 50
Chlorodibromomethane 0.0500 0.04677 mg/Kg 94 66 - 134 6 50 8
Chloroethane 0.0500 0.05317 mg/Kg 106 53 - 144 4 50
Chloroform 0.0500 0.04874 mg/Kg 97 76 - 130 8 49
Chloromethane 0.0500 0.04823 mg/Kg 96 23 - 150 3 50
9
cis-1,2-Dichloroethene 0.0500 0.04804 mg/Kg 96 75 - 125 9 50
cis-1,3-Dichloropropene 0.0500 0.05508 mg/Kg 110 73 - 148 9 50
10
Dibromomethane 0.0500 0.05254 mg/Kg 105 71 - 130 3 50
Dichlorodifluoromethane 0.0500 0.05912 mg/Kg 118 12 - 144 3 50
11
Ethylbenzene 0.0500 0.05021 mg/Kg 100 80 - 134 7 50
Hexachlorobutadiene 0.0500 0.04743 mg/Kg 95 65 - 148 9 50 12
Isopropylbenzene 0.0500 0.05074 mg/Kg 101 80 - 150 8 50
Methyl tert-butyl ether 0.0500 0.04998 mg/Kg 100 70 - 136 1 50 13
Methylene Chloride 0.0500 0.04947 mg/Kg 99 68 - 144 5 50
Naphthalene 0.0500 0.05006 mg/Kg 100 69 - 150 0 50
n-Butylbenzene 0.0500 0.04705 mg/Kg 94 72 - 152 9 50
N-Propylbenzene 0.0500 0.04592 mg/Kg 92 75 - 137 8 50
p-Isopropyltoluene 0.0500 0.04807 mg/Kg 96 77 - 141 7 50
sec-Butylbenzene 0.0500 0.04724 mg/Kg 94 79 - 141 8 50
Styrene 0.0500 0.05176 mg/Kg 104 82 - 137 8 50
tert-Butylbenzene 0.0500 0.05009 mg/Kg 100 80 - 132 7 50
Tetrachloroethene 0.0500 0.05119 mg/Kg 102 78 - 140 8 50
Toluene 0.0500 0.05146 mg/Kg 103 80 - 132 7 50
trans-1,2-Dichloroethene 0.0500 0.04856 mg/Kg 97 76 - 128 8 50
trans-1,3-Dichloropropene 0.0500 0.05049 mg/Kg 101 62 - 139 5 50
Trichloroethene 0.0500 0.05143 mg/Kg 103 77 - 127 7 50
Trichlorofluoromethane 0.0500 0.05020 mg/Kg 100 50 - 140 2 50
Vinyl chloride 0.0500 0.05368 mg/Kg 107 47 - 136 1 50
Xylenes, Total 0.100 0.1010 mg/Kg 101 80 - 137 9 50
LCSD LCSD

MB MB
1,1,1,2-Tetrachloroethane ND 0.00200 mg/Kg 07/08/14 14:09 1
1,1,2,2-Tetrachloroethane ND 0.00200 mg/Kg 07/08/14 14:09 1
Page 29 of 55 7/22/2014
QC Sample Results 1
4
MB MB 5
1,1-Dichloroethane ND 0.00200 mg/Kg 07/08/14 14:09 1 6
1,1-Dichloroethene ND 0.00200 mg/Kg 07/08/14 14:09 1
1,1-Dichloropropene ND 0.00200 mg/Kg 07/08/14 14:09 1 7
1,2,3-Trichloropropane ND 0.00200 mg/Kg 07/08/14 14:09 1 8
1,2-Dibromo-3-Chloropropane ND 0.00500 mg/Kg 07/08/14 14:09 1
9
1,2-Dibromoethane (EDB) ND 0.00200 mg/Kg 07/08/14 14:09 1
10
11
1,3-Dichlorobenzene ND 0.00200 mg/Kg 07/08/14 14:09 1 12
1,4-Dichlorobenzene ND 0.00200 mg/Kg 07/08/14 14:09 1 13
2-Butanone (MEK) ND 0.0500 mg/Kg 07/08/14 14:09 1
2-Hexanone ND 0.0500 mg/Kg 07/08/14 14:09 1
4-Methyl-2-pentanone (MIBK) ND 0.0500 mg/Kg 07/08/14 14:09 1
Acetone ND 0.0500 mg/Kg 07/08/14 14:09 1
Benzene ND 0.00200 mg/Kg 07/08/14 14:09 1
Bromobenzene ND 0.00200 mg/Kg 07/08/14 14:09 1
Bromochloromethane ND 0.00200 mg/Kg 07/08/14 14:09 1
Bromodichloromethane ND 0.00200 mg/Kg 07/08/14 14:09 1
Bromoform ND 0.00200 mg/Kg 07/08/14 14:09 1
Bromomethane ND 0.00200 mg/Kg 07/08/14 14:09 1
Carbon disulfide ND 0.00500 mg/Kg 07/08/14 14:09 1
Carbon tetrachloride ND 0.00200 mg/Kg 07/08/14 14:09 1
Chlorobenzene ND 0.00200 mg/Kg 07/08/14 14:09 1
Chlorodibromomethane ND 0.00200 mg/Kg 07/08/14 14:09 1
Chloroethane ND 0.00500 mg/Kg 07/08/14 14:09 1
Chloroform ND 0.00200 mg/Kg 07/08/14 14:09 1
Chloromethane ND 0.00200 mg/Kg 07/08/14 14:09 1
cis-1,2-Dichloroethene ND 0.00200 mg/Kg 07/08/14 14:09 1
cis-1,3-Dichloropropene ND 0.00200 mg/Kg 07/08/14 14:09 1
Dibromomethane ND 0.00200 mg/Kg 07/08/14 14:09 1
Dichlorodifluoromethane ND 0.00200 mg/Kg 07/08/14 14:09 1
Ethylbenzene ND 0.00200 mg/Kg 07/08/14 14:09 1
Hexachlorobutadiene ND 0.00500 mg/Kg 07/08/14 14:09 1
Isopropylbenzene ND 0.00200 mg/Kg 07/08/14 14:09 1
Methyl tert-butyl ether ND 0.00200 mg/Kg 07/08/14 14:09 1
Methylene Chloride ND 0.0100 mg/Kg 07/08/14 14:09 1
Naphthalene ND 0.00500 mg/Kg 07/08/14 14:09 1
n-Butylbenzene ND 0.00200 mg/Kg 07/08/14 14:09 1
N-Propylbenzene ND 0.00200 mg/Kg 07/08/14 14:09 1
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4
MB MB 5
p-Isopropyltoluene ND 0.00200 mg/Kg 07/08/14 14:09 1 6
sec-Butylbenzene ND 0.00200 mg/Kg 07/08/14 14:09 1
Styrene ND 0.00200 mg/Kg 07/08/14 14:09 1 7
tert-Butylbenzene ND 0.00200 mg/Kg 07/08/14 14:09 1
Tetrachloroethene ND 0.00200 mg/Kg 07/08/14 14:09 1 8
Toluene ND 0.00200 mg/Kg 07/08/14 14:09 1
trans-1,2-Dichloroethene ND 0.00200 mg/Kg 07/08/14 14:09 1
trans-1,3-Dichloropropene ND 0.00200 mg/Kg 07/08/14 14:09 1
9
Trichloroethene ND 0.00200 mg/Kg 07/08/14 14:09 1
Trichlorofluoromethane ND 0.00200 mg/Kg 07/08/14 14:09 1
10
Vinyl chloride ND 0.00200 mg/Kg 07/08/14 14:09 1
11
MB MB 12
13
Toluene-d8 (Surr) 101 70 - 130 07/08/14 14:09 1
Spike LCS LCS %Rec.
1,1-Dichloroethene 0.0500 0.05346 mg/Kg 107 75 - 131
1,1-Dichloropropene 0.0500 0.04829 mg/Kg 97 79 - 127
1,2,3-Trichloropropane 0.0500 0.05406 mg/Kg 108 65 - 139
1,2-Dibromo-3-Chloropropane 0.0500 0.06685 mg/Kg 134 49 - 142
1,2-Dibromoethane (EDB) 0.0500 0.05356 mg/Kg 107 80 - 135
2-Butanone (MEK) 0.250 0.3130 mg/Kg 125 61 - 132
2-Hexanone 0.250 0.3004 mg/Kg 120 57 - 148
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4-Chlorotoluene 0.0500 0.04485 mg/Kg 90 77 - 138 6
4-Methyl-2-pentanone (MIBK) 0.250 0.2982 mg/Kg 119 59 - 138
Acetone 0.250 0.3032 mg/Kg 121 51 - 149 7
Benzene 0.0500 0.05238 mg/Kg 105 75 - 127
Bromobenzene 0.0500 0.04449 mg/Kg 89 75 - 130 8
Bromochloromethane 0.0500 0.06132 mg/Kg 123 70 - 132
Bromodichloromethane 0.0500 0.05826 mg/Kg 117 68 - 135
Bromoform 0.0500 0.08036 * mg/Kg 161 36 - 150
9
Bromomethane 0.0500 0.05001 mg/Kg 100 43 - 142
Carbon disulfide 0.0500 0.05777 mg/Kg 116 74 - 135
10
Carbon tetrachloride 0.0500 0.06039 mg/Kg 121 70 - 141
Chlorobenzene 0.0500 0.05057 mg/Kg 101 84 - 125
11
Chlorodibromomethane 0.0500 0.06083 mg/Kg 122 66 - 134
Chloroethane 0.0500 0.04981 mg/Kg 100 53 - 144 12
Chloroform 0.0500 0.05027 mg/Kg 101 76 - 130
Chloromethane 0.0500 0.03906 mg/Kg 78 23 - 150 13
cis-1,2-Dichloroethene 0.0500 0.04942 mg/Kg 99 75 - 125
cis-1,3-Dichloropropene 0.0500 0.05030 mg/Kg 101 73 - 148
Dibromomethane 0.0500 0.05624 mg/Kg 112 71 - 130
Dichlorodifluoromethane 0.0500 0.05161 mg/Kg 103 12 - 144
Hexachlorobutadiene 0.0500 0.04996 mg/Kg 100 65 - 148
Isopropylbenzene 0.0500 0.04707 mg/Kg 94 80 - 150
Methyl tert-butyl ether 0.0500 0.03656 mg/Kg 73 70 - 136
Methylene Chloride 0.0500 0.05501 mg/Kg 110 68 - 144
n-Butylbenzene 0.0500 0.04133 mg/Kg 83 72 - 152
N-Propylbenzene 0.0500 0.04286 mg/Kg 86 75 - 137
p-Isopropyltoluene 0.0500 0.04569 mg/Kg 91 77 - 141
sec-Butylbenzene 0.0500 0.04330 mg/Kg 87 79 - 141
Styrene 0.0500 0.05093 mg/Kg 102 82 - 137
tert-Butylbenzene 0.0500 0.04337 mg/Kg 87 80 - 132
Tetrachloroethene 0.0500 0.05222 mg/Kg 104 78 - 140
Toluene 0.0500 0.04640 mg/Kg 93 80 - 132
trans-1,2-Dichloroethene 0.0500 0.05361 mg/Kg 107 76 - 128
trans-1,3-Dichloropropene 0.0500 0.05328 mg/Kg 107 62 - 139
Trichloroethene 0.0500 0.05268 mg/Kg 105 77 - 127
Trichlorofluoromethane 0.0500 0.05034 mg/Kg 101 50 - 140
Vinyl chloride 0.0500 0.05003 mg/Kg 100 47 - 136
Xylenes, Total 0.100 0.09156 mg/Kg 92 80 - 137
LCS LCS
Page 32 of 55 7/22/2014
QC Sample Results 1
Lab Sample ID: LCSD 490-175076/4 Client Sample ID: Lab Control Sample Dup 4
5
1,1,1,2-Tetrachloroethane 0.0500 0.06336 mg/Kg 127 80 - 136 3 50 6
1,1,2,2-Tetrachloroethane 0.0500 0.05346 mg/Kg 107 66 - 134 1 50 7
1,1-Dichloroethane 0.0500 0.05125 mg/Kg 102 75 - 124 1 50 8
1,1-Dichloroethene 0.0500 0.05269 mg/Kg 105 75 - 131 1 50
1,1-Dichloropropene 0.0500 0.04798 mg/Kg 96 79 - 127 1 50 9
1,2,3-Trichloropropane 0.0500 0.05464 mg/Kg 109 65 - 139 1 50 10
0.0500
0.0500
0.04433
0.06652
mg/Kg
mg/Kg
89
133
77 - 139
49 - 142
0
0
50
50
11
1,2-Dibromoethane (EDB) 0.0500 0.05370 mg/Kg 107 80 - 135 0 50
12
13
2-Butanone (MEK) 0.250 0.3011 mg/Kg 120 61 - 132 4 50
2-Hexanone 0.250 0.2980 mg/Kg 119 57 - 148 1 50
4-Methyl-2-pentanone (MIBK) 0.250 0.2917 mg/Kg 117 59 - 138 2 50
Acetone 0.250 0.2900 mg/Kg 116 51 - 149 4 50
Benzene 0.0500 0.05161 mg/Kg 103 75 - 127 1 50
Bromobenzene 0.0500 0.04479 mg/Kg 90 75 - 130 1 50
Bromochloromethane 0.0500 0.06018 mg/Kg 120 70 - 132 2 50
Bromodichloromethane 0.0500 0.05701 mg/Kg 114 68 - 135 2 50
Bromoform 0.0500 0.08043 * mg/Kg 161 36 - 150 0 50
Bromomethane 0.0500 0.05280 mg/Kg 106 43 - 142 5 50
Carbon disulfide 0.0500 0.05733 mg/Kg 115 74 - 135 1 50
Carbon tetrachloride 0.0500 0.05956 mg/Kg 119 70 - 141 1 50
Chlorobenzene 0.0500 0.05056 mg/Kg 101 84 - 125 0 50
Chlorodibromomethane 0.0500 0.06093 mg/Kg 122 66 - 134 0 50
Chloroethane 0.0500 0.05013 mg/Kg 100 53 - 144 1 50
Chloroform 0.0500 0.04974 mg/Kg 99 76 - 130 1 49
Chloromethane 0.0500 0.03813 mg/Kg 76 23 - 150 2 50
cis-1,2-Dichloroethene 0.0500 0.04861 mg/Kg 97 75 - 125 2 50
cis-1,3-Dichloropropene 0.0500 0.05077 mg/Kg 102 73 - 148 1 50
Dibromomethane 0.0500 0.05429 mg/Kg 109 71 - 130 4 50
Dichlorodifluoromethane 0.0500 0.05013 mg/Kg 100 12 - 144 3 50
Hexachlorobutadiene 0.0500 0.04918 mg/Kg 98 65 - 148 2 50
Isopropylbenzene 0.0500 0.04807 mg/Kg 96 80 - 150 2 50
Methyl tert-butyl ether 0.0500 0.03554 mg/Kg 71 70 - 136 3 50
Page 33 of 55 7/22/2014
QC Sample Results 1
4
Methylene Chloride 0.0500 0.05351 mg/Kg 107 68 - 144 3 50 6
Naphthalene 0.0500 0.04360 mg/Kg 87 69 - 150 3 50
n-Butylbenzene 0.0500 0.04083 mg/Kg 82 72 - 152 1 50 7
N-Propylbenzene 0.0500 0.04308 mg/Kg 86 75 - 137 0 50
p-Isopropyltoluene 0.0500 0.04545 mg/Kg 91 77 - 141 1 50 8
sec-Butylbenzene 0.0500 0.04337 mg/Kg 87 79 - 141 0 50
Styrene 0.0500 0.05216 mg/Kg 104 82 - 137 2 50
tert-Butylbenzene 0.0500 0.04335 mg/Kg 87 80 - 132 0 50
9
Tetrachloroethene 0.0500 0.05337 mg/Kg 107 78 - 140 2 50
Toluene 0.0500 0.04679 mg/Kg 94 80 - 132 1 50
10
trans-1,2-Dichloroethene 0.0500 0.05107 mg/Kg 102 76 - 128 5 50
trans-1,3-Dichloropropene 0.0500 0.05344 mg/Kg 107 62 - 139 0 50
11
Trichloroethene 0.0500 0.05319 mg/Kg 106 77 - 127 1 50
Trichlorofluoromethane 0.0500 0.04922 mg/Kg 98 50 - 140 2 50 12
Vinyl chloride 0.0500 0.04997 mg/Kg 100 47 - 136 0 50
Xylenes, Total 0.100 0.09290 mg/Kg 93 80 - 137 1 50 13
LCSD LCSD
Lab Sample ID: MB 490-174470/1-A Client Sample ID: Method Blank

MB MB
Page 34 of 55 7/22/2014
QC Sample Results 1
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued) 3
4
MB MB 5
3 & 4 Methylphenol ND 0.333 mg/Kg 07/03/14 10:13 07/03/14 20:30 1 6
3-Nitroaniline ND 0.833 mg/Kg 07/03/14 10:13 07/03/14 20:30 1 7
4-Chloro-3-methylphenol ND 0.333 mg/Kg 07/03/14 10:13 07/03/14 20:30 1 8
9
10
11
Benzo[a]anthracene ND 0.0670 mg/Kg 07/03/14 10:13 07/03/14 20:30 1 12
Benzo[b]fluoranthene ND 0.0670 mg/Kg 07/03/14 10:13 07/03/14 20:30 1 13
bis (2-chloroisopropyl) ether ND 0.333 mg/Kg 07/03/14 10:13 07/03/14 20:30 1
Chrysene ND 0.0670 mg/Kg 07/03/14 10:13 07/03/14 20:30 1
Dibenzofuran ND 0.333 mg/Kg 07/03/14 10:13 07/03/14 20:30 1
Diethyl phthalate ND 0.333 mg/Kg 07/03/14 10:13 07/03/14 20:30 1
Fluorene ND 0.0670 mg/Kg 07/03/14 10:13 07/03/14 20:30 1
diphenylamine)
Pyrene ND 0.0670 mg/Kg 07/03/14 10:13 07/03/14 20:30 1
Phenol ND 0.333 mg/Kg 07/03/14 10:13 07/03/14 20:30 1
Cresols ND 0.666 mg/Kg 07/03/14 10:13 07/03/14 20:30 1
Page 35 of 55 7/22/2014
QC Sample Results 1
4
MB MB 5
Butyl benzyl phthalate ND 0.333 mg/Kg 07/03/14 10:13 07/03/14 20:30 1 6
MB MB
7
2-Fluorophenol (Surr) 64 10 - 120 07/03/14 10:13 07/03/14 20:30 1 8
2,4,6-Tribromophenol (Surr) 77 10 - 120 07/03/14 10:13 07/03/14 20:30 1 9
Phenol-d5 (Surr) 68 10 - 120 07/03/14 10:13 07/03/14 20:30 1
Terphenyl-d14 (Surr) 85 13 - 120 07/03/14 10:13 07/03/14 20:30 1 10
Lab Sample ID: LCS 490-174470/2-A Client Sample ID: Lab Control Sample 11
Analysis Batch: 174526 Prep Batch: 174470 12
Spike LCS LCS %Rec.
13
1-Methylnaphthalene 1.67 1.331 mg/Kg 80 32 - 120
2,4,5-Trichlorophenol 1.67 1.548 mg/Kg 93 39 - 120
2,4,6-Trichlorophenol 1.67 1.548 mg/Kg 93 39 - 120
2,4-Dichlorophenol 1.67 1.370 mg/Kg 82 32 - 120
2,4-Dimethylphenol 1.67 1.486 mg/Kg 89 32 - 120
2,4-Dinitrophenol 3.33 2.172 mg/Kg 65 10 - 142
2,4-Dinitrotoluene 1.67 1.542 mg/Kg 93 43 - 120
2,6-Dinitrotoluene 1.67 1.561 mg/Kg 94 43 - 120
2-Chloronaphthalene 1.67 1.393 mg/Kg 84 34 - 120
2-Chlorophenol 1.67 1.362 mg/Kg 82 32 - 120
2-Methylphenol 1.67 1.410 mg/Kg 85 36 - 120
2-Methylnaphthalene 1.67 1.338 mg/Kg 80 28 - 120
2-Nitroaniline 1.67 1.590 mg/Kg 95 40 - 120
2-Nitrophenol 1.67 1.467 mg/Kg 88 29 - 120
3 & 4 Methylphenol 1.67 1.372 mg/Kg 82 37 - 120
3,3'-Dichlorobenzidine 1.67 1.380 mg/Kg 83 39 - 120
4,6-Dinitro-2-methylphenol 3.33 2.819 mg/Kg 85 27 - 134
4-Chloro-3-methylphenol 1.67 1.539 mg/Kg 92 38 - 120
4-Bromophenyl phenyl ether 1.67 1.515 mg/Kg 91 40 - 120
4-Chloroaniline 1.67 1.088 mg/Kg 65 35 - 120
4-Chlorophenyl phenyl ether 1.67 1.394 mg/Kg 84 42 - 120
4-Nitrophenol 3.33 3.061 mg/Kg 92 32 - 136
Acenaphthene 1.67 1.429 mg/Kg 86 36 - 120
Acenaphthylene 1.67 1.441 mg/Kg 86 38 - 120
Anthracene 1.67 1.479 mg/Kg 89 46 - 124
Benzo[a]anthracene 1.67 1.505 mg/Kg 90 45 - 120
Benzo[a]pyrene 1.67 1.494 mg/Kg 90 45 - 120
Page 36 of 55 7/22/2014
QC Sample Results 1
Lab Sample ID: LCS 490-174470/2-A Client Sample ID: Lab Control Sample
4
Benzo[b]fluoranthene 1.67 1.485 mg/Kg 89 42 - 120 6
Benzo[g,h,i]perylene 1.67 1.457 mg/Kg 87 38 - 120
Benzo[k]fluoranthene 1.67 1.462 mg/Kg 88 42 - 120 7
bis (2-chloroisopropyl) ether 1.67 1.300 mg/Kg 78 32 - 120
Carbazole 1.67 1.423 mg/Kg 85 44 - 120 8
Chrysene 1.67 1.475 mg/Kg 89 43 - 120
Dibenz(a,h)anthracene 1.67 1.508 mg/Kg 90 32 - 128
Dibenzofuran 1.67 1.379 mg/Kg 83 41 - 120
9
Dimethyl phthalate 1.67 1.445 J mg/Kg 87 55 - 120
Diethyl phthalate 1.67 1.452 mg/Kg 87 41 - 122
10
Di-n-butyl phthalate 1.67 1.548 mg/Kg 93 46 - 127
Di-n-octyl phthalate 1.67 1.613 mg/Kg 97 40 - 130
11
Fluorene 1.67 1.419 mg/Kg 85 42 - 120
Fluoranthene 1.67 1.448 mg/Kg 87 46 - 120 12
Hexachlorobenzene 1.67 1.533 mg/Kg 92 44 - 120
Hexachlorobutadiene 1.67 1.351 mg/Kg 81 31 - 120 13
Hexachlorocyclopentadiene 1.67 1.351 mg/Kg 81 24 - 120
Hexachloroethane 1.67 1.275 mg/Kg 77 33 - 120
Indeno[1,2,3-cd]pyrene 1.67 1.436 mg/Kg 86 41 - 121
Isophorone 1.67 1.433 mg/Kg 86 33 - 120
Nitrobenzene 1.67 1.332 mg/Kg 80 26 - 120
N-Nitrosodi-n-propylamine 1.67 1.259 mg/Kg 76 35 - 120
Pentachlorophenol 3.33 3.286 mg/Kg 99 44 - 134
Phenanthrene 1.67 1.434 mg/Kg 86 45 - 120
Pyrene 1.67 1.496 mg/Kg 90 43 - 120
Phenol 1.67 1.485 mg/Kg 89 30 - 120
Bis(2-chloroethoxy)methane 1.67 1.350 mg/Kg 81 32 - 120
Bis(2-chloroethyl)ether 1.67 1.215 mg/Kg 73 31 - 120
Bis(2-ethylhexyl) phthalate 1.67 1.628 mg/Kg 98 43 - 120
Butyl benzyl phthalate 1.67 1.602 mg/Kg 96 43 - 133
LCS LCS
Nitrobenzene-d5 (Surr) 78 27 - 120
2-Fluorophenol (Surr) 80 10 - 120
2-Fluorobiphenyl (Surr) 79 29 - 120
2,4,6-Tribromophenol (Surr) 95 10 - 120
Phenol-d5 (Surr) 82 10 - 120
Terphenyl-d14 (Surr) 94 13 - 120
Lab Sample ID: 490-56457-A-1-B MS Client Sample ID: Matrix Spike

Page 37 of 55 7/22/2014
QC Sample Results 1
4
1,2-Dichlorobenzene ND 1.67 1.053 mg/Kg 63 10 - 120 6
1-Methylnaphthalene 0.0903 1.67 1.194 mg/Kg 66 10 - 120
2,4,5-Trichlorophenol ND 1.67 1.225 mg/Kg 74 27 - 120 7
2,4,6-Trichlorophenol ND 1.67 1.240 mg/Kg 74 24 - 122
2,4-Dichlorophenol ND 1.67 1.135 mg/Kg 68 17 - 120 8
2,4-Dimethylphenol ND 1.67 1.056 mg/Kg 63 17 - 120
2,4-Dinitrophenol ND 3.33 0.5870 mg/Kg 18 10 - 150
2,4-Dinitrotoluene ND 1.67 1.231 mg/Kg 74 24 - 121
9
2,6-Dinitrotoluene ND 1.67 1.241 mg/Kg 74 24 - 120
2-Chloronaphthalene ND 1.67 1.197 mg/Kg 72 24 - 120
10
2-Chlorophenol ND 1.67 1.151 mg/Kg 69 25 - 120
2-Methylphenol ND 1.67 1.118 mg/Kg 67 23 - 120
11
2-Methylnaphthalene 0.0860 1.67 1.212 mg/Kg 68 13 - 120
2-Nitroaniline ND 1.67 1.279 mg/Kg 77 31 - 120 12
2-Nitrophenol ND 1.67 1.278 mg/Kg 77 23 - 120
3 & 4 Methylphenol ND 1.67 1.112 mg/Kg 67 19 - 120 13
3,3'-Dichlorobenzidine ND 1.67 ND mg/Kg 36 10 - 120
3-Nitroaniline ND 1.67 1.073 mg/Kg 64 31 - 120
4,6-Dinitro-2-methylphenol ND 3.33 1.503 mg/Kg 45 10 - 134
4-Chloro-3-methylphenol ND 1.67 1.179 mg/Kg 71 21 - 120
4-Bromophenyl phenyl ether ND 1.67 1.237 mg/Kg 74 31 - 120
4-Chloroaniline ND 1.67 1.001 mg/Kg 60 26 - 120
4-Chlorophenyl phenyl ether ND 1.67 1.144 mg/Kg 69 26 - 120
4-Nitroaniline ND 1.67 1.009 mg/Kg 61 28 - 120
4-Nitrophenol ND 3.33 2.157 mg/Kg 65 16 - 139
Acenaphthene 0.0890 1.67 1.235 mg/Kg 69 19 - 120
Acenaphthylene 0.0868 1.67 1.243 mg/Kg 69 25 - 120
Anthracene 0.320 1.67 1.337 mg/Kg 61 28 - 125
Benzo[a]anthracene 1.30 1.67 1.844 mg/Kg 33 23 - 120
Benzo[a]pyrene 1.14 1.67 1.763 mg/Kg 37 15 - 128
Benzo[b]fluoranthene 1.62 1.67 2.126 mg/Kg 31 12 - 133
Benzo[g,h,i]perylene 0.814 1.67 1.631 mg/Kg 49 22 - 120
Benzo[k]fluoranthene 0.726 1.67 1.521 mg/Kg 48 28 - 120
bis (2-chloroisopropyl) ether ND 1.67 1.139 mg/Kg 68 20 - 120
Carbazole ND 1.67 1.203 mg/Kg 64 25 - 123
Chrysene 1.34 1.67 1.865 mg/Kg 31 20 - 120
Dibenz(a,h)anthracene ND 1.67 1.319 mg/Kg 79 12 - 128
Dibenzofuran ND 1.67 1.178 mg/Kg 67 21 - 120
Dimethyl phthalate ND 1.67 ND mg/Kg 65 30 - 120
Diethyl phthalate ND 1.67 1.148 mg/Kg 69 29 - 122
Di-n-butyl phthalate ND 1.67 1.239 mg/Kg 74 29 - 126
Di-n-octyl phthalate ND 1.67 1.395 mg/Kg 84 27 - 130
Fluorene 0.0690 1.67 1.186 mg/Kg 67 20 - 120
Fluoranthene 2.22 1.67 2.178 F1 mg/Kg -2 10 - 143
Hexachlorobenzene ND 1.67 1.224 mg/Kg 74 25 - 120
Hexachlorobutadiene ND 1.67 1.137 mg/Kg 68 10 - 120
Hexachlorocyclopentadiene ND 1.67 0.8501 mg/Kg 51 10 - 120
Hexachloroethane ND 1.67 1.087 mg/Kg 65 10 - 120
Page 38 of 55 7/22/2014
QC Sample Results 1
4
Indeno[1,2,3-cd]pyrene 0.689 1.67 1.578 mg/Kg 53 22 - 121 6
Isophorone ND 1.67 1.193 mg/Kg 72 24 - 120
Naphthalene ND 1.67 1.171 mg/Kg 67 10 - 120 7
Nitrobenzene ND 1.67 1.166 mg/Kg 70 19 - 120
N-Nitrosodi-n-propylamine ND 1.67 1.095 mg/Kg 66 24 - 120 8
Pentachlorophenol ND 3.33 2.160 mg/Kg 65 19 - 145
Phenanthrene 1.41 1.67 1.684 F1 mg/Kg 17 21 - 122
Pyrene 2.07 1.67 2.247 F1 mg/Kg 10 20 - 123
9
Phenol ND 1.67 1.246 mg/Kg 75 15 - 120
Bis(2-chloroethoxy)methane ND 1.67 1.144 mg/Kg 69 24 - 120
10
Bis(2-chloroethyl)ether ND 1.67 1.058 mg/Kg 64 22 - 120
Bis(2-ethylhexyl) phthalate ND 1.67 1.371 mg/Kg 78 26 - 120
11
Butyl benzyl phthalate ND 1.67 1.346 mg/Kg 81 24 - 133
12
MS MS
Surrogate
Nitrobenzene-d5 (Surr)
%Recovery Qualifier
71
Limits
27 - 120
13
Phenol-d5 (Surr) 72 10 - 120
Lab Sample ID: 490-56457-A-1-C MSD Client Sample ID: Matrix Spike Duplicate
1-Methylnaphthalene 0.0903 1.61 1.154 mg/Kg 66 10 - 120 3 50
2,4,5-Trichlorophenol ND 1.61 1.212 mg/Kg 75 27 - 120 1 50
2,4,6-Trichlorophenol ND 1.61 1.257 mg/Kg 78 24 - 122 1 50
2,4-Dichlorophenol ND 1.61 1.144 mg/Kg 71 17 - 120 1 50
2,4-Dimethylphenol ND 1.61 1.153 mg/Kg 71 17 - 120 9 50
2,4-Dinitrophenol ND 3.23 0.7965 mg/Kg 25 10 - 150 30 50
2,4-Dinitrotoluene ND 1.61 1.256 mg/Kg 78 24 - 121 2 50
2,6-Dinitrotoluene ND 1.61 1.271 mg/Kg 79 24 - 120 2 50
2-Chloronaphthalene ND 1.61 1.197 mg/Kg 74 24 - 120 0 50
2-Chlorophenol ND 1.61 1.155 mg/Kg 72 25 - 120 0 50
2-Methylphenol ND 1.61 1.183 mg/Kg 73 23 - 120 6 50
2-Methylnaphthalene 0.0860 1.61 1.159 mg/Kg 66 13 - 120 4 50
2-Nitroaniline ND 1.61 1.332 mg/Kg 82 31 - 120 4 50
2-Nitrophenol ND 1.61 1.295 mg/Kg 80 23 - 120 1 50
3 & 4 Methylphenol ND 1.61 1.166 mg/Kg 72 19 - 120 5 50
3,3'-Dichlorobenzidine ND 1.61 0.7828 mg/Kg 48 10 - 120 27 50
Page 39 of 55 7/22/2014
QC Sample Results 1
4
4,6-Dinitro-2-methylphenol ND 3.23 1.595 mg/Kg 49 10 - 134 6 50 6
4-Chloro-3-methylphenol ND 1.61 1.231 mg/Kg 76 21 - 120 4 49
4-Bromophenyl phenyl ether ND 1.61 1.219 mg/Kg 75 31 - 120 1 37 7
4-Chloroaniline ND 1.61 1.027 mg/Kg 64 26 - 120 3 50
4-Chlorophenyl phenyl ether ND 1.61 1.146 mg/Kg 71 26 - 120 0 50 8
4-Nitrophenol ND 3.23 2.434 mg/Kg 75 16 - 139 12 45
Acenaphthene 0.0890 1.61 1.209 mg/Kg 69 19 - 120 2 50
9
Acenaphthylene 0.0868 1.61 1.227 mg/Kg 71 25 - 120 1 50
Anthracene 0.320 1.61 1.322 mg/Kg 62 28 - 125 1 49
10
Benzo[a]anthracene 1.30 1.61 2.072 mg/Kg 48 23 - 120 12 50
Benzo[a]pyrene 1.14 1.61 1.851 mg/Kg 44 15 - 128 5 50
11
Benzo[b]fluoranthene 1.62 1.61 2.149 mg/Kg 33 12 - 133 1 50
Benzo[g,h,i]perylene 0.814 1.61 1.639 mg/Kg 51 22 - 120 1 50 12
Benzo[k]fluoranthene 0.726 1.61 1.534 mg/Kg 50 28 - 120 1 45
bis (2-chloroisopropyl) ether ND 1.61 1.114 mg/Kg 69 20 - 120 2 50 13
Carbazole ND 1.61 1.190 mg/Kg 65 25 - 123 1 46
Chrysene 1.34 1.61 1.881 mg/Kg 33 20 - 120 1 49
Dibenz(a,h)anthracene ND 1.61 1.297 mg/Kg 80 12 - 128 2 50
Dibenzofuran ND 1.61 1.157 mg/Kg 68 21 - 120 2 50
Dimethyl phthalate ND 1.61 ND mg/Kg 66 30 - 120 2 46
Diethyl phthalate ND 1.61 1.165 mg/Kg 72 29 - 122 1 45
Di-n-butyl phthalate ND 1.61 1.220 mg/Kg 76 29 - 126 2 49
Di-n-octyl phthalate ND 1.61 1.386 mg/Kg 86 27 - 130 1 50
Fluorene 0.0690 1.61 1.184 mg/Kg 69 20 - 120 0 50
Fluoranthene 2.22 1.61 2.308 F1 mg/Kg 6 10 - 143 6 50
Hexachlorobenzene ND 1.61 1.232 mg/Kg 76 25 - 120 1 50
Hexachlorobutadiene ND 1.61 1.135 mg/Kg 70 10 - 120 0 50
Hexachlorocyclopentadiene ND 1.61 0.7897 mg/Kg 49 10 - 120 7 50
Hexachloroethane ND 1.61 1.078 mg/Kg 67 10 - 120 1 50
Indeno[1,2,3-cd]pyrene 0.689 1.61 1.575 mg/Kg 55 22 - 121 0 50
Isophorone ND 1.61 1.195 mg/Kg 74 24 - 120 0 50
Naphthalene ND 1.61 1.134 mg/Kg 67 10 - 120 3 50
Nitrobenzene ND 1.61 1.155 mg/Kg 71 19 - 120 1 50
N-Nitrosodi-n-propylamine ND 1.61 1.090 mg/Kg 68 24 - 120 0 50
Pentachlorophenol ND 3.23 2.327 mg/Kg 72 19 - 145 7 50
Phenanthrene 1.41 1.61 1.563 F1 mg/Kg 10 21 - 122 7 50
Pyrene 2.07 1.61 2.331 F1 mg/Kg 16 20 - 123 4 50
Phenol ND 1.61 1.274 mg/Kg 79 15 - 120 2 50
Bis(2-chloroethoxy)methane ND 1.61 1.143 mg/Kg 71 24 - 120 0 50
Bis(2-chloroethyl)ether ND 1.61 1.019 mg/Kg 63 22 - 120 4 50
Bis(2-ethylhexyl) phthalate ND 1.61 1.351 mg/Kg 79 26 - 120 2 50
Butyl benzyl phthalate ND 1.61 1.347 mg/Kg 83 24 - 133 0 50
MSD MSD
Page 40 of 55 7/22/2014
QC Sample Results 1
4
MSD MSD
5
6
Phenol-d5 (Surr) 70 10 - 120
7

8
Lab Sample ID: MB 490-174513/1-A Client Sample ID: Method Blank 9
MB MB
PCB-1016 ND 0.0333 mg/Kg 07/03/14 11:34 07/09/14 00:43 1
PCB-1221 ND 0.0333 mg/Kg 07/03/14 11:34 07/09/14 00:43 1 12
PCB-1232 ND 0.0333 mg/Kg 07/03/14 11:34 07/09/14 00:43 1
PCB-1242 ND 0.0333 mg/Kg 07/03/14 11:34 07/09/14 00:43 1
13
PCB-1248 ND 0.0333 mg/Kg 07/03/14 11:34 07/09/14 00:43 1
PCB-1254 ND 0.0333 mg/Kg 07/03/14 11:34 07/09/14 00:43 1
PCB-1260 ND 0.0333 mg/Kg 07/03/14 11:34 07/09/14 00:43 1
MB MB
DCB Decachlorobiphenyl (Surr) 108 20 - 150 07/03/14 11:34 07/09/14 00:43 1
Spike LCS LCS %Rec.
PCB-1016 0.167 0.1742 mg/Kg 105 65 - 125
PCB-1260 0.167 0.1673 mg/Kg 100 52 - 150
LCS LCS
Tetrachloro-m-xylene 93 19 - 147
DCB Decachlorobiphenyl (Surr) 110 20 - 150
Lab Sample ID: 490-56655-1 MS Client Sample ID: MW-1 53.5 to 54.5 ft.
PCB-1016 ND 0.164 0.1699 mg/Kg 104 42 - 140
PCB-1260 ND 0.164 0.1532 mg/Kg 94 37 - 159
MS MS
Page 41 of 55 7/22/2014
QC Sample Results 1
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued) 3
Lab Sample ID: 490-56655-1 MSD Client Sample ID: MW-1 53.5 to 54.5 ft. 4
5
PCB-1016 ND 0.166 0.1710 mg/Kg 103 42 - 140 1 50 6
PCB-1260 ND 0.166 0.1644 mg/Kg 99 37 - 159 7 50
MSD MSD
7
8
9
Method: 6010B - Metals (ICP) 10
MB MB 12
Barium ND 1.96 mg/Kg 07/11/14 11:11 07/15/14 21:58 1 13
Chromium ND 0.980 mg/Kg 07/11/14 11:11 07/15/14 21:58 1
Lead ND 0.980 mg/Kg 07/11/14 11:11 07/15/14 21:58 1
Spike LCS LCS %Rec.
Barium 800 810.6 mg/Kg 101 80 - 120
Chromium 80.0 84.56 mg/Kg 106 80 - 120
Lead 20.0 20.08 mg/Kg 100 80 - 120
Lab Sample ID: LCSD 490-176051/3-A Client Sample ID: Lab Control Sample Dup
Barium 784 782.5 mg/Kg 100 80 - 120 4 20
Chromium 78.4 81.61 mg/Kg 104 80 - 120 4 20
Lead 19.6 19.20 mg/Kg 98 80 - 120 5 20
Lab Sample ID: 250-20036-B-1-B MS Client Sample ID: Matrix Spike

Barium 205 769 950.4 mg/Kg 97 75 - 125
Page 42 of 55 7/22/2014
QC Sample Results 1
Method: 6010B - Metals (ICP) (Continued) 3
Lab Sample ID: 250-20036-B-1-C MSD Client Sample ID: Matrix Spike Duplicate 4
5
Barium 205 800 974.6 mg/Kg 96 75 - 125 3 20 6
Chromium 2070 80.0 1819 E 4 mg/Kg -319 75 - 125 7 20
Lead 10500 20.0 10350 E 4 mg/Kg -770 75 - 125 3 20 7
Method: 7471A - Mercury (CVAA) 8
MB MB
11
Mercury ND 0.0998 mg/Kg 07/11/14 09:47 07/11/14 13:07 1
12
13
Spike LCS LCS %Rec.
Mercury 0.166 0.1557 mg/Kg 94 80 - 120
Lab Sample ID: 490-56404-A-1-I MS Client Sample ID: Matrix Spike

Mercury ND 0.164 0.1747 mg/Kg 84 75 - 125
Lab Sample ID: 490-56404-A-1-J MSD Client Sample ID: Matrix Spike Duplicate
Mercury ND 0.161 0.1654 mg/Kg 79 75 - 125 5 20
Page 43 of 55 7/22/2014
QC Association Summary 1
GC/MS VOA 3
Prep Batch: 174266
4
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
490-56655-1 MW-1 53.5 to 54.5 ft. Total/NA Solid 5030B
5
6
490-56655-4 MS MW-4 28.5 to 30.0 ft. Total/NA Solid 5030B
490-56655-4 MSD MW-4 28.5 to 30.0 ft. Total/NA Solid 5030B
7
Analysis Batch: 174623 8
490-56655-1 MW-1 53.5 to 54.5 ft. Total/NA Solid 8260B 174266 9
490-56655-2 MW-2 28.5 to 30.0 ft. Total/NA Solid 8260B 174266
490-56655-3 MW-3 38.5 to 40.0 ft. Total/NA Solid 8260B 174266 10
LCS 490-174623/5 Lab Control Sample Total/NA Solid 8260B
LCSD 490-174623/6 Lab Control Sample Dup Total/NA Solid 8260B 11
MB 490-174623/9 Method Blank Total/NA Solid 8260B

12
Lab Sample ID
490-56655-4
Client Sample ID
MW-4 28.5 to 30.0 ft.
Prep Type
Total/NA
Matrix
Solid
Method
8260B
Prep Batch
174266
13
490-56655-4 MS MW-4 28.5 to 30.0 ft. Total/NA Solid 8260B 174266
490-56655-4 MSD MW-4 28.5 to 30.0 ft. Total/NA Solid 8260B 174266
LCSD 490-175076/4 Lab Control Sample Dup Total/NA Solid 8260B
GC/MS Semi VOA

Prep Batch: 174470
490-56457-A-1-B MS Matrix Spike Total/NA Solid 3550B
490-56457-A-1-C MSD Matrix Spike Duplicate Total/NA Solid 3550B
LCS 490-174470/2-A Lab Control Sample Total/NA Solid 3550B
MB 490-174470/1-A Method Blank Total/NA Solid 3550B

490-56457-A-1-B MS Matrix Spike Total/NA Solid 8270C 174470
490-56457-A-1-C MSD Matrix Spike Duplicate Total/NA Solid 8270C 174470
490-56655-1 MW-1 53.5 to 54.5 ft. Total/NA Solid 8270C 174470
LCS 490-174470/2-A Lab Control Sample Total/NA Solid 8270C 174470
MB 490-174470/1-A Method Blank Total/NA Solid 8270C 174470
Page 44 of 55 7/22/2014
GC Semi VOA 3
Prep Batch: 174513
4
490-56655-1 MS MW-1 53.5 to 54.5 ft. Total/NA Solid 3550B
5
490-56655-1 MSD MW-1 53.5 to 54.5 ft. Total/NA Solid 3550B
6
7
LCS 490-174513/2-A Lab Control Sample Total/NA Solid 3550B
MB 490-174513/1-A Method Blank Total/NA Solid 3550B 8
490-56655-1 MW-1 53.5 to 54.5 ft. Total/NA Solid 8082 174513 10
490-56655-1 MS MW-1 53.5 to 54.5 ft. Total/NA Solid 8082 174513
490-56655-1 MSD MW-1 53.5 to 54.5 ft. Total/NA Solid 8082 174513 11
490-56655-2 MW-2 28.5 to 30.0 ft. Total/NA Solid 8082 174513
490-56655-3 MW-3 38.5 to 40.0 ft. Total/NA Solid 8082 174513 12
490-56655-4 MW-4 28.5 to 30.0 ft. Total/NA Solid 8082 174513
LCS 490-174513/2-A Lab Control Sample Total/NA Solid 8082 174513
MB 490-174513/1-A Method Blank Total/NA Solid 8082 174513
13
Metals
Prep Batch: 175977
490-56404-A-1-I MS Matrix Spike Total/NA Solid 7471A
490-56404-A-1-J MSD Matrix Spike Duplicate Total/NA Solid 7471A
490-56655-1 MW-1 53.5 to 54.5 ft. Total/NA Solid 7471A
LCS 490-175977/2-A Lab Control Sample Total/NA Solid 7471A
MB 490-175977/1-A Method Blank Total/NA Solid 7471A
Prep Batch: 176051

250-20036-B-1-B MS Matrix Spike Total/NA Solid 3051
250-20036-B-1-C MSD Matrix Spike Duplicate Total/NA Solid 3051
490-56655-1 MW-1 53.5 to 54.5 ft. Total/NA Solid 3051
LCS 490-176051/2-A Lab Control Sample Total/NA Solid 3051
LCSD 490-176051/3-A Lab Control Sample Dup Total/NA Solid 3051
MB 490-176051/1-A Method Blank Total/NA Solid 3051

490-56404-A-1-I MS Matrix Spike Total/NA Solid 7471A 175977
490-56404-A-1-J MSD Matrix Spike Duplicate Total/NA Solid 7471A 175977
490-56655-1 MW-1 53.5 to 54.5 ft. Total/NA Solid 7471A 175977
Page 45 of 55 7/22/2014
Metals (Continued) 3
Analysis Batch: 176414 (Continued)
4
5
LCS 490-175977/2-A Lab Control Sample Total/NA Solid 7471A 175977
6
MB 490-175977/1-A Method Blank Total/NA Solid 7471A 175977
7
8
250-20036-B-1-B MS Matrix Spike Total/NA Solid 6010B 176051
LCS 490-176051/2-A Lab Control Sample Total/NA Solid 6010B 176051 9
LCSD 490-176051/3-A Lab Control Sample Dup Total/NA Solid 6010B 176051
MB 490-176051/1-A Method Blank Total/NA Solid 6010B 176051 10
11
250-20036-B-1-C MSD Matrix Spike Duplicate Total/NA Solid 6010B 176051 12
13
Page 46 of 55 7/22/2014
Lab Chronicle 1
Date Received: 07/02/14 08:15 4
Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
5
Total/NA Prep 5030B 5.70 g 5.0 mL 174266 07/02/14 16:08 JLP TAL NSH
Total/NA Analysis 8260B 1 5.70 g 5.0 mL 174623 07/04/14 05:00 KKK TAL NSH
6
Total/NA Prep 3550B 30.60 g 1.0 mL 174470 07/03/14 10:13 LOJ TAL NSH
Total/NA Analysis 8270C 1 30.60 g 1.0 mL 174526 07/03/14 23:09 KKH TAL NSH
7
8
Total/NA Analysis 8082 1 30.70 g 10.00 mL 175046 07/09/14 01:29 MGH TAL NSH
Total/NA Prep 3051 0.500 g 100 mL 176051 07/11/14 11:11 JBD TAL NSH 9
Total/NA Analysis 6010B 1 0.500 g 100 mL 177018 07/15/14 22:42 DBK TAL NSH
Total/NA Prep 7471A 0.625 g 100 mL 175977 07/11/14 09:47 NLI TAL NSH 10
Total/NA Analysis 7471A 1 0.625 g 100 mL 176414 07/11/14 13:56 NLI TAL NSH
11
Date Collected: 06/30/14 15:25 Matrix: Solid 12
13
Total/NA Prep 3051 0.500 g 100 mL 176051 07/11/14 11:11 JBD TAL NSH
Total/NA Prep 7471A 0.621 g 100 mL 175977 07/11/14 09:47 NLI TAL NSH

Total/NA Prep 7471A 0.602 g 100 mL 175977 07/11/14 09:47 NLI TAL NSH
Page 47 of 55 7/22/2014
Lab Chronicle 1
Date Received: 07/02/14 08:15 4
5
Total/NA Analysis 8260B 1 5.39 g 5.0 mL 175076 07/08/14 14:39 KKK TAL NSH 6
7
8
9
Total/NA Prep 7471A 0.605 g 100 mL 175977 07/11/14 09:47 NLI TAL NSH 10
Laboratory References:
11
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177
12
13
Page 48 of 55 7/22/2014
Method Summary 1
3
Method Method Description Protocol Laboratory
8260B Volatile Organic Compounds (GC/MS) SW846 TAL NSH
8270C Semivolatile Organic Compounds (GC/MS) SW846 TAL NSH
4
8082 Polychlorinated Biphenyls (PCBs) by Gas Chromatography SW846 TAL NSH
6010B Metals (ICP) SW846 TAL NSH
5
7471A Mercury (CVAA) SW846 TAL NSH
6
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. 7
Laboratory References: 8
9
10
11
12
13
Page 49 of 55 7/22/2014
Certification Summary 1
All certifications held by this laboratory are listed. Not all certifications are applicable to this report.
3
Authority Program EPA Region Certification ID Expiration Date 4
A2LA A2LA NA: NELAP & A2LA 12-31-15
A2LA ISO/IEC 17025 0453.07 12-31-15 5
Alaska (UST) State Program 10 UST-087 07-24-14 *
Arizona State Program 9 AZ0473 05-05-15 6
Arkansas DEQ State Program 6 88-0737 04-25-15
California NELAP 9 1168CA 10-31-14
Connecticut State Program 1 PH-0220 12-31-15
7
Florida NELAP 4 E87358 06-30-15
Illinois NELAP 5 200010 12-09-14
8
Iowa State Program 7 131 04-01-16
Kansas NELAP 7 E-10229 10-31-14
9
Kentucky (UST) State Program 4 19 06-30-15
Louisiana NELAP 6 30613 06-30-15 10
Maryland State Program 3 316 03-31-15
Massachusetts State Program 1 M-TN032 06-30-15 11
Minnesota NELAP 5 047-999-345 12-31-14
Mississippi State Program 4 N/A 06-30-14 * 12
Montana (UST) State Program 8 NA 02-24-20
Nevada State Program 9 TN00032 07-31-14 13
New Hampshire NELAP 1 2963 10-09-14
New Jersey NELAP 2 TN965 06-30-15
New York NELAP 2 11342 03-31-15
North Carolina (WW/SW) State Program 4 387 12-31-14
North Dakota State Program 8 R-146 06-30-14 *
Ohio VAP State Program 5 CL0033 10-16-15
Oklahoma State Program 6 9412 08-31-14
Oregon NELAP 10 TN200001 04-29-15
Pennsylvania NELAP 3 68-00585 06-30-15
Rhode Island State Program 1 LAO00268 12-30-14
South Carolina State Program 4 84009 (001) 02-28-14 *
South Carolina (DW) State Program 4 84009 (002) 02-23-17
Tennessee State Program 4 2008 02-23-17
Texas NELAP 6 T104704077 08-31-14
USDA Federal S-48469 10-30-16
Utah NELAP 8 TN00032 07-31-15
Virginia NELAP 3 460152 06-14-15
Washington State Program 10 C789 07-19-14 *
West Virginia DEP State Program 3 219 02-28-15
Wisconsin State Program 5 998020430 08-31-14
Wyoming (UST) A2LA 8 453.07 12-31-15
* Certification renewal pending - certification considered valid.
Page 50 of 55 7/22/2014
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Page 51 of 55 7/22/2014
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Page 52 of 55 7/22/2014
Page 1 of 2
1
Brown, Shali
2
From: Watson, Brian W. [bwwatson@terracon.com]

3
Sent: Wednesday, July 16, 2014 12:02 PM 4
To: Brown, Shali
Cc: Stamper, Travis T 5
Subject: RE: Proposed Sams Club #4062 - Terracon Project Number E2137034 / Test America Job No. 490- 6
56655
That is correct. Analysis of all samples (soil and groundwater) to include VOCs, SVOCs, PCBs, and Metals 7
(aluminum, barium, chromium, copper, iron, lead, magnesium, nickel, and zinc).
Thanks. 8
Brian W. Watson
9
Terracon
51 Lost Mound Drive, Suite 135 I Chattanooga, TN 37406
10
P [423] 602-2107 I F [423] 499-8099 I M [423] 463-6355
bwwatson@terracon.com I terracon.com 11
12
From: Brown, Shali [mailto:Shali.Brown@testamericainc.com]
Sent: Wednesday, July 16, 2014 12:49 PM
To: Watson, Brian W.
13
Cc: Stamper, Travis T
Subject: RE: Proposed Sams Club #4062 - Terracon Project Number E2137034 / Test America Job No. 490-56655
Hi Brian,
If you could please clarify what is being requested for addition and removal of tests. Based on your email below
and the attached COC I currently have the following…….
For the water samples you want us to add the full list of SVOC’s to replace the PAH’s, remove arsenic, cadmium,
selenium, and silver, then add aluminum, copper, iron, magnesium, nickel, and zinc.
For the soil samples you want us to remove arsenic, cadmium, selenium, and silver, then add aluminum, copper,
iron, magnesium, nickel, and zinc.
Please confirm.
Thanks,
Shali
From: Watson, Brian W. [mailto:bwwatson@terracon.com]

Sent: Wednesday, July 16, 2014 9:01 AM
To: Brown, Shali
Subject: Proposed Sams Club #4062 - Terracon Project Number E2137034 / Test America Job No. 490-56655
Dear Ms. Brown,
Thanks for talking with me this morning. As mentioned, I need to get a revision placed on the laboratory analysis
for the proposed Sams Club #4062 job (Terracon Project Number E2137034 / Test America Job No. 490‐56655).
Analysis of all samples (soil and groundwater) to include VOCs, SVOCs, PCBs, and Metals (aluminum, barium,
chromium, copper, iron, lead, magnesium, nickel, and zinc).
Page 53 of 55 7/22/2014
7/17/2014
Page 2 of 2
1
2
Let me know if you have any questions or comments.
3
Thanks. 4
Brian W. Watson
5
Terracon 6
P [423] 602-2107 I F [423] 499-8099 I M [423] 463-6355 7
bwwatson@terracon.com I terracon.com
8
Terracon provides environmental, facilities, geotechnical, and materials consulting engineering services delivered with 9
responsiveness, resourcefulness, and reliability.
10
Private and confidential as detailed here (www.terracon.com/disclaimer). If you cannot access hyperlink, please e- 11
mail sender.
12
Terracon provides environmental, facilities, geotechnical, and materials consulting engineering services delivered with
responsiveness, resourcefulness, and reliability. 13
Private and confidential as detailed here (www.terracon.com/disclaimer). If you cannot access hyperlink, please e-
mail sender.
Page 54 of 55 7/22/2014
7/17/2014
1
Login Sample Receipt Checklist
2
Client: Terracon Consulting Eng & Scientists Job Number: 490-56655-1 3
SDG Number: Alcoa, TN
Login Number: 56655 List Source: TestAmerica Nashville

4
List Number: 1
Creator: Gambill, Shane
5
Question Answer Comment 6
Radioactivity wasn't checked or is </= background as measured by a True
survey meter. 7
The cooler's custody seal, if present, is intact. True
Sample custody seals, if present, are intact. True 8
The cooler or samples do not appear to have been compromised or True
tampered with. 9
Samples were received on ice. True
Cooler Temperature is acceptable. True 10
Cooler Temperature is recorded. True 5.0
COC is present. True 11
COC is filled out in ink and legible. True
COC is filled out with all pertinent information. True
12
Is the Field Sampler's name present on COC? True
13
There are no discrepancies between the containers received and the COC. True
Samples are received within Holding Time. True
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. True
There is sufficient vol. for all requested analyses, incl. any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True
<6mm (1/4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. True
Page 55 of 55 7/22/2014
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4
5
ANALYTICAL REPORT
6
Tel: (615)726-0177
9
Client Project/Site: Sam's Club #4062 E2135031
11
For:
Terracon Consulting Eng & Scientists 12
51 Lost Mound Suite 135
Chattanooga, Tennessee 37406 13

7/17/2014 7:51:54 PM
(615)301-5031
Project/Site: Sam's Club #4062 E2135031 SDG: Alcoa, TN
2
Table of Contents 3
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
5
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 6
9
8
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10 9
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
10
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13 11
13
Page 2 of 15 7/17/2014
Sample Summary 1
Project/Site: Sam's Club #4062 E2135031 SDG: Alcoa, TN 2
3
490-56782-1 B-15 18.5-20ft Solid 07/01/14 11:12 07/03/14 08:05
4
5
6
7
8
9
10
11
12
13
Page 3 of 15 7/17/2014
Case Narrative 1
Job ID: 490-56782-1 3
4
Narrative
Job Narrative 5
490-56782-1
6
Comments
No additional comments. 7
Receipt
The sample was received on 7/3/2014 8:05 AM; the sample arrived in good condition, properly preserved and, where required, on ice. The
8
temperature of the cooler at receipt was 1.2º C.
9
GC/MS VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. 10
VOA Prep
11
12
13
Page 4 of 15 7/17/2014
Glossary 3
¤ Listed under the "D" column to designate that the result is reported on a dry weight basis
4
%R Percent Recovery
CFL Contains Free Liquid
5
DER Duplicate error ratio (normalized absolute difference) 6
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample 7
MDA Minimum detectable activity 8
MDC Minimum detectable concentration 9
10
NC Not Calculated
11
QC Quality Control
12
13
Page 5 of 15 7/17/2014
Client Sample ID: B-15 18.5-20ft Lab Sample ID: 490-56782-1 3
4
Benzene ND 0.00195 mg/Kg 07/05/14 10:54 07/05/14 17:22 1
Ethylbenzene ND 0.00195 mg/Kg 07/05/14 10:54 07/05/14 17:22 1 6
Xylenes, Total ND 0.00292 mg/Kg 07/05/14 10:54 07/05/14 17:22 1
Toluene ND 0.00195 mg/Kg 07/05/14 10:54 07/05/14 17:22 1 7
8
Toluene-d8 (Surr) 105 70 - 130 07/05/14 10:54 07/05/14 17:22 1
9
10
11
12
13
Page 6 of 15 7/17/2014
QC Sample Results 1
Lab Sample ID: 490-56764-A-1-D MS Client Sample ID: Matrix Spike 4
5
Benzene ND 0.0427 0.05245 mg/Kg 121 31 - 143 6
Ethylbenzene ND 0.0427 0.05116 mg/Kg 120 23 - 161
Xylenes, Total ND 0.0855 0.09823 mg/Kg 115 25 - 162 7
Toluene ND 0.0427 0.05070 mg/Kg 119 30 - 155
MS MS
8
9
Toluene-d8 (Surr) 105 70 - 130 10
11
Lab Sample ID: 490-56764-A-1-E MSD Client Sample ID: Matrix Spike Duplicate
13
Benzene ND 0.0433 0.04485 mg/Kg 102 31 - 143 16 50
Ethylbenzene ND 0.0433 0.04638 mg/Kg 107 23 - 161 10 50
Xylenes, Total ND 0.0865 0.08838 mg/Kg 102 25 - 162 11 50
Toluene ND 0.0433 0.04633 mg/Kg 107 30 - 155 9 50
MSD MSD

MB MB
Benzene ND 0.00200 mg/Kg 07/05/14 15:06 1
Ethylbenzene ND 0.00200 mg/Kg 07/05/14 15:06 1
Toluene ND 0.00200 mg/Kg 07/05/14 15:06 1
MB MB
Toluene-d8 (Surr) 106 70 - 130 07/05/14 15:06 1
Page 7 of 15 7/17/2014
QC Sample Results 1
Lab Sample ID: LCS 490-174705/3 Client Sample ID: Lab Control Sample 4
Spike LCS LCS %Rec.
5
Benzene 0.0500 0.05314 mg/Kg 106 75 - 127 6
Xylenes, Total 0.100 0.1027 mg/Kg 103 80 - 137 7
Toluene 0.0500 0.05176 mg/Kg 104 80 - 132
LCS LCS
8
9
Toluene-d8 (Surr) 105 70 - 130 10
11
13
Benzene 0.0500 0.05265 mg/Kg 105 75 - 127 1 50
Xylenes, Total 0.100 0.09966 mg/Kg 100 80 - 137 3 50
Toluene 0.0500 0.05164 mg/Kg 103 80 - 132 0 50
LCSD LCSD
Page 8 of 15 7/17/2014
GC/MS VOA 3
Prep Batch: 174601
4
490-56764-A-1-D MS Matrix Spike Total/NA Solid 5030B
490-56764-A-1-E MSD Matrix Spike Duplicate Total/NA Solid 5030B
5
Prep Batch: 174696 6
490-56782-1 B-15 18.5-20ft Total/NA Solid 5030B
7
490-56764-A-1-D MS Matrix Spike Total/NA Solid 8260B 174601 9
490-56764-A-1-E MSD Matrix Spike Duplicate Total/NA Solid 8260B 174601
490-56782-1 B-15 18.5-20ft Total/NA Solid 8260B 174696 10
LCSD 490-174705/4 Lab Control Sample Dup Total/NA Solid 8260B 11
12
13
Page 9 of 15 7/17/2014
Lab Chronicle 1
Client Sample ID: B-15 18.5-20ft Lab Sample ID: 490-56782-1 3
Date Received: 07/03/14 08:05 4
5
6
7
8
9
10
11
12
13
Page 10 of 15 7/17/2014
Method Summary 1
3
4
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
5
Laboratory References: 6
7
8
9
10
11
12
13
Page 11 of 15 7/17/2014
3
A2LA ISO/IEC 17025 0453.07 12-31-15 5
Alaska (UST) State Program 10 UST-087 07-24-14
7
8
Iowa State Program 7 131 05-01-14 *
Kansas NELAP 7 E-10229 10-31-14
9
Minnesota NELAP 5 047-999-345 12-31-14
Mississippi State Program 4 N/A 06-30-14 * 12
New York NELAP 2 11342 03-31-15
Oregon NELAP 10 TN200001 04-29-15
Texas NELAP 6 T104704077 08-31-14
Utah NELAP 8 TN00032 07-31-14
Washington State Program 10 C789 07-19-14
Wisconsin State Program 5 998020430 08-31-14
Wyoming (UST) A2LA 8 453.07 12-31-15
Page 12 of 15 7/17/2014
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Page 14 of 15 7/17/2014
1
2

4
List Number: 1
5
Radioactivity wasn't checked or is </= background as measured by a True
survey meter. 7
tampered with. 9
12
13
Sample Preservation Verified. N/A
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is N/A
<6mm (1/4").
Residual Chlorine Checked. N/A
Page 15 of 15 7/17/2014
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2
3
4
5
ANALYTICAL REPORT
6
Tel: (615)726-0177
9
Client Project/Site: Proposed Sams Club #4062 E2137034
Revision: 1 11
For: 12
Terracon Consulting Eng & Scientists
51 Lost Mound Suite 135 13
Chattanooga, Tennessee 37406

7/30/2014 2:59:15 PM
(615)301-5031
Project/Site: Proposed Sams Club #4062 E2137034 SDG: Alcoa, TN
2
Table of Contents 3
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
5
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 6
39
8
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42 9
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44
10
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46 11
13
Page 2 of 58 7/30/2014
Sample Summary 1
3
490-56655-5 MW-1 Water 07/01/14 12:00 07/02/14 08:15
490-56655-6 MW-2 Water 07/01/14 13:25 07/02/14 08:15
4
490-56655-7 MW-3 Water 07/01/14 14:00 07/02/14 08:15
490-56655-8 MW-4 Water 07/01/14 14:50 07/02/14 08:15
5
490-56655-9 Trip Blank Water 07/01/14 00:01 07/02/14 08:15
6
7
8
9
10
11
12
13
Page 3 of 58 7/30/2014
Case Narrative 1
Job ID: 490-56655-2 3
4
Narrative
Job Narrative 5
490-56655-2
6
Comments
073014 Revised Report to add additional analysis at client request: hexavalent chromium, metals, and full list SVOC. Reference attached
email for details. This report replaces the report previously issued on 070914.
7
This report contains analysis for the water samples only; refference report 490-56655-1 for soil sample analysis.
8
Receipt 9
The samples were received on 7/2/2014 8:15 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 5.0º C. 10
GC/MS VOA
Method(s) 8260B: Analyzed from vial composed of sample transfer from vials B and C. MW-4 (490-56655-8)
11
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. 12
GC/MS Semi VOA 13
Method(s) 8270C: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP) associated with batch 174259 and 178800.
Method(s) 8270C: The following samples were analyzed outside of analytical holding time because the request for the test was made
after the holding time for the sample expired. MW-1 (490-56655-5), MW-2 (490-56655-6), MW-3 (490-56655-7), MW-4 (490-56655-8).
Method(s) 8270C: Surrogate recovery for the following sample was outside of acceptance limits: MW-4 (490-56655-8). There was
insufficient sample to perform a re-extraction; therefore, the data have been reported.
GC Semi VOA
Method(s) 8082: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP) associated with batch 174487.
Metals
Method(s) 6010B: The following sample(s) was diluted due to the abundance of analytes: Fe MW-1 (490-56655-5), MW-2 (490-56655-6),
MW-3 (490-56655-7), MW-4 (490-56655-8). Elevated reporting limits (RLs) are provided.
General Chemistry
Method(s) 7196A: The following sample(s) was prepared and analyzed outside method defined holding time because the request for the
test was made after the holding time for the sample expired: MW-1 (490-56655-5), MW-2 (490-56655-6), MW-3 (490-56655-7), MW-4
(490-56655-8).
Organic Prep
VOA Prep
Page 4 of 58 7/30/2014
Qualifiers 3
GC/MS Semi VOA
4
H Sample was prepped or analyzed beyond the specified holding time
X Surrogate is outside control limits
5
General Chemistry
6
H Sample was prepped or analyzed beyond the specified holding time
7
Glossary 8
¤ Listed under the "D" column to designate that the result is reported on a dry weight basis
9
%R Percent Recovery
CFL Contains Free Liquid 10
DER Duplicate error ratio (normalized absolute difference) 11
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample 12
MDA Minimum detectable activity 13
MDC Minimum detectable concentration
NC Not Calculated
QC Quality Control
Page 5 of 58 7/30/2014
Client Sample ID: MW-1 Lab Sample ID: 490-56655-5 3
Date Collected: 07/01/14 12:00 Matrix: Water
4
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 07/03/14 15:51 1
1,1,1-Trichloroethane ND 1.00 ug/L 07/03/14 15:51 1 6
1,1-Dichloroethane ND 1.00 ug/L 07/03/14 15:51 1
1,1-Dichloroethene ND 1.00 ug/L 07/03/14 15:51 1 8
1,1-Dichloropropene ND 1.00 ug/L 07/03/14 15:51 1
1,2,3-Trichlorobenzene ND 1.00 ug/L 07/03/14 15:51 1
1,2,3-Trichloropropane ND 1.00 ug/L 07/03/14 15:51 1
9
1,2,4-Trimethylbenzene ND 1.00 ug/L 07/03/14 15:51 1
10
1,2-Dibromo-3-Chloropropane ND 10.0 ug/L 07/03/14 15:51 1
1,2-Dibromoethane (EDB) ND 1.00 ug/L 07/03/14 15:51 1
11
1,2-Dichlorobenzene ND 1.00 ug/L 07/03/14 15:51 1
1,2-Dichloroethane ND 1.00 ug/L 07/03/14 15:51 1 12
1,2-Dichloropropane ND 1.00 ug/L 07/03/14 15:51 1
1,3,5-Trimethylbenzene ND 1.00 ug/L 07/03/14 15:51 1 13
2-Butanone (MEK) ND 50.0 ug/L 07/03/14 15:51 1
2-Chlorotoluene ND 1.00 ug/L 07/03/14 15:51 1
2-Hexanone ND 10.0 ug/L 07/03/14 15:51 1
4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L 07/03/14 15:51 1
Acetone ND 25.0 ug/L 07/03/14 15:51 1
Benzene ND 1.00 ug/L 07/03/14 15:51 1
Bromobenzene ND 1.00 ug/L 07/03/14 15:51 1
Bromochloromethane ND 1.00 ug/L 07/03/14 15:51 1
Bromodichloromethane ND 1.00 ug/L 07/03/14 15:51 1
Bromoform ND 1.00 ug/L 07/03/14 15:51 1
Bromomethane ND 1.00 ug/L 07/03/14 15:51 1
Carbon disulfide ND 1.00 ug/L 07/03/14 15:51 1
Carbon tetrachloride ND 1.00 ug/L 07/03/14 15:51 1
Chlorobenzene ND 1.00 ug/L 07/03/14 15:51 1
Chlorodibromomethane ND 1.00 ug/L 07/03/14 15:51 1
Chloroethane ND 1.00 ug/L 07/03/14 15:51 1
Chloroform ND 1.00 ug/L 07/03/14 15:51 1
Chloromethane ND 1.00 ug/L 07/03/14 15:51 1
cis-1,2-Dichloroethene ND 1.00 ug/L 07/03/14 15:51 1
cis-1,3-Dichloropropene ND 1.00 ug/L 07/03/14 15:51 1
Dibromomethane ND 1.00 ug/L 07/03/14 15:51 1
Dichlorodifluoromethane ND 1.00 ug/L 07/03/14 15:51 1
Ethylbenzene ND 1.00 ug/L 07/03/14 15:51 1
Hexachlorobutadiene ND 2.00 ug/L 07/03/14 15:51 1
Isopropylbenzene ND 1.00 ug/L 07/03/14 15:51 1
Methyl tert-butyl ether ND 1.00 ug/L 07/03/14 15:51 1
Methylene Chloride ND 5.00 ug/L 07/03/14 15:51 1
Page 6 of 58 7/30/2014
Client Sample ID: MW-1 Lab Sample ID: 490-56655-5
3
4
Naphthalene ND 5.00 ug/L 07/03/14 15:51 1
n-Butylbenzene ND 1.00 ug/L 07/03/14 15:51 1 6
N-Propylbenzene ND 1.00 ug/L 07/03/14 15:51 1
p-Isopropyltoluene ND 1.00 ug/L 07/03/14 15:51 1
sec-Butylbenzene ND 1.00 ug/L 07/03/14 15:51 1
7
Styrene ND 1.00 ug/L 07/03/14 15:51 1
tert-Butylbenzene ND 1.00 ug/L 07/03/14 15:51 1
8
Tetrachloroethene 102 1.00 ug/L 07/03/14 15:51 1
Toluene ND 1.00 ug/L 07/03/14 15:51 1
9
trans-1,2-Dichloroethene ND 1.00 ug/L 07/03/14 15:51 1
trans-1,3-Dichloropropene ND 1.00 ug/L 07/03/14 15:51 1 10
Trichloroethene ND 1.00 ug/L 07/03/14 15:51 1
Trichlorofluoromethane ND 1.00 ug/L 07/03/14 15:51 1 11
Vinyl chloride ND 1.00 ug/L 07/03/14 15:51 1
Xylenes, Total ND 2.00 ug/L 07/03/14 15:51 1 12
13
Toluene-d8 (Surr) 92 70 - 130 07/03/14 15:51 1

1,2,4-Trichlorobenzene ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
1,3-Dichlorobenzene ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
1-Methylnaphthalene ND H 1.82 ug/L 07/23/14 13:07 07/29/14 23:38 1
2,4,5-Trichlorophenol ND H 22.7 ug/L 07/23/14 13:07 07/29/14 23:38 1
Acenaphthene ND 1.92 ug/L 07/03/14 07:37 07/03/14 15:42 1
2,4-Dichlorophenol ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Acenaphthylene ND 1.92 ug/L 07/03/14 07:37 07/03/14 15:42 1
2,4-Dimethylphenol ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Anthracene ND 1.92 ug/L 07/03/14 07:37 07/03/14 15:42 1
2,4-Dinitrophenol ND H 22.7 ug/L 07/23/14 13:07 07/29/14 23:38 1
Benzo[a]anthracene ND 1.92 ug/L 07/03/14 07:37 07/03/14 15:42 1
2,4-Dinitrotoluene ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Benzo[a]pyrene ND 1.92 ug/L 07/03/14 07:37 07/03/14 15:42 1
Benzo[b]fluoranthene ND 1.92 ug/L 07/03/14 07:37 07/03/14 15:42 1
2-Chloronaphthalene ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Benzo[g,h,i]perylene ND 1.92 ug/L 07/03/14 07:37 07/03/14 15:42 1
2-Chlorophenol ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Benzo[k]fluoranthene ND 1.92 ug/L 07/03/14 07:37 07/03/14 15:42 1
2-Methylphenol ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
2-Nitroaniline ND H 22.7 ug/L 07/23/14 13:07 07/29/14 23:38 1
2-Nitrophenol ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Page 7 of 58 7/30/2014
3
4
3 & 4 Methylphenol ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
3,3'-Dichlorobenzidine ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1 6
4,6-Dinitro-2-methylphenol ND H 22.7 ug/L 07/23/14 13:07 07/29/14 23:38 1
4-Chloro-3-methylphenol ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
7
4-Bromophenyl phenyl ether ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
4-Chloroaniline ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
8
4-Chlorophenyl phenyl ether ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Chrysene ND 1.92 ug/L 07/03/14 07:37 07/03/14 15:42 1
9
4-Nitrophenol ND H 22.7 ug/L 07/23/14 13:07 07/29/14 23:38 1 10
Dibenz(a,h)anthracene ND 1.92 ug/L 07/03/14 07:37 07/03/14 15:42 1
bis (2-chloroisopropyl) ether ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1 11
Carbazole ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Dibenzofuran ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1 12
Dimethyl phthalate ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Diethyl phthalate ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1 13
Di-n-butyl phthalate ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Di-n-octyl phthalate ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Fluoranthene ND 1.92 ug/L 07/03/14 07:37 07/03/14 15:42 1
Fluorene ND 1.92 ug/L 07/03/14 07:37 07/03/14 15:42 1
Hexachlorobenzene ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Hexachlorobutadiene ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Hexachlorocyclopentadiene ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Hexachloroethane ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Indeno[1,2,3-cd]pyrene ND 1.92 ug/L 07/03/14 07:37 07/03/14 15:42 1
Isophorone ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Nitrobenzene ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
N-Nitrosodi-n-propylamine ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Naphthalene ND 1.92 ug/L 07/03/14 07:37 07/03/14 15:42 1
n-Nitrosodiphenylamine(as ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
diphenylamine)
Pentachlorophenol ND H 22.7 ug/L 07/23/14 13:07 07/29/14 23:38 1
Phenol ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Phenanthrene ND 1.92 ug/L 07/03/14 07:37 07/03/14 15:42 1
Cresols ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Bis(2-chloroethoxy)methane ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Pyrene ND 1.92 ug/L 07/03/14 07:37 07/03/14 15:42 1
Bis(2-chloroethyl)ether ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Bis(2-ethylhexyl) phthalate ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1
Butyl benzyl phthalate ND H 9.09 ug/L 07/23/14 13:07 07/29/14 23:38 1

Terphenyl-d14 (Surr) 86 13 - 120 07/03/14 07:37 07/03/14 15:42 1
Page 8 of 58 7/30/2014
3
4
5
Phenol-d5 (Surr) 25 10 - 120 07/23/14 13:07 07/29/14 23:38 1
Terphenyl-d14 (Surr) 59 13 - 120 07/23/14 13:07 07/29/14 23:38 1 6
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography 7
PCB-1016 ND 0.446 ug/L 07/03/14 10:40 07/03/14 14:27 1 8
PCB-1221 ND 0.446 ug/L 07/03/14 10:40 07/03/14 14:27 1
PCB-1232 ND 0.446 ug/L 07/03/14 10:40 07/03/14 14:27 1
PCB-1242 ND 0.446 ug/L 07/03/14 10:40 07/03/14 14:27 1
9
PCB-1248 ND 0.446 ug/L 07/03/14 10:40 07/03/14 14:27 1
PCB-1254 ND 0.446 ug/L 07/03/14 10:40 07/03/14 14:27 1
10
PCB-1260 ND 0.446 ug/L 07/03/14 10:40 07/03/14 14:27 1
11
Tetrachloro-m-xylene 94 10 - 150 07/03/14 10:40 07/03/14 14:27 1 12
13
Aluminum 228 1.00 mg/L 07/08/14 12:51 07/08/14 21:09 10
Barium 1.94 0.100 mg/L 07/08/14 12:51 07/08/14 21:09 10
Chromium 0.512 0.0500 mg/L 07/08/14 12:51 07/08/14 21:09 10
Copper 0.641 0.100 mg/L 07/08/14 12:51 07/08/14 21:09 10
Iron 601 1.00 mg/L 07/08/14 12:51 07/08/14 21:09 10
Lead 0.901 0.0500 mg/L 07/08/14 12:51 07/08/14 21:09 10
Magnesium 116 10.0 mg/L 07/08/14 12:51 07/08/14 21:09 10
Nickel 1.36 0.100 mg/L 07/08/14 12:51 07/08/14 21:09 10
Zinc 1.60 0.500 mg/L 07/08/14 12:51 07/08/14 21:09 10

Mercury ND 0.000200 mg/L 07/07/14 09:47 07/08/14 11:06 1
General Chemistry
Chromium, hex 0.0170 H 0.0100 mg/L 07/24/14 11:51 1
Page 9 of 58 7/30/2014
4
9
10
11
2-Hexanone ND 10.0 ug/L 07/03/14 16:19 1
Acetone ND 25.0 ug/L 07/03/14 16:19 1
Benzene ND 1.00 ug/L 07/03/14 16:19 1
Bromoform ND 1.00 ug/L 07/03/14 16:19 1
Page 10 of 58 7/30/2014
3
4
7
Styrene ND 1.00 ug/L 07/03/14 16:19 1
8
Tetrachloroethene 26.0 1.00 ug/L 07/03/14 16:19 1
Toluene ND 1.00 ug/L 07/03/14 16:19 1
9
13
Toluene-d8 (Surr) 93 70 - 130 07/03/14 16:19 1

Page 11 of 58 7/30/2014
3
4
7
8
Chrysene ND 1.92 ug/L 07/03/14 07:37 07/03/14 16:05 1
9
Fluorene ND 1.92 ug/L 07/03/14 07:37 07/03/14 16:05 1
diphenylamine)
Phenol ND H 9.09 ug/L 07/23/14 13:07 07/30/14 00:01 1
Cresols ND H 9.09 ug/L 07/23/14 13:07 07/30/14 00:01 1
Pyrene ND 1.92 ug/L 07/03/14 07:37 07/03/14 16:05 1

Terphenyl-d14 (Surr) 48 13 - 120 07/03/14 07:37 07/03/14 16:05 1
Page 12 of 58 7/30/2014
3
4
5
Phenol-d5 (Surr) 30 10 - 120 07/23/14 13:07 07/30/14 00:01 1
Terphenyl-d14 (Surr) 80 13 - 120 07/23/14 13:07 07/30/14 00:01 1 6
PCB-1016 ND 0.446 ug/L 07/03/14 10:40 07/03/14 14:40 1 8
PCB-1221 ND 0.446 ug/L 07/03/14 10:40 07/03/14 14:40 1
PCB-1232 ND 0.446 ug/L 07/03/14 10:40 07/03/14 14:40 1
PCB-1242 ND 0.446 ug/L 07/03/14 10:40 07/03/14 14:40 1
9
PCB-1248 ND 0.446 ug/L 07/03/14 10:40 07/03/14 14:40 1
PCB-1254 ND 0.446 ug/L 07/03/14 10:40 07/03/14 14:40 1
10
PCB-1260 ND 0.446 ug/L 07/03/14 10:40 07/03/14 14:40 1
11
13
Aluminum 92.1 1.00 mg/L 07/08/14 12:51 07/08/14 21:12 10
Barium 1.48 0.100 mg/L 07/08/14 12:51 07/08/14 21:12 10
Chromium 0.220 0.0500 mg/L 07/08/14 12:51 07/08/14 21:12 10
Copper 0.183 0.100 mg/L 07/08/14 12:51 07/08/14 21:12 10
Iron 229 1.00 mg/L 07/08/14 12:51 07/08/14 21:12 10
Lead 0.120 0.0500 mg/L 07/08/14 12:51 07/08/14 21:12 10
Magnesium 40.6 10.0 mg/L 07/08/14 12:51 07/08/14 21:12 10
Nickel 0.420 0.100 mg/L 07/08/14 12:51 07/08/14 21:12 10
Zinc ND 0.500 mg/L 07/08/14 12:51 07/08/14 21:12 10

Mercury ND 0.000200 mg/L 07/07/14 09:47 07/08/14 11:08 1
General Chemistry
Chromium, hex ND H 0.0100 mg/L 07/24/14 11:55 1
Page 13 of 58 7/30/2014
4
9
10
11
2-Hexanone ND 10.0 ug/L 07/03/14 16:48 1
Acetone ND 25.0 ug/L 07/03/14 16:48 1
Benzene ND 1.00 ug/L 07/03/14 16:48 1
Bromoform ND 1.00 ug/L 07/03/14 16:48 1
Page 14 of 58 7/30/2014
3
4
7
Styrene ND 1.00 ug/L 07/03/14 16:48 1
8
Tetrachloroethene ND 1.00 ug/L 07/03/14 16:48 1
Toluene ND 1.00 ug/L 07/03/14 16:48 1
9
13
Toluene-d8 (Surr) 91 70 - 130 07/03/14 16:48 1

Page 15 of 58 7/30/2014
3
4
7
8
Chrysene ND 1.92 ug/L 07/03/14 07:37 07/03/14 16:28 1
9
Fluorene ND 1.92 ug/L 07/03/14 07:37 07/03/14 16:28 1
diphenylamine)
Phenol ND H 8.93 ug/L 07/23/14 13:07 07/30/14 00:24 1
Cresols ND H 8.93 ug/L 07/23/14 13:07 07/30/14 00:24 1
Pyrene ND 1.92 ug/L 07/03/14 07:37 07/03/14 16:28 1

Terphenyl-d14 (Surr) 74 13 - 120 07/03/14 07:37 07/03/14 16:28 1
Page 16 of 58 7/30/2014
3
4
5
Phenol-d5 (Surr) 29 10 - 120 07/23/14 13:07 07/30/14 00:24 1
Terphenyl-d14 (Surr) 51 13 - 120 07/23/14 13:07 07/30/14 00:24 1 6
PCB-1016 ND 0.446 ug/L 07/03/14 10:40 07/03/14 14:53 1 8
PCB-1221 ND 0.446 ug/L 07/03/14 10:40 07/03/14 14:53 1
PCB-1232 ND 0.446 ug/L 07/03/14 10:40 07/03/14 14:53 1
PCB-1242 ND 0.446 ug/L 07/03/14 10:40 07/03/14 14:53 1
9
PCB-1248 ND 0.446 ug/L 07/03/14 10:40 07/03/14 14:53 1
PCB-1254 ND 0.446 ug/L 07/03/14 10:40 07/03/14 14:53 1
10
PCB-1260 ND 0.446 ug/L 07/03/14 10:40 07/03/14 14:53 1
11
13
Aluminum 179 1.00 mg/L 07/08/14 12:51 07/08/14 21:16 10
Barium 1.37 0.100 mg/L 07/08/14 12:51 07/08/14 21:16 10
Chromium 0.306 0.0500 mg/L 07/08/14 12:51 07/08/14 21:16 10
Copper 0.345 0.100 mg/L 07/08/14 12:51 07/08/14 21:16 10
Iron 333 1.00 mg/L 07/08/14 12:51 07/08/14 21:16 10
Lead 0.197 0.0500 mg/L 07/08/14 12:51 07/08/14 21:16 10
Magnesium 50.3 10.0 mg/L 07/08/14 12:51 07/08/14 21:16 10
Nickel 0.508 0.100 mg/L 07/08/14 12:51 07/08/14 21:16 10
Zinc 0.550 0.500 mg/L 07/08/14 12:51 07/08/14 21:16 10

Mercury ND 0.000200 mg/L 07/07/14 09:47 07/08/14 11:10 1
General Chemistry
Page 17 of 58 7/30/2014
4
9
10
11
2-Hexanone ND 10.0 ug/L 07/03/14 17:16 1
Acetone ND 25.0 ug/L 07/03/14 17:16 1
Benzene ND 1.00 ug/L 07/03/14 17:16 1
Bromoform ND 1.00 ug/L 07/03/14 17:16 1
Page 18 of 58 7/30/2014
3
4
7
Styrene ND 1.00 ug/L 07/03/14 17:16 1
8
Tetrachloroethene 21.3 1.00 ug/L 07/03/14 17:16 1
Toluene ND 1.00 ug/L 07/03/14 17:16 1
9
13
Toluene-d8 (Surr) 92 70 - 130 07/03/14 17:16 1

Page 19 of 58 7/30/2014
3
4
7
8
Chrysene ND 1.92 ug/L 07/03/14 07:37 07/03/14 16:51 1
9
Fluorene ND 1.92 ug/L 07/03/14 07:37 07/03/14 16:51 1
diphenylamine)
Phenol ND H 9.26 ug/L 07/23/14 13:07 07/30/14 00:47 1
Cresols ND H 9.26 ug/L 07/23/14 13:07 07/30/14 00:47 1
Pyrene ND 1.92 ug/L 07/03/14 07:37 07/03/14 16:51 1

Terphenyl-d14 (Surr) 55 13 - 120 07/03/14 07:37 07/03/14 16:51 1
2-Fluorophenol (Surr) 3 X 10 - 120 07/23/14 13:07 07/30/14 00:47 1
Page 20 of 58 7/30/2014
3
4
5
Phenol-d5 (Surr) 2 X 10 - 120 07/23/14 13:07 07/30/14 00:47 1
Terphenyl-d14 (Surr) 68 13 - 120 07/23/14 13:07 07/30/14 00:47 1 6
PCB-1016 ND 0.446 ug/L 07/03/14 10:40 07/03/14 15:06 1 8
PCB-1221 ND 0.446 ug/L 07/03/14 10:40 07/03/14 15:06 1
PCB-1232 ND 0.446 ug/L 07/03/14 10:40 07/03/14 15:06 1
PCB-1242 ND 0.446 ug/L 07/03/14 10:40 07/03/14 15:06 1
9
PCB-1248 ND 0.446 ug/L 07/03/14 10:40 07/03/14 15:06 1
PCB-1254 ND 0.446 ug/L 07/03/14 10:40 07/03/14 15:06 1
10
PCB-1260 ND 0.446 ug/L 07/03/14 10:40 07/03/14 15:06 1
11
13
Aluminum 1580 10.0 mg/L 07/08/14 12:51 07/08/14 21:20 10
Barium 40.1 1.00 mg/L 07/08/14 12:51 07/08/14 21:20 10
Chromium 2.73 0.500 mg/L 07/08/14 12:51 07/08/14 21:20 10
Copper 3.81 1.00 mg/L 07/08/14 12:51 07/08/14 21:20 10
Iron 4390 10.0 mg/L 07/08/14 12:51 07/08/14 21:20 10
Lead 3.39 0.500 mg/L 07/08/14 12:51 07/08/14 21:20 10
Magnesium 364 100 mg/L 07/08/14 12:51 07/08/14 21:20 10
Nickel 6.91 1.00 mg/L 07/08/14 12:51 07/08/14 21:20 10
Zinc 5.47 5.00 mg/L 07/08/14 12:51 07/08/14 21:20 10

Mercury 0.00267 0.000200 mg/L 07/07/14 09:47 07/08/14 11:12 1
General Chemistry
Page 21 of 58 7/30/2014
Client Sample ID: Trip Blank Lab Sample ID: 490-56655-9 3
4
9
10
11
2-Hexanone ND 10.0 ug/L 07/03/14 12:05 1
Acetone ND 25.0 ug/L 07/03/14 12:05 1
Benzene ND 1.00 ug/L 07/03/14 12:05 1
Bromoform ND 1.00 ug/L 07/03/14 12:05 1
Page 22 of 58 7/30/2014
Client Sample ID: Trip Blank Lab Sample ID: 490-56655-9
3
4
7
Styrene ND 1.00 ug/L 07/03/14 12:05 1
8
Toluene ND 1.00 ug/L 07/03/14 12:05 1
9
13
Toluene-d8 (Surr) 92 70 - 130 07/03/14 12:05 1
Page 23 of 58 7/30/2014
QC Sample Results 1
Lab Sample ID: MB 490-174385/6 Client Sample ID: Method Blank 4
Matrix: Water Prep Type: Total/NA
MB MB
5
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 07/03/14 11:08 1 6
1,1,1-Trichloroethane ND 1.00 ug/L 07/03/14 11:08 1
1,1,2,2-Tetrachloroethane ND 1.00 ug/L 07/03/14 11:08 1 7
1,1,2-Trichloroethane ND 1.00 ug/L 07/03/14 11:08 1
1,1-Dichloroethene ND 1.00 ug/L 07/03/14 11:08 1
1,1-Dichloropropene ND 1.00 ug/L 07/03/14 11:08 1 9
1,2,3-Trichloropropane ND 1.00 ug/L 07/03/14 11:08 1 10
ND
ND
1.00
10.0
ug/L
ug/L
07/03/14 11:08
07/03/14 11:08
1
1
11
12
13
2-Hexanone ND 10.0 ug/L 07/03/14 11:08 1
Acetone ND 25.0 ug/L 07/03/14 11:08 1
Benzene ND 1.00 ug/L 07/03/14 11:08 1
Bromoform ND 1.00 ug/L 07/03/14 11:08 1
Page 24 of 58 7/30/2014
QC Sample Results 1
4
MB MB 5
Methylene Chloride ND 5.00 ug/L 07/03/14 11:08 1 6
p-Isopropyltoluene ND 1.00 ug/L 07/03/14 11:08 1 8
Styrene ND 1.00 ug/L 07/03/14 11:08 1
9
Toluene ND 1.00 ug/L 07/03/14 11:08 1
10
trans-1,3-Dichloropropene ND 1.00 ug/L 07/03/14 11:08 1
11
MB MB
Toluene-d8 (Surr) 92 70 - 130 07/03/14 11:08 1
Spike LCS LCS %Rec.
1,1,1,2-Tetrachloroethane 50.0 52.76 ug/L 106 74 - 135
1,1,1-Trichloroethane 50.0 49.42 ug/L 99 78 - 135
1,1,2,2-Tetrachloroethane 50.0 51.84 ug/L 104 69 - 131
1,1,2-Trichloroethane 50.0 54.09 ug/L 108 80 - 124
1,1-Dichloroethane 50.0 60.38 ug/L 121 78 - 125
1,1-Dichloroethene 50.0 61.56 ug/L 123 79 - 124
1,1-Dichloropropene 50.0 51.85 ug/L 104 80 - 122
1,2,3-Trichlorobenzene 50.0 48.00 ug/L 96 62 - 133
1,2,3-Trichloropropane 50.0 47.59 ug/L 95 70 - 131
1,2,4-Trimethylbenzene 50.0 47.35 ug/L 95 77 - 126
1,2-Dibromo-3-Chloropropane 50.0 53.79 ug/L 108 54 - 125
1,2-Dibromoethane (EDB) 50.0 52.65 ug/L 105 80 - 129
1,2-Dichlorobenzene 50.0 51.24 ug/L 102 80 - 121
1,2-Dichloroethane 50.0 51.73 ug/L 103 77 - 121
1,2-Dichloropropane 50.0 54.97 ug/L 110 75 - 120
1,3,5-Trimethylbenzene 50.0 46.52 ug/L 93 77 - 127
1,3-Dichloropropane 50.0 53.50 ug/L 107 80 - 125
Page 25 of 58 7/30/2014
QC Sample Results 1
4
2,2-Dichloropropane 50.0 49.31 ug/L 99 43 - 161 6
2-Butanone (MEK) 250 296.8 ug/L 119 62 - 133
2-Chlorotoluene 50.0 45.72 ug/L 91 75 - 126 7
2-Hexanone 250 275.8 ug/L 110 60 - 142
4-Chlorotoluene 50.0 46.72 ug/L 93 75 - 130 8
4-Methyl-2-pentanone (MIBK) 250 273.5 ug/L 109 60 - 137
Acetone 250 313.8 ug/L 126 54 - 145
Benzene 50.0 53.40 ug/L 107 80 - 121
9
Bromobenzene 50.0 46.76 ug/L 94 68 - 130
Bromochloromethane 50.0 55.67 ug/L 111 78 - 129
10
Bromodichloromethane 50.0 53.55 ug/L 107 75 - 129
Bromoform 50.0 57.47 ug/L 115 46 - 145
11
Bromomethane 50.0 49.96 ug/L 100 41 - 150
Carbon disulfide 50.0 61.71 ug/L 123 77 - 126 12
Carbon tetrachloride 50.0 51.13 ug/L 102 64 - 147
Chlorobenzene 50.0 51.33 ug/L 103 80 - 120 13
Chlorodibromomethane 50.0 53.78 ug/L 108 69 - 133
Chloroethane 50.0 53.24 ug/L 106 72 - 120
Chloroform 50.0 51.14 ug/L 102 73 - 129
Chloromethane 50.0 50.39 ug/L 101 12 - 150
cis-1,2-Dichloroethene 50.0 56.28 ug/L 113 76 - 125
cis-1,3-Dichloropropene 50.0 54.15 ug/L 108 74 - 140
Dibromomethane 50.0 52.15 ug/L 104 71 - 125
Dichlorodifluoromethane 50.0 49.98 ug/L 100 37 - 127
Ethylbenzene 50.0 49.37 ug/L 99 80 - 130
Hexachlorobutadiene 50.0 52.63 ug/L 105 49 - 146
Isopropylbenzene 50.0 49.50 ug/L 99 80 - 141
Methyl tert-butyl ether 50.0 51.70 ug/L 103 72 - 133
Methylene Chloride 50.0 55.96 ug/L 112 79 - 123
Naphthalene 50.0 47.50 ug/L 95 62 - 138
n-Butylbenzene 50.0 49.09 ug/L 98 68 - 132
N-Propylbenzene 50.0 45.85 ug/L 92 75 - 129
p-Isopropyltoluene 50.0 47.00 ug/L 94 75 - 128
sec-Butylbenzene 50.0 46.79 ug/L 94 76 - 128
Styrene 50.0 52.33 ug/L 105 80 - 127
tert-Butylbenzene 50.0 45.74 ug/L 91 76 - 126
Tetrachloroethene 50.0 50.75 ug/L 101 80 - 126
Toluene 50.0 49.49 ug/L 99 80 - 126
trans-1,2-Dichloroethene 50.0 60.53 ug/L 121 79 - 126
trans-1,3-Dichloropropene 50.0 53.76 ug/L 108 63 - 134
Trichloroethene 50.0 52.73 ug/L 105 80 - 123
Trichlorofluoromethane 50.0 50.28 ug/L 101 65 - 124
Vinyl chloride 50.0 57.00 ug/L 114 68 - 120
Xylenes, Total 100 99.21 ug/L 99 80 - 132
LCS LCS
Page 26 of 58 7/30/2014
QC Sample Results 1
4
LCS LCS
5
6
7
Matrix: Water Prep Type: Total/NA 8
1,1,1,2-Tetrachloroethane 50.0 52.45 ug/L 105 74 - 135 1 16 10
1,1,1-Trichloroethane 50.0 48.58 ug/L 97 78 - 135 2 17
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
50.0
50.0
51.89
54.45
ug/L
ug/L
104
109
69 - 131
80 - 124
0
1
20
15
11
1,1-Dichloroethane 50.0 59.64 ug/L 119 78 - 125 1 17
1,1-Dichloroethene 50.0 60.39 ug/L 121 79 - 124 2 17
12
1,1-Dichloropropene 50.0 51.20 ug/L 102 80 - 122 1 17
1,2,3-Trichlorobenzene 50.0 47.88 ug/L 96 62 - 133 0 25
13
1,2,3-Trichloropropane 50.0 47.53 ug/L 95 70 - 131 0 19
1,2,4-Trichlorobenzene 50.0 47.89 ug/L 96 63 - 133 0 19
1,2,4-Trimethylbenzene 50.0 46.83 ug/L 94 77 - 126 1 16
1,2-Dibromo-3-Chloropropane 50.0 52.71 ug/L 105 54 - 125 2 24
1,2-Dibromoethane (EDB) 50.0 53.24 ug/L 106 80 - 129 1 15
1,2-Dichlorobenzene 50.0 50.65 ug/L 101 80 - 121 1 15
1,2-Dichloroethane 50.0 51.02 ug/L 102 77 - 121 1 17
1,2-Dichloropropane 50.0 54.86 ug/L 110 75 - 120 0 17
1,3,5-Trimethylbenzene 50.0 46.49 ug/L 93 77 - 127 0 17
2-Butanone (MEK) 250 293.7 ug/L 117 62 - 133 1 19
2-Chlorotoluene 50.0 45.72 ug/L 91 75 - 126 0 17
2-Hexanone 250 274.7 ug/L 110 60 - 142 0 15
4-Chlorotoluene 50.0 46.68 ug/L 93 75 - 130 0 18
4-Methyl-2-pentanone (MIBK) 250 274.3 ug/L 110 60 - 137 0 17
Acetone 250 308.8 ug/L 124 54 - 145 2 21
Benzene 50.0 52.89 ug/L 106 80 - 121 1 17
Bromobenzene 50.0 47.05 ug/L 94 68 - 130 1 20
Bromochloromethane 50.0 54.40 ug/L 109 78 - 129 2 17
Bromodichloromethane 50.0 52.57 ug/L 105 75 - 129 2 18
Bromoform 50.0 56.77 ug/L 114 46 - 145 1 16
Bromomethane 50.0 53.23 ug/L 106 41 - 150 6 50
Carbon disulfide 50.0 60.57 ug/L 121 77 - 126 2 21
Carbon tetrachloride 50.0 50.28 ug/L 101 64 - 147 2 19
Chlorobenzene 50.0 50.93 ug/L 102 80 - 120 1 14
Chlorodibromomethane 50.0 53.67 ug/L 107 69 - 133 0 15
Chloroethane 50.0 53.00 ug/L 106 72 - 120 0 20
Chloroform 50.0 50.50 ug/L 101 73 - 129 1 18
Chloromethane 50.0 51.90 ug/L 104 12 - 150 3 31
Page 27 of 58 7/30/2014
QC Sample Results 1
4
cis-1,2-Dichloroethene 50.0 55.79 ug/L 112 76 - 125 1 17 6
cis-1,3-Dichloropropene 50.0 53.21 ug/L 106 74 - 140 2 15
Dibromomethane 50.0 52.24 ug/L 104 71 - 125 0 16 7
Dichlorodifluoromethane 50.0 49.64 ug/L 99 37 - 127 1 18
Ethylbenzene 50.0 48.78 ug/L 98 80 - 130 1 15 8
Hexachlorobutadiene 50.0 51.82 ug/L 104 49 - 146 2 23
Isopropylbenzene 50.0 49.29 ug/L 99 80 - 141 0 16
Methyl tert-butyl ether 50.0 51.82 ug/L 104 72 - 133 0 16
9
Methylene Chloride 50.0 54.60 ug/L 109 79 - 123 2 17
Naphthalene 50.0 47.63 ug/L 95 62 - 138 0 26
10
n-Butylbenzene 50.0 48.48 ug/L 97 68 - 132 1 18
N-Propylbenzene 50.0 45.79 ug/L 92 75 - 129 0 17
11
p-Isopropyltoluene 50.0 46.99 ug/L 94 75 - 128 0 16
sec-Butylbenzene 50.0 46.72 ug/L 93 76 - 128 0 16 12
Styrene 50.0 51.93 ug/L 104 80 - 127 1 24
tert-Butylbenzene 50.0 45.57 ug/L 91 76 - 126 0 16 13
Tetrachloroethene 50.0 50.37 ug/L 101 80 - 126 1 16
Toluene 50.0 49.56 ug/L 99 80 - 126 0 15
trans-1,2-Dichloroethene 50.0 59.71 ug/L 119 79 - 126 1 16
trans-1,3-Dichloropropene 50.0 53.64 ug/L 107 63 - 134 0 14
Trichloroethene 50.0 51.58 ug/L 103 80 - 123 2 17
Trichlorofluoromethane 50.0 49.75 ug/L 100 65 - 124 1 18
Vinyl chloride 50.0 56.64 ug/L 113 68 - 120 1 17
Xylenes, Total 100 98.31 ug/L 98 80 - 132 1 15
LCSD LCSD
Lab Sample ID: 490-56651-B-1 MS Client Sample ID: Matrix Spike

1,1,1,2-Tetrachloroethane ND 50.0 52.90 ug/L 106 73 - 141
1,1,1-Trichloroethane ND 50.0 51.04 ug/L 102 76 - 149
1,1,2,2-Tetrachloroethane ND 50.0 49.72 ug/L 99 56 - 143
1,1,2-Trichloroethane ND 50.0 52.94 ug/L 106 74 - 134
1,1-Dichloroethane ND 50.0 60.31 ug/L 121 71 - 139
1,1-Dichloroethene ND 50.0 60.83 ug/L 122 70 - 142
1,1-Dichloropropene ND 50.0 51.80 ug/L 104 76 - 139
1,2,3-Trichlorobenzene ND 50.0 42.95 ug/L 86 55 - 138
1,2,3-Trichloropropane ND 50.0 45.14 ug/L 90 53 - 144
1,2,4-Trichlorobenzene ND 50.0 43.73 ug/L 87 60 - 136
1,2,4-Trimethylbenzene ND 50.0 46.15 ug/L 92 69 - 136
1,2-Dibromo-3-Chloropropane ND 50.0 48.59 ug/L 97 52 - 126
Page 28 of 58 7/30/2014
QC Sample Results 1
4
1,2-Dibromoethane (EDB) ND 50.0 51.65 ug/L 103 75 - 137 6
1,2-Dichlorobenzene ND 50.0 50.11 ug/L 100 79 - 128
1,2-Dichloroethane ND 50.0 51.10 ug/L 102 64 - 136 7
1,2-Dichloropropane ND 50.0 53.52 ug/L 107 67 - 131
1,3,5-Trimethylbenzene ND 50.0 46.50 ug/L 93 69 - 139 8
9
2-Butanone (MEK) ND 250 287.0 ug/L 115 50 - 138
10
2-Chlorotoluene ND 50.0 44.56 ug/L 89 67 - 138
2-Hexanone ND 250 261.8 ug/L 105 50 - 150
11
4-Chlorotoluene ND 50.0 46.15 ug/L 92 69 - 138
4-Methyl-2-pentanone (MIBK) ND 250 264.6 ug/L 106 50 - 147 12
Acetone ND 250 289.4 ug/L 116 45 - 141
Benzene ND 50.0 53.30 ug/L 107 75 - 133 13
Bromobenzene ND 50.0 44.45 ug/L 89 60 - 138
Bromochloromethane ND 50.0 55.00 ug/L 110 67 - 139
Bromodichloromethane ND 50.0 53.12 ug/L 106 70 - 140
Bromoform ND 50.0 55.91 ug/L 112 42 - 147
Bromomethane ND 50.0 41.92 ug/L 84 16 - 163
Carbon disulfide ND 50.0 58.60 ug/L 117 48 - 152
Carbon tetrachloride ND 50.0 53.62 ug/L 107 62 - 164
Chlorobenzene ND 50.0 50.32 ug/L 101 80 - 129
Chlorodibromomethane ND 50.0 52.73 ug/L 105 66 - 140
Chloroethane ND 50.0 53.39 ug/L 107 58 - 137
Chloroform ND 50.0 51.18 ug/L 102 66 - 138
Chloromethane ND 50.0 48.37 ug/L 97 10 - 169
cis-1,2-Dichloroethene ND 50.0 55.58 ug/L 111 68 - 138
cis-1,3-Dichloropropene ND 50.0 50.66 ug/L 101 71 - 141
Dibromomethane ND 50.0 51.72 ug/L 103 58 - 140
Dichlorodifluoromethane ND 50.0 50.29 ug/L 101 40 - 127
Ethylbenzene ND 50.0 48.76 ug/L 98 79 - 139
Hexachlorobutadiene ND 50.0 51.63 ug/L 103 45 - 155
Isopropylbenzene ND 50.0 50.17 ug/L 100 80 - 153
Methyl tert-butyl ether ND 50.0 49.20 ug/L 98 66 - 141
Methylene Chloride ND 50.0 54.20 ug/L 108 64 - 139
Naphthalene ND 50.0 42.35 ug/L 85 55 - 140
n-Butylbenzene ND 50.0 49.07 ug/L 98 66 - 141
N-Propylbenzene ND 50.0 45.69 ug/L 91 69 - 142
p-Isopropyltoluene ND 50.0 47.15 ug/L 94 71 - 137
sec-Butylbenzene ND 50.0 46.95 ug/L 94 73 - 138
Styrene ND 50.0 52.31 ug/L 105 61 - 148
tert-Butylbenzene ND 50.0 45.19 ug/L 90 70 - 138
Tetrachloroethene ND 50.0 51.57 ug/L 103 72 - 145
Toluene ND 50.0 49.30 ug/L 99 75 - 136
trans-1,2-Dichloroethene ND 50.0 59.67 ug/L 119 66 - 143
trans-1,3-Dichloropropene ND 50.0 51.43 ug/L 103 59 - 135
Page 29 of 58 7/30/2014
QC Sample Results 1
4
Trichloroethene ND 50.0 53.01 ug/L 106 73 - 144 6
Trichlorofluoromethane ND 50.0 53.22 ug/L 106 58 - 139
Vinyl chloride ND 50.0 57.42 ug/L 115 56 - 129 7
Xylenes, Total ND 100 99.55 ug/L 100 74 - 141
MS MS 8
1,2-Dichloroethane-d4 (Surr) 95 70 - 130 9
Dibromofluoromethane (Surr) 105 70 - 130 10
11
Lab Sample ID: 490-56651-C-1 MSD Client Sample ID: Matrix Spike Duplicate
13
1,1,1,2-Tetrachloroethane ND 50.0 51.70 ug/L 103 73 - 141 2 16
1,1,1-Trichloroethane ND 50.0 50.27 ug/L 101 76 - 149 2 17
1,1,2,2-Tetrachloroethane ND 50.0 51.44 ug/L 103 56 - 143 3 20
1,1,2-Trichloroethane ND 50.0 52.82 ug/L 106 74 - 134 0 15
1,1-Dichloroethane ND 50.0 60.14 ug/L 120 71 - 139 0 17
1,1-Dichloroethene ND 50.0 62.80 ug/L 126 70 - 142 3 17
1,1-Dichloropropene ND 50.0 52.77 ug/L 106 76 - 139 2 17
1,2,3-Trichlorobenzene ND 50.0 46.35 ug/L 93 55 - 138 8 25
1,2,3-Trichloropropane ND 50.0 46.18 ug/L 92 53 - 144 2 19
1,2,4-Trichlorobenzene ND 50.0 46.65 ug/L 93 60 - 136 6 19
1,2,4-Trimethylbenzene ND 50.0 46.62 ug/L 93 69 - 136 1 16
1,2-Dibromo-3-Chloropropane ND 50.0 52.11 ug/L 104 52 - 126 7 24
1,2-Dibromoethane (EDB) ND 50.0 50.75 ug/L 101 75 - 137 2 15
1,2-Dichlorobenzene ND 50.0 50.41 ug/L 101 79 - 128 1 15
1,2-Dichloroethane ND 50.0 50.47 ug/L 101 64 - 136 1 17
1,2-Dichloropropane ND 50.0 53.98 ug/L 108 67 - 131 1 17
1,3,5-Trimethylbenzene ND 50.0 46.44 ug/L 93 69 - 139 0 17
2-Butanone (MEK) ND 250 293.9 ug/L 118 50 - 138 2 19
2-Chlorotoluene ND 50.0 45.48 ug/L 91 67 - 138 2 17
2-Hexanone ND 250 270.6 ug/L 108 50 - 150 3 15
4-Chlorotoluene ND 50.0 46.80 ug/L 94 69 - 138 1 18
4-Methyl-2-pentanone (MIBK) ND 250 274.7 ug/L 110 50 - 147 4 17
Acetone ND 250 301.2 ug/L 120 45 - 141 4 21
Benzene ND 50.0 53.08 ug/L 106 75 - 133 0 17
Bromobenzene ND 50.0 46.04 ug/L 92 60 - 138 4 20
Bromochloromethane ND 50.0 54.11 ug/L 108 67 - 139 2 17
Bromodichloromethane ND 50.0 52.04 ug/L 104 70 - 140 2 18
Bromoform ND 50.0 54.45 ug/L 109 42 - 147 3 16
Page 30 of 58 7/30/2014
QC Sample Results 1
Lab Sample ID: 490-56651-C-1 MSD Client Sample ID: Matrix Spike Duplicate
4
Bromomethane ND 50.0 50.07 ug/L 100 16 - 163 18 50 6
Carbon disulfide ND 50.0 59.52 ug/L 119 48 - 152 2 21
Carbon tetrachloride ND 50.0 52.80 ug/L 106 62 - 164 2 19 7
Chlorobenzene ND 50.0 50.19 ug/L 100 80 - 129 0 14
Chlorodibromomethane ND 50.0 52.02 ug/L 104 66 - 140 1 15 8
Chloroethane ND 50.0 54.17 ug/L 108 58 - 137 1 20
Chloroform ND 50.0 50.49 ug/L 101 66 - 138 1 18
Chloromethane ND 50.0 50.64 ug/L 101 10 - 169 5 31
9
cis-1,2-Dichloroethene ND 50.0 55.51 ug/L 111 68 - 138 0 17
cis-1,3-Dichloropropene ND 50.0 51.21 ug/L 102 71 - 141 1 15
10
Dibromomethane ND 50.0 50.35 ug/L 101 58 - 140 3 16
Dichlorodifluoromethane ND 50.0 50.62 ug/L 101 40 - 127 1 18
11
Ethylbenzene ND 50.0 48.95 ug/L 98 79 - 139 0 15
Hexachlorobutadiene ND 50.0 53.06 ug/L 106 45 - 155 3 23 12
Isopropylbenzene ND 50.0 49.65 ug/L 99 80 - 153 1 16
Methyl tert-butyl ether ND 50.0 50.30 ug/L 101 66 - 141 2 16 13
Methylene Chloride ND 50.0 54.29 ug/L 109 64 - 139 0 17
Naphthalene ND 50.0 46.44 ug/L 93 55 - 140 9 26
n-Butylbenzene ND 50.0 49.70 ug/L 99 66 - 141 1 18
N-Propylbenzene ND 50.0 46.36 ug/L 93 69 - 142 1 17
p-Isopropyltoluene ND 50.0 47.98 ug/L 96 71 - 137 2 16
sec-Butylbenzene ND 50.0 48.07 ug/L 96 73 - 138 2 16
Styrene ND 50.0 50.95 ug/L 102 61 - 148 3 24
tert-Butylbenzene ND 50.0 46.27 ug/L 93 70 - 138 2 16
Tetrachloroethene ND 50.0 51.43 ug/L 103 72 - 145 0 16
Toluene ND 50.0 48.94 ug/L 98 75 - 136 1 15
trans-1,2-Dichloroethene ND 50.0 60.50 ug/L 121 66 - 143 1 16
trans-1,3-Dichloropropene ND 50.0 51.32 ug/L 103 59 - 135 0 14
Trichloroethene ND 50.0 52.79 ug/L 106 73 - 144 0 17
Trichlorofluoromethane ND 50.0 53.51 ug/L 107 58 - 139 1 18
Vinyl chloride ND 50.0 59.22 ug/L 118 56 - 129 3 17
Xylenes, Total ND 100 97.70 ug/L 98 74 - 141 2 15
MSD MSD

MB MB
Page 31 of 58 7/30/2014
QC Sample Results 1
4
MB MB 5
Anthracene ND 2.00 ug/L 07/02/14 15:47 07/03/14 14:09 1 6
Benzo[a]pyrene ND 2.00 ug/L 07/02/14 15:47 07/03/14 14:09 1 7
Benzo[g,h,i]perylene ND 2.00 ug/L 07/02/14 15:47 07/03/14 14:09 1 8
Chrysene ND 2.00 ug/L 07/02/14 15:47 07/03/14 14:09 1
9
Fluorene ND 2.00 ug/L 07/02/14 15:47 07/03/14 14:09 1
10
11
Pyrene ND 2.00 ug/L 07/02/14 15:47 07/03/14 14:09 1 12
Surrogate
MB MB
%Recovery Qualifier Limits Prepared Analyzed Dil Fac
13
Terphenyl-d14 (Surr) 91 13 - 120 07/02/14 15:47 07/03/14 14:09 1
Spike LCS LCS %Rec.
Acenaphthene 40.0 31.87 ug/L 80 46 - 120
Acenaphthylene 40.0 32.28 ug/L 81 48 - 120
Anthracene 40.0 37.02 ug/L 93 58 - 130
Benzo[a]anthracene 40.0 35.83 ug/L 90 57 - 120
Benzo[a]pyrene 40.0 38.42 ug/L 96 57 - 124
Benzo[b]fluoranthene 40.0 37.31 ug/L 93 51 - 125
Benzo[g,h,i]perylene 40.0 44.47 ug/L 111 51 - 123
Benzo[k]fluoranthene 40.0 37.46 ug/L 94 51 - 120
Chrysene 40.0 36.53 ug/L 91 55 - 120
Dibenz(a,h)anthracene 40.0 46.53 ug/L 116 50 - 125
Fluoranthene 40.0 34.03 ug/L 85 56 - 120
Fluorene 40.0 35.21 ug/L 88 52 - 120
Indeno[1,2,3-cd]pyrene 40.0 43.67 ug/L 109 54 - 125
Naphthalene 40.0 28.88 ug/L 72 37 - 120
Phenanthrene 40.0 34.85 ug/L 87 56 - 120
Pyrene 40.0 34.78 ug/L 87 53 - 129
LCS LCS
Page 32 of 58 7/30/2014
QC Sample Results 1
MB MB
5
1,2,4-Trichlorobenzene ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1 6
1,3-Dichlorobenzene ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
1,4-Dichlorobenzene ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1 7
1,2-Dichlorobenzene ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
1-Methylnaphthalene ND 2.00 ug/L 07/23/14 13:07 07/29/14 22:52 1 8
2,4,5-Trichlorophenol ND 25.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
2,4,6-Trichlorophenol ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1 9
2,4-Dichlorophenol ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
2,4-Dimethylphenol ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1 10
2,4-Dinitrophenol ND 25.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
2,4-Dinitrotoluene
2,6-Dinitrotoluene
ND
ND
10.0
10.0
ug/L
ug/L
07/23/14 13:07
07/23/14 13:07
07/29/14 22:52
07/29/14 22:52
1
1
11
2-Chloronaphthalene ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
2-Chlorophenol ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
12
2-Methylphenol ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
2-Methylnaphthalene ND 2.00 ug/L 07/23/14 13:07 07/29/14 22:52 1
13
2-Nitroaniline ND 25.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
2-Nitrophenol ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
3 & 4 Methylphenol ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
3,3'-Dichlorobenzidine ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
4,6-Dinitro-2-methylphenol ND 25.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
4-Chloro-3-methylphenol ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
4-Bromophenyl phenyl ether ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
4-Chloroaniline ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
4-Chlorophenyl phenyl ether ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
4-Nitrophenol ND 25.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
bis (2-chloroisopropyl) ether ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
Carbazole ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
Dibenzofuran ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
Dimethyl phthalate ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
Diethyl phthalate ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
Di-n-butyl phthalate ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
Di-n-octyl phthalate ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
Hexachlorobenzene ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
Hexachlorobutadiene ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
Hexachlorocyclopentadiene ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
Hexachloroethane ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
Isophorone ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
Nitrobenzene ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
N-Nitrosodi-n-propylamine ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
n-Nitrosodiphenylamine(as ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
diphenylamine)
Pentachlorophenol ND 25.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
Phenol ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
Cresols ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
Bis(2-chloroethoxy)methane ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
Page 33 of 58 7/30/2014
QC Sample Results 1
4
MB MB 5
Bis(2-chloroethyl)ether ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1 6
Bis(2-ethylhexyl) phthalate ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1
Butyl benzyl phthalate ND 10.0 ug/L 07/23/14 13:07 07/29/14 22:52 1 7
MB MB
2-Fluorophenol (Surr) 38 10 - 120 07/23/14 13:07 07/29/14 22:52 1 9
2,4,6-Tribromophenol (Surr) 78 10 - 120 07/23/14 13:07 07/29/14 22:52 1 10
Phenol-d5 (Surr) 26 10 - 120 07/23/14 13:07 07/29/14 22:52 1
Terphenyl-d14 (Surr) 87 13 - 120 07/23/14 13:07 07/29/14 22:52 1 11
Spike LCS LCS %Rec.
13
1-Methylnaphthalene 40.0 24.84 ug/L 62 36 - 120
2,4,5-Trichlorophenol 40.0 32.02 ug/L 80 40 - 129
2,4,6-Trichlorophenol 40.0 32.02 ug/L 80 39 - 135
2,4-Dichlorophenol 40.0 28.31 ug/L 71 38 - 120
2,4-Dimethylphenol 40.0 33.31 ug/L 83 21 - 126
2,4-Dinitrophenol 80.0 43.53 ug/L 54 20 - 150
2,4-Dinitrotoluene 40.0 32.89 ug/L 82 46 - 132
2,6-Dinitrotoluene 40.0 33.30 ug/L 83 54 - 128
2-Chloronaphthalene 40.0 25.56 ug/L 64 39 - 120
2-Chlorophenol 40.0 25.53 ug/L 64 40 - 120
2-Methylphenol 40.0 26.60 ug/L 67 38 - 120
2-Methylnaphthalene 40.0 24.41 ug/L 61 31 - 120
2-Nitroaniline 40.0 33.47 ug/L 84 46 - 131
2-Nitrophenol 40.0 29.39 ug/L 73 32 - 120
3 & 4 Methylphenol 40.0 24.10 ug/L 60 33 - 120
3,3'-Dichlorobenzidine 40.0 35.93 ug/L 90 46 - 129
4,6-Dinitro-2-methylphenol 80.0 59.62 ug/L 75 19 - 150
4-Chloro-3-methylphenol 40.0 30.41 ug/L 76 44 - 120
4-Bromophenyl phenyl ether 40.0 29.99 ug/L 75 47 - 127
4-Chloroaniline 40.0 28.35 ug/L 71 44 - 120
4-Chlorophenyl phenyl ether 40.0 27.60 ug/L 69 50 - 120
4-Nitrophenol 80.0 25.66 ug/L 32 10 - 120
bis (2-chloroisopropyl) ether 40.0 25.49 ug/L 64 44 - 120
Carbazole 40.0 31.38 ug/L 78 54 - 123
Dibenzofuran 40.0 27.80 ug/L 70 50 - 120
Page 34 of 58 7/30/2014
QC Sample Results 1
4
Dimethyl phthalate 40.0 30.38 ug/L 76 53 - 127 6
Diethyl phthalate 40.0 30.60 ug/L 76 54 - 128
Di-n-butyl phthalate 40.0 32.68 ug/L 82 54 - 140 7
Di-n-octyl phthalate 40.0 36.18 ug/L 90 50 - 142
Hexachlorobenzene 40.0 29.64 ug/L 74 48 - 131 8
Hexachlorobutadiene 40.0 21.59 ug/L 54 28 - 120
Hexachlorocyclopentadiene 40.0 19.26 ug/L 48 17 - 120
Hexachloroethane 40.0 21.59 ug/L 54 30 - 120
9
Isophorone 40.0 27.94 ug/L 70 47 - 120
Nitrobenzene 40.0 26.31 ug/L 66 36 - 120
10
N-Nitrosodi-n-propylamine 40.0 28.34 ug/L 71 51 - 120
Pentachlorophenol 80.0 70.37 ug/L 88 21 - 150
11
Phenol 40.0 11.74 ug/L 29 14 - 120
Bis(2-chloroethoxy)methane 40.0 27.66 ug/L 69 44 - 120 12
Bis(2-chloroethyl)ether 40.0 24.80 ug/L 62 47 - 120
Bis(2-ethylhexyl) phthalate 40.0 34.49 ug/L 86 47 - 138 13
Butyl benzyl phthalate 40.0 34.97 ug/L 87 51 - 146
LCS LCS
Phenol-d5 (Surr) 27 10 - 120

MB MB
PCB-1016 ND 0.500 ug/L 07/03/14 10:40 07/03/14 14:00 1
PCB-1221 ND 0.500 ug/L 07/03/14 10:40 07/03/14 14:00 1
PCB-1232 ND 0.500 ug/L 07/03/14 10:40 07/03/14 14:00 1
PCB-1242 ND 0.500 ug/L 07/03/14 10:40 07/03/14 14:00 1
PCB-1248 ND 0.500 ug/L 07/03/14 10:40 07/03/14 14:00 1
PCB-1254 ND 0.500 ug/L 07/03/14 10:40 07/03/14 14:00 1
PCB-1260 ND 0.500 ug/L 07/03/14 10:40 07/03/14 14:00 1
MB MB
Page 35 of 58 7/30/2014
QC Sample Results 1
Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued) 3
Spike LCS LCS %Rec.
5
PCB-1016 8.00 7.832 ug/L 98 23 - 139 6
PCB-1260 8.00 7.341 ug/L 92 36 - 144
LCS LCS
7
8
9
Method: 6010B - Metals (ICP) 10
MB MB 12
Barium ND 0.0100 mg/L 07/08/14 12:51 07/08/14 19:32 1 13
Chromium ND 0.00500 mg/L 07/08/14 12:51 07/08/14 19:32 1
Lead ND 0.00500 mg/L 07/08/14 12:51 07/08/14 19:32 1
Spike LCS LCS %Rec.
Barium 2.00 2.145 mg/L 107 80 - 120
Chromium 0.200 0.2161 mg/L 108 80 - 120
Lead 0.0500 0.05180 mg/L 104 80 - 120
Lab Sample ID: LCSD 490-175197/3-A Client Sample ID: Lab Control Sample Dup
Barium 2.00 2.120 mg/L 106 80 - 120 1 20
Chromium 0.200 0.2131 mg/L 107 80 - 120 1 20
Lead 0.0500 0.05060 mg/L 101 80 - 120 2 20

MB MB
Mercury ND 0.000200 mg/L 07/07/14 09:47 07/08/14 10:36 1
Page 36 of 58 7/30/2014
QC Sample Results 1
Method: 7470A - Mercury (CVAA) (Continued) 3
Spike LCS LCS %Rec.
5
Mercury 0.00100 0.001040 mg/L 104 80 - 120 6
Lab Sample ID: 490-56590-C-1-B MS Client Sample ID: Matrix Spike 7
9
Mercury ND 0.00100 0.0009966 mg/L 100 75 - 125
Lab Sample ID: 490-56590-C-1-C MSD Client Sample ID: Matrix Spike Duplicate
10
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit 12
Mercury ND 0.00100 0.0009121 mg/L 91 75 - 125 9 20
13
Method: 7196A - Chromium, Hexavalent

MB MB
Chromium, hex ND 0.0100 mg/L 07/24/14 11:05 1

MB MB
Chromium, hex ND 0.0100 mg/L 07/24/14 11:05 1
Spike LCS LCS %Rec.
Chromium, hex 0.100 0.09900 mg/L 99 85 - 115
Spike LCS LCS %Rec.
Chromium, hex 0.100 0.09900 mg/L 99 85 - 115
Page 37 of 58 7/30/2014
QC Sample Results 1
Method: 7196A - Chromium, Hexavalent (Continued) 3
Lab Sample ID: 490-57912-E-1 MS Client Sample ID: Matrix Spike 4
5
Chromium, hex ND 0.100 0.1090 mg/L 109 85 - 115 6
Lab Sample ID: 490-57912-E-1 MSD Client Sample ID: Matrix Spike Duplicate 7
9
Chromium, hex ND 0.100 0.1070 mg/L 107 85 - 115 2 10
Lab Sample ID: 490-57912-E-1 DU Client Sample ID: Duplicate

10
Sample Sample DU DU RPD
Analyte Result Qualifier Result Qualifier Unit D RPD Limit 12
Chromium, hex ND ND mg/L NC 20
13
Page 38 of 58 7/30/2014
GC/MS VOA 3
4
490-56651-B-1 MS Matrix Spike Total/NA Water 8260B
490-56651-C-1 MSD Matrix Spike Duplicate Total/NA Water 8260B
5
490-56655-5 MW-1 Total/NA Water 8260B
6
7
490-56655-9 Trip Blank Total/NA Water 8260B
LCS 490-174385/3 Lab Control Sample Total/NA Water 8260B 8
LCSD 490-174385/4 Lab Control Sample Dup Total/NA Water 8260B
MB 490-174385/6 Method Blank Total/NA Water 8260B 9
GC/MS Semi VOA 10
Prep Batch: 174259 11
490-56655-5 MW-1 Total/NA Water 3510C 12
490-56655-6 MW-2 Total/NA Water 3510C
LCS 490-174259/2-A Lab Control Sample Total/NA Water 3510C
MB 490-174259/1-A Method Blank Total/NA Water 3510C

LCS 490-174259/2-A Lab Control Sample Total/NA Water 8270C 174259
MB 490-174259/1-A Method Blank Total/NA Water 8270C 174259
Prep Batch: 178800


LCS 490-178800/2-A Lab Control Sample Total/NA Water 8270C 178800
MB 490-178800/1-A Method Blank Total/NA Water 8270C 178800
Page 39 of 58 7/30/2014
GC Semi VOA 3
Prep Batch: 174487
4
5
6
7
490-56655-5 MW-1 Total/NA Water 8082 174487 9
490-56655-6 MW-2 Total/NA Water 8082 174487
490-56655-7 MW-3 Total/NA Water 8082 174487 10
490-56655-8 MW-4 Total/NA Water 8082 174487
LCS 490-174487/2-A Lab Control Sample Total/NA Water 8082 174487 11
MB 490-174487/1-A Method Blank Total/NA Water 8082 174487
12
Metals
Prep Batch: 174849
13
490-56590-C-1-B MS Matrix Spike Total/NA Water 7470A
490-56590-C-1-C MSD Matrix Spike Duplicate Total/NA Water 7470A
490-56655-5 MW-1 Total/NA Water 7470A
LCS 490-174849/2-A Lab Control Sample Total/NA Water 7470A
MB 490-174849/1-A Method Blank Total/NA Water 7470A
Prep Batch: 175197

LCS 490-175197/2-A Lab Control Sample Total/NA Water 3010A
LCSD 490-175197/3-A Lab Control Sample Dup Total/NA Water 3010A
MB 490-175197/1-A Method Blank Total/NA Water 3010A

490-56590-C-1-B MS Matrix Spike Total/NA Water 7470A 174849
490-56590-C-1-C MSD Matrix Spike Duplicate Total/NA Water 7470A 174849
490-56655-5 MW-1 Total/NA Water 7470A 174849
LCS 490-174849/2-A Lab Control Sample Total/NA Water 7470A 174849
MB 490-174849/1-A Method Blank Total/NA Water 7470A 174849
Page 40 of 58 7/30/2014
Metals (Continued) 3
4
490-56655-5 MW-1 Total/NA Water 6010B 175197
5
6
LCS 490-175197/2-A Lab Control Sample Total/NA Water 6010B 175197
LCSD 490-175197/3-A Lab Control Sample Dup Total/NA Water 6010B 175197
7
MB 490-175197/1-A Method Blank Total/NA Water 6010B 175197
8
General Chemistry
9
10
490-57912-E-1 DU Duplicate Total/NA Water 7196A
490-57912-E-1 MS Matrix Spike Total/NA Water 7196A 13
490-57912-E-1 MSD Matrix Spike Duplicate Total/NA Water 7196A
LCS 490-179666/13 Lab Control Sample Total/NA Water 7196A
LCS 490-179666/3 Lab Control Sample Total/NA Water 7196A
MB 490-179666/12 Method Blank Total/NA Water 7196A
MB 490-179666/4 Method Blank Total/NA Water 7196A
Page 41 of 58 7/30/2014
Lab Chronicle 1
Date Received: 07/02/14 08:15 4
5
Total/NA Analysis 8260B 1 10 mL 10 mL 174385 07/03/14 15:51 JMG TAL NSH
6
Total/NA Prep 3510C 260 mL 1 mL 174259 07/03/14 07:37 LSR TAL NSH
Total/NA Analysis 8270C 1 260 mL 1 mL 174374 07/03/14 15:42 BES TAL NSH
7
Total/NA Prep 3510C 275 mL 1.0 mL 178800 07/23/14 13:07 FXM TAL NSH
Total/NA Analysis 8270C 1 275 mL 1.0 mL 180225 07/29/14 23:38 BES TAL NSH
8
Total/NA Analysis 8082 1 140 mL 5 mL 174507 07/03/14 14:27 MGH TAL NSH 9
Total/NA Prep 3010A 50 mL 50 mL 175197 07/08/14 12:51 JBD TAL NSH
Total/NA Analysis 6010B 10 50 mL 50 mL 175386 07/08/14 21:09 DBK TAL NSH 10
Total/NA Prep 7470A 30 mL 30 mL 174849 07/07/14 09:47 NLI TAL NSH
Total/NA Analysis 7470A 1 30 mL 30 mL 175228 07/08/14 11:06 NLI TAL NSH 11
Total/NA Analysis 7196A 1 10 mL 10 mL 179666 07/24/14 11:51 BLM TAL NSH
12

Total/NA Analysis 8082 1 140 mL 5 mL 174507 07/03/14 14:40 MGH TAL NSH

Total/NA Analysis 6010B 10 50 mL 50 mL 175386 07/08/14 21:12 DBK TAL NSH

Total/NA Analysis 7470A 1 30 mL 30 mL 175228 07/08/14 11:08 NLI TAL NSH


Page 42 of 58 7/30/2014
Lab Chronicle 1
Date Received: 07/02/14 08:15 4
5
Total/NA Analysis 6010B 10 50 mL 50 mL 175386 07/08/14 21:16 DBK TAL NSH 6
7
8
Date Received: 07/02/14 08:15 10
11
12
13

Total/NA Analysis 6010B 10 5 mL 50 mL 175386 07/08/14 21:20 DBK TAL NSH

Client Sample ID: Trip Blank Lab Sample ID: 490-56655-9


Page 43 of 58 7/30/2014
Method Summary 1
3
8270C Semivolatile Organic Compounds (GC/MS) SW846 TAL NSH
4
8082 Polychlorinated Biphenyls (PCBs) by Gas Chromatography SW846 TAL NSH
6010B Metals (ICP) SW846 TAL NSH
5
7470A Mercury (CVAA) SW846 TAL NSH
7196A Chromium, Hexavalent SW846 TAL NSH 6
Protocol References: 7
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
8
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177 9
10
11
12
13
Page 44 of 58 7/30/2014
3
A2LA ISO/IEC 17025 0453.07 12-31-15 5
Alaska (UST) State Program 10 UST-087 10-31-14
7
8
Iowa State Program 7 131 04-01-16
Kansas NELAP 7 E-10229 10-31-14
9
Minnesota NELAP 5 047-999-345 12-31-14
Mississippi State Program 4 N/A 06-30-15 12
New York NELAP 2 11342 03-31-15
Oregon NELAP 10 TN200001 04-29-15
Texas NELAP 6 T104704077 08-31-14
Utah NELAP 8 TN00032 07-31-15
Washington State Program 10 C789 07-19-15
Wisconsin State Program 5 998020430 08-31-14 *
Wyoming (UST) A2LA 8 453.07 12-31-15
Page 45 of 58 7/30/2014
Page 1 of 3
1
Brown, Shali
2

3
Sent: Tuesday, July 22, 2014 3:58 PM 4
To: Brown, Shali
Cc: Stamper, Travis T; Whitmill, Dallas E 5
56655
Please proceed. 7
Thanks.
Brian W. Watson 8
Terracon 9
P [423] 602-2107 I F [423] 499-8099 I M [423] 463-6355 10
11
Sent: Tuesday, July 22, 2014 4:38 PM
12
13
Importance: High
Hi Brian,
The water samples which originally requested PAH’s were extracted for PAH’s only so the full list SVOC cannot be
reported from our current data. It appears we have one container remaining so we can re-extract out of hold for
the other compounds but they will be qualified as out of hold and we will have to charge for the additional
extraction/analysis. Do you want to proceed with the re-extraction/analysis?
Shali
Announcing TotalAccess 4.0 – Online access to your data. New homepage with easier access to your data,
multiple search criteria including sampling date and much more! Contact your Account Executive or Project
Manager today to arrange for a live demonstration
Please let us know if we met your expectations by rating the service you received from TestAmerica on this
project by visiting our website at: Project Feedback
SHALI BROWN
Project Manager
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING

Nashville, TN 37204
Tel 615.301.5031(direct) Fax 615.276.3404
Main 1-651-726-0177 x212
www.testamericainc.com

To: Brown, Shali
Page 46 of 58 7/30/2014
7/22/2014
Page 2 of 3
1
2
That is correct. Analysis of all samples (soil and groundwater) to include VOCs, SVOCs, PCBs, and Metals
3
Thanks. 4
Brian W. Watson
5
Terracon
51 Lost Mound Drive, Suite 135 I Chattanooga, TN 37406 6
P [423] 602-2107 I F [423] 499-8099 I M [423] 463-6355

8
To: Watson, Brian W. 9
Subject: RE: Proposed Sams Club #4062 - Terracon Project Number E2137034 / Test America Job No. 490-56655 10
Hi Brian, 11
If you could please clarify what is being requested for addition and removal of tests. Based on your email below 12
13
Please confirm.
Thanks,
Shali

To: Brown, Shali
Dear Ms. Brown,
Thanks.
Brian W. Watson
Terracon
Page 47 of 58 7/30/2014
7/22/2014
Page 3 of 3
1

2
P [423] 602-2107 I F [423] 499-8099 I M [423] 463-6355
4
6
mail sender. 7
9
mail sender.
11
13
mail sender.
Page 48 of 58 7/30/2014
7/22/2014
1
Brown, Shali 2
From: Watson, Brian W. [bwwatson@terracon.com] 3
To: Brown, Shali
4
Subject: RE: Proposed Sams Club #4062 - Terracon Project Number E2137034 / Test America Job
No. 490-56655 5
6
Yes, please. Thanks.
Sent from my Android phone using TouchDown (www.nitrodesk.com)

7
-----Original Message----- 8
From: Brown, Shali [Shali.Brown@testamericainc.com]
Received: Wednesday, 23 Jul 2014, 4:57PM 9
To: Watson, Brian W. [bwwatson@terracon.com]
CC: Stamper, Travis T [ttstamper@terracon.com]
Subject: RE: Proposed Sams Club #4062 - Terracon Project Number E2137034 / Test America 10
Job No. 490-56655
11
We can but they will be qualified as out of hold. Holding time for Hexavalent Chromium is
24 hrs from sample collection. Do you want us to proceed with analysis? 12
Announcing TotalAccess 4.0 – Online access to your data. New homepage with easier access
to your data, multiple search criteria including sampling date and much more! Contact your
13
Account Executive or Project Manager today to arrange for a live demonstration Please let
us know if we met your expectations by rating the service you received from TestAmerica on
this project by visiting our website at: Project
Feedback<http://secure.testamericainc.com/snaponline/s.asp?k=140312408469>
SHALI BROWN
Project Manager
TestAmerica

Nashville, TN 37204
Tel 615.301.5031(direct) Fax 615.276.3404 Main 1-651-726-0177 x212
www.testamericainc.com ________________________________
To: Brown, Shali
Subject: RE: Proposed Sams Club #4062 - Terracon Project Number E2137034 / Test America
Job No. 490-56655
Hey Shali,
I have another request for this job.

Can you run Chromium (VI) on groundwater samples?
Thanks.
Brian W. Watson
Terracon
51 Lost Mound Drive, Suite 135 I Chattanooga, TN 37406 P [423] 602-2107 I F [423]
499-8099 I M [423] 463-6355 bwwatson@terracon.com<mailto:bwwatson@terracon.com> I
terracon.com<http://www.terracon.com>

1
Page 49 of 58 7/30/2014
1
Job No. 490-56655 2
Good Morning Brian,
3
The expected due date is Monday the 28th.
4
Shali
5
to your data, multiple search criteria including sampling date and much more! Contact your
Account Executive or Project Manager today to arrange for a live demonstration Please let 6
us know if we met your expectations by rating the service you received from TestAmerica on
this project by visiting our website at: Project 7
SHALI BROWN 8
Project Manager
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING 9
2960 Foster Creighton Drive 10
Nashville, TN 37204
Tel 615.301.5031(direct) Fax 615.276.3404 Main 1-651-726-0177 x212
www.testamericainc.com ________________________________ 11
Sent: Wednesday, July 23, 2014 9:46 AM 12
To: Brown, Shali
13
Job No. 490-56655
Hey Shali,
When can I expect the results?
Thanks.
Brian W. Watson
Terracon
From: Watson, Brian W.

To: 'Brown, Shali'
Cc: Stamper, Travis T; Whitmill, Dallas E
Job No. 490-56655
Please proceed.
Thanks.
Brian W. Watson
Terracon

Job No. 490-56655
Page 50 of 58 7/30/2014
1
Importance: High
Hi Brian,
2
The water samples which originally requested PAH’s were extracted for PAH’s only so the 3
full list SVOC cannot be reported from our current data. It appears we have one container
remaining so we can re-extract out of hold for the other compounds but they will be 4
qualified as out of hold and we will have to charge for the additional
extraction/analysis. Do you want to proceed with the re-extraction/analysis?
5
Shali
6
to your data, multiple search criteria including sampling date and much more! Contact your 7
Account Executive or Project Manager today to arrange for a live demonstration Please let
us know if we met your expectations by rating the service you received from TestAmerica on 8
this project by visiting our website at: Project
SHALI BROWN 9
Project Manager
TestAmerica 10
2960 Foster Creighton Drive 11

Nashville, TN 37204
Tel 615.301.5031(direct) Fax 615.276.3404 Main 1-651-726-0177 x212 12
www.testamericainc.com<http://www.testamericainc.com>
________________________________
13
To: Brown, Shali
Job No. 490-56655
That is correct. Analysis of all samples (soil and groundwater) to include VOCs, SVOCs,
PCBs, and Metals (aluminum, barium, chromium, copper, iron, lead, magnesium, nickel, and
zinc).
Thanks.
Brian W. Watson
Terracon

Job No. 490-56655
Hi Brian,
If you could please clarify what is being requested for addition and removal of tests.
Based on your email below and the attached COC I currently have the following…….
For the water samples you want us to add the full list of SVOC’s to replace the PAH’s,
remove arsenic, cadmium, selenium, and silver, then add aluminum, copper, iron, magnesium,
nickel, and zinc.
For the soil samples you want us to remove arsenic, cadmium, selenium, and silver, then
add aluminum, copper, iron, magnesium, nickel, and zinc.
Please confirm.
Page 51 of 58 7/30/2014
1
Thanks,
Shali
2
________________________________ 3
Sent: Wednesday, July 16, 2014 9:01 AM 4
To: Brown, Shali
Subject: Proposed Sams Club #4062 - Terracon Project Number E2137034 / Test America Job
5
No. 490-56655
6
Dear Ms. Brown,
7
Thanks for talking with me this morning. As mentioned, I need to get a revision placed on
the laboratory analysis for the proposed Sams Club #4062 job (Terracon Project Number
E2137034 / Test America Job No. 490-56655). 8
Analysis of all samples (soil and groundwater) to include VOCs, SVOCs, PCBs, and Metals 9

10
Thanks. 11
Brian W. Watson
12
Terracon
13
Terracon provides environmental, facilities, geotechnical, and materials consulting

engineering services delivered with responsiveness, resourcefulness, and reliability.
________________________________
Private and confidential as detailed here
(www.terracon.com/disclaimer<http://www.terracon.com/disclaimer>). If you cannot access
hyperlink, please e-mail sender.

________________________________
Private and confidential as detailed here
(www.terracon.com/disclaimer<http://www.terracon.com/disclaimer>). If you cannot access
hyperlink, please e-mail sender.

________________________________
Private and confidential as detailed here (www.terracon.com/disclaimer). If you cannot
access hyperlink, please e-mail sender.

________________________________

Page 52 of 58 7/30/2014
1
________________________________

2
3
4
5
6
7
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13
Page 53 of 58 7/30/2014
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Page 54 of 58 7/30/2014
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Page 55 of 58 7/30/2014
Page 1 of 2
1
Brown, Shali
2

3
Sent: Wednesday, July 16, 2014 12:02 PM 4
To: Brown, Shali
Cc: Stamper, Travis T 5
56655
That is correct. Analysis of all samples (soil and groundwater) to include VOCs, SVOCs, PCBs, and Metals 7
Thanks. 8
Brian W. Watson
9
Terracon
10
P [423] 602-2107 I F [423] 499-8099 I M [423] 463-6355
12
13
Hi Brian,
If you could please clarify what is being requested for addition and removal of tests. Based on your email below
Please confirm.
Thanks,
Shali

To: Brown, Shali
Dear Ms. Brown,
Page 56 of 58 7/30/2014
7/17/2014
Page 2 of 2
1
2
3
Thanks. 4
Brian W. Watson
5
Terracon 6
P [423] 602-2107 I F [423] 499-8099 I M [423] 463-6355 7
8
10
mail sender.
12
mail sender.
Page 57 of 58 7/30/2014
7/17/2014
1
2

4
List Number: 1
5
Radioactivity wasn't checked or is </= background as measured by a survey True
meter. 7
tampered with. 9
12
13
Sample Preservation Verified. True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True
<6mm (1/4").
Residual Chlorine Checked. True
Page 58 of 58 7/30/2014
7/22/2014
Mr. Travis Stamper
Terracon Consulting Engineers
51 Lost Mound Dr
Chattanooga TN 37406
Project Name: Sam's Club - Alcoa

Project #: E2137034
Workorder #: 1407110
Dear Mr. Travis Stamper
The following report includes the data for the above referenced project for sample(s)
received on 7/8/2014 at Air Toxics Ltd.
The data and associated QC analyzed by TO-15 are compliant with the project
requirements or laboratory criteria with the exception of the deviations noted in the
attached case narrative.
Thank you for choosing Air Toxics Ltd. for your air analysis needs. Air Toxics Ltd. is
committed to providing accurate data of the highest quality. Please feel free to contact
the Project Manager: Ausha Scott at 916-985-1000 if you have any questions regarding
the data in this report.
Regards,
Ausha Scott
Project Manager
Page 1 of 23
WORK ORDER #: 1407110
Work Order Summary
CLIENT: Mr. Travis Stamper BILL TO: Accounts Payable

Terracon Consulting Engineers Terracon Consulting Engineers
51 Lost Mound Dr 51 Lost Mound Dr
Chattanooga, TN 37406 Chattanooga, TN 37406
PHONE: 423-699-3111 P.O. # E2137034

FAX: PROJECT # E2137034 Sam's Club - Alcoa
DATE RECEIVED: 07/08/2014 CONTACT: Ausha Scott
DATE COMPLETED: 07/22/2014
RECEIPT FINAL
FRACTION # NAME TEST VAC./PRES. PRESSURE
01A SG-1 TO-15 3.5 "Hg 15.4 psi
02A SG-2 TO-15 2.6 "Hg 14.9 psi
03A SG-3 TO-15 3.9 "Hg 15 psi
04A SG-4 TO-15 4.7 "Hg 15.4 psi
05A SG-5 TO-15 3.9 "Hg 15.2 psi
06A Lab Blank TO-15 NA NA
07A CCV TO-15 NA NA
08A LCS TO-15 NA NA
08AA LCSD TO-15 NA NA
CERTIFIED BY: DATE: 07/22/14
Technical Director
Certification numbers: AZ Licensure AZ0775, CA NELAP - 12282CA, NJ NELAP - CA016, NY NELAP - 11291,
TX NELAP - T104704434-13-6, UT NELAP CA009332013-4, VA NELAP - 460197, WA NELAP - C935
Name of Accrediting Agency: NELAP/ORELAP (Oregon Environmental Laboratory Accreditation Program)
Accreditation number: CA300005, Effective date: 10/18/2013, Expiration date: 10/17/2014.
Eurofins Air Toxics Inc.. certifies that the test results contained in this report meet all requirements of the NELAC standards
This report shall not be reproduced, except in full, without the written approval of Eurofins Air Toxics, Inc.
180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 9563
(916) 985-1000 . (800) 985-5955 . FAX (916) 985-1020
Page 2 of 23
LABORATORY NARRATIVE
EPA Method TO-15
Terracon Consulting Engineers
Workorder# 1407110
Five 1 Liter Summa Canister samples were received on July 08, 2014. The laboratory performed analysis
via EPA Method TO-15 using GC/MS in the full scan mode.
This workorder was independently validated prior to submittal using 'USEPA National Functional
Guidelines' as generally applied to the analysis of volatile organic compounds in air. A rules-based, logic
driven, independent validation engine was employed to assess completeness, evaluate pass/fail of relevant
project quality control requirements and verification of all quantified amounts.
Receiving Notes
There were no receiving discrepancies.
Analytical Notes
There were no analytical discrepancies.
Definition of Data Qualifying Flags
Eight qualifiers may have been used on the data analysis sheets and indicates as follows:
B - Compound present in laboratory blank greater than reporting limit (background subtraction not
performed).
J - Estimated value.
E - Exceeds instrument calibration range.
S - Saturated peak.
Q - Exceeds quality control limits.
U - Compound analyzed for but not detected above the reporting limit, LOD, or MDL value. See
data page for project specific U-flag definition.
UJ- Non-detected compound associated with low bias in the CCV
N - The identification is based on presumptive evidence.
File extensions may have been used on the data analysis sheets and indicates
as follows:
a-File was requantified
b-File was quantified by a second column and detector
r1-File was requantified for the purpose of reissue
Page 3 of 23
Summary of Detected Compounds
EPA METHOD TO-15 GC/MS FULL SCAN
Client Sample ID: SG-1

Lab ID#: 1407110-01A
Rpt. Limit Amount Rpt. Limit Amount
Compound (ppbv) (ppbv) (ug/m3) (ug/m3)
2-Propanol 4.6 11 11 27
4-Methyl-2-pentanone 1.2 2.3 4.8 9.3

Lab ID#: 1407110-02A
2-Propanol 4.4 11 11 27
4-Methyl-2-pentanone 1.1 2.5 4.5 10

Lab ID#: 1407110-03A
Acetone 12 14 28 34
2-Propanol 4.6 10 11 25

Lab ID#: 1407110-04A
Ethanol 4.9 5.1 9.2 9.6
Acetone 12 21 29 51
2-Propanol 4.9 12 12 28

Lab ID#: 1407110-05A
Acetone 12 12 28 29
Page 4 of 23
Summary of Detected Compounds

Lab ID#: 1407110-05A
2-Propanol 4.7 7.3 12 18
Page 5 of 23
Lab ID#: 1407110-01A
File Name: j071010 Date of Collection: 7/7/14 11:48:00 AM

Dil. Factor: 2.32 Date of Analysis: 7/10/14 12:37 PM
Freon 12 1.2 Not Detected 5.7 Not Detected
Chloromethane 12 Not Detected 24 Not Detected
Vinyl Chloride 1.2 Not Detected 3.0 Not Detected
1,3-Butadiene 1.2 Not Detected 2.6 Not Detected
Bromomethane 12 Not Detected 45 Not Detected
Chloroethane 4.6 Not Detected 12 Not Detected
Ethanol 4.6 Not Detected 8.7 Not Detected
1,1-Dichloroethene 1.2 Not Detected 4.6 Not Detected
Acetone 12 Not Detected 28 Not Detected
2-Propanol 4.6 11 11 27
Carbon Disulfide 4.6 Not Detected 14 Not Detected
3-Chloropropene 4.6 Not Detected 14 Not Detected
Methylene Chloride 12 Not Detected 40 Not Detected
Methyl tert-butyl ether 1.2 Not Detected 4.2 Not Detected
trans-1,2-Dichloroethene 1.2 Not Detected 4.6 Not Detected
Hexane 1.2 Not Detected 4.1 Not Detected
1,1-Dichloroethane 1.2 Not Detected 4.7 Not Detected
2-Butanone (Methyl Ethyl Ketone) 4.6 Not Detected 14 Not Detected
cis-1,2-Dichloroethene 1.2 Not Detected 4.6 Not Detected
Tetrahydrofuran 1.2 Not Detected 3.4 Not Detected
Chloroform 1.2 Not Detected 5.7 Not Detected
1,1,1-Trichloroethane 1.2 Not Detected 6.3 Not Detected
Cyclohexane 1.2 Not Detected 4.0 Not Detected
Carbon Tetrachloride 1.2 Not Detected 7.3 Not Detected
2,2,4-Trimethylpentane 1.2 Not Detected 5.4 Not Detected
Benzene 1.2 Not Detected 3.7 Not Detected
Heptane 1.2 Not Detected 4.8 Not Detected
Trichloroethene 1.2 Not Detected 6.2 Not Detected
1,2-Dichloropropane 1.2 Not Detected 5.4 Not Detected
1,4-Dioxane 4.6 Not Detected 17 Not Detected
Bromodichloromethane 1.2 Not Detected 7.8 Not Detected
cis-1,3-Dichloropropene 1.2 Not Detected 5.3 Not Detected
Toluene 1.2 Not Detected 4.4 Not Detected
trans-1,3-Dichloropropene 1.2 Not Detected 5.3 Not Detected
Tetrachloroethene 1.2 Not Detected 7.9 Not Detected
2-Hexanone 4.6 Not Detected 19 Not Detected
Page 6 of 23
Lab ID#: 1407110-01A
File Name: j071010 Date of Collection: 7/7/14 11:48:00 AM

Dibromochloromethane 1.2 Not Detected 9.9 Not Detected
1,2-Dibromoethane (EDB) 1.2 Not Detected 8.9 Not Detected
Chlorobenzene 1.2 Not Detected 5.3 Not Detected
Ethyl Benzene 1.2 Not Detected 5.0 Not Detected
m,p-Xylene 1.2 Not Detected 5.0 Not Detected
o-Xylene 1.2 Not Detected 5.0 Not Detected
Styrene 1.2 Not Detected 4.9 Not Detected
Bromoform 1.2 Not Detected 12 Not Detected
Cumene 1.2 Not Detected 5.7 Not Detected
1,1,2,2-Tetrachloroethane 1.2 Not Detected 8.0 Not Detected
Propylbenzene 1.2 Not Detected 5.7 Not Detected
4-Ethyltoluene 1.2 Not Detected 5.7 Not Detected
1,3,5-Trimethylbenzene 1.2 Not Detected 5.7 Not Detected
1,3-Dichlorobenzene 1.2 Not Detected 7.0 Not Detected
alpha-Chlorotoluene 1.2 Not Detected 6.0 Not Detected
1,2,4-Trichlorobenzene 4.6 Not Detected 34 Not Detected
Hexachlorobutadiene 4.6 Not Detected 49 Not Detected
Container Type: 1 Liter Summa Canister

Method
Surrogates %Recovery Limits
Toluene-d8 99 70-130
1,2-Dichloroethane-d4 98 70-130
4-Bromofluorobenzene 98 70-130
Page 7 of 23
Lab ID#: 1407110-02A
File Name: j071011 Date of Collection: 7/7/14 12:14:00 PM

Acetone 11 Not Detected 26 Not Detected
2-Propanol 4.4 11 11 27
4-Methyl-2-pentanone 1.1 2.5 4.5 10
Page 8 of 23
Lab ID#: 1407110-02A


Method
Page 9 of 23
Lab ID#: 1407110-03A

Acetone 12 14 28 34
2-Propanol 4.6 10 11 25
Page 10 of 23
Lab ID#: 1407110-03A


Method
Page 11 of 23
Lab ID#: 1407110-04A

Ethanol 4.9 5.1 9.2 9.6
Acetone 12 21 29 51
2-Propanol 4.9 12 12 28
Page 12 of 23
Lab ID#: 1407110-04A

Dibromochloromethane 1.2 Not Detected 10 Not Detected

Method
Toluene-d8 100 70-130
Page 13 of 23
Lab ID#: 1407110-05A

Acetone 12 12 28 29
2-Propanol 4.7 7.3 12 18
4-Methyl-2-pentanone 1.2 Not Detected 4.8 Not Detected
Page 14 of 23
Lab ID#: 1407110-05A

Dibromochloromethane 1.2 Not Detected 10 Not Detected

Method
Page 15 of 23
Client Sample ID: Lab Blank
Lab ID#: 1407110-06A
File Name: j071007 Date of Collection: NA

Dil. Factor: 1.00 Date of Analysis: 7/10/14 10:17 AM
Chloromethane 5.0 Not Detected 10 Not Detected
Bromomethane 5.0 Not Detected 19 Not Detected
Chloroethane 2.0 Not Detected 5.3 Not Detected
Acetone 5.0 Not Detected 12 Not Detected
2-Propanol 2.0 Not Detected 4.9 Not Detected
Carbon Disulfide 2.0 Not Detected 6.2 Not Detected
3-Chloropropene 2.0 Not Detected 6.3 Not Detected
Methylene Chloride 5.0 Not Detected 17 Not Detected
2-Butanone (Methyl Ethyl Ketone) 2.0 Not Detected 5.9 Not Detected
1,4-Dioxane 2.0 Not Detected 7.2 Not Detected
4-Methyl-2-pentanone 0.50 Not Detected 2.0 Not Detected
2-Hexanone 2.0 Not Detected 8.2 Not Detected
Page 16 of 23
Client Sample ID: Lab Blank
Lab ID#: 1407110-06A

Bromoform 0.50 Not Detected 5.2 Not Detected
Container Type: NA - Not Applicable

Method
Toluene-d8 100 70-130
Page 17 of 23
Client Sample ID: CCV
Lab ID#: 1407110-07A

Compound %Recovery
Freon 12 89
Freon 114 94
Chloromethane 99
Vinyl Chloride 90
1,3-Butadiene 89
Bromomethane 96
Chloroethane 91
Freon 11 89
Ethanol 88
Freon 113 92
1,1-Dichloroethene 94
Acetone 82
2-Propanol 91
Carbon Disulfide 86
3-Chloropropene 91
Methylene Chloride 88
Methyl tert-butyl ether 92
trans-1,2-Dichloroethene 92
Hexane 92
1,1-Dichloroethane 91
2-Butanone (Methyl Ethyl Ketone) 94
cis-1,2-Dichloroethene 95
Tetrahydrofuran 92
Chloroform 92
1,1,1-Trichloroethane 92
Cyclohexane 98
Carbon Tetrachloride 93
2,2,4-Trimethylpentane 97
Benzene 91
1,2-Dichloroethane 92
Heptane 99
Trichloroethene 97
1,2-Dichloropropane 96
1,4-Dioxane 92
Bromodichloromethane 96
cis-1,3-Dichloropropene 100
4-Methyl-2-pentanone 94
Toluene 95
trans-1,3-Dichloropropene 95
1,1,2-Trichloroethane 95
Tetrachloroethene 97
2-Hexanone 94
Page 18 of 23
Client Sample ID: CCV
Lab ID#: 1407110-07A

Compound %Recovery
Dibromochloromethane 97
1,2-Dibromoethane (EDB) 98
Chlorobenzene 96
Ethyl Benzene 99
m,p-Xylene 98
o-Xylene 99
Styrene 102
Bromoform 98
Cumene 97
1,1,2,2-Tetrachloroethane 95
Propylbenzene 97
4-Ethyltoluene 106
1,3,5-Trimethylbenzene 98
1,2,4-Trimethylbenzene 100
1,3-Dichlorobenzene 97
alpha-Chlorotoluene 101
1,2,4-Trichlorobenzene 98
Hexachlorobutadiene 97

Method
Toluene-d8 100 70-130
Page 19 of 23
Client Sample ID: LCS
Lab ID#: 1407110-08A

Method
Compound %Recovery Limits
Freon 12 84 70-130
Freon 114 91 70-130
Chloromethane 92 70-130
Vinyl Chloride 85 70-130
1,3-Butadiene 84 70-130
Bromomethane 92 70-130
Chloroethane 84 70-130
Freon 11 84 70-130
Ethanol 86 70-130
Freon 113 100 70-130
1,1-Dichloroethene 98 70-130
Acetone 83 70-130
2-Propanol 85 70-130
Carbon Disulfide 75 70-130
3-Chloropropene 88 70-130
Methylene Chloride 90 70-130
Methyl tert-butyl ether 88 70-130
trans-1,2-Dichloroethene 75 70-130
Hexane 90 70-130
1,1-Dichloroethane 89 70-130
2-Butanone (Methyl Ethyl Ketone) 90 70-130
cis-1,2-Dichloroethene 104 70-130
Tetrahydrofuran 87 70-130
Chloroform 90 70-130
1,1,1-Trichloroethane 89 70-130
Cyclohexane 97 70-130
Carbon Tetrachloride 91 70-130
2,2,4-Trimethylpentane 95 70-130
Benzene 88 70-130
Heptane 96 70-130
Trichloroethene 92 70-130
1,2-Dichloropropane 90 70-130
1,4-Dioxane 92 70-130
Bromodichloromethane 93 70-130
cis-1,3-Dichloropropene 98 70-130
4-Methyl-2-pentanone 87 70-130
Toluene 91 70-130
trans-1,3-Dichloropropene 85 70-130
Tetrachloroethene 92 70-130
2-Hexanone 82 70-130
Page 20 of 23
Client Sample ID: LCS
Lab ID#: 1407110-08A

Method
Dibromochloromethane 94 70-130
1,2-Dibromoethane (EDB) 91 70-130
Chlorobenzene 89 70-130
Ethyl Benzene 91 70-130
m,p-Xylene 89 70-130
o-Xylene 90 70-130
Styrene 95 70-130
Bromoform 96 70-130
Cumene 93 70-130
1,1,2,2-Tetrachloroethane 88 70-130
Propylbenzene 92 70-130
4-Ethyltoluene 98 70-130
1,3,5-Trimethylbenzene 88 70-130
1,3-Dichlorobenzene 91 70-130
alpha-Chlorotoluene 103 70-130
1,2,4-Trichlorobenzene 88 70-130
Hexachlorobutadiene 87 70-130

Method
Toluene-d8 101 70-130
Page 21 of 23
Client Sample ID: LCSD
Lab ID#: 1407110-08AA

Method
Freon 12 83 70-130
Freon 114 90 70-130
Chloromethane 90 70-130
Vinyl Chloride 83 70-130
1,3-Butadiene 83 70-130
Bromomethane 90 70-130
Chloroethane 82 70-130
Freon 11 83 70-130
Ethanol 84 70-130
Freon 113 99 70-130
1,1-Dichloroethene 98 70-130
Acetone 80 70-130
2-Propanol 84 70-130
Carbon Disulfide 74 70-130
3-Chloropropene 87 70-130
Methylene Chloride 88 70-130
Methyl tert-butyl ether 86 70-130
trans-1,2-Dichloroethene 74 70-130
Hexane 88 70-130
2-Butanone (Methyl Ethyl Ketone) 89 70-130
cis-1,2-Dichloroethene 103 70-130
Tetrahydrofuran 86 70-130
Chloroform 90 70-130
Cyclohexane 96 70-130
Carbon Tetrachloride 91 70-130
2,2,4-Trimethylpentane 93 70-130
Benzene 87 70-130
Heptane 94 70-130
Trichloroethene 91 70-130
1,2-Dichloropropane 88 70-130
1,4-Dioxane 91 70-130
Bromodichloromethane 94 70-130
cis-1,3-Dichloropropene 97 70-130
4-Methyl-2-pentanone 86 70-130
Toluene 89 70-130
trans-1,3-Dichloropropene 85 70-130
Tetrachloroethene 92 70-130
2-Hexanone 81 70-130
Page 22 of 23
Client Sample ID: LCSD
Lab ID#: 1407110-08AA

Method
Dibromochloromethane 96 70-130
1,2-Dibromoethane (EDB) 93 70-130
Chlorobenzene 89 70-130
Ethyl Benzene 92 70-130
m,p-Xylene 89 70-130
o-Xylene 90 70-130
Styrene 95 70-130
Bromoform 96 70-130
Cumene 91 70-130
1,1,2,2-Tetrachloroethane 88 70-130
Propylbenzene 92 70-130
4-Ethyltoluene 92 70-130
alpha-Chlorotoluene 103 70-130
1,2,4-Trichlorobenzene 95 70-130
Hexachlorobutadiene 93 70-130

Method
Toluene-d8 100 70-130
Page 23 of 23

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Lim

1.0 INTRODUCTION ................................................................................................................. 1

1.1 Standard of Care

1.2 Additional Scope Limitations

Responsive ■ Resourceful ■ Reliable 1

This repo ort can be re

The obje ective of this

2.1 Soil Sample Collection

Responsive ■ Resourrceful ■ Relia

Based on n the field screening

Upon completion of the soil sam

Responsive ■ Resourrceful ■ Relia

2.3 Soil-Gas Sampling Points

Five soil--gas samplinng points (deenoted as SG-1,

Responsive ■ Resourrceful ■ Relia

With the exception of Tetrachloro

3.4 Soil Gas Analy

Responsive ■ Resourrceful ■ Relia

Responsive ■ Resourrceful ■ Relia

This figure copied from USGS 7.5 minute Quadrangle

Temporary Monitoring Well

Soil-Gas Sampling Point

B-36 B-41 B-42 B-43

BASE DRAWING PROVIDED BY CLIENT

Project Manager: Project No.

DEPTH MATERIAL DESCRIPTION

2" diameter PVC.

Advancement Method: Notes:

WATER LEVEL OBSERVATIONS Well Started: 6/30/2014 Well Completed: 6/30/2014

Advancement Method: Notes:

WATER LEVEL OBSERVATIONS Well Started: 6/30/2014 Well Completed: 6/30/2014

DEPTH MATERIAL DESCRIPTION

Advancement Method: Notes:

WATER LEVEL OBSERVATIONS Well Started: 6/30/2014 Well Completed: 6/30/2014

- trace gravel at 38.5'

2" diameter PVC 45

Advancement Method: Notes:

WATER LEVEL OBSERVATIONS Well Started: 6/30/2014 Well Completed: 6/30/2014

DEPTH MATERIAL DESCRIPTION

light olive, at 13.5'

2" diameter PVC.

Advancement Method: Notes:

WATER LEVEL OBSERVATIONS Well Started: 7/1/2014 Well Completed: 7/1/2014

2" diameter PVC

Advancement Method: Notes:

WATER LEVEL OBSERVATIONS Well Started: 7/1/2014 Well Completed: 7/1/2014

DEPTH MATERIAL DESCRIPTION

2" diameter PVC.

Advancement Method: Notes:

WATER LEVEL OBSERVATIONS Well Started: 7/1/2014 Well Completed: 7/1/2014

2" diameter PVC

Advancement Method: Notes:

WATER LEVEL OBSERVATIONS Well Started: 7/1/2014 Well Completed: 7/1/2014

medium stiff to stiff, at 8.5'

Advancement Method: Notes:

WATER LEVEL OBSERVATIONS Boring Started: 6/1/2014 Boring Completed: 6/1/2014

Sample ID MW‐1 MW‐2 MW‐3 MW‐4

Note: For clarity only detected analytes are shown.

NE - Screening Levels Not Established

Sample ID MW‐1 MW‐2 MW‐3 MW‐4

Note: For Clarity only detected analytes are shown

Sample ID SG‐1 SG‐2 SG‐3 SG‐4 SG‐5

EPA RSL EPA RSL