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-Qualitative Analysis
-Establishes the chemical identity of the species in the sample
-Quantitative Analysis
-Determines the relative amount of species or analytes, in
numerical terms
1A—The Role of Analytical Chemistry
• 1-Picking a Method
• -The Essential First Step
• -Choice is sometimes difficult and requires experience and intuition
• -Consider the level of accuracy required
• -Selected method usually represents a compromise between the accuracy
needed and the time and money that are available for the analysis (time
consuming task)
• -Consider the number of samples to be analyzed
• -Consider the complexity of the sample and the number of components in the
sample
1C—Stepping Through A Typical Quantitative Analysis
• 4-Eliminating Interferences
• -Eliminate substances from the sample that may interfere with the
measurement step
• -Species other than the analyte that affect the final measurement are called
interferences
• -A scheme must be devised to isolate the analytes from interferences before
the final measurement is made.
• -Techniques or reactions that work for only one analyte are said to be specific
• -Techniques or reactions that apply for only a few analytes are selective
1C—Stepping Through A Typical Quantitative Analysis
• 6-Calculating Results
• -Computing analyte concentrations from experimental data is usually
relatively easy
• -Computations are based on raw experimental data collected in the
measurement step, the characteristics of the measurement instruments, and the
stoichiometry of the analytical reaction
1C—Stepping Through A Typical Quantitative Analysis