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Chemistry Experiment Double Indicator Titration 1: Procedure
Chemistry Experiment Double Indicator Titration 1: Procedure
Procedure
PartI 1. Transfer10.00gofthesampleontothewatchglassandweighittothenearest 0.01g. Prepareasolutionofthesamplein250mlvolumetricflask.
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ChemTAS
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Usingthefunnel,rinsetheburettewiththehydrochloricacidandfillitwiththe sameacid.Donotforgettorinseandfillthetip.Recordtheinitialburettereading intheTrialcolumnoftheResultsTable. Usingapipettefiller,rinsethepipettewithsomeofthesamplesolutionand carefullytransfer25.00cm3ofthesolutiontoaclean250cm3conicalflask. Add23dropsofthephenolphthaleinindicatorsolution. Runhydrochloricacidfromtheburetteintotheflask,withswirling,untilthesolu tionjustturncolor(Pinktocolorless). Recordthefinalburettereading. Refilltheburettewiththehydrochloricacid,andagainrecordtheinitialburette readingtothenears0.05cm3(onedrop). Add23dropsoftheMethylOrangeindicatorsolution. Runhydrochloricacidfromtheburetteintotheflask,withswirling,untilthesolu tionjustturncolor(YellowtoOrange).Recordthefinalburettereading. (Thefirstflaskmaybeusedasatrialrun,becauseyouwillprobablyovershootthe endpoint.) Repeatsteps49atleastthreetimesmore. Emptytheburetteandwashitcarefullyimmediatelyafterthetitration,especially ifithasagroundglasstap.
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ResultsandCalculations ResultTableI
Usingyourdata,youcanfillintheResultsTables.
moldm3 g g g g g dm3
ResultTablesII&III
Trial FinalBuretteReadings(I)/cm3 InitialBuretteReadings(I)/cm3 Volumeused(I)/cm3 MeanvolumeofHCl(aq)used(I)/cm3 FinalBuretteReadings(II)/cm3 InitialBuretteReadings(II)/cm3 Volumeused(II)/cm3 MeanvolumeofHCl(aq)used(II)/cm3 1st 2nd 3rd
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Calculation
Calculatethecompositionofthesamplebymass. END
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