Effect of Temperature and Sequestrants on Calcium Carbonate Precipitation

Table 2.
1 DETAILS OF THE SAMPLES PREPARED

Table 2.1.1 BLANK (WITHOUT ANY ADDITIVE)
S. No
Sample
Number
CaCl2
(ml)
Na2CO3
(ml)
Sequestrant
(ml)
Temperature
(oC)
Digestion
Time (h)
Initial pH
Final pH
S1
50
50
---
60
10
9.02
9.12
S2
50
50
---
100
10
9.02
9.23
S3
50
50
---
130
24
9.02
9.48
S4
50
50
---
170
48
9.02
9.45
S5
50
50
---
200
48
9.02
9.51
S6
50
50
---
230
48
9.02
9.52
Table 2.1.2 IN THE PRESENCE OF EDTA

S. No
Sample
Number
CaCl2
(ml)
Na2CO3
(ml)
EDTA
(ml)
Temperature
oC
Digestion
Time (h)
Initial pH
Final pH
S7
50
50
20
60
10
8.05
8.32
S8
50
50
20
100
10
8.05
8.45
S9
50
50
20
130
24
8.05
8.60
S 10
50
50
20
170
48
8.05
8.62
S 11
50
50
20
200
48
8.05
8.74
S 12
50
50
20
230
48
8.05
8.98
36
Table 2.1.3 IN THE PRESENCE OF NTA

S. No
Sample
Number
CaCl2
(ml)
Na2CO3
(ml)
NTA
(ml)
Temperature
(oC)
Digestion
Time (h)
Initial pH
Final pH
S 13
50
60
20
60
10
8.72
8.81
S 14
50
60
20
80
10
8.72
8.80
S 15
50
60
20
100
72
8.72
8.92
S 16
50
60
20
130
72
8.72
8.94
S 17
50
60
20
150
72
8.72
8.99
S 18
50
60
20
170
72
8.72
8.98
S 19
50
60
20
200
72
8.72
8.99
S 20
50
60
20
230
72
8.72
9.26
37
Table 2.1.4 IN THE PRESENCE OF HEDTA

S. No
Sample
Number
CaCl2
(ml)
Na2CO3
(ml)
HEDTA
(ml)
Temperature
(oC)
Digestion
Time (h)
Initial pH
Final pH
S 21
50
50
20
60
10
6.2
8.50
S 22
50
50
20
80
10
6.2
8.55
S 23
50
50
20
100
10
6.2
8.54
S 24
50
50
20
130
24
6.2
9.61
S 25
50
50
20
170
48
6.2
9.51
S 26
50
50
20
200
48
6.2
9.66
S 27
50
50
20
230
48
6.2
9.71
38
Table 2.1.5 IN THE PRESENCE OF DTPA
S. No
Sample
Number
CaCl2
(ml)
Na2CO3
(ml)
DTPA
(ml)
Temperature
(oC)
Digestion
Time (h)
Initial pH
Final pH
S 28
50
50
20
60
10
7.6
8.02
S 29
50
50
20
80
10
7.6
8.04
S 30
50
50
20
100
10
7.6
8.012
S 31
50
50
20
130
24
7.6
8.24
S 32
50
50
20
150
48
7.6
8.18
S 33
50
50
20
170
48
7.6
8.62
S 34
50
50
20
200
48
7.6
8.65
S 35
50
50
20
230
48
7.6
8.79
39
Table 2.1.6 IN THE PRESENCE OF HEDP (AQ-330)

S. No
Sample
Number
CaCl2
(ml)
Na2CO3
(ml)
HEDP(AQ-330) Temperature Digestion

(ml)
(oC)
Time (h)
S 36
50
50
20
60
S 37
50
50
20
S 38
50
50
S 39
50
S 40
6
7
Initial pH
Final pH
10
8.44
8.51
80
10
8.44
8.50
20
100
72
8.44
8.66
50
20
130
72
8.44
8.75
50
50
20
170
72
8.44
8.89
S 41
50
50
20
200
72
8.44
9.00
S 42
50
50
20
230
72
8.44
9.01
40
Table 2.1.7 IN THE PRESENCE OF HEDP (AQ-330)

S. No
Sample
Number
CaCl2
(ml)
Na2CO3
(ml)
HEDP(AQ-330) Temperature Digestion

(ml)
(oC)
Time (h)
S 43
50
50
10
60
S 44
50
50
10
S 45
50
50
S 46
50
S 47
6
7
Initial pH
Final pH
10
8.74
8.77
80
10
8.74
8.82
10
100
72
8.74
8.91
50
10
130
72
8.74
8.98
50
50
10
170
72
8.74
8.98
S 48
50
50
10
200
72
8.74
9.05
S 49
50
50
10
230
72
8.74
9.11
41
Table 2.1.8 IN THE PRESENCE OF EDTA AND HEDP

S. No
Sample
Number
CaCl2
(ml)
Na2CO3
(ml)
EDTA + HEDP Temperature Digestion

(ml)
(oC)
Time (h)
Initial
pH
Final pH
S 50
50
60
10+10
60
10
8.10
8.31
S 51
50
60
10+10
100
72
8.10
8.45
S 52
50
60
10+10
130
72
8.10
8.48
S 53
50
60
10+10
200
72
8.10
8.49
S 54
50
60
10+10
230
72
8.10
8.62
Table 2.1.9 IN PRESENCE OF EDTA AND NTA

S. No
Sample
Number
CaCl2
(ml)
Na2CO3
(ml)
EDTA + NTA Temperature

(ml)
(oC)
Digestion
Time (h)
Initial pH
Final pH
S 55
50
65
10+10
60
10
8.21
8.32
S 56
50
65
10+10
100
72
8.21
8.36
S 57
50
65
10+10
130
72
8.21
8.44
S 58
50
65
10+10
200
72
8.21
8.68
S 59
50
65
10+10
230
72
8.21
8.75
42
Table 2.1.10 IN THE PRESENCE OF HEDP AND NTA

S. No
Sample
Number
CaCl2
(ml)
Na2CO3
(ml)
HEDP + NTA
(ml)
Temperature
(oC)
Digestion
Time (h)
Initial pH
Final pH
S 60
50
60
10+10
60
10
8.30
8.45
S 61
50
60
10+10
100
72
8.30
8.77
S 62
50
60
10+10
130
72
8.30
8.91
S 63
50
60
10+10
200
72
8.30
9.16
S 64
50
60
10+10
230
72
8.30
9.21
Initial
pH
Final pH
Table 2.1.11 IN THE PRESENCE OF EDTA AND HEDTA

S. No
Sample
Number
CaCl2
(ml)
Na2CO3
(ml)
EDTA + HEDTA Temperature Digestion

(ml)
(oC)
Time (h)
S 65
50
65
10+10
60
10
6.46
7.21
S 66
50
65
10+10
100
72
6.46
7.44
S 67
50
65
10+10
130
72
6.46
7.75
S 68
50
65
10+10
200
72
6.46
7.90
S 69
50
65
10+10
230
72
6.46
7.89
43
Table 2.1.12 IN THE PRESENCE OF HEDP AND HEDTA

S. No
Sample
Number
CaCl2
(ml)
Na2CO3
(ml)
HEDP + HEDTA Temperature Digestion

Initial pH
(ml)
(oC)
Time (h)
S 70
50
60
10+10
60
10
6.71
8.10
S 71
50
60
10+10
100
72
6.71
8.24
S 72
50
60
10+10
130
72
6.71
8.44
S 73
50
60
10+10
200
72
6.71
8.51
S 74
50
60
10+10
230
72
6.71
8.45
Final pH
Table 2.1.13 IN THE PRESENCE OF NTA AND HEDTA

S. No
Sample
Number
CaCl2
(ml)
Na2CO3
(ml)
NTA + HEDTA Temperature Digestion

Initial pH
(ml)
(oC)
Time (h)
S 75
50
65
10+10
60
10
7.53
7.74
S 76
50
65
10+10
100
72
7.53
7.98
S 77
50
65
10+10
130
72
7.53
8.21
S 78
50
65
10+10
200
72
7.53
8.29
S 79
50
65
10+10
230
72
7.53
8.33
Final pH
44
Table 2.1.14 IN THE PRESENCE OF HEDP AND DTPA

S. No
Sample
Number
CaCl2
(ml)
Na2CO3
(ml)
HEDP + DTPA Temperature

(ml)
(oC)
Digestion
Initial pH
Time (h)
S 80
50
65
10+10
60
10
7.91
8.46
S 81
50
65
10+10
100
72
7.91
8.51
S 82
50
65
10+10
130
72
7.91
8.64
S 83
50
65
10+10
200
72
7.91
8.82
S 84
50
65
10+10
230
72
7.91
8.94
Initial
pH
Final pH
Final pH
Table 2.1.15 IN THE PRESENCE OF EDTA AND DTPA

S. No
Sample
Number
CaCl2
(ml)
Na2CO3
(ml)
EDTA + DTPA Temperature Digestion

(ml)
(oC)
Time (h)
S 85
50
70
10+10
60
10
7.87
8.09
S 86
50
70
10+10
100
72
7.87
8.24
S 87
50
70
10+10
130
72
7.87
8.54
S 88
50
70
10+10
200
72
7.87
8.69
S 89
50
70
10+10
230
72
7.87
8.72
45
Table 2.1.16 IN THE PRESENCE OF NTA AND DTPA

S. No
Sample
Number
CaCl2
(ml)
Na2CO3
(ml)
NTA + DTPA
(ml)
Temperature
(oC)
Digestion
Time (h)
Initial pH
Final pH
S 90
50
70
10+10
60
10
8.22
8.31
S 91
50
70
10+10
100
72
8.22
8.44
S 92
50
70
10+10
130
72
8.22
8.84
S 93
50
70
10+10
200
72
8.22
8.75
S 94
50
70
10+10
230
72
8.22
8.89
Table 2.1.17 IN THE PRESENCE OF HEDTA AND DTPA

S. No
Sample
Number
CaCl2
(ml)
Na2CO3
(ml)
HEDTA + DTPA Temperature Digestion

Initial pH
(ml)
(oC)
Time (h)
S 95
50
75
10+10
60
10
6.86
7.25
S 96
50
75
10+10
100
72
6.86
7.51
S 97
50
75
10+10
130
72
6.86
7.71
S 98
50
75
10+10
200
72
6.86
7.85
S 99
50
75
10+10
230
72
6.86
7.98
Final pH
46

Effect of Temperature and Sequestrants on Calcium Carbonate Precipitation

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Effect of Temperature and Sequestrants on Calcium Carbonate Precipitation

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Table 2.

1 DETAILS OF THE SAMPLES PREPARED

Table 2.1.2 IN THE PRESENCE OF EDTA

Table 2.1.3 IN THE PRESENCE OF NTA

Table 2.1.4 IN THE PRESENCE OF HEDTA

Table 2.1.5 IN THE PRESENCE OF DTPA

Table 2.1.6 IN THE PRESENCE OF HEDP (AQ-330)

HEDP(AQ-330) Temperature Digestion

Table 2.1.7 IN THE PRESENCE OF HEDP (AQ-330)

HEDP(AQ-330) Temperature Digestion

Table 2.1.8 IN THE PRESENCE OF EDTA AND HEDP

EDTA + HEDP Temperature Digestion

Table 2.1.9 IN PRESENCE OF EDTA AND NTA

EDTA + NTA Temperature

Table 2.1.10 IN THE PRESENCE OF HEDP AND NTA

Table 2.1.11 IN THE PRESENCE OF EDTA AND HEDTA

EDTA + HEDTA Temperature Digestion

Table 2.1.12 IN THE PRESENCE OF HEDP AND HEDTA

HEDP + HEDTA Temperature Digestion

Table 2.1.13 IN THE PRESENCE OF NTA AND HEDTA

NTA + HEDTA Temperature Digestion

Table 2.1.14 IN THE PRESENCE OF HEDP AND DTPA

HEDP + DTPA Temperature

Table 2.1.15 IN THE PRESENCE OF EDTA AND DTPA

EDTA + DTPA Temperature Digestion

Table 2.1.16 IN THE PRESENCE OF NTA AND DTPA

Table 2.1.17 IN THE PRESENCE OF HEDTA AND DTPA

HEDTA + DTPA Temperature Digestion

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