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Solutions To Chapter 6: Flow Through A Packed Bed of Particles Exercise 6.1
Solutions To Chapter 6: Flow Through A Packed Bed of Particles Exercise 6.1
(a) Calculate the voidage (volume fraction occupied by voids) of the bed.
(b) Calculate the pressure drop across the bed when the volume flow rate of liquid is
1.44 m3/h.
50
giving voidage, ε = 1 − = 0.5
2500 × 0.04 × 1
(b) With a liquid flow rate of 1.44 m3/h, the superficial liquid velocity through the
bed, U is given by:
1.44
U= = 0.01 m / s
3600 × A
Use the Ergun equation (Text-Equation 6.15) to estimate the pressure drop across the
bed at this flow rate:
Alternatively we could use the laminar part of the Ergun equation, which gives, (-Δp)
= 6000 Pa.
b) Calculate the superficial liquid velocity at which the frictional pressure drop across
the bed is 4130 Pa.
5
giving voidage, ε = 1 − π
= 0.4695
2000 × (0.1)2 × 0.6
4
Use the Ergun equation (Text-Equation 6.15) to estimate the relationship between
pressure drop across the bed and superficial liquid velocity:
(a) Calculate the diameter, xsv, of a sphere with the same surface-volume ratio as the
Raschig rings.
(d) Discuss how the pressure drop across the packing would vary with gas pressure
and temperature.
SB 190
Therefore, S = = = 655.2 m 2 / m 3
(1− ε) (1− 0.71)
If xsv is the diameter of a sphere with the same surface-volume ratio as the rings,
πx2sv 2 3
π 3 = 655.2 m / m
x
6 sv
Hence, xsv = 9.16 mm
Q 6
(b) Superficial gas velocity, U = 2 = = 1.91 m / s
D 22
π π
4 4
Using the Ergun equation (Text-Equation 6.15) to describe the relationship between
gas velocity and pressure drop across the packed bed,
With μ = 1.8 x 10-5 Pa.s, ρf = 1.2 kg/m3, xsv = 9.16 x 10-3 m and H = 5 m,
(c) We note that the turbulent component makes up 98% of the total. Hence, within
±10% of the quoted flow rate the pressure drop across the bed will increase with the
square of the superficial velocity and hence with the square of the flow rate:
(− Δp) ∝ Q2
1
ρf ∝
absolute temperature, T
1
Hence, (− Δp) ∝
T
EXERCISE 6.4: A solution of density 1100 kg/m3 and viscosity 2 x 10-3 Pas is
flowing under gravity at a rate of 0.24 kg/s through a bed of catalyst particles. The
bed diameter is 0.2 m and the depth is 0.5 m. The particles are cylindrical, with a
diameter of 1 mm and length of 2 mm. They are packed to give a voidage of 0.3.
Calculate the depth of liquid above the top of the bed. [Hint: apply the mechanical
energy equation between the bottom of the bed and the surface of the liquid]
π
Volume of one cylindrical particle = mm 3
2
2.5π
Surface-volume ratio of particles = = 5 mm2/mm3
π2
6
For a sphere of diameter xsv, surface-volume ratio =
x sv
Hence, diameter of sphere which has the same surface-volume ratio as the particles,
xsv = 1.2 mm
(− Δp) μU (1 − ε )2
= 150 2
H xsv ε 3
With μ = 0.002 Pa.s, ρf = 1100 kg/m3, xsv = 1.2 mm, ε = 0.3 and H = 0.5 m,
Expressed in terms of head of liquid, friction head loss through the bed, hloss =
13120
= 1.216 m
1100 × 9.81
Applying the mechanical energy balance between the liquid surface (position 1) and
the bottom of the packed bed (position 2): (Solution Manual-Figure 6.4.1)
U21 p U2 p
z1 + + 1 = z2 + 2 + 2 + h loss
2g ρ f g 2g ρ f g
The height of the packed bed is 0.5 m and so the depth of liquid above the bed is
0.716 m (1.216 - 0.5 m).
(− Δp) μU (1 − ε )2
= 150 2
H xsv ε 3
Referring to Chapter 7, the packed bed will fluidize when the buoyant weight of the
particles is supported. Using Text-Equation 7.2, the pressure drop at which this occurs
is:
Using the reduced Ergun equation, the superficial liquid velocity at which the packed
bed pressure drop is 3826 Pa is U = 4.25 x 10-4 m/s.
The Reynolds number is less than 10 and so our assumption that laminar flow
dominates is valid.
In summary then, the pressure drop increases linearly with liquid flow rate up to a
pressure drop of 3826 Pa at a superficial liquid velocity of 4.25 x 10-4 m/s. Beyond
this velocity the pressure drop will remain essentially constant with increasing liquid
flow rate, since the bed is fluidized (see Chapter 7).
(− Δp) μU (1 − ε )2 ρf U2 (1 − ε )
= 150 2 + 1.75
H xsv ε 3 xsv ε3
With μ = 2.0 x 10-5 Pa.s, ρf = 30 kg/m3, xsv = 1.46 x 10-3 m, (− Δp) =68.75 kPa
and ε = 0.25,
68.75 × 103 6 2
which gives = 50666U + 1.726 × 10 U
H
11320
Gas volumetric flowrate, Q = UA = = 3.144 m3 / s
3600
Substituting gives:
0.681H 2 + 21.467H3 = 1.0
Calculate:
(a) the time required to collect 1200 litre of filtrate at a constant pressure drop of 400
kPa with the same feed slurry.
(b) the time required to wash the resulting filter cake with 500 litre of water (same
properties as the filtrate) at a pressure drop of 200 kPa.
r φμ
and an intercept 2 c Veq on the t/V axis.
A (−Δp)
r c φμ
hence, = 4625
2A (− Δp)
2
r c φμ
and Veq = 800
A (−Δp)
2
t 9.25 × 10 9
= (0.5V + 0.0865)
V 4(−Δp )
which applies to the filtration of the same slurry in the same filter at any pressure
drop.
(a) To calculate the time required to pass 1200 litre (1.2 m3) of filtrate at a pressure
drop of 400 kPa, we substitute V = 1.2 m3 and (-Δp) = 400 x 103 Pa in the above
equation, giving: t = 4763 sec (or 79.4 minutes)
(b) During the filtration the cake thickness is continuously increasing and, since the
pressure drop is constant, the volume flow rate of filtrate will continuously decrease.
The filtration rate is given by Text-Equation 6.26.
1 dV
=
(− Δp)A
A dt rc μ(V + Veq )φ
Substituting the volume of filtrate passed at the end of the filtration period (V = 1.2
m3), r c φμ = 9.25 × 109 Pas/m2, Veq = 0.0865 m3 and (-Δp) = 400 x 103 Pa, we find
dV −4 3
the filtration rate at the end of the filtration period is = 1.34 × 10 m /s
dt
⎛ 200 × 10 3 ⎞
flowrate of wash water (at 200 kPa) = 1.34 × 10 −4 × ⎜ 3 ⎟ = 6.7 × 10
−5 3
m /s
⎝ 400 × 10 ⎠
Hence, the time needed to pass 0.5 m3 of wash water at this rate is 7462 sec (or 124.3
minutes)
EXERCISE 6.8: A laboratory leaf filter has an area of 0.1 m2, operates at a
constant pressure drop of 400 kPa and produces the following results during a test on
filtration of a slurry:
Volume of filtrate 19 31 41 49 56 63
collected (litre)
Time (sec) 300 600 900 1200 1500 1800
(a) Calculatethe time required to collect 1.5 m3 of filtrate during filtration of the same
slurry at a constant pressure drop of 300 kPa on a similar full-scale filter with and
area of 2 m2.
(b) Calculate the rate of passage of filtrate at the end of the filtration in part (a).
(c) Calculate the time required to wash the resulting filter cake with 0.5 m3 of water
at a constant pressure drop of 200 kPa.
Assume the cake is incompressible and that the flow properties of the filtrate are the
same as those of the wash solution.)
r c φμ
hence, = 2.904 x 105
2A (− Δp)
2
r c φμ
and Veq = 10300
A (−Δp)
2
t 2.323 × 10 9
= (0.5V + 0.0177)
V 4(−Δp )
which applies to the full-scale filter (area 2 m2) using the same slurry at any pressure
drop.
(a) To calculate the time required to pass 1.5 m3 of filtrate through the full-scale filter
at a pressure drop of 300 kPa, we substitute V = 1.5 m3 and (-Δp) = 300 x 103 Pa in
the above equation, giving: t = 2229 sec (or 37.1 minutes)
(b) During the filtration the cake thickness is continuously increasing and, since the
pressure drop is constant, the volume flow rate of filtrate will continuously decrease.
The filtration rate is given by Text-Equation 6.26.
1 dV
=
(− Δp)A
A dt rc μ(V + Veq )φ
Substituting the volume of filtrate passed at the end of the filtration period (V = 1.5
m3), r c φμ = 2.323 × 109 Pas/m2, Veq = 0.0177 m3 and (-Δp) = 300 x 103 Pa, we find
dV −4 3
the filtration rate at the end of the filtration period is = 3.40 × 10 m /s
dt
EXERCISE 6.9: A leaf filter has an area of 1.73 m2, operates at a constant
pressure drop of 300 kPa and produces the following results during a test on filtration
of a slurry:
Assuming that the cake is incompressible and that the flow properties of the filtrate
are the same as those of the wash solution, calculate:
(a) the time required to collect 1 m3 of filtrate during filtration of the same slurry at a
constant pressure drop of 400 kPa.
(c) the time required to wash the resulting filter cake with 0.8 m3 of water at a
constant pressure drop of 250 kPa.
r c φμ
hence, = 2960
2A (− Δp)
2
r c φμ
and Veq = 1000
A (−Δp)
2
t 5.32 × 109
= (0.5V + 0.169)
V 1.732 (−Δp)
which applies to the filtration of the same slurry in the same filter at any pressure
drop.
(a) To calculate the time required to pass 1.0 m3 of filtrate at a pressure drop of 400
kPa, we substitute V = 1.0 m3 and (-Δp) = 400 x 103 Pa in the above equation, giving:
t = 2973 sec (or 49.5 minutes)
(b) During the filtration the cake thickness is continuously increasing and, since the
pressure drop is constant, the volume flow rate of filtrate will continuously decrease.
The filtration rate is given by Text-Equation 6.26.
1 dV
=
(− Δp)A
A dt rc μ(V + Veq )φ
Substituting the volume of filtrate passed at the end of the filtration period (V = 1.0
m3), r c φμ = 5.32 × 109 Pas/m2, Veq = 0.169 m3 and (-Δp) = 400 x 103 Pa, we find
dV −4 3
the filtration rate at the end of the filtration period is = 1.923 × 10 m /s
dt