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Heat Treating

Metallurgical ‘Fine Points’ of


Induction Hardening
Valery Rudnev, Inductoheat Group, Madison Heights, Mich.

Certain metallurgical phenomena and principles of heat treatment fre-


quently are incorrectly assumed or improperly used in the application
of induction hardening.

ardening of steels and cast distribution in induction surface hardening for surface hardening. After 4.1 seconds of
irons represents the most is controlled by selection of frequency, time, heating, the surface layer reaches a final
popular application of induc- power and workpiece/coil geometry [1]. temperature of approximately 1050˚C
tion heat treatment (Fig. 1). Hardening of steels and cast iron compo- (1920˚F). The core temperature does not
Induction hardening is a complex combina- nents may be done for the purpose of rise significantly due to several factors, such
tion of electromagnetic, heat transfer, and obtaining certain properties including, but as an electromagnetic skin effect and rela-
metallurgical phenomena [1]. Due to the not limited to, strength, fatigue and wear tively short heating time. Because of these
physics of electromagnetic induction, heat- resistance. The traditional description of factors, the heat soak from the surface
ing can be localized to areas where metal- the steel hardening procedure involves toward the core is not sufficient to equalize
lurgical changes are desired. The three most heating the entire component, or a part of temperature along the radius.
common forms of induction hardening are the component that needs to be hardened, After the heating stage is completed, the
surface hardening, through hardening, and to the austenitizing temperature, holding it quenching stage begins. The high tempera-
selective hardening. Depending on the spe- if necessary for a period long enough to ture of the workpiece surface layer begins to
cific application, selective hardening is achieve complete transformation to austen- decrease in the first stage of quenching.
sometimes considered a part of surface hard- ite, and then rapidly cooling it below the Figure 2 shows that after 2 seconds of
ening or through hardening. martensite start (Ms) temperature, where quenching, the surface temperature is
The first step in designing an induction- martensite transformation begins. reduced by as much as 450˚C (810˚F),
hardening machine is to specify the required For example, Fig. 2 shows the dynamics resulting in a workpiece surface temperature
hardness pattern including surface hardness, of the induction heating of a carbon steel of 600˚C (1110˚F). At this point, the maxi-
case depth and transition zone. Temperature cylinder and its cooling during quenching mum temperature is located at a distance of
3 mm (0.120 in.) below the surface. After 5
seconds of quenching, the surface tempera-
ture decreases almost to the temperature of

Core Surface

1200
4.1 Sec.
1000
3.2 Sec.
Temperature, ˚C

800 1 Sec.
Quenching

1.8 Sec.
600 1.5 Sec.
400
2 Sec.
200

0 6 Sec.
0 2 4 6 8 10
Radius, mm

Fig. 2. Dynamics of induction heating of a car-


bon steel cylinder (20 mm OD) and its cool-
ing during quenching (F = 40 kHz) [1]; red is
Fig. 1. Dual shaft induction scanner heating and blue is cooling.

IndustrialHeating.com – March 2005 1


Heat Treating

1200 2192˚F 1100


E
Austenite Annealed steel
910˚C 2012˚F
1100 (γ-Fe) Austenite 1050
1670˚F
A''3 (γ-Fe) Normalied steel
1000 Acm 1832˚F
G 1000 Quenched and tempered

Temperature, ˚C
v''>v'>v'
900 1652˚F
A'cm
Austenite (γ-Fe)
Temperature, ˚C

950
+ Cementite (Fe3C) 1472˚F
800 Austenite
Ferrite
A1 723˚C (1333˚F) 900
700 P 1292˚F
S

Eutectoid
Perlite

Ferrite 600 Ferrite (α-Fe) Cementite (Fe3C) 1112˚F 850


(α-Fe) + Perlite + Perlite

500 932˚F 800


0 0.2 0.4 0.6 0.8 1.0 1.2 1.4 1.6 1.8 2.0
100 1000
Carbon content, weight % Rate of heating, ˚C/sec

Fig. 3. Lower left portion of the iron-iron carbide equilibrium phase trans- Fig. 4. Effect of initial microstructure and heating rate on A3 crit-
formation diagram ical temperature for AISI type 1042 steel [3,4]

the quenchant, while the core still remains the effect of heating the metal to elevated composition and the heating/cooling rate.
quite warm at a temperature above 400˚C temperatures or metal cooling that causes a The greater the rate of heating/cooling, the
(750˚F). transformation in its crystalline structure. It greater will be the difference between the Ac
In some cases, heat treaters do not cool is also used to determine the range of tem- and Ar temperatures.
the part completely, and after unloading the peratures in which certain types of heat Induction hardening is a very fast
part from the induction coil, it is kept for treatment of the steel may be carried out. process. Heat intensity often exceeds a mag-
some time on the shop floor. During that Often, heat treat practitioners use this dia- nitude of 100˚C/sec (180˚F/sec), and in
time, the heat of the warm core travels gram to determine hardening temperatures. some cases reaches 900˚C/sec (1620˚F/sec)
toward the surface, eventually resulting in a However, it is important to be aware that and even higher. Therefore, the process of
uniform temperature distribution within the this diagram might be misleading in majori- phase transformation cannot be considered
part. In this case, the remaining heat is used ty of induction hardening applications as equilibrium, and the phenomenon of
for a slight temper back (self-tempering), because it is valid only for the equilibrium thermal hysteresis is always pronounced.
which imparts some ductility to the part. condition of plain carbon steel at a pressure Fast heating drastically affects the kinet-
At first glance, this operation is very of one atmosphere. The existence of non- ics of the austenite formation, shifting it
straightforward. However, in many cases, equilibrium conditions, appreciable toward higher temperatures to create suffi-
certain metallurgical phenomena and prin- amounts of alloying elements, pressure cient conditions for the required diffusion-
ciples of heat treatment frequently are other than atmospheric and certain prior based processes [2]. Figure 4 shows the effect
incorrectly assumed or improperly used in treatment can significantly shift the critical of the heating rate on the Ac3 critical tem-
induction hardening. It is important to look temperatures. peratures of steel [3, 4]. The inability of the
closer at the “fine points” of metallurgical One of the major requirements of an classical Fe-Fe3C diagram to take into con-
theory to ensure optimal results. Following equilibrium condition is sufficiently slow sideration heating intensity noticeably lim-
are some examples that illustrate this. heating. Ideally, for sufficiently slow heat- its its use to predict required temperatures in
ing/cooling, transformation temperatures induction hardening applications.
Can you directly apply the iron-iron should be approximately the same in heat- The microstructure of steel prior to heat
carbide (Fe-Fe3C) equilibrium phase- ing as well as in cooling resulting in no treatment (sometimes referred to as initial
transformation diagram to induction appreciable difference between the Ac and structure, structure of the parent material,
hardening of steel? Ar critical temperatures. However, from a and structure of the “green” part) also has a
When iron is alloyed with a different per- practical standpoint, the equilibrium condi- pronounced effect on the results of the heat
cent of carbon, the critical temperatures tion simply does not exist in induction treatment and required process parameters.
often are determined based on the Fe-Fe3C hardening. This includes, but is not limited to, the
diagram. Figure 3 shows the lower left-hand The Ac temperatures are always higher austenitizing temperature and the time
part of this diagram representing the heat than Ar temperatures. The difference required to hold at that temperature.
treatment of steels. This widely used dia- between Ac and Ar temperatures represents As can be seen from Fig. 4, even for
gram represents a graph of temperature ver- a thermal hysteresis, which is a function of induction hardening of AISI 1042 plain car-
sus carbon content of the steel and shows several factors including the metal chemical bon steel, depending on the heat intensity

2 March 2005 – IndustrialHeating.com


0mm 0.5mm 1mm 1.5mm 2mm 2.5mm 800
70 Eutectoid temperature
γ––> Pearlite
700
60 Quenched and Coarse pearlite
tempered Transformation
600 ends
50
Fine pearlite
Hardness, HRC

α + Fe3C

Temperature, ˚C
500

<–– Hardness
Normalized
40
Upper bainite
400 γ––> Bainite
30
Transformation
begins Low bainite
20 Annealed 300 50%
Ms
10 200

0 100
0 0.02 0.04 0.06 0.08 0.1 M90% M50% γ––> Martensite
Distance below surface, in. 0
Surface 1 10 100 10000 10000
Time, sec.
Fig. 5. Effect of initial microstructure in AISI type 1070 steel bars on
response to surface hardening using 450-kHz induction generator Fig. 6. Time-temperature isothermal transformation diagram for AISI
operated at a power density of 2.5 kW/cm2 (16 kW/in.2) [5] type 1020 plain carbon steel, austenitized at 900˚C; grain size: 6 [3,7]

and structure prior to induction hardening, the ferrite. The ferrite clusters or bands can Can time-temperature-transformation
the required hardening temperatures range function as one large ferrite grain and often (TTT) and continuous-cooling-trans-
from 1620 to 2000˚F (880 to 1095˚C) for will be retained in the austenite upon fast formation (CCT) diagrams be directly
annealed prior microstructures, 1550 to heat up [1]. After quenching, a complex fer- applied in induction hardening?
1830˚F (840 to 1000˚C) for normalized ritic-martensitic microstructure can be TTT and CCT diagrams are widely used in
prior microstructures and 1510 to 1710˚F formed. Scattered soft and hard spots and the heat treat industry to determine the end
(820 to 930˚C for quenched and tempered poor mechanical properties characterize products of austenite transformation when
microstructures. this structure. Appreciably higher tempera- steel is cooled below the A1 critical temper-
A quenched and tempered microstruc- tures and longer heat times are required to ature (Figs. 6 and 7). The nomenclature
ture is the most favorable prior microstruc- austenitize those structures. It is strongly used on these diagrams to represent a par-
ture [1] followed by a normalized structure recommended to avoid the segregated and ticular structure is: A = austenite, F = fer-
consisting of fine pearlite, which provides banded initial microstructures of “green” rite, P = pearlite, B = bainite and M =
rapid transformation allowing one to reduce parts. martensite. Double letters are sometimes
the required temperature for austenite for- Steels containing large stable carbides used to emphasize a certain feature of a par-
mation. This results in fast and consistent (i.e., spheroidized microstructures) also ticular structure. For example, CP = coarse
metal response to induction hardening with have poor response to induction hardening, pearlite, FP = fine pearlite, UB = upper bai-
a minimum amount of grain growth, the and require prolonged heating and higher nite and LB = lower bainite.
smallest shape/size distortion, surface oxida- temperatures to complete austenitization. Time is plotted on the x axis (a logarith-
tion, minimum required heating energy and Longer heating time leads to grain growth, mic scale) versus temperature on the y axis
well-defined (crisp) hardness pattern with a the appearance of coarse martensite forma- (Fig. 6). A distinguishing feature of TTT
short transition zone (Fig. 5). This type of tion, an extended transition zone, surface diagrams is the presence of two S-shaped
initial structure can also result in higher oxidation/decarburization and increased curves (sometimes referred to as C-shaped
hardness and deeper hardened case depth shape distortion. Coarse martensite has a curves). The left solid curve represents the
compared with other structures. negative effect on such important proper- beginning (the start) of the transformation
An initial steel microstructure contain- ties as toughness, impact strength and process and the right solid curve designates
ing a significant amount of coarse pearlite bending fatigue strength, and is susceptible the end of the isothermal transformation.
and, most importantly, coarse ferrite or to cracking. Often TTT diagrams show a curve between
clusters or bands of ferrite, is considered to Thus, when determining the appropriate the transformation start and end curves
have an unfavorable structure. Ferrite is induction hardening temperatures for a car- that represents the completion of 50% of
practically a pure iron and contains an bon steel component, it is imperative to the transformation of the austenite.
insufficient amount (less than 0.025%) of remember the limitations of the equilibrium Because there is no representation of car-
carbon required for the martensite transfor- Fe-Fe3C phase transformation diagram and bon content or combination of alloying
mation. Large areas (clusters or bands) of to take into account the specifics of the elements for the steel under consideration,
ferrite require a long time for carbon to be process including the heat intensity and a different chart is required for each chem-
able to diffuse into the carbon-poor area of microstructure of the green part. ical composition to be analyzed.

IndustrialHeating.com – March 2005 3


Heat Treating

CCT diagrams allow prediction of the 1600


final microstructure of the steel taking into Ac1 800˚C
account the continuous nature of the 1400
13% F 15% F
process during cooling of austenite. CCT 700˚C
1200 35% F
diagrams are typically slightly shifted to F
5% F 600˚C
lower temperatures and longer times com-

Temperature, ˚F
P 65% F
pared with TTT diagrams. Although TTT 1000
85% F 500˚C
(isothermal transformation) and CCT dia- 10% B
B 15% F
grams are helpful, it is important to remem- 800
F - Ferrite 400˚C
ber that there are several limitations when P - Pearlite
trying to apply the diagrams to induction 600 B- Bainite
300˚C
M - Mart.
hardening. M
Both TTT and the CCT diagrams were 400 70% B 200˚C
developed assuming homogeneous austen- Hardness ––> C60 C58 C31 C24 B96
200 100˚C
ite, which is not always the case in induc-
100 101 102 103 104 105
tion hardening. Inhomogeneous austenite
Cooling time, sec.
means there is a nonuniform distribution of
carbon. Therefore, cooling of high and low Fig. 7. Continuous cooling transformation (CCT) diagram for AISI type 15B41 steel (0.42%C,
carbon concentration areas of inhomoge- 1.61% Mn, 0.29% Si, 0.006% P, 0.019% S, 0.004% B), grain size: 7-8 [8]
neous austenite would be represented by dif-
ferent CCT curves having different critical
cooling curves. TTT diagrams assume an
isothermal process where the steel compo-
nent upon cooling is held at a fixed temper-
ature below the A1 critical temperature,
which is never the case in induction hard-
ening. While CCT diagrams take into con-
sideration continuous cooling during
quenching, the cooling curve assumes a
constant cooling rate, which is often not a
valid assumption, particularly in induction
scan hardening applications. Fig. 8. Typical machined scanning inductor with integral quench (left) and cross section of a
In addition the samples used to develop single turn scan coil showing quench chamber and coil cooling chamber (right)
these diagrams had small cross sections.
Therefore, there will be some inherent
errors in trying to apply the curves to mod- during quenching. than many small impingements. The
erate or large sized components, as well as Therefore, while TTT and CCT dia- quench holes are typically placed facing
complex-shaped parts. Components having grams are useful in helping the heat treater the heated component at 0.1875 to 0.250
a different surface area-to-volume ratio have to understand the basic phenomena and in. (~5 to 6 mm) intervals and have a stag-
different cooling characteristics. principles of heat treatment, it is important gered pattern. The orifice size is related to
In induction hardening, the heat to be aware of its inherent limitations when the specifics of quenching requirements
exchange process between the surface of the applying to induction hardening. including coil-to-workpiece geometry, air
heated component and the quenchant is a gap between the quench block and the
function, among other factors, of the surface Are there any peculiarities in workpiece surface, quench concentration
temperature, which is not constant. In addi- quenching techniques used in induc- and required flow, etc. In some cases, the
tion, the workpiece temperature (austenitiz- tion hardening? quench is built into the coil (Fig. 8), while
ing temperature) prior to applying quen- Spray quenching is typically used in induc- a barrel or quench block is separate from
chant is typically not the same as assumed tion hardening applications. Spray the coil in other cases.
in the CCT diagrams. In addition, the tem- quenching works best if the component is The intensity of spray quenching
perature distribution prior to quenching is rotated during the quenching operation, depends on the flow rate; the angle at which
nonuniform. The existence of a cold core which ensures uniformity in quenching. By the quenchant strikes the workpiece sur-
that functions as a heat sink has a marked rotating symmetrical parts, the workpiece face; and temperature, purity and type of
effect on the severity of the cooling rate simulates a constant impingement rather quenchant. Different types of quenchants

4 March 2005 – IndustrialHeating.com


used include water, polymer-based media References 6. Krauss, G., Steels: Heat Treatment and
and, to lesser extent, oil and forced air. 1. Rudnev, V., Loveless, D., et al., Handbook of Processing Principles, ASM Intl., 1999
The classical cooling curves widely pub- Induction Heating, Marcel Dekker, 2003 7. Golovin, G. and Zamjatin, M., High-Frequency
2. Rudnev, V. Can the Fe-Fe3C phase transforma- Induction Heat Treating, Mashinostroenie, St.
lished in the literature representing three
tion diagram be directly applied in induction Petersburg, Russia, 1990
stages of quenching; that is, the vapor blan-
ket (A-stage), nucleate boiling (B-stage) hardening of steel, Professor Induction Series, Additional fine points of induction heating
and convective cooling (C-stage), cannot Heat Treating Prog., ASM Intl., June/July, 2003 treating will be discussed in Part 2 of this article
be applied directly with spray quenching. 3. Semiatin, S. and Stutz, D., Induction Heat in the May 2005 issue of IH.
Due to the nature of spray quenching, the Treatment of Steel, ASM Intl., 1986 For more information: Valery Rudnev is Group
first two stages are greatly suppressed in 4. Feuerstein,W. and Smith,W., Trans. ASM, 46, Director, Science & Technology, Inductoheat
time. At the same time, cooling during the 1270, 1954 Group, Inductoheat Inc., 32251 N. Avis Dr.,
convection stage is more intense with spray 5. Brooks, C., Principles of the Heat Treatment Madison Heights, MI 48071; tel: 248-585-9393; fax:
quenching plus rotation of the component of Plain Carbon and Low Alloy Steels, ASM 248-589-1062; e-mail: rudnev@indctoheat.com;
than represented by classical cooling curves. Intl., 1996 Web: www.inductoheat.com
The differences are of both a quantita-
tive and qualitative nature. This includes,
Additional related information may be found by searching for these (and other) key words/terms
but is not limited to, specifics of film forma-
via BNP Media LINX at www.industrialheating.com: induction hardening, surface hardening, selec-
tion and heat transfer through the vapor
tive hardening, induction coil, coil geometry, induction heating, equilibrium phase diagram, critical
blanket during the initial stage of quench- temperatures, prior microstructure, TTT diagram, CCT diagram, spray quench, self quench, mass
ing, as well as kinetics of formation, growth quench, self tempering.
and removal of bubbles from the surface of
the heated component during the nucleate
boiling stage [7]. The film thickness of the
vapor blanket during the A-stage of
quenching is typically much thinner with
spray quenching than that obtained with
quenching in a tank, and depends on flow
rate, impingement angle and other charac-

1
teristics of a spray quenching system.
Transition between the A-stage and B-
stage of quenching is smoother with spray
quenching than shown on classical cooling
curves for quenching in the tank. During

⁄3
nucleate boiling, bubbles are a smaller size
because they do not have sufficient time to
grow. Much larger numbers of bubbles are
formed during spray quenching and the
intensity with which they remove heat from
the surface of the component is substantial-
ly greater compared with bulk (tank)
quenching. This is one of the most impor-
tant factors responsible for more intensive
quench severity of spray quenching.
In some surface hardening applications
requiring shallower case depths, self-

Squar
quenching is used. In some cases, the effect
of thermal conduction away from the sur-
face by the cold core provides sufficient
cooling to miss the nose of the continuous
cooling curve. This self-quenching tech-
nique (also known as mass quenching)
allows the elimination of using liquid quen-
chants to achieve a shallow case. IH
Info # xx or www.IHadinfo.cc
IndustrialHeating.com – March 2005 5

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