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  • Perhitungan Destilasi

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    Mirawati Suripto Riders
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    The document describes calculations to determine: 1) The volume of ethanol solutions of varying concentrations (20%, 23%, 26%, 42%) 2) The density of each ethanol solution 3) The mass of ethanol (Xe) in each solution 4) Results from three distillation runs including mass of condensate and residue collected 5) Mass balances for each distillation run to calculate mass losses The calculations involve determining volumes and densities of ethanol solutions and using these values along with masses measured to find the mass of ethanol in each solution and collected in distillation experiments. Mass balances on the distillation runs quantify any mass losses during the processes.

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    lampiran b

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    The document describes calculations to determine: 1) The volume of ethanol solutions of varying concentrations (20%, 23%, 26%, 42%) 2) The density of each ethanol solution 3) The mass of ethanol (Xe) in each solution 4) Results from three distillation runs including mass of condensate and residue collected 5) Mass balances for each distillation run to calculate mass losses The calculations involve determining volumes and densities of ethanol solutions and using these values along with masses measured to find the mass of ethanol in each solution and collected in distillation experiments. Mass balances on the distillation runs quantify any mass losses during the processes.

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    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
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    11 views7 pages

    Perhitungan Destilasi

    Uploaded by

    Mirawati Suripto Riders
    The document describes calculations to determine: 1) The volume of ethanol solutions of varying concentrations (20%, 23%, 26%, 42%) 2) The density of each ethanol solution 3) The mass of ethanol (Xe) in each solution 4) Results from three distillation runs including mass of condensate and residue collected 5) Mass balances for each distillation run to calculate mass losses The calculations involve determining volumes and densities of ethanol solutions and using these values along with masses measured to find the mass of ethanol in each solution and collected in distillation experiments. Mass balances on the distillation runs quantify any mass losses during the processes.

    Copyright:

    © All Rights Reserved
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    of 7

    LAMPIRAN B

    PERHITUNGAN

    B.1 Menghitung Volume Etanol


    B.1.1 Menghitung Volume Etanol : Volume aquades (50 ml)
    a. Untuk Etanol 20%
    % Etanol murni . V1 = % etanol encer . V2
    0,96 × V1 = 20 % × 50 ml
    0,96 × V1 = 10 ml

    V1 = ,

    V1 = 10,50 ml
    b. Untuk Etanol 23%
    % Etanol murni . V1 = % etanol encer . V2
    0,96 × V1 = 23 % × 50 ml
    0,96 × V1 = 11,5 ml
    ,
    V1 = ,

    V1 = 12 ml
    c. Untuk Etanol 26%
    % Etanol murni . V1 = % etanol encer . V2
    0,96 × V1 = 26 % × 50 ml
    0,96 × V1 = 13 ml

    V1 = ,

    V1 = 14 ml
    B.1.2 Menghitung Volume Etanol : Volume aquades (500 ml)
    Untuk Etanol 42%
    % Etanol murni . V1 = % etanol encer . V2
    0,96 × V1 = 42 % × 50 ml
    0,96 × V1 = 210 ml

    V1 = ,

    V1 = 219 ml
    B.2 Menghitung Densitas Etanol ( )
    Diketahui : Massa picnometer kosong = 14,44 gr
    Volume picnometer = 5 ml
    a. Untuk Etanol 20%
    Dik : Picnometer berisi etanol = 20,48 gr
    Massa etanol 20% = (picnometer + etanol) – (picnometer kosong)
    = 20,48 gr – 14,44 gr
    = 6,04 gr
    =
    ,
    =

    = 1,208 gr/ml
    b. Untuk Etanol 23%
    Dik : Picnometer berisi etanol = 20,41 gr
    Massa etanol 20% = (picnometer + etanol) – (picnometer kosong)
    = 20,41 gr – 14,44 gr
    = 5,97 gr
    =
    ,
    =

    = 1,194 gr/ml
    c. Untuk Etanol 26%
    Dik : Picnometer berisi etanol = 20,08 gr
    Massa etanol 20% = (picnometer + etanol) – (picnometer kosong)
    = 20,08 gr – 14,44 gr
    = 5,64 gr
    =
    ,
    =

    = 1,128 gr/ml
    d. Untuk Etanol 42%
    Dik : Picnometer berisi etanol = 20,37 gr
    Massa etanol 20% = (picnometer + etanol) – (picnometer kosong)
    = 20,37 gr – 14,44 gr
    = 5,93 gr
    =
    ,
    =

    = 1,186 gr/ml

    B.3 Menghitung Xe
    a. Untuk Etanol 20%
    Dik : = 1,208 gr/ml
    V = 10,5 ml
    ( . . )
    Xe = ( . . ) ( )

    ( , / × , )× . )
    = ( , / × , × . ) ( . )( / )
    ,
    =( , , )
    = 6,03× 10

    b. Untuk Etanol 23%


    Dik : = 1,194 gr/ml
    V = 12 ml
    ( . . )
    Xe = ( . . ) ( )

    ( , / × )× . )
    = ( , / × × . ) ( )( / )
    ,
    =( , )
    = 7,97× 10

    c. Untuk Etanol 26%


    Dik : = 1,128 gr/ml
    V = 14 ml
    ( . . )
    Xe = ( . . ) ( )

    ( , / × )× . )
    = ( , / × × . ) ( )( / )
    ,
    =( , )
    = 10,23× 10
    B.4 Menghitung Xe umpan sebanyak 500 ml untuk Etanol 42%
    Dik : = 1,186 gr/ml
    V = 219 ml
    ( . . )
    Xe = ( . . ) ( )

    ( , / × )× . )
    = ( , / × × . ) ( )( / )
    ,
    =( , )
    = 6,37× 10

    Massa labu kosong 500 ml = 184 gr


    Erlenmeyer kosong 250 ml = 104,98 gr
    Baker glass kosong 500 ml = 214, 96 gr
    Picnometer kosong 5 ml = 14,44 gr
    Massa labu 500 ml + etanol 42% = 734 gr
    Massa umpan = 734-184 = 550 gr

    Run I (45 menit)

    Massa erlenmeyer + kondensat = 238,69 gr


    Massa picnometer 5 ml + kondensat = 19,34 gr
    Massa baker glass 500 ml + refluks = 550 gr
    Massa picnometer 5 ml + refluks = 19,3 gr
    Massa kondensat = (erlenmeyer + kondensat) – (erlenmeyer kosong)
    = 238,69 gr – 104,98 gr
    = 133,71 gr
    Massa picnometer kondensat = (picnometer + kondensat) – (picnometer kosong)
    = 19,34 gr – 14,44 gr
    = 4,9 gr
    Massa refluks = (baker glass + refluks) – (baker glass kosong)
    = 550 gr – 214, 96 gr
    = 385,04 gr
    Massa picnometer refluks = (picnometer + refluks) – (picnometer kosong)
    = 19,3 gr – 14,44 gr
    = 4,86 gr
    ρ =
    ,
    =

    = 0,98 gr/ml
    ρ =
    ,
    =

    = 0,972 gr/ml
    Kondensat yang didapat adalah 138,61 gr

    Run II (60 menit)

    Massa Erlenmeyer + kondensat = 249,2 gr


    Massa picnometer 5 ml + kondensat = 19,31 gr
    Massa baker glass 500 ml + refluks = 525 gr
    Massa picnometer 5 ml + refluks = 19,34 gr
    Massa kondensat = (erlenmeyer + kondensat) – (erlenmeyer kosong)
    = 249,2 gr – 104,98 gr
    = 144,22 gr
    Massa picnometer kondensat = (picnometer + kondensat) – (picnometer kosong)
    = 19,31 gr – 14,44 gr
    = 4,87 gr
    Massa refluks = (baker glass + refluks) – (baker glass kosong)
    = 525 gr gr – 214, 96 gr
    = 310,04 gr
    Massa picnometer refluks = (picnometer + refluks) – (picnometer kosong)
    = 19,34 gr – 14,44 gr
    = 4,9 gr
    ρ =
    ,
    =

    = 0,972 gr/ml
    ρ =
    ,
    =

    = 0,98 gr/ml
    Kondensat yang didapat adalah 149,09 gr

    Run III (75 menit)

    Massa erlenmeyer + kondensat = 260 gr


    Massa picnometer 5 ml + kondensat = 19,28 gr
    Massa baker glass 500 ml + refluks = 510 gr
    Massa picnometer 5 ml + refluks = 19,4 gr
    Massa kondensat = (erlenmeyer + kondensat) – (erlenmeyer kosong)
    = 260 gr –104, 98 gr
    = 155,02 gr
    Massa picnometer kondensat = (picnometer + kondensat) – (picnometer kosong)
    = 19,28 gr – 14,44 gr
    = 4,84 gr
    Massa refluks = (baker glass + refluks) – (baker glass kosong)
    = 510 gr gr – 214, 96 gr
    = 295,04 gr
    Massa picnometer refluks = (picnometer + refluks) – (picnometer kosong)
    = 19,4 gr – 14,44 gr
    = 4,96 gr
    ρ =
    ,
    =

    = 0,96 gr/ml
    ρ =
    ,
    =

    = 0,992 gr/ml
    Kondensat yang didapat adalah 159,86 gr
    B.5 Menghitung Neraca Massa
    Run I
    Neraca massa total, A = B + C
    550 gr = 138,61 gr + 389,9 gr
    Berarti kehilangan massa pada proses ini sebanyak 21,49 gr
    Run II
    Neraca massa total, A = B + C
    528,51 gr = 149,09 gr + 314,94 gr
    Berarti kehilangan massa pada proses ini sebanyak 64,48 gr
    Run I
    Neraca massa total, A = B + C
    464,03 gr = 159,86 gr + 300 gr
    Berarti kehilangan massa pada proses ini sebanyak 4,17 gr

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