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  • Lampiran B Perhitungan: Asam Asetat

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    This document contains calculations for an experiment producing ethyl acetate. It provides the densities, volumes, and molecular weights used to calculate the moles and masses of acetic acid, ethanol, and ethyl acetate involved. It then shows the percent yield calculation comparing the experimental volume of ethyl acetate produced to the theoretical stoichiometric volume. An appendix documents the experimental procedure with photos of the equipment, mixing, reflux, distillation, washing, and final product. The calculations show a 50.57% yield was obtained.

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    This document contains calculations for an experiment producing ethyl acetate. It provides the densities, volumes, and molecular weights used to calculate the moles and masses of acetic acid, ethanol, and ethyl acetate involved. It then shows the percent yield calculation comparing the experimental volume of ethyl acetate produced to the theoretical stoichiometric volume. An appendix documents the experimental procedure with photos of the equipment, mixing, reflux, distillation, washing, and final product. The calculations show a 50.57% yield was obtained.

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    © All Rights Reserved
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    15 views4 pages

    Lampiran B Perhitungan: Asam Asetat

    Uploaded by

    Thur
    This document contains calculations for an experiment producing ethyl acetate. It provides the densities, volumes, and molecular weights used to calculate the moles and masses of acetic acid, ethanol, and ethyl acetate involved. It then shows the percent yield calculation comparing the experimental volume of ethyl acetate produced to the theoretical stoichiometric volume. An appendix documents the experimental procedure with photos of the equipment, mixing, reflux, distillation, washing, and final product. The calculations show a 50.57% yield was obtained.

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    © All Rights Reserved
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    of 4

    LAMPIRAN B

    PERHITUNGAN

    Asam Asetat

    ρasam asetat = 1,058 gram/ml


    Volume asam asetat = 17 ml
    Mr asam asetat = 60

    ρ = ,m-V.
    m =Vxρ
    = 17 ml x 1,058 gram/ml
    = 17,986 gram

    n = = = 0,3 mmol

    Etanol
    ρetanol = 0,789 gram/ml
    Volume etanol = 47 ml
    Mr etanol = 46
    ρ =,m-V.
    m = V xρ
    = 47 ml x0,789 gram/ml
    = 37,083 gram

    n = = = 0,8 mmol

    Densitas Etil Asetat


    Piknometer kosong = 15,31 gram
    Piknometer berisi etil asetat = 23,886 gram
    Volume piknometer = 10 ml

    ρ = ,m-V. = = 0,855 gram/ml

    Perhitungan Rendemen
    CH3COOH + C2H5OH → C4H8O2 + H2O
    M 0,3 0,8 - -
    R 0,3 0,3 0,3 0,3
    S - 0,5 0,3 0,3
    Mr = 88 ; ρ = 0,89 gram/ml

    n =

    m = n . Mr
    = 0,3 . 88
    = 26,4 gram

    ρ =,m-V.

    v = = = 29,6629 ml

    % rendemen = ,V Etil Asetat hasil praktikum-V Etil Asetat secara stoikiometri . x


    100%

    = x 100%

    = 50,57 %
    LAMPIRAN C
    DOKUMENTASI PELAKSANAAN PRAKTIKUM

    Gambar C.1 Perlengkapan bahan Gambar C.2 Pencampuran asam


    asetat, asam sulfat dan etanol

    Gambar C.3 Proses refluks Gambar C.4 Hasil refluks


    Gambar C.5Proses destilasi Gambar C.6 Hasil destilat

    Gambar C.7 Proses pencucian Gambar C.8 Etil asetat

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