APPENDIKS C

NERACA MASSA

Data-data perencanaan produksi

1 Kapasitas Produksi = 150000 ton/tahun
= 18.93939 ton/jam
= 18939.39 kg/jam
2 Hari kerja = 330 hari/tahun
3 Jam kerja = 24 jam operasi
4 Basis perhitungan = 1 jam operasi

Data Komponen dan Berat Molekul

Zat BM
(NH4)2SO4 132
H2SO4 98
NH3 17
N 14
H2O 18
S R FIX
O2 32
N2 28
H 1
O 16

1. Belt Conveyor
Fungsi :

<1 BELT CONVEYOR <2

> B-150 >

Inlet outlet
Komponen <1> <2>
x mass massa x mass massa
(NH4)2SO4 0.994 27852.84 0.994 27852.84
H2SO4 0.001 27.85284 0.001 27.85284
H2O 0.005 139.2642 0.005 139.2642
NH3 3.57E-05 0
Petrocoat 3.57E-05 1 28020.96 1
Total 28020.9552647059 28020.9552647059
2. Screen

<3> <1>
SCREEN
B-150

<4>

Efisiensi : (NH4)2SO4 kristal 0.8

(NH4)2SO4 larutan 0.2

Inlet Outlet
Komponen <3> <4> <1>
xmass mass xmass mass xmass mass
(NH4)2SO4 0.994 34816.05 0.994 6963.21 0.994 27852.84
H2SO4 0.000994 34.81605 0.000994 6.96321 0.001 27.85284
H2O 0.00497 174.0802 0.00497 34.81605 0.005 139.2642
NH3
Petrocoat 3.57E-05 1.25 3.57E-05 0.25 3.57E-05 1
Sub total 1 35026.19 1 7005 1 28021
Total 35026.1940808823 35026.1940808823

3. Bucket Elevator

<5> <3>
BUCKET ELEVATOR
B-150

Inlet outlet
Komponen <4> <3>
x mass massa x mass massa
(NH4)2SO4 0.994 34816.05 0.994 34816.05
H2SO4 0.000994 34.81605 0.000994 34.81605
H2O 0.00497 174.0802 0.00497 174.0802
Petrocoat 3.57E-05 1.25 3.57E-05 1.25
Sub total 1 35026.19 1 35026.19
Total 35026.1940808823 35026.1940808823
4. Belt Conveyor

<5 BELT CONVEYOR <4

> B-150 >

Inlet outlet
Komponen <4> <3>
x mass massa x mass massa
(NH4)2SO4 0.994 34816.05 0.994 34816.05
H2SO4 0.000994 34.81605 0.000994 34.81605
H2O 0.00497 174.0802 0.00497 174.0802
Petrocoat 3.57E-05 1.25 3.57E-05 1.25
Sub total 1 35026.19 1 35026.19
Total 35026.1940808823 35026.1940808823

5. Rotary Dryer

<8>

<6> DRYER <5>

B-150

<7>

Inlet Outlet
Komponen <6> <7> <5>
xmass mass xmass mass xmass mass
(NH4)2SO4 0.985773 34816.05 0 0 0.994 34816.05
H2SO4 0.000986 34.81605 0 0 0.000994 34.81605
H2O 0.013205 466.3942 0 0 0.00497 174.0802
Petrocoat 3.54E-05 1.25 0 0 3.57E-05 1.25
N2 0 0 0.21 4092.396 0 0
O2 0 0 0.79 15395.2 0 0
Sub total 1 35318.51 1 19487.6 1 35026.19
Total 54806.1075577667 54806.1075577667
6. Screw Conveyor

<10>

<9> <6>
Screw Conveyor
B-150

Inlet outlet
Komponen <9> <10> <6>
xmass mass xmass mass xmass mass
(NH4)2SO4 0.985808 34816.05 0 0 0.985773 34816.05
H2SO4 0.000986 34.81605 0 0 0.000986 34.81605
H2O 0.013206 466.3942 0 0 0.013205 466.3942
Petrocoat 0 0 1 1.25 3.54E-05 1.25
Sub total 1 35317.26 1 1.25 1 35318.51
Total 35318.5080731516 35318.5080731516

7. Sceen

<11> SCREEN <9>

B-150

<12>

Efisiensi : (NH4)2SO4 kristal 0.8

(NH4)2SO4 larutan 0.2

Inlet Outlet
Komponen <11> <9> <12>
xmass mass xmass mass xmass mass
(NH4)2SO4 43520.06 0.985808 0.985808 34816.05 0.985808 8704.012
H2SO4 43.52006 0.000986 0.000986 34.81605 0.000986 8.704012
H2O 582.9928 0.013206 0.013206 466.3942 0.013206 116.5986
Petrocoat 0 0 0 0 0 0
Sub total 44146.57 1 1 35317.26 1 8829.315
 Total 1 44146.5725914395

8. Centrifuge

<13> Centrifuge <11>

B-150

<14>

Efisiensi : (NH4)2SO4 kristal 0.5

(NH4)2SO4 larutan 0.5

Inlet Outlet
Komponen <13> <11> <14>
xmass mass xmass mass xmass mass
(NH4)2SO4 0.985808 87040.12 0.985808 43520.06 0.985808 43520.06
H2SO4 0.000986 87.04012 0.000986 43.52006 0.000986 43.52006
H2O 0.013206 1165.986 0.013206 582.9928 0.013206 582.9928
Petrocoat 0 0 0 0 0 0
Sub total 1 88293.15 1 44146.57 1 44146.57
Total 88293.1451828789 88293.1451828789

9. Screw Conveyor

<14> <13>
Screw Conveyor
B-150

Inlet Outlet
Komponen <4> <3>
xmass mass xmass mass
(NH4)2SO4 0.985808 87040.12 0.985808 87040.12
H2SO4 0.000986 87.04012 0.000986 87.04012
H2O 0.013206 1165.986 0.013206 1165.986
Petrocoat 0 0 0 0
 Sub total 1 88293.15 1 88293.15
Total 88293.1451828789 88293.1451828789

10. Saturator (1)

<16>

<15> <14>
Saturator
B-150

Konversi 0.995
2NH3 + H2SO4 → (NH4)2SO4
m 1318.78968917 660.283
r 1318.78968917 659.3948 659.3948
s 0 0.888164 659.3948

Inlet
<4> <3>
Komponen mol mol
xmass mass (kmol/ja xmass mass (kmol/ja
m) m)
(NH4)2SO4 0 0 0 0 0 0
H2SO4 0 0 0 0.9823 64707.73 660.283
H2O 0 0 0 0.0177 1165.986 64.77698
NH3 1 22419.42 1318.79 0 0 0
Petrocoat 0 0 0 0 0 0
Sub total 1 22419.42 1318.79 1 65873.72 725.06
Total 152009.046603803

11. Wet Cyclone

<17>
 <17>

<16> <15>
Wet Cyclone
B-150

<18>

Inlet Outlet
Komponen <16> <17> <15>
xmass mass xmass mass xmass mass
(NH4)2SO4 0 0 0 0 0 0
H2SO4 0 0 0 0 0 0
H2O 0.014778 292.314 1 3442.462 0 0
Petrocoat 0 0 0 0 0 0
N2 0.206897 4092.396 0 0 0.21 4092.396
O2 0.778325 15395.2 0 0 0.79 15395.2
Sub total 1 19779.91 1 3442.462 1 19487.6
Total 23222.3749796352 23222.3749796352

12. Dissolution Tank

<18>

<4> <19>
Dissolution Tank
inlet
B-150 outlet
Komponen <4> <18> <19>
xmass mass xmass mass xmass mass
(NH4)2SO4 0.994 6963.21 0 0 0.648343 6963.21
H2SO4 0.000994 6.96321 0 0 0.000648 6.96321
H2O 0.00497 34.81605 1 3734.775 0.350986 3769.592
NH3
Petrocoat 3.57E-05 0.25 0 0 2.33E-05 0.25
Sub total 1 7005.239 1 3734.775 1 10740.01
Total 10740.01 0 0 0 10740.01 0
13. Mother Liquor Tank

<12>

<15>

<19> Inlet <20>

Komponen <19> Dissolution Tank
<12> <15>
B-150
xmass mass xmass mass xmass mass
(NH4)2SO4 0.648343 6963.21 0.985808 8704.012 0.985808 43520.06
H2SO4 0.000648 6.96321 0.000986 8.704012 0.000986 43.52006
H2O 0.350986 3769.592 0.013206 116.5986 0.013206 582.9928
Petrocoat 2.33E-05 0.25 0 0 0 0
NH3 0 0 0 0 0 0
Sub total 1 10740.01 1 8829.315 1 44146.57
Total 63715.9014209239
 Outlet
<8>
xmass mass
0 0
0 0
0.0148 292.314
0 0
0.2069 4092.396
0.7783 15395.2
1 19779.91
54806.1075577667
 Outlet
<20> <14>
mol mol
xmass mass (kmol/ja xmass mass (kmol/ja
m) m)
0.92892 #NAME? #NAME? 0.985808 87040.12 659.3948
0.00093 0 0.000986 87.04012 0.888164
0.07014 0 0.013206 1165.986 64.77698
3.9E-06 0 0 0 0
0 0 0 0
1 88293.15 725.06
0
 Outlet
<18>
xmass mass
0 0
0 0
1 3734.775
0 0
0 0
0 0
1 3734.775
23222.3749796352
 outlet
<20>
xmass mass
0.9289 59187.28
0.0009 59.18728
0.0701 4469.183
4E-06 0.25
0 0
1 63715.9
63715.901420924
 Data-data perencanaan produksi
1 Kapasitas Produksi = 150000 ton/tahun
= 18.939394 ton/jam
2 Hari kerja = 330 hari/tahun
3 Jam kerja = 24 jam operasi
4 Basis perhitungan = 1 jam operasi

Data Komponen dan Berat Molekul

Zat BM
(NH4)2SO4 132
H2SO4 98
NH3 17
N 14
H2 O 18
S 32

1 Rotary Dryer
Fungsi :

<2> <3>
<1> ROTARY DRYER <4>
B-150

Laju alir massa

Parameter Keterangan Komposisi
(kg/tahun)
N 3.98 0.21
S 4.55 0.24
H2O 0.19 0.01
Asam Bebas 0.02 0.001

8.73 0.461
Total 18.9394

Mencari Massa N
(NH4)2SO4 = 3.98
= 2 x BM N x massa (NH4)2SO4
BM P2O5
2. Screw Conveyor 0.2121212121 0.0606060606 #NAME?

<5>

<6> SCREW CONVEYOR <1>

J-145

3. CENTRIFUGE

<8> <6>
CENTRIFUGE
H-140

<7>

asumsi mother liqour 0.05

ZA kristal 0.95
jam operasi
jam operasi

9.18
4.02

Komponen Inlet Outle

<1> <2> <3>

xmass mass xmol xmass mass xmol xmass mass
S 0.24 4.55 0.14 0 0 0 0 -
N 0.21 3.98 0.28 0 0 0 0 -
Asam bebas 0.001 0.02 0.00 0 0 0 0 -
H2O 0.02 0.38 0.02 0 0 0 0.01 0.19
O2 0 - 0 0.21 9.18 0.29 0.21 9.18
N2 0 - 0 0.79 4.02 0.14 0.79 4.02
0.471 8.92 0.45 1 13.20 0.43 1.01 13.39
22.12
 Inlet Outlet
Komponen <6> <5> <1>
xmass mass xmol xmass mass xmol xmass mass
S 0.24 4.55 0.14 0 0 0 0.24 4.55
N 0.21 3.98 0.28 0 0 0 0.21 3.98
Asam bebas 0.001 0.02 0.00 0 0 0 0.001 0.02
H2O 0.02 0.38 0.02 0 0 0 0.02 0.38
Petrocoat 0 0 0 0.05 0.95 0.05 0.95
TOTAL 0.471 8.92 0.45 0.05 0.9469697 0.521 9.87
9.87 9.87

Input output
Komponen <8> <7> <6>
xmass massa mol xmass massa mol xmass massa
N 0 0.24 4.55
S 0 0.21 3.98
asam bebas 0 0.001 0.02
H2O 0 0.02 0.38
(NH4)2SO4
terlarut
 Outlet

<3> <4>
xmol xmass mass xmol
- 0.24 4.55 0.14
- 0.21 3.98 0.28
- 0.001 0.02 0.00
0.01 0.01 0.19 0.01
0.29 0 0 0
0.1435714 0 0 0
0.44 0.461 8.73 0.44
22.12
Outlet
<1>
xmol
0.14
0.28
0.00
0.02

9.87

<6>
mol
0.14
0.28
0.00
0.02
Kapasitas Produksi = 150,000 ton/tahun 454.54545
= 19 ton/jam 18.939394
Hari kerja = 330 hari/tahun
Jam kerja = 24 jam operasi
Basis perhitungan = 1 jam operasi

screw konveyor

screen

komp <1> <7>

za 23,674 4,735 18,939
ab 23 5 18
aie 118 24 94.5
petrocoat 1 0 1
23,816 4,763 19,053
23,816

dryer produk
komp <5> <4> <6> <3>
za 23,674 23,674
ab 23 23
air 267 149 118
petrocoat 1 1
o2 2,086 2,086
n2 7,846 7,846
total 9,932 23,965 10,081 23,816
33,897 33,897
m= 9,932 kg/jam
q1 401,265
t
q2 40,126
80 celcius

saturator
t3

massa*cp za+mab*cpab.....

cp za 1.67
cp h2so4 4.19

rh 54%
suhu udara 32 C
humidity 15 kg uap ait ut 1kg udara kering (grafik)
 1 Kapasitas Produksi = 150,000
= 18.939393939
= 27852.838235
2 Hari kerja = 330
3 Jam kerja = 24
4 Basis perhitungan = 1

Data Komponen dan Berat Molekul

Zat BM
(NH4)2SO4 132
H2SO4 98
NH3 17
N 14
H2 O 18
S R FIX
O2 32
N2 28
H 1
O 16

persen
N = 2 x BM N
BM ZA
= 0.2121212121
H = 8 X BM H
BM ZA
= 0.0606060606
S = 1 x BM S
BM ZA
= #VALUE!
O = 4 X BM O
BM ZA
= 0.4848484848

1. belt konveyor
<32> BELT CONVEYOR <33>
J-150
 BELT CONVEYOR
J-150

Inlet outlet Inlet

Komponen <32> <33> <32 final>
x mass massa x mass massa x mass massa
(NH4)2SO4 0.994 27852.83824 0.994 27852.8382 0.391 18939.930
H2SO4 0.001 27.85283824 0.001 27.8528382 0.001 20725.415
H2O 0.005 139.2641912 0.005 139.264191 0.005 1569.403
NH3 0 0 0.000 0 7174.2959091 7174.296
Petrocoat 3.5687577E-05 1 3.5687577E-05 1 2.066E-05 1.000
N2 0 0 0 0
O2 0 0 0 0
Sub Total 1.00 28,020.96 1.00 28,020.96 7,174.69 48,410.04
Total 28020.9552647059 28020.9552647059 48410.0437194015

<30>
2. screen SCREEN
H-173

<31>
Efisiensi : produk 0.8
mother liquor 0.2

Inlet Outlet
Komponen <30> <31> <32>
xmass mass xmass mass xmass mass
(NH4)2SO4 0.994 34816.04779 0.994 6963.210 0.994 27852.838
H2SO4 0.001 34.81604779 0.001 6.963 0.001 27.853
H2O 0.005 174.080239 0.005 34.816 0.005 139.264
NH3 0.000 0 0.000 0.000 0.000 0.000
Petrocoat 0.000 1.25 0.000 0.250 0.000 1.000
N2 0.000 0 0.000 0.000 0.000 0.000
O2 0.000 0 0.000 0.000 0.000 0.000
Sub total 1 35026.19408 1 7005.23882 1 28020.9552647
Total 35026.1940808823 35026.1940808823

3. Bucket Elevator
<29> <30>
BUCKET ELEVATOR
J-172
 Inlet Outlet
Komponen <29> <30>
xmass mass mol xmass mass mol
(NH4)2SO4 0.3912396797 23674.9125 179.35539773 0.39123968 23674.9125 179.355397727
H2SO4 0.4281222139 25906.76887 264.35478437 0.42812221 25906.768868 264.354784368
H2O 0.0324189485 1961.753395 108.98629971 0.03241895 1961.7533948 108.986299713
NH3 0.1481985009 8967.869886 527.52175802 0.1481985 8967.8698864 527.521758021
Petrocoat 2.065687E-05 1.25 2.06569E-05 1.25 0
N2 0 0 0 0 0 0
O2 0 0 0 0 0 0
Sub total 1 60512.55465 1080.2182398 1 60512.554649 1080.21823983
Total 60512.5546492519 60512.5546492519

4. Belt Conveyor

<28 <29
BELT CONVEYOR >
>
B-150

Inlet Outlet
Komponen <29> <30>
xmass mass mol xmass mass mol
(NH4)2SO4 0.3912396797 23674.9125 179.35539773 0.39123968 23674.9125 179.355397727
H2SO4 0.4281222139 25906.76887 264.35478437 0.42812221 25906.768868 264.354784368
H2O 0.0324189485 1961.753395 108.98629971 0.03241895 1961.7533948 108.986299713
NH3 0.1481985009 8967.869886 527.52175802 0.1481985 8967.8698864 527.521758021
Petrocoat 2.065687E-05 1.25 0 2.06569E-05 1.25 0
N2 0 0 0 0 0 0
O2 0 0 0 0 0 0
Sub total 1 60512.55465 1080.2182398 1 60512.554649 1080.21823983
Total 60512.5546492519 60512.5546492519

3. Dryer

<27>
<28> ATAU <30>
<26> >
DRYER
R-150
 DRYER
R-150

<43>

Inlet Outlet Inlet

Komponen
<43> <26> <27> <28> <43 final> <26 final>
(NH4)2SO4 0 34816.04779 0 34816.0478 0 23674.9125
H2SO4 0 34.81604779 0 34.8160478 0 25906.768868
H2O 0 466.3942312 292.31399227 174.080239 0 2254.06738711
NH3 0 0 0 0 0 8967.86988636
Petrocoat 0 1.25 0 1.25 0 1.25
N2 4092.39589177 0 4092.3958918 0 4092.3958918 0
O2 15395.2035928 0 15395.203593 0 15395.203593 0
Total 19487.5994846 35318.50807 19779.913477 35026.1941 19487.599485 60804.8686415
Sub Total 54806.1075577667 54806.1075577667 80292.4681261363

Cp ZA 1.67
Cp H2SO4 4.19 (3.856 menurut murphy dengan suhu asumsi 32)
3.856
Cp Air 4.178 ( 4.178 kj/k.kg menurut http://www.vaxasoftware.com/index.php pada suhu 32 )
Cp NH3 4.6024
Cp Petrocoat 1.39
Cp N2 1.04
(www.EngineeringToolBox.com)
Cp O2 0.919
Cp Udara 1.01
m 19487.5994846 udara kering
Q1 m Cp ΔT
787299.0
Q2 58466.2375978

<26 final> 8047.22894 80% suhu referensi 32

<28 final> 8047.229 20%
Massa Udara kering -13245.6187
inlet
Komponen <43 final> udara kering 150 C <26 final> ZA
m cp ∆T Q m cp
(NH4)2SO4 0 1.67 118 0 8047.22894 1.67
N2 -10464.038789 1.04 118 -1284146.84 0 1.04
O2 -2781.5799312 0.919 118 -301640.091 0 0.919
Total -13245.61872 0 0 -1585786.93 8047.22894 0
Sub Total -5198.389779779
FOBJ ABS ((∑inlet - ∑outlet)/∑inlet)
1.1542036E-08

<43 final> 150

<26 final> 70
<27 final> 110
<28 final> 80
suhu referens 32

Inlet
Komponen <43 final> <26 final>
m Cp ∆T Q m Cp
(NH4)2SO4 0 1.67 118 0 23674.9125 1.67
H2SO4 0 4.19 118 0 25906.768868 3.856
H2O 0 4.178 118 0 2254.0673871 4.178
NH3 0 4.6024 118 0 8967.8698864 4.6024
Petrocoat 0 1.39 118 0 1.25 1.39
N2 4092.39589177 1.04 118 502218.824 0 1.04
O2 15395.2035928 0.919 118 1669486.67 0 0.919
Total 19487.5994846 0 0 2171705.49 60804.868642 0
Sub Total 80292.4681261363
∑inlet

FOBJ ABS ((∑inlet - ∑outlet)/∑inlet)

0

5. Screw Conveyor
<24>

<23>
Screw Conveyor
J-153

Inlet outlet
Komponen <23> <24> <26>
xmass mass xmass mass xmass mass
(NH4)2SO4 0.9858083468 34816.04779 0 0 0.9857734569 34816.0477941
H2SO4 0.0009858083 34.81604779 0 0 0.0009857735 34.8160477941
H2O 0.0132058449 466.3942312 0 0 0.0132053775 466.39423124
NH3 0 0 0 0 0 0
Petrocoat 0 0 1 1.25 3.5392208E-05 1.25
N2 0 0 0 0 0 0
O2 0 0 0 0 0 0
Sub total 1 35317.25807 1 1.25 1 35318.5080732
Total 35318.5080731516 35318.5080731516

6. Screen
<21> SCREEN
H-148

<22>

Efisiensi: produk 0.8

mother liquor 0.2
inlet inlet oulet
Komponen <21> <21 final> <22>
xmass mass xmass mass xmass mass
(NH4)2SO4 0.9858083468 43520.05974 0.3893668342 29593.6406 0.9858083468 8704.01194853
H2SO4 0.0009858083 43.52005974 0.4260728135 32383.4611 0.0009858083 8.7040119485
H2O 0.0132058449 582.992789 0.0370712704 2817.58423 0.0132058449 116.59855781
NH3 0 0 0.1474890818 11209.8374 0 0
Petrocoat 0 0 0 0 0 0
N2 0 0 0 0
O2 0 0 0 0
Sub total 1 44146.57259 1 76004.5233 1 8829.31451829
Total 44146.5725914395 76004.5233019014 44146.5725914395

7. Centrifuge

<12> Centrifuge
R-140

<25>

Efisiensi : produk 0.5

mother liquor 0.5

Inlet outlet
Komponen <12> <12 final> <25>
xmass mass xmass mass xmass mass
(NH4)2SO4 0.9858083468 87040.11949 0.3893668342 59187.2813 0.9858083468 43520.0597426
H2SO4 0.0009858083 87.04011949 0.4260728135 64766.9222 0.0009858083 43.5200597426
H2O 0.0132058449 1165.985578 0.0370712704 5635.16847 0.0132058449 582.99278905
NH3 0 0 0.1474890818 22419.6747 0 0
Petrocoat 0 0 0 0 0 0
N2 0 0 0 0
O2 0 0 0 0
Sub total 1 88293.14518 1 152009.047 1 44146.5725914
Total 88293.1451828789 152009.046603803 88293.1451828789

8. Screw Conveyor

<5> <12>
Screw Conveyor
B-150

Inlet Outlet
Komponen <5> <12>
xmass mass xmass mass
(NH4)2SO4 0.3893668342 29593.6406 0.3893668342 29593.6406
H2SO4 0.4260728135 32383.4611 0.4260728135 32383.4611
H2O 0.0370712704 2817.5842 0.0370712704 2817.5842
NH3 0.1474890818 11209.8374 0.1474890818 11209.8374
N2 0 0.0000 0 0.0000
O2 0 0.0000 0 0.0000
Petrocoat 0 0.0000 0 0.0000
Sub total 1 76004.5233 1 76004.5233
Total 76004.5233 76004.5233

9. Cooler
<5> <12>
Cooler
B-150

Inlet Outlet
Komponen <5> <12>
xmass mass xmass mass
(NH4)2SO4 0.3893668342 29593.6406 0.3893668342 29593.6406
H2SO4 0.4260728135 32383.4611 0.4260728135 32383.4611
H2O 0.0370712704 2817.5842 0.0370712704 2817.5842
NH3 0.1474890818 11209.8374 0.1474890818 11209.8374
N2 0 0.0000 0 0.0000
O2 0 0.0000 0 0.0000
Petrocoat 0 0.0000 0 0.0000
 Sub total 1 76004.5233 1 76004.5233
Total 76004.5233 76004.5233

8. saturator

Inlet
Komponen <3> <4>
xmass mass mol xmass mass mol
(NH4)2SO4 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
H2SO4 0.0000 0.0000 0.0000 0.9823 64707.7349 660.2830
H2O 0.0000 0.0000 0.0000 0.0177 1165.9856 64.7770
NH3 1.0000 22419.4247 1318.7897 0.0000 0.0000 0.0000
N2
O2
Petrocoat 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Sub total 1.0000 22419.4247 1318.7897 1.0000 65873.7205 725.0600
Total 152009.0466

SATURATOR 2
Inlet
Komponen <3> <4>
xmass mass mol xmass mass mol
(NH4)2SO4 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
H2SO4 0.0000 0.0000 0.0000 0.9823 32353.8674 330.1415
H2O 0.0000 0.0000 0.0000 0.0177 582.9928 32.3885
NH3 1.0000 11209.7124 659.3948 0.0000 0.0000
N2 0.0000 0.0000 0.0000 0.0000
O2 0.0000 0.0000 0.0000 0.0000
Petrocoat 0.0000 0.0000 0.0000 0.0000
Sub total 1.0000 11209.7124 659.3948 1.0000 32936.8602 362.5300
Total 76004.5233

Konversi 0.995
2NH3 + H2SO4 → (NH4)2SO4

m 1318.78968917 660.28300907
r 1318.78968917 659.39484459 659.39484459
s 0.8881644845 659.39484459

9. WET CYCLONE
Inlet Outlet
Komponen
<27> <39> <41> <40>
(NH4)2SO4 0
H2SO4 0
H2O 292.313992269 3442.461503 3734.7755 <27>
NH3 0
Petrocoat 0
N2 4092.39589177 4092.3958918
O2 15395.2035928 15395.203593
Total 19779.9134769 3442.461503 19487.599485 3734.7755
Sub Total 23222.3749796352 23222.3749796352

Q3 = 1358484.45759
Mair 3442.46150275 kg/jam
T 126.18279159
densitas air 1 kg/L
Volume udara 3,442.46 L/jam
908.81 Gallon/jam
15.15 gallon/menit (perry chapter 10 gambar 10.26)

10. Dissolution Drum

inlet outlet
Komponen <35> <36> <37>
xmass mass xmass mass xmass mass
(NH4)2SO4 0.9940003106 6963.210 0 0 0.6483426704 6963.210
H2SO4 0.0009940003 6.963 0 0 0.0006483427 6.9632095588
H2O 0.0049700016 34.816 1 3734.7755 0.3509857095 3769.59154281
NH3 0.000 0
Petrocoat 3.5687577E-05 0.250 0 0 2.3277436E-05 0.25
Sub total 1 7005.238816 1 3734.7755 1 10740.0143112
Total 10740.0143111965 10740.0143111965

11. Mother Liquor Tank

Inlet
Komponen <13> <7> <8>
xmass mass xmass mass xmass mass
(NH4)2SO4 0.6483426704 6963.209559 0.9858083468 8704.01195 0.9858083468 43520.0597426
H2SO4 0.0006483427 6.963209559 0.0009858083 8.70401195 0.0009858083 43.5200597426
H2O 0.3509857095 3769.591543 0.0132058449 116.598558 0.0132058449 582.99278905
Petrocoat 2.3277436E-05 0.25 0 0 0 0
NH3 0 0 0 0 0 0
Sub total 1 10740.01431 1 8829.31452 1 44146.5725914
Total 63715.9014209239

Inlet
Komponen <13> <7> <8>
xmass mass xmass mass xmass mass
(NH4)2SO4 0.0040521417 43.52005974 9.8580834679 87040.1195 0 0
H2SO4 0.0542823103 582.992789 0.0098580835 87.0401195 0 0
H2O 0 0 0.1320584487 1165.98558 0 0
Petrocoat 0 0 0 0 0 0
NH3 0 0 0 0 0 0
Sub total 0.058334452 626.5128488 10 88293.1452 0 0
Total 88919.6580316714
 ton/tahun
ton/jam
kg/jam
hari/tahun
jam operasi
jam operasi

<33>
 outlet
<33 final>
x mass massa
0.391 18939.930
0.001 20725.415
0.005 1569.403
0.603 7174.296
2.07E-05 1.000

1.00 48,410.04
48410.0437194015

<32>
SCREEN
H-173

<31>

Inlet Outlet
<30 final> <31 final> <32 final>
xmass mass xmass mass xmass mass
0.676 23674.9125 0.676 4734.983 0.391 18939.930
0.740 25906.76887 0.740 5181.354 0.001 20725.415
0.056 1961.753395 0.056 392.351 0.005 1569.403
0.256 8967.869886 0.256 1793.574 0.603 7174.296
0.000 1.25 0.000 0.250 0.000 1.000

1.7276372 60512.55465 2 12102.51093 1 48410.043719

60512.5546492519 60512.5546492519
> ATAU <30>
 Outlet
<27 final> <28 final>
0 23674.9125
0 25906.76887
292.31399 1961.753395
0 8967.869886
0 1.25
4092.3959 0
15395.204 0
19779.913 60512.55465
80292.4681261363

Th in 150 C
Th Out 110 C
Tc Out 80 C
hp pada suhu 32 ) Tc in 70 C

Outlet
70 C <27 final> 110 C <28 final> ZA
∆T Q m cp ∆T Q m cp
38 510677.1485 0 1.67 78 0 8047.229 1.67
38 0 -10464.0388 1.04 78 -848842.82653 0 1.04
38 0 -2781.57993 0.919 78 -199389.21262 0 0.919
0 510677.1485 -13245.6187 0 0 -1048232.0392 8047.229 0
-5198.389719779
 Outlet
<26 final> <27 final> <28 final>
∆T Q m Cp ∆T Q m Cp
38 1502409.947 0 1.67 78 0 23674.913 1.67
38 3796067.029 0 3.856 78 0 25906.769 3.856
38 357864.7546 292.3139923 4.178 78 95260.453057 1961.7534 4.178
38 1568401.526 0 4.6024 78 0 8967.8699 4.6024
38 66.025 0 1.39 78 0 1.25 1.39
38 0 4092.395892 1.04 78 331975.15474 0 1.04
38 0 15395.20359 0.919 78 1103558.9839 0 0.919
0 7224809.281 19779.91348 0 0 1530794.5917 60512.555 0
80292.4681261363
∑outlet

<26>
Conveyor
-153

Inlet outlet
<23 final> <24 final> <26 final>
xmass mass xmass mass xmass mass
0.3893668 23674.9125 0 0 0.3893588298 23674.9125
0.4260728 25906.76887 0 0 0.4260640545 25906.768868
0.0370713 2254.067387 0 0 0.0370705083 2254.0673871
0.1474891 8967.869886 0 0 0.1474860498 8967.8698864
0 0 1 1.25 2.055756E-05 1.25
 0
0
1 60803.61864 1 1.25 1 60804.868642
60804.8686415211 60804.8686415211

CREEN <23>
H-148

<22>

oulet oulet
<23> <22 final> <23 final>
xmass mass xmass mass xmass mass
0.9858083 34816.04779 0.389366834 5918.728125 0.3893668342 23674.9125
0.0009858 34.81604779 0.426072814 6476.692217 0.4260728135 25906.768868
0.0132058 466.3942312 0.03707127 563.5168468 0.0370712704 2254.0673871
0 0 0.147489082 2241.967472 0.1474890818 8967.8698864
0 0 0 0 0 0
0 0
0 0
1 35317.25807 1 15200.90466 1 60803.618642
44146.5725914395 76004.5233019014

ge <21>

outlet
<21> <25 final> <21 final>
xmass mass xmass mass xmass mass
0.9858083 43520.05974 0.389366834 29593.64063 0.3893668342 29593.640625
 0.0009858 43.52005974 0.426072814 32383.46109 0.4260728135 32383.461085
0.0132058 582.992789 0.03707127 2817.584234 0.0370712704 2817.5842339
0 0 0.147489082 11209.83736 0.1474890818 11209.837358
0 0 0 0 0 0
0 0
0 0
1 44146.57259 1 76004.5233 1 76004.523302
88293.1451828789 152009.046603803
 outlet hasil reaksi outlet final
<39> <4> <5>
xmass mass mol xmass mass mol(kmol/jam) xmass mass
0.9289 59187.2813 448.3885 0.9858 87040.1195 659.3948 0.3894 59187.2813
0.0009 59.1873 0.6040 0.0010 87.0401 0.8882 0.4261 64766.9222
0.0701 4469.1829 248.2879 0.0132 1165.9856 64.7770 0.0371 5635.1685
0.0000 0.2500 0.0000 0.0000 0.0000 0.0000 0.1475 22419.6747
0.0000 0.0000 0.0000
0.0000 0.0000 0.0000
0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
1.0000 63715.9014 697.2804 1.0000 88293.1452 725.0600 1.0000 152009.0466
152009.0466 152009.0466

outlet hasil reaksi outlet final

<39> <4> <5>
xmass mass mol xmass mass mol(kmol/jam) xmass mass
0.9289 29593.6406 224.1942 0.0000 0.3894 29593.6406
0.0009 29.5936 0.3020 0.0000 0.4261 32383.4611
0.0701 2234.5914 124.1440 0.0371 2817.5842
0.0000 0.1250 0.0074 0.1475 11209.8374
0.0000 0.0000 0.0000 0.0000
0.0000 0.0000 0.0000 0.0000
0.0000 0.0000 0.0000 0.0000
1.0000 31857.9507 348.6475 1.0000 76004.5233
76004.5233 76004.5233

<39>
 <39>

<27> <41>
Wet Cyclone
R-160

<40>

<35>

<36> <37>
Dissolution Tank
F-176

outlet
<39>
xmass mass
0.9289248 59187.28125
0.0009289 59.18728125
0.0701423 4469.18289
3.9237E-06 0.25
0 0
1 63715.90142
63715.9014209239

outlet
<39> <22>
<25>
xmass mass
<38> <39>
1.3667489 87083.63955 <38> <39>
0.0105159 670.0329085 Mother Liquor Tank
0.0182998 1165.985578 F-146
0 0
0 0
1.3955646 88919.65803
88919.6580316714
 inlet
80 C Komponen <43 final> udara kering 150 C
∆T Q m cp ∆T Q
48 645065.88 (NH4)2SO4 0 1.67 40 0
48 0 N2 7846.28 1.04 40 326405.25
48 0 O2 2085.72 0.919 40 76671.067
0 645065.88 Total 9932 0 0 403076.32
Sub Total 940631.208392
 FOBJ ABS ((∑inlet - ∑outlet)/∑inlet)
0.75

<28 final>
∆T Q
48 1897781
48 4795032
48 393417.87
48 1981138.8
48 83.4
48 0
48 0
0 9067453.1
 <3>
outlet final
<5>
mol(kmol/jam) <4> <5>
448.3885 Saturator
660.8870 B-150
313.0649
1318.8044

0.0000
2741.1448
152009.0466

outlet final
<5>
mol(kmol/jam)
224.1942
330.4435
156.5325
659.4022

1370.5724
76004.5233
<37>

<39>
<39>
 inlet Outlet
<26 final> ZA 70 C <27 final> 110 C <28 final>
m cp ∆T Q m cp ∆T Q m
8047.2289 1.67 40 537554.89 0 1.67 10 0 8047.229
0 1.04 40 0 7846.28 1.04 10 81601.312 0
0 0.919 40 0 2085.72 0.919 10 19167.767 0
0 0 0 537554.89 9932 0 0 100769.08 8047.229
940631.208392 235157.8031
<5>
let
ZA 80 C
cp ∆T Q
1.67 10 134388.72
1.04 10 0
0.919 10 0
0 0 134388.72
.8031
 LAMPIRAN C
NERACA MASSA

Data-data perencanaan produksi :

1 Kapasitas produksi = 155,000 ton/tahun
= 19.5707071 ton/tahun
= 19570.7071 kg/tahun
2. Hari kerja = 330 hari/tahun
3. Jam kerja = 24 jam operasi
4. Basis perhitungan = 1 jam operasi

Data komponen dan berat molekul :

Zat BM
(NH4)2SO4 132
H2SO4 98
NH3 17
N 14
H2 O 18
S 32
O2 32
N2 28
H 1
O 16

1. Saturator

<3>

<4> <5>
Saturator
B-150

Konversi = 0.995

2NH3 + H2SO4 → (NH4)2SO4

M 1318.7896891711 660.2830090701
R 1318.7896891711 659.3948445856 659.3948445856
S 0 0.8881644845 659.3948445856
 Inlet
Komponen <4> <3>
xmass mass mol xmass mass mol
(NH4)2SO4 0 0 0 0 0 0
H2SO4 0 0 0 0.9823 64707.73 660.283
H2O 0 0 0 0.0177 1165.986 64.77698
NH3 1 22419.42 1318.78969 0 0 0
Petrocoat 0 0 0 0 0 0
N2 0 0 0 0 0 0
O2 0 0 0 0 0 0
Sub total 1 22419.42 1318.78969 1 65873.72 725.06
Total 152009.046603803

2. Screw Conveyor

<5> <12>
Screw Conveyor
B-150

Inlet Outlet
Komponen <5> <12>
xmass mass xmass mass
(NH4)2SO4 0.389367 59187.2813 0.389367 59187.28
H2SO4 0.426073 64766.9222 0.426073 64766.92
H2O 0.037071 5635.16847 0.037071 5635.168
NH3 0.147489 22419.6747 0.147489 22419.67
Petrocoat 0 0 0 0
N2 0 0 0 0
O2 0 0 0 0
Sub total 1 152009.047 1 152009
Total 152009.046603803 152009.0466038

3. Centrifuge

<12> Centrifuge <21>

B-150

<25>
 Efisiensi : (NH4)2SO4 kristal 0.5
(NH4)2SO4 larutan 0.5

Inlet Outlet
Komponen <12> <21> <25>
xmass mass xmass mass xmass mass
(NH4)2SO4 0.38936683 59187.28 0.38936683 29593.64 0.389367 29593.64
H2SO4 0.42607281 64766.92 0.42607281 32383.46 0.426073 32383.46
H2O 0.03707127 5635.168 0.03707127 2817.584 0.037071 2817.584
NH3 0.14748908 22419.67 0.14748908 11209.84 0.147489 11209.84
Petrocoat 0 0 0 0 0 0
N2 0 0 0 0 0 0
O2 0 0 0 0 0 0
Sub total 1 152009 1 76004.52 1 76004.52
Total 152009.046603803 152009.046603803

4. Screen
<21> <23>
SCREEN
B-150

<22>

Efisiensi : (NH4)2SO4 kristal 0.8

(NH4)2SO4 larutan 0.2

Inlet Outlet
Komponen <21> <22> <23>
xmass mass xmass mass xmass mass
(NH4)2SO4 0.38936683 29593.64 0.38936683 23674.91 0.389367 5918.728
H2SO4 0.42607281 32383.46 0.42607281 25906.77 0.426073 6476.692
H2O 0.03707127 2817.584 0.03707127 2254.067 0.037071 563.5168
NH3 0.14748908 11209.84 0.14748908 8967.87 0.147489 2241.967
Petrocoat 0 0 0 0 0 0
N2 0 0 0 0 0 0
O2 0 0 0 0 0 0
Sub total 1 76004.52 1 60803.62 1 15200.9
Total 76004.5233019014 76004.5233019014
5. Screw Conveyor

<24>

<23> <25>
Screw Conveyor
B-150

Inlet outlet
Komponen <23> <24> <25>
xmass mass xmass mass xmass mass
(NH4)2SO4 0.38936683 23674.91 0 0 0.389359 23674.91
H2SO4 0.42607281 25906.77 0 0 0.426064 25906.77
H2O 0.03707127 2254.067 0 0 0.037071 2254.067
NH3 0.14748908 8967.87 0 0 0.147486 8967.87
Petrocoat 0 0 1 1.25 2.06E-05 1.25
N2 0 0 0 0 0 0
O2 0 0 0 0 0 0
Sub total 1 60803.62 1 1.25 1 60804.87
Total 60804.8686415211 60804.868641521

6. Rotary Dryer

<27>

<25> <28>
DRYER
B-150

<43>

Inlet Outlet
Komponen <25> <43> <27>
 Komponen
xmass mass xmass mass xmass mass
(NH4)2SO4 0.38935883 23674.91 0 0 0 0
H2SO4 0.42606405 25906.77 0 0 0 0
H2O 0.03707051 2254.067 0 0 0.014778 292.314
NH3 0.14748605 8967.87 0 0 0 0
Petrocoat 2.0558E-05 1.25 0 0 0 0
N2 0 0 0.21 4092.396 0.206897 4092.396
O2 0 0 0.79 15395.2 0.778325 15395.2
Sub total 1 60804.87 1 19487.6 1 19779.91
Total 80292.4681261363 100072.381603021

7. Belt Conveyor

<28> BELT CONVEYOR <29>

B-150

Inlet outlet
Komponen <28> <29>
x mass massa x mass massa
(NH4)2SO4 0.29485845 23674.91 0.29485845 23674.91
H2SO4 0.32265503 25906.77 0.32265503 25906.77
H2O 0.02807321 2254.067 0.02807321 2254.067
NH3 0.11169005 8967.87 0.11169005 8967.87
Petrocoat 1.5568E-05 1.25 1.5568E-05 1.25
N2 0.05096861 4092.396 0.05096861 4092.396
O2 0.19173908 15395.2 0.19173908 15395.2
Sub total 1 80292.47 1 80292.47
Total 80292.4681261363 80292.4681261363

8. Bucket elevator

<29> <30>
BUCKET ELEVATOR
B-150

Inlet outlet
Komponen <29> <30>
x mass massa x mass massa
(NH4)2SO4 0.29485845 23674.91 0.29485845 23674.91
H2SO4 0.32265503 25906.77 0.32265503 25906.77
H2O 0.02807321 2254.067 0.02807321 2254.067
 NH3 0.11169005 8967.87 0.11169005 8967.87
Petrocoat 1.5568E-05 1.25 1.5568E-05 1.25
N2 0.05096861 4092.396 0.05096861 4092.396
O2 0.19173908 15395.2 0.19173908 15395.2
Sub total 1 80292.47 1 80292.47
Total 80292.4681261363 80292.4681261363

9. Screen

<30> <32>
SCREEN
B-150

<31>

Efisiensi : (NH4)2SO4 kristal 0.8

(NH4)2SO4 larutan 0.2

Inlet Outlet
Komponen <30> <31> <32>
xmass mass xmass mass xmass mass
(NH4)2SO4 0.29485845 23674.91 0.29485845 4734.983 0.294858 18939.93
H2SO4 0.32265503 25906.77 0.32265503 5181.354 0.322655 20725.42
H2O 0.02807321 2254.067 0.02807321 450.8135 0.028073 1803.254
NH3 0.11169005 8967.87 0.11169005 1793.574 0.11169 7174.296
Petrocoat 1.5568E-05 1.25 1.5568E-05 0.25 1.56E-05 1
N2 0.05096861 4092.396 0.05096861 818.4792 0.050969 3273.917
O2 0.19173908 15395.2 0.19173908 3079.041 0.191739 12316.16
Sub total 1 80292.47 1 16058.49 1 64234
Total 80292.4681261363 80292.4681261363

10. Belt Conveyor

<32> BELT CONVEYOR <33>

B-150

Inlet outlet
Komponen <32> <33>
x mass massa x mass massa
 (NH4)2SO4 0.29485845 18939.93 0.29485845 18939.93
H2SO4 0.32265503 20725.42 0.32265503 20725.42
H2O 0.02807321 1803.254 0.02807321 1803.254
NH3 0.11169005 7174.296 0.11169005 7174.296
Petrocoat 1.5568E-05 1 1.5568E-05 1
N2 0.05096861 3273.917 0.05096861 3273.917
O2 0.19173908 12316.16 0.19173908 12316.16
Sub total 1 64234 1 64234
Total 64233.974500909 64233.974500909

11. Wet Cyclone

<39>

<27> <40>
Wet Cyclone
B-150

<41>

Inlet Outlet
Komponen <27> <39> <40>
xmass mass xmass mass xmass mass
(NH4)2SO4 0 0 0 0 0 0
H2SO4 0 0 0 0 0 0
H2O 0.01477833 292.314 1 3442.462 0 0
NH3 0 0 0 0 0 0
Petrocoat 0 0 0 0 0 0
N2 0.20689655 4092.396 0 0 0.21 4092.396
O2 0.77832512 15395.2 0 0 0.79 15395.2
Sub total 1 19779.91 1 3442.462 1 19487.6
Total 23222.3749796352 23222.3749796352

12. Dissolution Tank

<35>

<36> <37>
Dissolution Tank
B-150
 inlet outlet
Komponen <36> <35> <37>
xmass mass xmass mass xmass mass
(NH4)2SO4 0 0 0.29485845 4734.983 0.239222 4734.983
H2SO4 0 0 0.32265503 5181.354 0.261774 5181.354
H2O 1 3734.775 0.02807321 450.8135 0.211465 4185.589
NH3 0 0 0.11169005 1793.574 0.090615 1793.574
Petrocoat 0 0 1.5568E-05 0.25 1.26E-05 0.25
N2 0 0 0.05096861 818.4792 0.041351 818.4792
O2 0 0 0.19173908 3079.041 0.15556 3079.041
Sub total 1 3734.775 1 16058.49 1 19793.27
Total 19793.2691202473 19793.269120247

13. Mother Liquor Tank

<22>
<25>

<38> <39>
Dissolution Tank
B-150

Inlet
Komponen <38> <25> <22>
xmass mass xmass mass xmass mass
(NH4)2SO4 0.23922185 4734.983 0.38936683 29593.64 0.389367 23674.91
H2SO4 0.26177352 5181.354 0.42607281 32383.46 0.426073 25906.77
H2O 0.21146527 4185.589 0.03707127 2817.584 0.037071 2254.067
NH3 0.09061535 1793.574 0.14748908 11209.84 0.147489 8967.87
Petrocoat 1.2631E-05 0.25 0 0 0 0
N2 0.04135139 818.4792 0 0 0 0
O2 0.15555999 3079.041 0 0 0 0
Sub total 1 19793.27 1 76004.52 1 60803.62
Total 156601.41106367
 Outlet hasil reaksi Outlet final
<4A> <3A> <5>
xmass mass mol xmass massmol(kmol/jam)xmass mass
0.928925 59187.28 448.3885 0.985808 87040.12 659.3948 0.389367 59187.28
0.000929 59.18728 0.603952 0.000986 87.04012 0.888164 0.426073 64766.92
0.070142 4469.183 248.2879 0.013206 1165.986 64.77698 0.037071 5635.168
3.92E-06 0.25 0 0 0 0 0.147489 22419.67
0 0 0 0 0 0 0 0
0 0 0 0 0 0 0 0
0 0 0 0 0 0 0 0
1 63715.9 697.2804 1 88293.15 725.06 1 152009
0 152009.046603803
Outlet
<28>
 xmass mass
0.294858 23674.91
0.322655 25906.77
0.028073 2254.067
0.11169 8967.87
1.56E-05 1.25
0.050969 4092.396
0.191739 15395.2
1 80292.47
100072.381603021
 Outlet
<41>
xmass mass
0 0
0 0
1 3734.775
0 0
0 0
0 0
0 0
1 3734.775
23222.3749796352
 outlet
<39>
xmass mass
0.37039 58003.54
0.405307 63471.58
0.059113 9257.241
0.140301 21971.28
1.6E-06 0.25
0.005227 818.4792
0.019662 3079.041
1 156601
156601.41106367
 Outlet final
<5>
mol(kmol/jam)
448.3885
660.887
313.0649
1318.804
0
0
0
2741.145
152009.046603803
 APENDIKS
SPESIFIKASI SATURATOR
1. SATURATOR
Fungsi : Untuk mereaksikan NH3 dan H2SO4

Kondisi Operasi
T: 120 °C
P: 1 atm
14.7 psig
θ: 4 jam
Vl: 75 %
Material: SA 240 Grade M Type 316
f: 18750
PengelasaDouble Welded but joint
E: 0.8
C (faktor 1/16 in
0.0625
LS 1.5 d
sudut 120
tg 120 1.73

Komposisi Feed Saturator

Komponem (kg/jam)m (lb/jam) ρ (lb/ft3) V (ft3)
H2SO4 #REF! #REF! 114.04 #REF!
H2O #REF! #REF! 62.4 #REF!
NH3 #REF! #REF! 0.0445 #REF!
Total TOTAL #REF!

V total Tan = V liquid / Volume total liquid

= 188584/0,75
= 75 %
= #REF! ft3
V total Tan = #REF! m

Mencari ukuran silinder

V total = V1 + V2 + V3
#REF! = (π/24 * d3/tg1/2 ɤ) + (π/4 d2 LS) + (0,0843 d3)
#REF! = (3,14/24*d3/tg1/2 120) + (3,14/4 d2 1,5 d) + (0,0843 d3)
#REF! = (3,14/24*d3/1,73) + (3,14/4 d2 1,5 d) + (0,0843 d3)
#REF! = (0,0756262 d3) + (1,1775 d2) + (0,0843 d3)
 #REF! = 1.3374262 d3
d3 = #REF!
d = #REF! ft Standarisasi OD
d = #REF! in 132 in
d = #REF! m 11 ft

Mencari Tinggi Silinder

Ls = 1,5 x d
Ls = 16.5 ft
= 5.0292 m
= 198 in

Mencari Tebal Silinder

ts = Pi x do + C
2 (FE + 0,4 Pi)
= 14,7 x 11 + 0.0625
2 ((18750 x 0,8) + (0,4 x 14,7))
= 0.1271547 in

= 0.1271547 x 16
16
ts = 2.0344745
~ 1 1 in
16 2
= 0.1271547 in
= 0.0105962 ft
= 0.0032297 m

Mencari Ketinggian Tutup ata(Dishead)

Ha = 0,169 x d
Ha = 1.859 ft
= 0.5666232 m
= 22.308 in

Mencari Ketinggian Tutup b (Conical)

Hb = d
2 tg 1/2 ɤ
= 132
2 x tg 60
= 132
2 x 1,73
Hb = 38.150289 in
 = 3.1791908 ft
= 0.9690173 m
Mencari Tebal tutu(standar dished head)
tha = 0,885 x Pi x + C
2 (FE - 0,1 Pi)
= 0,885 x 14,7 x 66 + 0.0625
2 ((18750 x 0,8) - (0,1 x 14,7))
= 858.627 + 0.0625
29997.06
= 0.0911237 in
= 0.0911237 x 16
16
tha = 1.4579793 ~ 3 in
16 16
= 0.1875 in
= 0.015625 ft
= 0.0047625 m

Mencari Tebal tutup bawah (t(conical)

ts = do - di
2
0.127155 = 132 - di
2
0.254309 = 132 - di
di = 132 - di
di = 131.74569 ft
= 10.978808 in

thb = pi x di + C
2 (FE-0,6 Pi) Cos 1/2ɤ
= 14,7 X 10,854 + 0.0625
2((18750 x 0,8) - 0,6 x 14,7)) cos 60
= 161.38847 + 0.0625
14991.18
= 0.0732656 in
= 0.0732656 x 16
16
thb = 1.172249 ~ 3 in
16 16
= 0.1875 in
= 0.015625 ft
 = 0.0047625 m

LS = 16.5 ft
198 in
5.0292 m
Ha = 1.859 ft
22.308 in
0.5666232 m
Hb = 3.1791908 ft
38.150289 in
0.9690173 m
ts = 0.0105962 ft
0.1271547 in
0.0032297 m
tha = 0.015625 ft
0.1875 in
0.0047625 m
thb = 0.015625 ft
0.1875 in
0.0047625 m

PERANCANGAN SABUK PENGAMAN

Asumsi :
Sabuk Pe = 2
Tipe = Chanel
Ukuran = 3 in
Berat = 6 lb/ft
P = 14.7 psig
T = 120 C
= 248 F

Trial ts 1/2
ts = 1 1 = 1.5
2
Harga DO = 132(2 x 1 1/2)
Harga DO = 135 in

LI = Ls
n+1
= 198
2+1
 LI = 66

LI = 66
do 135
= 0.4888889

do = 135
ts 1 1/2
= 90

T 248 ~ 300 F
nilai B lihat grafik
B = 14,000
B = Pallowabel x do
ts
14000 = Pallowabel x 135
1.5
14000 = Pallowabel x 90
allowabel = 14000
90
allowabel = 155.55556

Pallowabe > Pkenyataan

155.5556 > 14.7 (sudah memenuhi)

%delp = Pallowabel - Pi x 100%

Pi
= 155.55556 - 14.7 x 100%
14.7
%delp = 958.20106 %

%delp < 20% ( Belum memenuhi)

PERANCANGAN PENYANGGA

Ha = 22.308 in
Hb = 38.15029 in
LS = 198 in
Asumsi:
Penyangga = 4
Tipe = I Beam
 berat = 14.75 lb/ft
ukuran = 5 in
berat total beserta isi = #REF! lb
berat tutup atas dan bawah = 104830 lb

Tinggi tota = 258.45829 in

Berat isi = #REF! lb/jam

Conical
V3 = 112.2033 ft
Density of = 0.285 lb/in3
= 492.48 lb/ft3
massa con = 55257.881 lb

V2 = 1567.2525 ft
massa sel = 771840.51 lb

Dishead = 100.65848 ft3

massa dis = 49572.287 lb
Total
massa = 876,671 lb
saturator

Desain Leg
P = ΣW
n
(909,820+104830,1684)lb
=
4
P = #REF! lb
Apabila digunalkan I Beam berukuran 3 in, berat 7,5 lb/ft,
maka dari tabel (2-11), didapatkan :
A = 4.29 in2
I(I-I) = 15 in4
r(I-I) = 1.87 in
b = 3.284 in
I(2-2) = 1.7 in
r(2-2) = 0.63 in
h = 5 in

Apabila Leg dipasang dengan beban konsentris :

I = 258.45829
 r(I-I) 1.87
= 138.21299 in

fc = I/r(61-200)
= 18000
1+I2/18000r2
= 18000
(1+(258,458289)2/18000 x (1,87)2)
= 18000
2.0612683
fc = 8732.4875 in

A Perhitungan = P
fc aman
= #REF!
8732.4875
A Perhitungan = #REF! in2

A tersedia = 4.29 in2

A tersedia > A Perhitung(sudah memadahi)

fc aman dengan beban konsentris

fc aman = fc - fc konsentris
fc = 0-60 15000
fc konsent = P x (1,5 + 1/2 x b )
[ I (i-i)/h x (1/2 x b) ]

fc aman = 15,000 - P x (1,5 + 1/2 x b )

[ I (I-I)/h x (1/2 x b) ]
= 15,000 - 8975 x (1,5 + 1/2 x 3,284)
[ 15 /(5 x (1/2 x 3,284)]
= 15,000 - #REF!
1.8270402
= 15,000 - #REF!
fc aman = #REF!

A = P
fc aman
= #REF!
#REF!
 A = #REF! in2
A tersedia = 4.29 in2
A perhitu = #REF! in2
A tersedia > A perhitung( Belum memenuhi )

Desain Lug
Apabila leg dipasang dengan beban konsentris

lhp = hI + 2dbaut = (5+2)in

bhp = bI + 2dbaut = (3,284 + 2)in
hhp = 5/3 x Ihp = (5/3 x 7 in)
ahp = 1/2 Ihp = (1/2 x 7 in )

lhp = 7 in
bhp = 5.284 in
hhp = 11.666667 in
ahp = 3.5 in

β = Akar 3(1 - μ2)

(1/2 d2 x ts2 )
β = 0.0094893 in

M = β3 x t2 x P x C x (1/2d)2
12 ( 1- μ2) bhp - hhp
= #REF!
659.20014
M = #REF! lb in

Tebal horizontal plate dihitung sesuai dengan persamaan (2-75) :

thp = akar 6M
f allowable
thp = #REF! in
#REF! x 16
16
= #REF! ~ 1 1
16 4
in
 tg = 3/8 x thp
tg = 0.09375

PERANCANGAN BASE PLATE

Fondasi dibuat dari dari beton dengan bea 600 psi
600 lb/in2

A base pla = P
fbp in2
= 14.958333

A base pla = lbp*pbp

A base pla = [(0,8*b.lbeam)+2*n]*[(0,95*h.lbeam)+2*n]
14.95833 = 81.472533 *n
n = 5.4466318 in harga n sementara

sehingga
pbp = (0,8*b.lbeam)+2*n
= 15.120464 in
lbp = (0,95*h.lbeam)+2*n
= 21.976597 in

sehingga desain base plate

pbp = 38 in 1444 in2
n = 8.5 in 72.25 in3
m = 10.5375 in in4
lbp = 45 in 2025 in2
tbp = 0.2595363 in 7/8 in

ukuran angker baut

Abaut = 0.1869792 in2 0.2 in2
Dbaut = 0.2110369 in 0.5 in
Jumlah uli = 13 ulir

DESAIN NOZZLE

nozzle dibuat dari pipa sch 40

Q NH3 12 ft3 visc. NH3 0.00677 lb/ft.s
Q H2SO4 1 ft3 visc. H2S 0.017941 lb/ft.s
Q condens 158 ft3 visc. Con 0.0672 lb/ft.s
Q ZA 12 ft3 visc. ZA 1 lb/ft.s
A 2(phi/d)^2
0.162969 ft2
Nre Nh3
Nre H2SO4

Diameter optimal 3,9*Q^0,45*ρ^0,13

Diameter optimal 8 in 1 ft
Diameter optimal 8 in 1 ft
Diameter optimal Z 40 in 3 ft
Diameter optimal C 65 in 5 ft

Pengecekan diamater ketika menghasilkanQ/A

v NH3 76 ft3/jam 0.0211 ft3/detik
v H2SO4 7 ft3/jam 0.0019 ft3/detik
v condens 967 ft3/jam 0.2686 ft3/detik
v ZA 72 ft3/jam 0.0201 ft3/detik

Mencari nilai Nre al(ρ.d.v)/u

Nre NH3 335 <2100
Nre H2SO4 15,555 >2100
Nre condensate ### >2100
Nre ZA 2,642,269 >2100

Dimensi nozzle pada input aliran NH3 dan H2SO4 (dalam in)
d nominal 8 in lebar flan 13.5 in
di 7.98 in tebal flan 0.125 in
do 9*(11/16)in tinggi noz 4 in
6.1875 in

Dimensi nozzle pada input aliran NH3 dan H2SO4 (dalam ft)
d nominal 1 ft lebat flan 1.12455 ft
di 0.664734 ft tebal flan 0.0104125 ft
do 9*(11/16)ft tinggi noz 0.3332 ft
0.515419 ft

Dimensi nozzle pada input aliran Condensate dan ZA (dalam in)

d nominal 24 in lebar flan 32 in
di 23 in tebal flan 0.875 in
do 26(1/8) in tinggi noz 6 in
3.25 in
Dimensi nozzle pada input aliran Condensate dan ZA (dalam ft)
d nominal 2 ft lebat flan 2.6656 ft
di 2 ft tebal flan 0.0728875 ft
do 26(1/8) ft tinggi noz 0.4998 ft
0.270725 ft

Perancangan Manhole
Tinggi Tangki 16.5 ft
Tinggi Tangki max 20 ft
P Saturator 14.7 psia
P equivalen 8.7 psi
Diameter manhole 24 in 1.9992 ft
Tebal shell 0.375 in 0.0312375 ft
Tebal flange 0.25 in 0.020825 ft
 LAMPIRAN G
PERHITUNGAN UNIT PEMISAH DAN PENCAMPURAN

1. Screen (H-148)
Fungsi : Memisahkan produk Amonium Sulfat berdasarkan ukuran
yaitu 30 mesh dan yang tidak sesuai akan dikembalikan ke
mother liquor tank

Rate masuk = 76004.52 kg/jam

= 76.00452 ton/jam
Ukuran produk yang diinginkan = 30 mesh
(Sumber : PT. Petrokimia Gresik)

Standar ukuran screen (sieve clear opening) =

Mesh mm in
28 0.589 0.0232
30 0.542 0.02135
32 0.495 0.0195
(Sumber : Geankoplis A.5-3, hal 998)

Berdasarkan ukuran produk yang diinginkan, maka menggunakan

screen tipe square and slightly rectangular openings

(Sumber : Perry, Tabel 19.7)

Ukuran wire diameter :

Mesh mm in
28 0.318 0.0125
30 0.309 0.01215
32 0.3 0.0118
(Sumber : Geankoplis A.5-3, hal 998)
Pehitungan =

1. Cu = Unit capacity
= 1.8 ton/(h x ft2)
= 0.075001 ton/hari

2. Foa = 100[a/(a+d)]2
= 40.56388

3. Luas screen = 0,4 x Ct

Cu x Foa x Fs
= 0,4 x 76,0045
1,8 x 40,5639 x 1
= 0.4163777105
Keterangan =
Ct = Rate masuk
Cu = Kapasitas screen
Foa = Open area factor
Fs = Slotted area factor (diasumsikan 1)
 (Sumber : Buku Perry)

(Sumber : Perry)

SPESIFIKASI
Jenis ayakan = Square and slightly rectangular openings
Kapasitas ayakan = 76.0045233019 ton/jam
Bukaan ayakan = 30 mesh
Diameter plat = 0.309 mm
Luas ayakan = 0.0387231271 m2
Bahan konstruksi = Carbon steel
Jumlah = 1

2. Screen (H-173)
Fungsi : Memisahkan produk Amonium Sulfat berdasarkan ukuran
yaitu 30 mesh dan yang tidak sesuai akan dikembalikan ke
dissolution drum

Rate masuk = 60512.55 kg/jam

= 60.51255 ton/jam
Ukuran produk yang diinginkan = 30 mesh
(Sumber : PT. Petrokimia Gresik)

Standar ukuran screen (sieve clear opening) =

Mesh mm in
28 0.589 0.0232
30 0.542 0.02135
32 0.495 0.0195
(Sumber : Geankoplis A.5-3, hal 998)
Berdasarkan ukuran produk yang diinginkan, maka menggunakan
screen tipe square and slightly rectangular openings

(Sumber : Perry, Tabel 19.7)

Ukuran wire diameter :

Mesh mm in
28 0.318 0.0125
30 0.309 0.01215
32 0.3 0.0118
(Sumber : Geankoplis A.5-3, hal 998)

Pehitungan =

1. Cu = Unit capacity
= 1.8 ton/(h x ft2)
= 0.075001 ton/hari
2. Foa = 100[a/(a+d)]2
= 40.56388

3. Luas screen = 0,4 x Ct

Cu x Foa x Fs
= 0,4 x 60,5126
1,8 x 40,5639 x 1
= 0.3315076243
Keterangan =
Ct = Rate masuk
Cu = Kapasitas screen
Foa = Open area factor
Fs = Slotted area factor (diasumsikan 1)

(Sumber : Buku Perry)

(Sumber : Perry)

SPESIFIKASI
Jenis ayakan = Square and slightly rectangular openings
Kapasitas ayakan = 60.5125546493 ton/jam
Bukaan ayakan = 30 mesh
Diameter plat = 0.309 mm
Luas ayakan = 0.0308302091 m2
Bahan konstruksi = Carbon steel
Jumlah = 1
 LAMPIRAN G
PERHITUNGAN UNIT PEMISAH DAN PENNCAMPURAN

Kondisi Operasi
T: 120 °C
P: 1 atm
14.7 psig
θ: 4 jam
Vl: 75 %
Material: SA 240 Grade M Type 316
f: 18750
PengelasanDouble Welded but joint
E: 0.8
C (faktor ko 1/16 in
0.0625
LS 1.5 d
sudut 120
tg 120 1.73

m (kg/jam)m (lb/jam) m (kg/jam) m (lb/jam)m (kg/jam)m (lb/jam)

Komponen ρ (lb/ft3)
< 25 > < 22 > <37 >
(NH4)2SO4 29593.64 65,106 5,919 13,021 6963.2096 15319.061 70.5
H2SO4 32383.46 71243.614 6476.69222 14,249 6.9632096 15.319061 114.04
H2O 2817.584 6198.6853 563.516847 1,240 3769.5915 8293.1014 62.4
NH3 0 0 2241.96747 4,932 0 0 0.0445
Sub total 142,548 28,510 23627.481
TOTAL 194,685

V (ft3) V (ft3) V (ft3)

Komponen
< 25 > < 22 > < 37 >
(NH4)2SO4 923 185 217.291646
H2SO4 625 125 0.13433059
H2O 99 20 132.902266
NH3 - 110,839 0
Sub total 1,648 111,168 350.328242
TOTAL 113,166

V total Tangki = V liquid / Volume total liquid

= /0,75
= 75 %
= 113,166 ft3
V total Tangki = m

Mencari ukuran silinder

V total = V1 + V2 + V3
113,166 = (π/24 * d3/tg1/2 ɤ) + (π/4 d2 LS) + (0,0843 d3)
113,166 = (3,14/24*d3/tg1/2 120) + (3,14/4 d2 1,5 d) + (0,0843 d3)
113,166 = (3,14/24*d3/1,73) + (3,14/4 d2 1,5 d) + (0,0843 d3)
113,166 = (0,0756262 d3) + (1,1775 d2) + (0,0843 d3)
113,166 = 1.3374262 d3

d3 = 84,615
d = 43.901802 ft Standarisasi OD
d = 526.82162 in 132 in
d = 13.381269 m 11 ft
Mencari Tinggi Silinder
Ls = 1,5 x d
Ls = 16.5 ft
= 5.0292 m
= 198 in

Mencari Tebal Silinder

ts = Pi x do + C
2 (FE + 0,4 Pi)
= 14,7 x 132 + 0.0625
2 ((18750 x 0,8) + (0,4 x 14,7))
= 0.1271673 in

= 0.1271673 x 16
16
ts = 2.0346772 ~ 3 in
16 16
= 0.1875 in
= 0.015625 ft
= 0.004763 m

Mencari Ketinggian Tutup atas(Dishead)

Ha = 0,169 x d
Ha = 1.859 ft
= 0.5666232 m
 = 22.308 in

Mencari Ketinggian Tutup bawah (dishead)

Hb = 0,169 x d
Hb = 1.859 ft
= 0.5666232 m
= 22.308 in

Mencari Tebal tutup atas ( betuk standary dished head )

tha = 0,885 x Pi x r + C
2 (FE - 0,1 Pi)
= 0,885 x 14,7 x 66 + 0.0625
2 ((18750 x 0,8) - (0,1 x 14,7))
= 858.627 + 0.0625
29997.06
= 0.0911237 in
= 0.0911237 x 16
16
tha = 1.4579793 ~ 3 in
16 16
= 0.1875 in
= 0.015625 ft
= 0.004763 m

Mencari Tebal tutup bawah ( betuk standary dished head )

thb = 0,885 x Pi x r + C
2 (FE - 0,1 Pi)
= 0,885 x 14,7 x 66 + 0.0625
2 ((18750 x 0,8) - (0,1 x 14,7))
= 858.627 + 0.0625
29997.06
= 0.0911237 in
= 0.0911237 x 16
16
thb = 1.4579793 ~ 3 in
16 16
= 0.1875 in
= 0.015625 ft
= 0.004763 m
 LS = 16.5 ft
198 in
5.0292 m
Ha = 1.859 ft
22.308 in
0.5666232 m
Hb = 1.859 ft
22.308 in
0.5666232 m
ts = 0.015625 ft
0.1875 in
0.0047625 m
tha = 0.015625 ft
0.1875 in
0.0047625 m
thb = 0.015625 ft
0.1875 in
0.0047625 m

PERANCANGAN SABUK PENGAMAN

Asumsi :
Sabuk
= 2
Pengaman
Tipe = Chanel
Ukuran = 3 in
Berat = 6 lb/ft
P = 14.7 psig
T = 70 C
= 158 F

Trial ts 7/16
ts = 7 = 0.4375
16
Harga DO = 132(2 x 3/16)
Harga DO = 132.375 in

LI = Ls
 n+1
= 198
2+1
LI = 66

LI = 66
do 132.375
= 0.4985836

do = 132.375
ts 4/9
= 302 4/7

T 158 ~ 200 F
nilai B lihat grafik
B = 4500
B = Pallowabel x do
ts
4500 = Pallowabel x 132.375
0.4375
4500 = Pallowabel x 302.5714
Pallowabel = 4500
302.57143
Pallowabel = 14.872521

Pallowabel > Pkenyataan

14.872521 > 14.7 (sudah memenuhi)

%delp = Pallowabel - Pi x 100%

Pi
= 14.872521 - 14.7 x 100%
14.7
%delp = 1.1736139 %

%delp < 20% ( sudah memenuhi)

PERANCANGAN PENYANGGA

Ha = 22.308 in
Hb = 22.308 in
 LS = 198 in
Asumsi:
Penyangga = 4
Tipe = I Beam
berat = 14.75 lb/ft
ukuran = 5 in
berat total beserta isi = 1,077,042 lb
berat tutup atas dan bawah = 827098.392 lb

Tinggi total (I) = 242.616 in

Berat Isi = 194,685

Dised head
V3 = 112.2033 ft
Density of s = 0.285 lb/in3
= 492.48 lb/ft3
massa = 55257.881 lb

V2 = 1567.2525 ft
massa selim = 771840.51 lb

V3 Dished head
massa dish = 55257.881 lb
Total
massa = 882,356 lb
saturator

Desain Leg
P = ΣW
n
(55257,88+771840,5)lb
=
4
P = 476,035 lb
Apabila digunalkan I Beam berukuran 3 in, berat 7,5 lb/ft,
maka dari tabel (2-11), didapatkan :
A = 4.29 in2
I(I-I) = 15 in4
r(I-I) = 1.87 in
b = 3.284 in
I(2-2) = 1.7 in
r(2-2) = 0.63 in
h = 5 in
 Apabila Leg dipasang dengan beban konsentris :
I = 242.616
r(I-I) 1.87
= 129.74118 in

fc = I/r(61-200)
= 18000
1+I2/18000r2
= 18000
(1+(246,616)2/18000 x (1,87)2)
= 18000
1.935154
fc = 9301.5851 in

A Perhitungan = P
fc aman
= 476035
9301.5851
A Perhitungan = 51.17784 in2

A tersedia = 4.29 in2

A tersedia > A Perhitung(sudah memadahi)

fc aman dengan beban konsentris

fc aman = fc - fc konsentris
fc = 0-60 15000
fc konsentr = P x (1,5 + 1/2 x b )
[ I (i-i)/h x (1/2 x b) ]

fc aman = 15,000 - P x (1,5 + 1/2 x b )

[ I (I-I)/h x (1/2 x b) ]
= 15,000 - 8975 x (1,5 + 1/2 x 3,284)
[ 15 /(5 x (1/2 x 3,284)]
= 15,000 - 1495702
1.82704
= 15,000 - 818647.6
fc aman = -803,648

A = P
 fc aman
= 476035
-803,648
A = -0.592343 in2
A tersedia = 4.29 in2
A perhitun = -0.592343 in2
A tersedia > A perhitung( Belum memenuhi )