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Feed (F = 100 mol/h) at boiling point at 303.9 kPa. With xFA = 0,4, xFB = 0,25, xFC = 0,20 and
xFD = 0,15 where components A = n-butane, B = n-pentane, C = n-hexane and D = n-heptane,
will be separate in a column. 80% of B is recovered in the distillate and 80% of C in the bottoms.
Calculate:
(a) D and W moles/h
(b) Temperature of feed, dew point of distillate and boiling point of bottoms
(c) Minimum stages for total reflux and distribution of other components in the distillate and bottom
(d) N theoretic , Ne & Ns if R= 1.2 Rmin
Penyelesaian:
a. Menentukan D dan W
No Komponen Xf F Xf*F Yd*D
1 A(LNK) 0.4 100 40 40
2 B(LK) 0.25 100 25 20
3 C(HK) 0.2 100 20 4
4 D(HNK) 0.15 100 15 0
∑ 100 64
b. 1. Menentukan Dew Point
P= 303.9 kPa= 2.9993 atm= 2279.4375
T= 332.8307 K
No Komponen Yd In Pi Pi K=Pi/P
1 Butana 0.625 8.4569 4707.6506 2.0653
2 Pentana(LK) 0.3125 7.3760 1597.1584 0.7007
3 Hexana(HK) 0.0625 6.3399 566.7283 0.2486
4 Heptana 0 5.3377 208.0299 0.0913
∑
Data Antoine
Komponen A B C
Butana 15.6782 2154.9 -34.42
Pentana(LK) 15.8333 2477.07 -39.94
Hexana(HK) 15.8366 2697.55 -48.78
Heptana 15.8737 2911.32 -56.51
c. 1. Stage Minimum
1. Dew Point
No Komponen Yd K,d αd
1 Butana 0.625 2.0653 8.3067
2 Pentana(LK) 0.3125 0.7007 2.8182
3 Hexana(HK) 0.0625 0.2486 1.0000
4 Heptana 0 0.0913 0.3671
Dik: D= 64
Xld= 0.3125
Xhd= 0.0625
Xhw= 0.4444
Xlw= 0.1389
W= 36
No Komponen (αi*Xid)/(αi-θ)
1 Butana 0.7710
2 Pentana(LK) 0.6650
3 Hexana(HK) -0.3021
4 Heptana -0.0017
∑ 1.1321
Rm+1= 1.1321
Rmin= 0.1321
TUGAS MULTI-COMPONENT DISTIL
Yd Xw*W Xw
0.625 0 0
0.3125 5 0.1389
0.0625 16 0.4444
0 15 0.4167
36
2.Menentukan Bubble Point
mmHg P= 2279.4375 mmHg
T= 383.5584 K
xi=yi/ki No Komponen Xw In Pi Pi
0.3026 1 Butana 0 9.5061 13442.1378
0.4460 2 Pentana(LK) 0.1389 8.6245 5566.4854
0.2514 3 Hexana(HK) 0.4444 7.7789 2389.6034
0.0000 4 Heptana 0.4167 6.9719 1066.2459
1.0000 ∑
2.Bubble Point
No Komponen Xw K,w αw
1 Butana 0 5.8971 5.6253
2 Pentana(LK) 0.1389 2.4420 2.3295
3 Hexana(HK) 0.4444 1.0483 1.0000
4 Heptana 0.4167 0.4678 0.4462
g distribusi HNK
Xdw
Xw Xw*W
0.0152 0.5472155036
0.1389 5
0.4444 16
0.4095 14.7436382637
36
θ= 1.2069
Data Antoine
Pi K=Pi/P αi=Ki/KHK (αi*Xif)/(αi-θ) Komponen A
8288.6576 3.6363 6.0217 0.5003 Butana 15.6782
3133.8027 1.3748 2.2767 0.5320 Pentana(LK) 15.8333
1376.4660 0.6039 1.0000 -0.9669 Hexana(HK) 15.8364
504.4598 0.2213 0.3665 -0.0654 Heptana 15.8737
0.0000
T DISTILATION
d. Menentukan Ne dan Ns
Dik: R=1,2Rmin
Maka:
R= 0.1585
R/(R+1)= 0.1368
Rmin/(Rmin+1)= 0.1167
N= 11
Ne+Ns= 11
Log(Ne/Ns)= 0,206 log ((Xhf/Xlf)*(W/D)(X
log(Ne/Ns)= 0.0714
Ne/Ns= 1.1788
Ne= 1.1788
Ne+Ns= 11
1,1788Ns+Ns= 11
2,1788 Ns= 11
Ns= 5.0487
Ne= 1.1788
Ne= 5.9513
feed tray= 5.9513
B C
2154.9 -34.42
2477.07 -39.94
2687.55 -46.02
2911.32 -56.51
engan data:
theorical stages
theorical stages
Xd Xiw
0.6164 0.0152
0.3125 0.1389
0.0625 0.4444
0.0040 0.4095
theorical stages
theorical stages
6 log ((Xhf/Xlf)*(W/D)(Xlw/Xhd)^2))
Ns
Ns