Professional Documents
Culture Documents
(Reaffirmed 2004)
Edition 2.2
(2007-08)
Indian Standard
CONCRETE ADMIXTURES — SPECIFICATION
( First Revision )
(Incorporating Amendment Nos. 1 & 2)
ICS 91.100.30
© BIS 2008
Price Group 7
Cement and Concrete Sectional Committee, CED 2
FOREWORD
This Indian Standard (First Revision) was adopted by the Bureau of Indian Standards, after the
draft finalized by the Cement and Concrete Sectional Committee had been approved by the Civil
Engineering Division Council.
Admixtures are materials added to the concrete before or during its mixing, with a view to
modifying one or more of the properties of concrete in the plastic or hardened state. An important
feature of the majority of admixtures for concrete is that it is difficult to quantitatively evaluate
the behaviour of the concrete under various possible circumstances. Therefore, performance of an
admixture is evaluated by comparing the properties of concrete with the admixture under test
with those of concrete without any admixture or with a reference admixture. This standard lays
down the procedure for such a relative evaluation of admixtures for concrete.
In recent time there has been a lot of development in the field of admixtures. Superplasticizers,
both normal and retarding type, constitute a major group of admixtures used by site engineers
now. Superplasticizers help in lowering the water/cement ratio so as to contribute to the
enhancement of durability. In this first revision of the standard, first published in 1979,
requirements of superplasticizers in detail and methods of determination of flow of concrete of
high workability have been added.
This standard also gives uniformity tests which demonstrate that a particular consignment is
similar to material that has previously been submitted to the acceptance test.
The admixtures covered in this standard are intended mainly for modifying a single property in
concrete, but some of the admixtures available in the market are often capable of modifying more
than one property of the concrete. In addition, an admixture may be used to improve the desirable
properties of concrete in more than one way. For example, water reducing admixtures ( see 3.4 )
may be used to improve the workability of concrete with the same water and cement contents, to
increase the compressive strength without changing the workability by reduction of the water
content in the concrete mix or to effect saving in cement content by reduction in both the cement
and water contents in the mix while maintaining the same workability and compressive strength
as in the reference concrete. In such cases, the procedure of evaluation of the admixture may have
to be appropriately chosen. This standard also provided for evaluation of admixtures for specific
use with the materials and mix proportions to be used on the work.
The performance of concrete admixtures including superplasticizers depend upon both the
admixtures and the cement and their compatibility, in addition to the concrete mix proportions and
the environmental conditions in the field. Among the characteristics of the cement, which affect the
performance of concrete admixtures including superplasticizers are the C3A, SO3 and alkali contents,
nature of sulphates, and the fineness. The ambient temperature and humidity conditions influence
the performance of set-controlling admixtures and affect the retention of enhanced workability
(slump loss) when water-reducing admixtures and superplasticizers are used. While no
generalisation of these effects is possible, it is nevertheless necessary to evaluate concrete admixtures
for specific use with the concrete-making materials and mix proportions to be used on the work, under
field conditions. This standard also provides for such specific evaluation of an admixture, in addition
to the general evaluation for conformity to the requirements of this standard.
The requirements of integral waterproofing admixtures are covered in IS 2645 : 1975
‘Specification for integral cement waterproofing compounds ( first revision )’.
This edition 2.2 incorporates Amendment No. 1 (January 2003) and Amendment No. 2 (August 2007).
Side bar indicates modification of the text as the result of incorporation of the amendments.
For the purpose of deciding whether a particular requirement of this standard is complied with,
the final value, observed or calculated, expressing the result of a test or analysis, shall be rounded
off in accordance with IS 2 : 1960 ‘Rules for rounding off numerical values ( revised )’. The number
of significant places retained in the rounded off value should be the same as that of the specified
value in this standard.
IS 9103 : 1999
Indian Standard
CONCRETE ADMIXTURES — SPECIFICATION
( First Revision )
1 SCOPE 3.2 Accelerating Admixture or Accelerator
1.1 This standard covers the chemical An admixture when added to concrete, mortar
and air-entraining admixtures including or grout, increases the rate of hydration of a
superplasticizers, solid or liquid or emulsion, to hydraulic cement, shortens the time of set, or
be added to cement concrete at the time of increases the rate of hardening or strength
mixing so as to achieve the desired property in development.
concrete, in the plastic or hardened state.
3.3 Retarding Admixture or Retarder
1.2 The different types of admixtures covered
in this standard are as follows: An admixture which delays the setting of
cement paste, and hence of mixtures, such as
a) Accelerating admixtures, mortar or concrete containing cement.
b) Retarding Admixtures,
c) Water-reducing admixtures, 3.4 Water Reducing Admixture or
d) Air-entraining admixtures, and Workability Aid
e) Superplasticizing admixtures. An admixture which either increases
1.3 The chloride content in the admixture shall be workability of freshly mixed mortar or concrete
declared by the manufacturer. Superplasticizers without increasing water content or maintains
are expected to be chloride free. workability with a reduced amount of water.
1.3.1 Admixtures that contain relatively large 3.5 Air-Entraining Admixtures
amounts of chloride may accelerate corrosion of An admixture for concrete or mortar which
prestressing steel. Where corrosion of such causes air to be incorporated in the form of
steel is of major concern, compliance with the minute bubbles in the concrete or mortar
requirement of this specification does not during mixing, usually to increase workability
constitute assurance of acceptability of the
and resistance to freezing and thawing and
admixture for use in prestressed concrete. In
disruptive action of de-icing salts.
case of reinforced concrete, to minimize the
chances of deterioration of concrete, the total 3.6 Superplasticizing Admixtures
chloride content in the concrete should be An admixture for mortar or concrete which
limited as specified in IS 456. imparts very high workability or allows a large
2 NORMATIVE REFERENCES decrease in water content for a given workability.
The Indian Standards listed in Annex A 3.7 Retarding Superplasticizing Admixture
contain provisions which, through reference in Superplasticizing admixture that imparts
this text, constitute provision of this standard. prolonged workability retention and retards
At the time of publication the editions indicated setting.
were valid. All standards are subject to
revision, and parties to agreement based on 4 REQUIREMENTS FOR ADMIXTURES
this standard are encouraged to investigate the Concrete made with admixtures when
possibility of applying the most recent edition compared with identical concrete made without
of the standards indicated in Annex A. the admixture in accordance with 7 and 8 shall
3 TERMINOLOGY conform to the requirements appropriate to the
type of admixture given in Table 1A and Table
3.0 For the purpose of this standard, the 1B, except in the case of air-entraining
following definitions shall apply. admixture. In the case of air-entraining
3.1 Admixtures admixtures, a reference admixture of approved
A material other than water, aggregates, and quality shall be used in the control concrete to
hydraulic cement and additives like pozzolana entrain identical amount of air.
or slag and fibre reinforcement used as an NOTE — If required by the purchaser, the concrete with
ingredient of concrete or mortar and added to air-entraining admixture may be tested for resistance to
freezing and thawing in accordance with the procedure
the batch immediately before or during its given in Annex B, in such case the relative durability
mixing to modify one or more of the properties factor of the concrete with admixture under test shall be
of concrete in the plastic or hardened state. not less than 80.
1
IS 9103 : 1999
Normal Retarding Type
Initial
Max –3 +3 ±1 — + 1.5 +4
Min –1 +1 — — — +1
Final
Max –2 +3 ±1 — ± 1.5 +3
Min –1 +1 — — — —
1 day — — — — 140 —
3 days 125 90 110 90 125 125
7 days 100 90 110 90 125 125
28 days 100 90 110 90 115 115
6 months 90 90 100 90 100 100
1 year 90 90 100 90 100 100
v) Flexural strength, 8.2.2
percent of control
sample, Min
2
IS 9103 : 1999
Normal Retarding Type
(1) (2) (3) (4) (5)
i) Flow 510 mm - 620 mm 510 mm - 620 mm 7.2.1.1
ii) Loss of workability on standing At 45 min the slump shall be At 2 h the slump shall be 7.2.1.2
not less than that of control not less than that of control
mix concrete at 15 min mix concrete at 15 min
iii) Minimum compressive strength, 8.2.1
percent of control mix concrete
7 days 90 90
28 days 90 90
6 months 90 90
1 year 90 90
3
IS 9103 : 1999
4
IS 9103 : 1999
5
IS 9103 : 1999
c) The chloride ion content relative to the manufacture) and aggregates (quarry or
cement mass contributed by the pit or for material dredged from seas,
recommended dosage or dosages expressed estuaries or river the locality);
as percentage by mass of chloride ion; b) The quantity of admixture used in the
d) Recommended storage conditions, test mix concretes;
maximum storage time before use and c) The values of slump, w/c ratio and cement
necessary safety precautions, for content for each batch of the control and
example, toxic or corrosive; test mix concretes; and
e) Any known incompatibility with other d) The air content of each batch of the
admixture or with certain types of cement control and test mix concrete.
etc;
f) The recommended dosage or dosages; 11 BIS Certification Marking
g) The effect of underdosage and The product may also be marked with Standard
overdosages; and Mark.
h) Expiry date. 11.1 The use of Standard Mark is governed by
10.3 Information Concerning the the provisions of Bureau of Indian Standards
Admixture Acceptance Test Act, 1986 and the Rules and Regulations made
thereunder. The details of conditions under
The following information shall be provided by which the licence for the use of Standard Mark
the manufacturer in a printed form, if may be granted to manufacturers or producers
requested: may be obtained from the Bureau of Indian
a) The source of cement (works of Standards.
ANNEX A
( Clause 2 )
6
IS 9103 : 1999
ANNEX B
( Note under Clause 4 )
ANNEX C
( Clause 7.2.1.1 )
C-0 This method covers determination of the Diameter of the base : 200 ± 2 mm
flow of fresh mixed superplasticized concrete of Diameter of top : 130 ± 2 mm
high workability. Height : 200 ± 2 mm
The slump cone shall be provided with two
C-1 APPARATUS
metal foot pieces at the bottom and two handles
at the top.
C-1.1 The Slump Cone
C-1.2 Tamping Bar
The slump cone for receiving the freshly mixed The tamping bar shall be made of hardwood
concrete shall consist of a frustrum of cone of and having a 40 mm × 40 mm section of length
minimum thickness of 1.5 mm metal, with the 200 mm, with a circular section to form a
following internal dimensions: handle to the bar.
7
IS 9103 : 1999
ANNEX D
( Clause 7.2.4 )
9
IS 9103 : 1999
ANNEX E
( Clause 10.1 )
E-1 DRY MATERIAL CONTENT temperature. Stopper the weighing bottle and
The dry material content in the liquid or weigh to nearest 0.001 g. Again place the bottle
non-liquid samples shall be determined and stopper in the oven for one hour and repeat
according to the following procedures. the drying and the weighing etc. The weight
should become constant.
E-1.1 Liquid Admixture
Calculation:
Place 25 to 30 g of preheated, completely dry
sand in a wide mouth glass weighing bottle (60 Find the weight of sample and the dried
mm dia, 30 mm height) provided with ground residue.
glass stopper. Place the bottle with sand and Weight of bottle and sand = W1
stopper in the electric oven and dry for 17 ± 1/4 Weight of bottle, sand and = W2
h at 105 ± 2ºC. (The period of drying may be sample
shortened if sand is already dry.) Transfer the
bottle with stopper to a desiccator and allow to Weight of sample = W2 – W1
cool to room temperature and weigh nearest to Weight of bottle, sand and = W3
0.001 g. Remove the stopper and with the help dried residue
of a pipette evenly distribute 4 ml of the liquid
Weight of dried residue = W3 – W1
over the sand. Insert the stopper and place the
bottle and stopper in the oven. Dry for 17 + 1/4 W3 – W1
h at 105 ± 2ºC. At the end of the drying period Percent residue on drying = ------------------------- × 100
transfer to a desiccator, cool to room W2 – W1
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IS 9103 : 1999
11
IS 9103 : 1999
ANNEX F
( Foreword )
COMMITTEE COMPOSITION
Cement and Concrete Sectional Committee, CED 2
Chairman
DR H. C. VISVESVARYA
Chandrika, 63-64 East Park Road, Malleswaram, Bangalore 560003
Members Representing
( Continued on page 13 )
12
IS 9103 : 1999
Members Representing
SHRI PRAFULLA KUMAR Ministry of Transport, Department of Surface Transport, Roads
Wing, New Delhi
SHRI P. P. NAIR ( Alternate )
MEMBER SECRETARY Central Board of Irrigation and Power, New Delhi
DIRECTOR (CIVIL) ( Alternate )
SHRI SUDESH DHIMAN, CE Engineer-in-Chief’s Branch, Army Headquarters, New Delhi
SHRI DINESH SIKAND, ADDITIONAL CE ( Alternate )
SHRI Y. R. PHULL Central Road Research Institute (CSIR), New Delhi
SHRI S. S. SEEHRA ( Alternate )
SHRI Y. R. PHULL Indian Roads Congress, New Delhi
SHRI A. K. SHARMA ( Alternate )
DR C. RAJKUMAR National Council for Cement and Building Materials, New Delhi
DR K. MOHAN ( Alternate )
SHRI G. RAMDAS Directorate General of Supplies and Disposals, New Delhi
SHRI R. C. SHARMA ( Alternate )
SHRI S. A. REDDI Gammon India Ltd, Mumbai
REPRESENTATIVE Builder’s Association of India, Mumbai
SHRI J. S. SANGANERIA Geological Survey of India, Calcutta
SHRI L. N. AGARWAL ( Alternate )
SHRI S. B. SURI Central Soil and Materials Research Station, New Delhi
SHRI N. CHANDRASEKARAN ( Alternate )
SUPERINTENDING ENGINEER (DESIGN) Public Works Department, Government of Tamil Nadu, Chennai
EXECUTIVE ENGINEER (S. M. R. DIVISION) ( Alternate )
SHRI A. K. CHADHA Hindustan Prefab Ltd, New Delhi
SHRI J. R. SIL( Alternate )
DR H. C. VISVESVARAYA The Institution of Engineers (India), Calcutta
SHRI D. C. CHATURVEDI ( Alternate )
SHRI VINOD KUMAR, Director General, BIS ( Ex-officio Member )
Director (Civ Engg)
Member-Secretary
SHRI J. K. PRASAD
Additional Director (Civ Engg), BIS
Convener
DR A. K. MULLICK National Council for Cement and Building Materials, New Delhi
Members
SHRI C. R. ALIMCHANDANI Stup Consultants Ltd, Mumbai
SHRI S. RANGARAJAN ( Alternate )
DR P. C. CHOWDHARY Torsteel Research Foundation in India, Calcutta
DR C. S. VISHWANATH ( Alternate )
SHRI J. P. DESAI Gujarat Ambuja Cement Ltd, Ahmedabad
SHRI B. K. JAGETIA ( Alternate )
DIRECTOR Central Soil Materials Research Station, New Delhi
SHRI N. CHANDRASEKARAN ( Alternate )
JOINT DIRECTOR STANDARDS (B&S)/CB-II Research, Designs and Standards Organization, Lucknow
JOINT DIRECTOR STANDARDS (B&S)/CB-I ( Alternate )
( Continued on page 14 )
13
IS 9103 : 1999
Members Representing
SUPERINTENDING ENGINEER (DESIGNS) Central Public Works Department, New Delhi
EXECUTIVE ENGINEER (DESIGNS) ( Alternate )
SHRI V. K. GHANEKAR Structural Engineering Research Centre, Ghaziabad
SHRI D. S. PRAKASH RAO ( Alternate )
SHRI S. K. GUHA THAKURTA Gannon Dunkerley and Co Ltd, Mumbai
SHRI S. P. SANKARANARAYANAN ( Alternate )
SHRI J. S. HINGORANI Associated Consulting Services, Mumbai
SHRI A. P. REMEDIOS ( Alternate )
SHRI LALIT KUMAR JAIN In personal capacity ( Consulting Structural Engineer 36, Old
Sneh Nagar, Wardha Road, Nagpur 440015 )
SHRI M. P. JAISINGH Central Building Research Institute (CSIR), Roorkee
SHRI B. KAMESWARA RAO ( Alternate )
CHIEF ENGINEER & JOINT SECRETARY Public Works Department, Mumbai
SUPERINTENDING ENGINEER ( Alternate )
PROF S. KRISHNAMOORTHY Indian Institute of Technology, New Delhi
SHRI K. K. NAYAR ( Alternate )
DR S. C. MAITI National Council for Cement and Building Materials, New Delhi
MANAGING DIRECTOR Hindustan Prefab Ltd, New Delhi
SHRI M. KUNDU ( Alternate )
SHRI M. K. MUKHERJEE Ministry of Transport (Roads Wing), New Delhi
SHRI N. K. SINHA ( Alternate )
SHRI B. V. B. PAL The Associated Cement Co Ltd, Mumbai
SHRI M. G. DANDAVATE ( Alternate )
SHRI A. B. PHADKE The Hindustan Construction Co Ltd, Mumbai
SHRI D. M. SAVUR ( Alternate )
SHRI Y. R. PHULL Central Road Research Institute, New Delhi
SHRI S. S. SEEHRA ( Alternate I )
SHRI SATENDER KUMAR ( Alternate II )
SHRI A. S. PRASAD RAO Structural Engineering Research Centre (CSIR), Chennai
SHRI K. MANI ( Alternate )
SHRI K. L. PRUTHI National Building and Construction Corporation Ltd, New Delhi
SHRI J. R. GABRIEL ( Alternate )
SHRI B. D. RAHALKER Nuclear Power Corporation, Mumbai
SHRI U. S. P. VERMA ( Alternate )
SHRI HANUMENTHA RAO A. P. Engineering Research Laboratories, Hyderabad
SHRI G. RAMAKRISHNEN ( Alternate )
SHRI S. A. REDDI Gammon India Ltd, Mumbai
DR N. V. NAYAK ( Alternate )
SHRI S. C. SAWHNEY Engineers India Ltd, New Delhi
SHRI R. P. MEHROTRA ( Alternate )
SHRI J. R. SHARMA Army Headquarters, Engineer-in-Chief’s Branch, New Delhi
SHRI SURINDER MOHAN ( Alternate )
PROF M. S. SHETTY Indian Concrete Institute, Chennai
SHRI B. T. UNWALLA In personal capacity ( 15/9, Rustam Baug, Victoria Road,
Mumbai 400027 )
DIRECTOR (C&MDD) Central Water Commission, New Delhi
DEPUTY DIRECTOR (C&MDD) ( Alternate )
14
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harmonious development of the activities of standardization, marking and quality certification of goods and
attending to connected matters in the country.
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Enquiries relating to copyright be addressed to the Director (Publications), BIS.