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Lab Manuals 2CH403 IPC Jan 2020 PDF
Lab Manuals 2CH403 IPC Jan 2020 PDF
Laboratory Manual
Jan 2020
2CH403 - Instrumentation and Process Control
Chemical Engineering Department
SoE, IT-NU
List of Experiment
Sr. No. Objective
1. Study of dynamic characteristics (speed of response) of instrument
(thermometer).
2. To study resistance temperature detector (RTD) and calibrate it.
10. To study response of multi capacity (non - interacting tanks in series) system
to step input.
11. To study response of multi capacity (interacting tanks in series) system to step
input.
12. To study response of second order (u-tube manometer) system to step input.
Apparatus: 250 ml glass beakers, Mercury thermometer, CCl4 thermometer & Stop watch.
Procedure:
1. Take 250 ml water in a glass beaker, put it on a hot plate & heat the water up to 100 0C.
Dip the given thermometers in the beaker and wait till the thermometer indicates
1000C. Note down the time taken by the thermometers for the change.
2. Take out the thermometers from water beaker and allow it to cool up to room
temperature. Note down the time required for it.
3. Take 250 ml Oil in a glass beaker, put it on a hot plate & heat the oil up to 1200C. Dip
the given thermometers in the beaker and wait till the thermometers indicates 1200C.
Note down the time taken by the thermometers for the change.
4. Take out the thermometers from oil beaker and allow it to cool up to room temperature.
Note down the time required for it.
5. Repeat the same procedure with water for two different temperatures (700C and 600C).
6. Repeat the above procedure with for two different temperatures (90 0C and 800C).
Observation Table:
0
Room temperature: _____________ C
Thermometer type: _________&_________
CONCLUSION:
________________________________________________________________________________
________________________________________________________________________________
________________________________________________________
QUIZ:
Marks: Signature:
2CH403 - Instrumentation and Process Control
Chemical Engineering Department
SoE, IT-NU
Apparatus: Resistance temperature detector, thermometer, 250 ml glass beaker, heating mental, stop
watch, resistance measuring element
Theory:
RTDs are among the most accurate, reproducible, stable, and available thermal elements. A metal
resistance element changes its resistance with temperature. Resistance thermometry is based upon the
increasing electrical resistance of conductors with increasing temperature. Pure elements have been
used for measurement of temperature by this effect and the method is one of the most accurate ones.
The relation between the resistance and change in temprrature is expressed by the following equation.
Rt = Ro [ 1 + T + T2 + T3 + ............]
Where , , ...... Are temp. Coefficient of resistance. In the narrow ranges of operation
and higher order coefficients are negligibly small so that Rt is given by
Rt = Ro [1 + T]
is positive for a metal resistance element. The commonly used metals are platinum, copper and
nickel. All RTDs require the following consideration in their manufacture. Wire wound sensors must
be supported on materials closely matching the wire in thermal expansion to minimize strain effects.
Additional assembly materials, such as cements should not introduce additional strain in the operating
temp. range. The final assembly must be stable. Only high purity materials and clean assembly method
should be used to avoid sources of contamination. The choice of material will be governed by (a) High
temperature coefficient. (b) High resistivity of the material. (c) Linearity of relation between
resistance and temperature.(d) Stability of the electrical characteristics of the material and resistance
to contamination.
Normally used metal in RTD is Pt. Generally Pt100 is a very common RTD. In this 100 indicates the
resistance of Pt wire is 100 at 0 0C.Certain RTD. are constructed having the resistance element
exposed, such as anemometory experiments, most are constructed so that fine wire element is coiled
and loosely supported on mica form. The coil is annealed and is then placed in a protective sheath.
Extra care is taken to fabricate the element so that the effects of mechanical shock are minimised.
After its end wire are connected, it is fixed in place with varnish or the other encapsulating material.
The entire sheath is often hermetically sealed, a fill material such as magnesium oxide or aluminium
oxide being included. A Mechanically fitting is usually attached to the sheath. This is often
2CH403 - Instrumentation and Process Control
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accomplished with an attached electrical terminal block or sometimes with a loading spring which
gives the tip of the sheath positive contact with its thermowell. This also prevents vibration. The low
thermal mass of these electrical resistance thermometers provides excellent response.
Procedure:
1. Clean the glass beaker with water and fill it with water/oil up to half of the volume.
2. Put the glass beaker on the heating mental, start heater and raise the temperature of water/oil
and wait till it reach at steady state temperature.
3. Join the RTD with resistance measuring element and insert RTD into the glass beaker.
4. For each five degree temperature rise in water/oil note down the temperature indicated by
temperature indicator and resistance by resistance measuring element simultaneously in the
observation table.
Observation table:
Sr. Temperature, Resistance, Sr. Temperature, Resistance,
No. deg. C. ohm. No. deg. C. ohm.
1. 10.
2. 11.
3. 12.
4. 13.
5. 14.
6. 15.
7. 16.
8. 17.
9. 18.
Calculations :
Rt = Ro [ 1 + T]
Where, = temp. Coefficient of resistance
Rt = resistance at any temperature
Ro = intercept of the graph
[ 1 + T] = Rt/ Ro
T = [Rt/ Ro ] -1
= {[ Rt/ Ro ] -1}/ T
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Graph: Draw plot of resistance verses temperature and find value of and R0 from graph. R0 is
intercept on Y axis at T = 0. Slop of the graph is R0.
Note: Draw graph from 0 °C on X axis. Do not kink X axis.
Compare with standard graph of PT100 RTD.
Results:
Experimental Graphical
Co-efficient ()
resistance (Ro)
Conclusion :
_______________________________________________________________________________
_______________________________________________________________________________
_______________________________________________________________________________
Quiz:
1. Explain difference between SPRT and PT 100 RTD.
2. Write brief note about different types of RTD.
3. State advantages & disadvantages of RTD.
4. What is difference between 2-wire, 3- wire and 4- wire RTDs?
Marks: Signature:
2CH403 - Instrumentation and Process Control
Chemical Engineering Department
SoE, IT-NU
STUDY OF THERMOCOUPLE
Objectives: To study thermocouple and calibrate it.
Apparatus: Thermocouple (J type), thermometer, 250 ml glass beaker, heating mental, stop watch,
milivoltmeter.
Materials: Water/oil.
Theory:
The salient features of the thermocouple are:
Two dissimilar conductors in the form of rod or wire electrically insulated except at the hot
junction.
A refractory sheath to afford protection from injurious furnace gases. Another metal sheath
may also be used to prevent mechanical damage.
Cold junction temperature Control.
An instrument for measuring e.m.f., either a milivoltmeter or for more accurate measurement
a potentiometer system.
Compensating leads to allow the measuring instrument to be sited at considerable distance
from the thermocouple without the necessity for using expensive couple materials as extension
leads.
Thermocouples are low-cost, small convenient, wide range, reasonably stable, accurate and fast.
They are used for measuring high temp. as well as low temp. Thermocouple provides an accurate
and reliable indication of temperature for many kinds of industrial application. Imparting heat to
the junction of two dissimilar metals causes a small continuous e.m.f to be generated. Seebeck
discovered these phenomena in 1821; the thermal e.m.f is produced in a thermocouple. Electric
circuit when the temp. at the two junctions are different. Based on this the thermocouples are
constructed. An ordinary thermocouple consists of two different kinds of wires, each of which
must be made of a homogeneous metal or alloy. The wires are fastened together at one end to form
a measuring junction. The free ends of the two wires are connected to the measuring instrument
to form a closed path in which current flow. After the thermocouple wires connect to the measuring
instrument, the junction is designated as reference junction and it is maintained at constant temp.
It is most important that each section of wire in a given circuit be homogeneous, since, with no
change in the composition or physical properties along its length, the circuit emf depends only
upon the metals employed and the junction temp., circuit emf are independent of both length and
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dia. of wires as well as the method by which the junction is made, it may be welded, soldered,
twisted or an intimate contact
2) Precision of calibration.
3) Resistance to corrosion and oxidation.
4) Linear relation of emf to temp. so that scale is more easily read.
In order to protect them the thermocouple wire, it is usually covered by thermal insulation (e.g.
ceramic) and a sheath for mechanical protection (e.g. thermo-well)
Procedure:
1. Clean the 250 ml glass beaker with water and fill the beaker with water up to half of the
volume.
2. Put the glass beaker on the heater, start heater and raise the temperature of water and wait for
the steady state (850 c) to reach.
3. Join the thermocouple with mill voltmeter and insert thermocouple into the glass beaker.
4. For each 50C temperature rise in water note down the temperature indicated by thermometer
and mV indicated by milivoltmeter simultaneously table.
Observation Table:
Sr. Temperature, Milivolt meter Sr. Temperature, Milivolt meter
No. deg. C. reading(mv) No. deg. C. reading(mv)
1. 10.
2. 11.
3. 12.
4. 13.
5. 14.
6. 15.
7. 16.
8. 17.
9. 18.
Graph: Draw a graph of mV versus Temp. Compare the graph with the standard curve of “J”
type thermocouple.
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CONCLUSION:
________________________________________________________________________________
________________________________________________________________________________
_______________________________________________________________________
QUIZ:
1. Explain principle of thermocouple.
2. Give example of industrial applications of thermocouple.
3. Give name of five thermocouples with their temperature range.
4. Write about see back effect.
Procedure:
1. Clean the glass beaker with water and fill it with water up to half of the volume.
2. Put the glass beaker on the heater, start heater and raise the temperature of water and wait
steady state to reach.
3. Join the thermistor with resistance measuring element and insert thermistor into the glass
beaker.
4. For each five degree temp. rise in water note down the temp. by temp. indicator and resistance-
by-resistance measuring element simultaneously in the observation table.
Observations:
Observation Table:
Positive Thermistor
Sr. Temperature Temperature Resistance, ln Rt ( 1/T0 ) – ( 1/Tx )
o
No. C K ohm.
Rt, (+Ve type)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Negative Thermistor
Sr. Temperature Temperature Resistance, ln Rt ( 1/T0 ) – ( 1/Tx )
o
No. C K ohm.
Rt, (-Ve type)
1
2
3
4
5
6
7
8
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9
10
11
12
13
14
15
Graph:
Plot graph of ln Rt versus (1/T0) – (1/Tx )
Draw straight line on max points of the graph.
Intercept of graph on y axis is ln R0
Slope of graph = b = temperature coefficient for the thermistor.
CALCULATION:
Find out the value of temperature coefficient, b for the thermistor and compare its value with the
practical value.
Use following equation: ln Rt = ln Ro + b [(1/T0 ) – ( 1/Tx ) ]
Compare Graph with standard curve
RESULTS:
Positive Thermistor Negative Thermistor
Experimental Graphical Experimental Graphical
Co-efficient (b)
resistance (Ro), Ω
CONCLUSION:
________________________________________________________________________________
________________________________________________________________________________
________________________________________________________________________________
QUIZ:
1. What is principle of thermistor ?
2. What are different shapes of thermistor sensors?
3. Write advantages & disadvantages of thermistor .
Level Measuring instrument is of six types visual Gauge glass, Float type, Float activated, Level and
shaft mechanism, Magnetic float, Head measurement. Air purge method falls under head
measurement category. If the density or specific gravity of liquid in the open type vessel is known the
only pressure measurement can lead for measurement of liquid level. This is the indirect method of
liquid level measurement device. This system is satisfactory for all liquids. The only limitation is the
clogging of bubble pipe in a sinusoidal system such as chemical slurries etc. A known length (Say lm)
and diameter (1/2 -1 inch) is lowered into the vessel. A pressure gauge or a manometer of suitable
range is connected separately to the upper end of a bubbler system. It operates by building up a
pressure in the feed line until the gas escapes and flow stabilizes at a rate determined by valve in the
feed line. The pressure in bubbler pipe necessary to cause flow is just equal to the pressure exerted by
liquid head above the tip of feed line. So by knowing specific gravity of the liquid, its level can be
measured in the open vessel.
Procedure:
1. Fill the tank with water.
2. Start the compression & adjust the flow such that a known no. of bubbles (i.e. one by one)
are coming out of bubbler pipe.
3. Take the readings of water level in the tank and level difference in manometer.
Observation Table:
Level Difference
Sr. Liquid level H P= Hg
(H – H0)
No. cm. gm / cm.s2
( cm of water column )
1.
2.
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3.
4.
5.
6.
7.
8.
9.
10.
CALCULATIONS :
P= Hg
CONCLUSION:
_______________________________________________________________________________
_______________________________________________________________________________
_______________________________________________________________________________
QUIZ:
1. Describe different methods for direct level measurement.
2. Write brief description of hydrostatic methods used for level measurement.
3. Explain different methods used for level measurement of solids.
The amount of voltage in either secondary winding is proportional to movement of core. Hence
we have an indication of linear motion. By noting which output voltage increasing or decreasing.
We can determine the direction of motion.
The output voltage signal can also applied to a recorder or to a controller that can restore moving
system to its normal position.
The output voltage of an L.V.D.T. is a linear function of core displacement within limited range
of motion say about 5 mm from null position.
Procedure:
1. Connect mains cord to 230V supply switch on unit and see that the supply LED glows.
2. Observe mains output of signal generation on C.R.O. and adjust the frequency to 1KHz which
is excitation frequency of L.V.D.T.
3. Now connect signal generator is set for excitation signal requirement of L.V.D.T. Connect
signal generator output as excitation signal input of L.V.D.T.
4. Connect output of L.V.D.T. to A.C. milivoltmeter.
5. Keep micrometer fully clockwise position observe & record output.
6. Now rotate micrometer anti clock wise, one position at a time & for each position observe &
record the output.
7. Plot graph of output voltage V/s input displacement.
Observations Table:
RESULT:
CONCLUSION:
________________________________________________________________________________
________________________________________________________________________________
________________________________________________________________________________
________________________________________________
Quiz:
1. What is an LVDT?
2. Why use an LVDT?
3. How does an LVDT work?
4. Give details of LVDTs and their support electronics.
5. What types of industries and applications use LVDTs?
Materials: Water.
Theory:
Consider a thermometer bulb positioned in a flowing stream of fluid for which the temperature ti
varies with time and tt is the temperature indicated by the thermometer. The following assumptions
are made:
1. All the resistance to heat transfer lies in the film surrounding the bulb. The resistance offered
by glass and mercury is negligible.
2. All the thermal capacity is in the mercury and the temp. is uniform throughout.
3. The glass wall containing mercury does not expand or contract during transient response.
At steady state,
h a(ti S - ttS) = m cp d ttS/dt = 0 ------------------------------------(2)
Ti - T = dT /dt -------------------------------------(5)
The parameter is called as time const. of the system and has the unit of time. The expression of eq.
(6) is called the transfer function of the system.
Ti(s) = A / s
T(s) = (A / s) *1/(s + 1)
c1 = a and c2 = -A
y(s) = A/s - A/(s +1/)
Procedure:
1. Heat the water in 250 ml glass beaker up to approximately 1000C.
2. Dip the given thermometers in the beaker and note down the time required by the thermometer
for every 5 0C raise in temperature from room temperature to till it attend the final steady state
temperature.
3. Now take out the thermometer from the beaker and put in cold water beaker. Note down the
initial temperature indicated by the thermometer.
4. Note down the time required for every 50C decrement from initial temperature indicated by
the thermometer bulb to till it attend the final steady state temperature.
Observation Table:
CALCULATIONS :
Amplitude A = T f – Ti
y(t) = Tt- Ti
y(t) = A(1 – e (-t/))
Where = time constant
Find (practically) from y(t) = A(1 – e (-t/) ).
Find (graphically) on x- axis at 0.632 on y axis.
Graph :
Plot graph of [y(t)/A] Vs Time (for both systems)
RESULTS:
1 System –1
2 System –2
CONCLUSION:
________________________________________________________________________________
________________________________________________________________________________
________________________________________________________________________________
QUIZ:
Materials: Water
Theory:
The Impulse response of a first order system can be developed as below
Magnitude of Impulse = A
X(S) = A
Y(S)/X(S) = 1/(s +1)
Y(S) = A/(s +1) = (A/)/ (s+1/)
Take Inverse Laplace Transformation
Y(t) = A (e-t/) /
Procedure:
(1) Arrange the Apparatus for liquid level system.
(2) Start the pump and allow the flow of water through control valve.
(3) Maintain steady state flow at least six times and each time note down level of tank
(4) Find out the resistance and time constant of tank.
(5) Now maintain one steady state flow rate and note down level in tank.
(6) Give an impulse input to flow of tank by adding water by beakers very quickly.
(7) Note down time taken for addition and quantity of water added.
(8) Start stop watch and note down variation in level with time of tank.
(9) Finally note down steady state flow rate and level of tank.
Observations:
Initial level in tank before Impulse Input is given = __________mm, (h1, 0)
Highest level in tank after Impulse Input is given = __________mm, (h2, h)
Final level in tank after Impulse Input is given = __________mm, (h2, 0)
Amplitude A = (h2, max) - (h2,final) = __________mm
Area of Tank 1, A1 = __________ m2
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Observation Table - 01
Sr. Flow rate Flow rate Tank-1 Height
No. LPH Q, m3/s h1,m
1 1500
2 2000
3 2500
4 3000
Graph:
1. Q h1
CALCULATIONS:
From graph Q h1 slope =________& R1 = 1/slope= ________s/m2
1 = A1* R1 = _______s
Observation Table - 02
Tank-1 Height, Time in Height diff. y(t)= Percent change from steady
Sr. No.
h2,x,mm sec h2,x - h2,0 state = [y(t)/A]*100
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
CALCULATIONS :
Amplitude A = (h2, max) - (h2,final)
y(t) = h2,x - h2,0
y(t) = A (e-t/) /
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Graph :
Plot graph of y(t)[= (h2,x - h2,0)] Vs Time
RESULTS:
(Experimentally) = _____________ sec.
(Graphically)= ___________ sec.
(Practically)= ___________ sec.
CONCLUSION:
_______________________________________________________________________________________________________
_______________________________________________________________________________________________________
______________________________________________________________________
QUIZ:
1. Explain meaning of liquid level system.
2. Explain difference between step input and impulse input.
3. How we can increase or decrease time constant of liquid level system?
Materials: 1 N NaOH
Theory:
The transfer function of the first order system can be represented as:
Y(s) / X(s) = 1/ (1+ s)
For mixing process, = V/q
Where, = Time constant,
V= Volume of mixture
q= Volumetric flowrate
If a step input of A is given, response curve will follow
y(t )- y(s) = A(1-e-t /)
Where,
y (t)= Conc. of overflow at time t.
y(s) = Steady state conc.
Steady state conc. y(s) = 4 gm/lit of NaOH solution at time t=0 and when fresh water is passed
in to the vessel then step input being negative.
A= y() - y(s) = 0- 4 = -4 gm/lit.
Procedure:
1. Fill up the vessel with ____ N NaOH solution up to the overflow condition
2. Run the stirrer
3. Pass tape water in the vessel at know flowrate and start stopwatch.
4. Take reading with conductivity meter at interval of one minute.
5. Find concentration of each sample by calibration curve of conductivity of NaOH solution.
Observations:
1. Vessel volume up to overflow V = __________m3
2. Tap water flow rate q = __________m3 / sec
3. The time constant =V/q = __________sec
4. Initial steady state concentration y(i) = __________ gm/lit.
5. Final concentration y() = 0 gm/lit.
6. Step input Amplitude, A= y() - y(s) = __________ gm/lit.
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Observation Table:
Conductivity
Sample Time, Concentration, Y(t)
reading Y(t) /A
No. sec y(t) =y(t)-y(i)
(V2)
1. 0
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
CALCULATION:
Amplitude A = y() - y(i)
Y(t) = y(t) - y(i)
Y(t) = A(1 – e (-t/) ); Where = time constant
RESULTS:
(Experimentally) = _____________ sec.
(Graphically)= ___________ sec.
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CONCLUSION:
___________________________________________________________________
___________________________________________________________________
___________________________________________________________________
_______________________________
QUIZ:
1. Why mixing process is considered as a first order system?
2. What are the factors affecting time constant of mixing process?
3. Write brief description of mixing process.
Objective: To study the response of multi capacity (modified first order) system in series using two
tank liquid level system (Non-interacting system) to step input.
Apparatus: Non-Interacting system Apparatus, stopwatch, scale etc.
Materials: Water
Theory:
Assumption:
(1) The liquid to be of constant density.
(2) The tanks to have uniform cross-sectional area.
(3) The flow resistance to be linear.
A balance on tank 1 gives
dh1
q – q1 =A1 ……………. (1)
dt
A balance on tank 2 gives
dh2
q 1 – q2 =A2 …………………… (2)
dt
The flow-head relationships for the two linear resistances are given by the expressions
h1
q1 = …………… (3)
R1
h2
q2 = ………….. (4)
R2
Combining equations (1) and (3) and introducing deviation variables give the transfer function for
tank 1
Q1 S 1
…………… (5)
Q S 1s 1
H 2 s 1 R2
……….. (7)
Qs 1s 1 2 s 1
The overall transfer function of equation (7) is the product of two first order transfer functions,
each one of which is the transfer function of a single tank operating independently of the other.
Inversion of equation (7) by means of partial fraction expansion gives
t t
1 1
H 2 (t ) A R2 [1 1 2 ( e 1 e 2 )]
1 2 2 1
Procedure:
1. Arrange the Apparatus for non-interacting system.
2. Start the pump and allow the flow of water through control valve.
3. Maintain steady state flow at least six times and each time note down levels of tank-1 and
tank-2.
4. Find out the resistance and time constant of each tank.
5. Now maintain one steady state flow rate and note down level in tank-2.
6. Give a step change to flow of tank-1 by regulating the control valve quickly (i.e. Open control
valve quickly by three of four turns).
7. Start stop watch and note down variation (increase) in level with time of tank-2.
8. Finally note down steady state flow rate and levels of both tanks.
Observations:
Sr.No Observations
1. Length of tank-1(L1)= _____________ m
2. Width of tank-1(W1)= = _____________ m
3. Cross sectional area of tank-1 A1 =L1 *W1 = _____________ m2
4. Length of tank-2(L2)= _____________ m
5. Width of tank-2(W2)= = _____________ m
6. Cross sectional area of tank-2 A2 =L2 *W2 = _____________ m2
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Observation Table - 01
Sr. Flow rate Tank-1 Height Tank-2 Height
No. Q, m3/s h1,m h2,m
Observation Table - 02
Initial level in tank-2 before step change is given =__________ m, (h2,0)
Final level in tank-2 after step change is given = ___________ m, (h2,f)
Amplitude A = (h2,f) - (h2,0) = __________m
Practical Theoretical
Tank-2 Height Tank-2 Height
Sr. Time
Tank-2 Height, Deviation, Tank-2 Height, Deviation,
No. t
h2,x H2,x m = h2,x - h2,x H2,x m = h2,x -
h2,0 h2,0
Graph:
2. Q h1
3. Q h2
4. H2 (t) / (h2 - h2,0) t (Practically)
5. H2 (t) / (h2 - h2,0) t (Theoretically)
CALCULATIONS:
From graph Q h1 slope =_______________& R1 = 1/slope= ________________s/m2
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RESULTS:
1 = R1 =
2 = R2 =
CONCLUSION:
________________________________________________________________________________
________________________________________________________________________________
QUIZ:
1. Explain meaning of non-interacting tanks in series.
2. Draw three non interacting tanks in series.
3. If we increase no. on tanks in series, what effect we could see on response? Explain with
graphical representation.
Aim: To study the response of multi capacity (modified first order) system in series using two tank
liquid level system (interacting system)
Apparatus:
Interacting system Apparatus, stopwatch, scale etc.
Chemicals:
Water
Theory:
Assumption: (1) The liquid to be of constant density. (2) The tanks to have uniform cross-sectional
area. (3) The flow resistance to be linear.
A balance on tank 1 gives
dh1
q – q1 =A1 ……………. (1)
dt
A balance on tank 2 gives
dh2
q 1 – q2 =A2 …………………… (2)
dt
The flow-head relationships for the two linear resistances are given by the expressions
1
q1 = h1 h2 …………… (3)
R1
h2
q2 = ………….. (4)
R2
At steady state, equations (1) and (2) can be written
qs – q1s = 0 ………………… (5)
q1s - q2s = 0 ………………… (6)
Subtracting equations (5) from equation (1) and equation (6) from equation (2) and introducing
deviation variables give
dH 1
Q Q1 A1 …………… (7)
dt
dH 2
Q1 Q2 A2 ………… (8)
dt
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H 2 s R2
Q s 1 2 s 2 1 2 A1R2 s 1 ……….. (15)
Procedure:
Arrange the Apparatus for interacting system.
Start the pump and allow the flow of water through control valve.
Maintain steady state flow at least six times and each time note down levels of tank-1 and tank-2
Find out the resistance and time constant of each tank.
Now maintain one steady state flow rate and note down level in tank-2
Give a step change to flow of tank-1 by regulating the control valve quickly (i.e Open control
valve quickly by three of four turns)
Start stop watch and note down variation (increase) in level with time of tank-2
Finally note down steady state flow rate and levels of both tanks
Observations:
Interacting system data:
Tank-1 Tank-2
Length, cm
Width, cm
Area, m2
Table-01
Observation Table - 02
Initial level in tank-2 before step change is given =__________ m, (h2,0)
Final level in tank-2 after step change is given = ___________ m, (h2,f)
Amplitude A = (h2,f) - (h2,0) = __________m
Write equation derived for theoretical H2:____________________________________
Practical Theoretical
Tank-2 Height Tank-2 Height
Sr. Time
Tank-2 Height, Deviation, Tank-2 Height, Deviation,
No. t
h2,x H2,x m = h2,x - h2,x H2,x m = h2,x -
h2,0 h2,0
Graphs:
Q h1 - h2
Q h2
H2 (t) / (h2 - h2,0) t (Practically)
H2 (t) / (h2 - h2,0) t (Theoretically)
Calculations:
Table-03
Practically Theoretically
Sr. Time
Y(t) = H2 (t) Y(t)/ A = Y(t)/ A =
No. T Y(t) = H2 (t)
= h2,x - h2,0 H2 (t)/(h2,f- h2,0) H2 (t)/(h2,f- h2,0)
Results:
1 = R1 =
2 = R2 =
Conclusion:
Objective: To study the step response of a U-tube manometer and to find the value of time lag ()
and damping coefficient ( ) for the system.
Where,
P2,P1=pressures at the top of legs 2 & 1 respectively.
A2,A1= Cross sectional areas of leg 2 & 1 respectively (e.g. A1=A2=A)
=density of fluid.
m=mass of fluid = AL
v= avg. velocity of fluid in the tube.
h=deviation of liq.level from initial plane to steady state.
L=length of liq. in manometer.
Poiseuille’s eq. can be used to relate the fluid friction force to flow velocity.
dh R 4 P
A ------------------------------------------------ ( 2 )
dt 8 L
Where,
R=radius of pipe through which liq. follows.
= viscosity of the flowing liquid.
dv d 2h
4b
dt dt 2
from equations (3) & (4); equation (1) becomes,
8 AL dh d 2h
PA 2 gAh AL 2
R 2 dt dt
2CH403 - Instrumentation and Process Control
Chemical Engineering Department
SoE, IT-NU
Defining above equation for steady state and subtracting from above equation we get:
4 AL dH d 2H
PA 2 gAH AL
R 2 dt 2dt 2
Where H is a deviation variable and is given as follows:
H 2h hs
dividing both the sides by gA
d 2 H L 4 L dH P
H ___________________ (5)
dt 2 2 g gR 2 dt g
L
Let 2 6
2g
4 L
2 7
gR 2
1
KP
g
d 2H dH
2 2
2 H K P P ________________________(8)
dt dt
Taking Laplace transform, transfer function is obtained as
H ( s) K
2 2 P 9
P ( s ) s 2s 1
Eq. (6) & (7) indicate inherent second order dynamic characteristic of manometer.
Now if unit step function is given
Output for <1 i.e. for under damped system, output for the system will be given as follows:
t t 1 2 2
1 1 1 10
H (t ) K P 1 e sin tan
1 2
Procedure:
Observation:
Sr. No. Height of liquid Time Sr. No. Height of liquid in Time
in manometer t (sec) manometer H, cm t (sec)
H, cm
1.
2.
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
13.
14.
15.
16.
17.
Graphs:
Height of liquid in manometer H time t
Results:
Properties Theoretical Graphical Properties Theoretical Graphical
Decay ratio
Rise time
Conclusion: