Professional Documents
Culture Documents
SENIOR PROJECT 2
NTA LEVEL 8
June, 2018
TITLE: EFFECT OF STABILIZING ADDITIVES AND MINERAL FILLERS ON THE
PERFORMANCE OF GAP GRADED HOT MIX ASPHALT (GGHM A)
This project is submitted to the Dar es Salaam Institute of Technology as a partial fulfilment of
Bachelor of Engineering in Civil Engineering
Author
MATHIAS, Kulwa
June, 2018
DECLARATION
I, MATHIAS, Kulwa declare that, the project entitled “Effect of Stabilizing additives and Mineral
fillers on the Performance of Gap-Graded Hot Mix Asphalt (GGHMA)”.Submitted in partial
fulfillment of the requirements for the award of Bachelor of Engineering in Civil Engineering with
specialization in Transportation Engineering during 2017-2018 session at the Dar es Salaam Institute of
Technology (DIT). To the best of my knowledge, the results contained in this project have not been
submitted to any other University/Institute for the award of any degree/diploma. Wherever any
researchers or other authors information used it has been well cited its source for academic safety.
i
ABSTRACT
In an effort to address the rampant failures happening in heavy duty roads, more heavy duty and busiest
roads are nowadays designed using Gap-Graded Hot Mix Asphalt (GGHMA) in which major example
of it is Stone Mastic Asphalt concrete(SMA). Many highway agencies like TANROADS and TARURA
in Tanzania have not clearly set specific stabilizing additives and mineral fillers to be of consideration
during design of the Stone mastic asphalt concrete leaving this task to pavement engineers to decide
what stabilizing additives should be used and why not the other one. For that reason there is a need for
highway agencies and researchers to know what stabilizing additive and mineral filler to be used in
developing an appropriate design to perform effectively. There should be no dilemmarity to the asphalt
designer on what best mineral filler to use in their design. In deciding type of a specific stabilizing
additive one should really know why can I choose cellulose fiber s and not mineral fibers? Why can I
choose lime not fly-ash or marble dust or limestone dust or crush dust or cement as my mineral filler?
In the current situation on the use of stabilizing additives and mineral fillers in a full scale project ar e
allowed only after data has been collected from project where the additives and fillers had been
previously used and its performance seen. It is something shocking in the era of Science and
Technology with full equipped pavement material laboratories to wait for a pilot study for some years
or copy some data which were used somewhere where our weather condition differ from where the data
belongs to.
For that reason there is a need to assess the effect of different stabilizing additives and mineral fillers
to be used in design of GGHMA which require greater care in the choice and use of different stabilizing
additives and mineral fillers.
The significance of this study are remaining superior to pavement engineers and highway agencies that
they will easily understand the best stabilizing additives and mineral filler from Laboratory analysis
developed. Also from the findings asphalt producers should refinery produce asphalt for specific duty
with refinery added stabilizing additives. Last but not least, there shall be reduced number of pilot
projects to be made by highway agencies and researchers which will largely save cost for investing in
pilot studies in which we don’t even know how well it will perfor m.
In this study the chosen stabilizing additives are Plastic (Polyvinyl Chloride (PVC)), Reclaimed
Rubber (Recycled Tires) and cellulose fibers are to be tested with same mineral filler which is ultra -
white hydrated lime hereby known as Active Filler abbreviated by ‘AF’.
Through this study extensive knowledge in hot mi x asphalt design principles, material knowledge
especially aggregates, asphalt binder, stabilizing additives and mineral fillers and general
understanding in civil material laboratory instrumentations is gained by the doer. This was my real
long term desire and need.
ii
DEDICATION
This project is dedicated to My Mother, Sabina, whose wise instructions and loving guidance in life
have prepared me for the challenges and joys yet to come. My Wife, Helen and my son, Brighton who
stuck by me through the project, writing and completing this project, after ALL they are with me and
they will always be with me forever. My uncle, Seleman, whose pride and honor in family has helped
me become good as I can be.
Finally, my special dedication my specia l prayers go to my late father Mzee Mnyeti Mathias, Nh’aghara
(May your soul rest in peace in Heaven). You was Chief of Defense, the General Commander, the
guardian, priest and doctor of your own son, counselor and I don’t know exactly who you’re in my life.
You were more than a father. I still remember your last word at your last bed. I graved you in my inner
heart. Please you may rest in peace in Heaven.
iii
ACKNOWLEDGEMENT
First and foremost, praise and sincere thanks goes to the Almighty for being blessed with
highly motivating, supporting and inspiring Parents and Friends to keep up in my life.
I would like also to thank several individuals for their help and contribution in making this project a
success at this point of data collection. I first acknowledge Dr. J. Musagasa, PhD., as my advisor, my
supervisor, my mentor, and my lecturer in Highway Engineering Material module. His guidance,
management, and encouragement allowed me not only to likely completing the B.Eng. process, but to
prosper in my endeavors and enjoy myself along the way. Thank you Dr. Musagasa, you was calm in
the storm and you will always be. Furthermore, this project could not have been at this stage in the time
frame established without the dedication of Eng. Malisa, Senior Pavement Design Engineer at Central
Material Laboratory-TANROADS, who’s instrumentation experience and attention to detail proved
invaluable.
The topic of this project is based on the work of some great engineers. I acknowledge the guidance and
friendship given by Miss Christina (CML). It was through her efforts that I was able to first understand
the mix design principles that are presented in this project. My long term comrade Mr. Mathias Mandalu
Gwisu, a senior material technician at T ANROADS Regional Office Dar es Salaam, you were more
than a friend in assisting and sharing knowledge with me. May God bless you.
Also, I would like to thank Mr. Mtorah of Central Material Laboratory. Through Mtorah, CML donated
all the asphalt, mineral filler and some of my stabilizing additives and aggregate materials necessary
for the GGHMA mix design and provided unlimited access to their own lab, which prov ed extremely
beneficially. Mtorah and Clement also provided considerable insight into the nuances of MoW’s,
AASHTO, ASTM, and THM specifications and mix design criteria.
In closing, I thank the Central Material Laboratory for their helping hand and providing me the
opportunity to help improve the state-of-the-art in asphalt mix design. If it was army am sure I could
be promoted to F-7 NATO military rank. Thank you CML.
iv
TABLE OF CONTENTS
DECLARATION ................................................................................................................................................ i
ABSTRACT ....................................................................................................................................................... ii
DEDICATION .................................................................................................................................................. iii
ACKNOWLEDGEMENT ................................................................................................................................ iv
TABLE OF CONTENTS ................................................................................................................................... v
LIST OF TABLES ............................................................................................................................................ ix
LIST OF FIGURES ........................................................................................................................................... x
LIST OF ABBREVIATIONS ........................................................................................................................... xi
CHAPTER ONE ................................................................................................................................................. 1
INTRODUCTION ............................................................................................................................................. 1
1.1 General Introduction ................................................................................................................................ 1
1.2 Problem Statement ............................................................................................................................... 2
1.3 Objectives of the study ......................................................................................................................... 2
1.3.1 Main Objective of the Project ............................................................................................................ 2
1.3.2 Specific Objectives of the Study ........................................................................................................ 2
1.4 Significance of the Study ...................................................................................................................... 2
1.5 The Scope of the Study ......................................................................................................................... 3
1.6 Limitations of the study ........................................................................................................................ 3
CHAPTER TWO ................................................................................................................................................ 4
LITERATURE REVIEW................................................................................................................................... 4
2.1 Gap Graded Hot Mix Asphalt (GGHMA) ................................................................................................ 4
2.2 Philosophy of GGHMA mix design ......................................................................................................... 5
2.3 Overview of GGHMA Mix Design Procedure......................................................................................... 5
2.4 Coarse Aggregates ................................................................................................................................... 7
2.5 Fine Aggregates ....................................................................................................................................... 7
2.6 Asphalt Binder ......................................................................................................................................... 7
2.7 Mineral Fillers .......................................................................................................................................... 8
2.8 Stabilizing Additives ................................................................................................................................ 8
Step 2: Trial Gradations ................................................................................................................................. 9
Determination of Voids in Coarse Aggregates (VCA)................................................................................. 10
ix
Selection of Target Asphalt Content ............................................................................................................ 11
2.8 The Bailey Method ................................................................................................................................ 13
2.8 1 Basic Principles ............................................................................................................................... 14
2.8.2 Aggregate Packing ........................................................................................................................... 14
2.8.3 Coarse and Fine Aggregate .............................................................................................................. 15
2.8.4 Combining Aggregates by Volume .................................................................................................. 16
2.8.5 Loose Unit Weight of Coarse Aggregate ......................................................................................... 16
2.8.6 Rodded Unit Weight of Coarse Aggregate....................................................................................... 17
2.8.7 Chosen Unit Weight of Coarse Aggregate ....................................................................................... 17
2.9 stabilizing additives in bituminous mixes .............................................................................................. 18
2.9.1 Fibre as an additive.......................................................................................................................... 19
CHAPTER THREE ......................................................................................................................................... 20
METHODOLOGY ........................................................................................................................................... 20
3.1 Research design ...................................................................................................................................... 20
3.1.1 Material Selection ............................................................................................................................ 20
3.1.2 Selecting Optimum Gradation ......................................................................................................... 20
3.1.3 Selecting Design Binder Content ..................................................................................................... 21
3.1.4 Evaluating Draindown test............................................................................................................... 21
3.1.5 Test Specimens ................................................................................................................................ 21
3.2 Methods and Materials ........................................................................................................................... 22
3.3 SM14 Specimens molding Procedure flow Chart .................................................................................. 24
CHAPTER FOUR ............................................................................................................................................ 25
PRESENTATION OF RESULTS ................................................................................................................... 25
4.1 AGGREGATES ..................................................................................................................................... 25
4.1.1 Consensus properties tests ............................................................................................................... 25
4.1.1.1 Gradations of Aggregates.............................................................................................................. 25
4.1.1.2 Flakiness Index Test ..................................................................................................................... 25
4.1.1.3 Specific gravity and water absorption ........................................................................................... 27
4.1.1.4 Fine aggregate angularity test ....................................................................................................... 27
4.1.1.5 Clay content (Sand equivalent test) ............................................................................................... 28
4.1.2 Source Properties tests on aggregates .............................................................................................. 28
4.1.2.1 Soundness test ............................................................................................................................... 29
4.1.2.2 Strength test .................................................................................................................................. 30
4.1.2.3 Toughness Test ............................................................................................................................. 30
x
4.1.3 Blending of the aggregates .............................................................................................................. 31
4.2 Asphalt binder properties tests ............................................................................................................... 31
4.2.1 Bitumen penetration test .................................................................................................................. 32
4.2.2 Softening Point Test ......................................................................................................................... 32
4.2.3 Flash and Fire Point ......................................................................................................................... 32
4.2.4 Density and Relative density of binder ............................................................................................ 33
4.2.5 Brookfield Dynamic Viscosity Test ................................................................................................ 33
4.2.6 Ductility test .................................................................................................................................... 34
CHAPTER FIVE .............................................................................................................................................. 35
Data Analysis and Discussion of results............................................................................................................. 35
5.1 Aggregates Properties.................................................................................................................................. 35
5.1.1 Aggregate Particle Size Distribution.................................................................................................. 35
5.1.2 Aggregate Specific Gravity and Absorption ...................................................................................... 36
5.1.4 Bulk specific gravity (G sb) and apparent specific gravity (G sa) of the aggregates .............................. 39
5.1.5 Fine Aggregate Angularity ................................................................................................................ 39
5.1.6 Clay Content ..................................................................................................................................... 40
5.1.7 Aggregates Flakiness Index (FI) ........................................................................................................ 40
5.2 .1 Ten Percent Fines (TFV) .................................................................................................................. 41
5.2.2 Los Angeles Abrasion Test ............................................................................................................... 42
5.2.3 Sulfate Soundness Test (AASHTO T104 – 97).................................................................................. 43
5.3.2 Blend Specific gravity ....................................................................................................................... 45
5.3.1 Marshall Mix Design of SMA using Cellulose fibres stabilizing additive ........................................... 46
5.3.3 Marshall Mix Design of SMA14 using Reclaimed Rubber (8% of the binder) as stabilizing additive . 48
5.3.4 Marshall Mix Design of SMA14 usin Polyvinyl Chloride (PVC) (8% of the binder) as stabilizing ..... 50
5.3.5 Draindown Test analysis ................................................................................................................... 53
CONCLUSION................................................................................................................................................. 54
RECOMMENDATIONS ................................................................................................................................. 55
REFERENCES ................................................................................................................................................ 56
APPENDICE
xi
LIST OF TABLES
Table 1: Stone Mastic Gradation Specification Bands based on %passing by volume ..................................... 10
Table 3: Flakiness Index Table of results ....................................................................................................... 26
Table 4: Summary results on specific gravities and water absorption for selected aggregates.......................... 26
Table 5: % air void in loosely compacted fine aggregate (in SMA design) ..................................................... 27
Table 6: Table showing Sand equivalent results ............................................................................................. 27
Table 7: The summary results of the Soundness test ....................................................................................... 28
Table 8: TFV results...................................................................................................................................... 29
Table 9: LAA results ..................................................................................................................................... 29
Table 11: Penetration results.......................................................................................................................... 31
Table 12: Softening point of the binder .......................................................................................................... 31
Table 13: Results of Flash point and Fire point .............................................................................................. 32
Table 14: Result of Relative Density and Density of the binder ...................................................................... 32
Table 15: Results of the Brookfield dynamic Viscosity .................................................................................. 33
Table 16: Results of the Ductility test of binder ............................................................................................. 33
xi
i
LIST OF FIGURES
Figure 1: Desirable Aggregates and Undesirable Aggregates ............................................................................ 6
Figure 2:Types of Mineral Fillers used in GGHMA............................................................................................. 8
Figure 3: Some Stabilizing additives used in GGHMA design.......................................................................... 9
Figure 4: Method of determining VCA in dry-rodded condition. .................................................................... 11
Figure 5: Loose Unit Weight Condition ......................................................................................................... 16
Figure 6: Rodded Unit Weight Condition....................................................................................................... 17
Figure 7: Selection of Chosen Unit Weight of Coarse Aggregate ................................................................... 18
Figure 8: Research Design flow Chart............................................................................................................ 20
Figure 9: The Flow chart of Marshall Mixing process .................................................................................... 24
Figure 10: Blending and grading of individual aggregates .............................................................................. 30
xi
ii
LIST OF ABBREVIATIONS
AF Active Filler
APA Asphalt Concrete Analyzer
CA Coarse Aggregates
FI Flakiness Index
HDAP Heavy Duty Asphalt Pavement
PG Performance Grade
PSD Particle Size Distribution
xi
v
CHAPTER ONE
INTRODUCTION
1.1 General Introduction
In an effort to address the rampant failures happening in heavy duty roads, more heavy duty and busiest
roads are nowadays designed using Gap-Graded Hot Mix Asphalt (GGHMA) in which major example
of it is Stone Mastic Asphalt concrete(SMA). Stone Mastic Asphalt (SMA) is material designed
specifically for making top layers on heavy duty roads (www.mainroads.qld.gov.au). The specificity of
stone mastic asphalt concrete composition and structure implies the mandatory presence of hard and
durable aggregates and mineral fillers, voluminous bitumen and small amount of stabilizing additives
for disperse reinforcing of a binder as a main structural components. For example Kibamba climbing
lane top layer was designed with DBM30 in 2014 but now (2017+) has been alternatively ware with
SMA. This show evident that SMA is an alternative choice for heavy duty roads if designed
appropriately. Many highway agencies like TANROADS and TARURA in Tanzania have not clearly
set specific stabilizing additives and mineral fillers to be of consideration during design of the Stone
mastic asphalt concrete leaving this task to pavement engineers to decide what stabilizing additives
should be used and why not the other one. For that reason there is a need for highway agencies and
researchers to know what stabilizing additive and mineral filler to be used in developing an appropriate
design to perform effectively. There should be no dilemmarity to the asphalt designer on what best
mineral filler to use in their design. In deciding type of a specific stabilizing additive one should really
know why can I choose cellulose fibers and not mineral fibers? Why can I choose lime not fly-ash or
marble dust or limestone dust or crush dust or cement as my mineral filler?
In the current situation on the use of stabilizing additives and mineral fillers in a full scale project are
allowed only after data has been collected from project where the additives and fillers had been
previously used and its performance seen. It is something shocking in the era of Science and
Technology with full equipped pavement material laboratories to wait for a pilot study for some years
or copy some data which were used somewhere where our weather condition differ from where the data
belongs to.
For that reason there is a need to assess the effect of different stabilizing additives and mineral filler s
to be used in design of GGHMA which require greater care in the choice and use of different stabilizing
additives and mineral fillers.
The significance of this study are remaining superior to pavement engineers and highway agencies that
they will easily understand the best stabilizing additives and mineral filler from Laboratory analysis
developed. Also from the findings asphalt producers should refinery produce asphalt for specific duty
with refinery added stabilizing additives. Last but not least, there shall be reduced number of pilot
projects to be made by highway agencies and researchers which will largely save cost for investing in
pilot studies in which we don’t even know how well it will perfor m.
1
In this study the chosen stabilizing additives are Plastic (Polyvinyl Chloride (PVC)), Reclaimed Rubber
(Recycled Tires) and cellulose fibers are to be tested with same mineral filler which is ultra-white
hydrated lime hereby known as Active Filler prefixed by ‘AF’.
For that reason there is a need to assess the effect of different stabilizing additives and mineral fillers
to be used in design of GGHMA which is just Stone Mastic Asphalt (SMA) which require greater car e
in the choice and use of different stabilizing additives and mineral fillers.
i. Pavement Engineers and Highway agencies will easily understand the best stabiliz ing
additives and mineral filler from Laboratory analysis developed.
2
ii. From the findings Asphalt Producers should refinery produce asphalt for specific duty
with refinery added stabilizing additives.
iii. Reduced number of Pilot Projects to be made by Highway Agencies and researchers.
3
CHAPTER TWO
4
Results from that research project were published in 1998, and, along with more recent experience and
research, they are the basis for the GGHMA mix design system described in this chapter.
2.2 Philosophy of GGHMA mix design
The philosophy of GGHMA mix design is not complicated.
The first principle is that a gap-graded blend of aggregate is needed so that the coarse particles will
have stone-on-stone contact.
The second principle is that the voids within the coarse aggregate skeleton must be filled with fine
aggregate, mineral filler, and asphalt binder. In order to provide increased durability, GGHMA has a
relatively high asphalt binder content.
This leads to the third principle of GGHMA mix design, which is that the aggregate must have a high
VMA value—typically 18 to 20%. This relatively high asphalt binder content can result in an increased
potential for draindown if not properly taken into account. Draindown can be a common problem in
GGHMA; it occurs when the asphalt binder and fine aggregate separate from the coarse aggregate
during storage, transport, or placement.
The fourth and final principle of GGHMA mix design is that small amounts of stabilizing additives,
such as mineral fibers or cellulose fibers, are usually needed to prevent draindown. The sections below
describe in detail how to design GGHMA to achieve the unique properties and excellent perfor mance
for which this mix type is known.
lime to reduce the potential of moisture damage, hydrated lime can be considered a portion of the
mineral filler. Because of the large percentage of coarse aggregate in GGHMA blends, natural crushed
aggregate stockpiles do not generally have sufficient materials passing the 0.075 -mm sieve to help fill
the voids of the stone skeleton, hence the need for mineral fillers. Without the use of mineral filler s to
fill the voids, GGHMA mixes would be very per meable.
The primary purpose for stabilizing additives is to reduce the potential for draindown. When added to
stiffen an asphalt binder, polymer modifiers can be considered a stabilizing additive. Likewise, mineral
fillers can also be considered a stabilizing additive, since these small particles help “soak up” the asphalt
binder. However, the most effective stabilizing additive is a fiber. Several types of fiber have been used
in GGHMA with cellulose and mineral fiber being the most common. Generally, cellulose fibers are
added at 0.3% of the total mix mass and mineral fibers are added at 0.4%. The followi ng sections
provide requirements for the various materials used to fabricate GGHMA. These requirements are
provided for guidance to agencies not having experience with these types of mixtures. Some agencies
have used other test methods and criteria with su ccess.
6
2.4 Coarse Aggregates
As described previously, the success of a GGHMA pavement depends heavily on the existence of stone-
on-stone contact. Therefore, in addition to angularity, shape, and texture, the toughness and durability
of the coarse aggregates must be such that they will not degrade during production, construction, and
service. Table 1 presents coarse aggregate requirements for GGHMA mixtures. The Los Angeles
Abrasion and Soundness tests should be required for individual stockpiles while the Flat or Elongated
and Uncompacted Voids tests should be required for the total aggregate blend.
2.5 Fine Aggregates
The role of fine aggregates in GGHMA is to help fill the voids between coarse aggregate particles.
Therefore, the primary requirements for fine aggregates in GGHMA are to ensure a durable and angular
material. Requirements for fine aggregates in GGHMA are provided in Table. The Uncompacted Voids
and Sand Equivalency tests should be required for the total aggregate blend, while the soundness test
should be applied to individual fine aggregate stockpiles.
7
2.7 Mineral Fillers
Mineral fillers used for GGHMA should be finely divided mineral matter such as crushed fines,
agricultural limes, or fly ash. Figure below illustrates some typically used mineral fillers. The mineral
filler should be free from organic impurities.
9
Stone mastic Gradation Specification bands (based on percentage passing by volume)
Table 1: Stone Mastic Gradation Specification Bands based on %passing by volume
10
Gcaγω− γs
𝑉𝐶𝐴� 𝑅� = Gcaγω
𝑥 100 (1)
Gca = Bulk specific gravity of coarse aggregates fraction in dry rodded condition
11
The minimum binder content values given in Table 2. have been calculated so that, in most cases, the
resulting mixes will meet the suggested minimum VMA of 17.0% at 4.0% air voids for GGHMA
mixtures.
Where;
Ps= percent of aggregate in the mixture
Pca= percent of coarse aggregate in the mixture
Gca= combined bulk specific gravity of the total aggregate
Gsb= bulk specific gravity of the coarse aggregate (coarser than break point sieve)
Once the VTM, VMA, and VCA are determined, each trial blend mixture is compared to the GGHMA
mixture requirements. Table 10-12 presents the requirements for GGHMA designs. The trial blend mix
that meets or exceeds the minimum VMA requirement, has an air void content between 3.5 and 4.5%,
and has a VCAMIX less than VCA is selected as the design gradation. If none meet these requirements,
12
additional aggregate blends should be evaluated. If one of the trial blends is very close to meeting these
requirements, with the air void content and VMA just outside their acceptable ranges, an adjustment in
the binder content might provide an acceptable mix design, as discussed
Step 4: Refine Design Asphalt Binder Content
Once the design gradation of the mixture is chosen, it may be necessary to raise or lower the asphalt
binder content to obtain the proper amount of air voids in the mixture. In this case, additional samples
are prepared using the selected gradation and varying the asphalt binder content. The optimum asphalt
binder content is chosen to produce 4.0% air voids in the mixture; because of typical error in volumetric
analysis, air void contents within ± 0.5% of this target are acceptable. The optimum asphalt binder
content should meet the minimum asphalt content requirements in Table 1 -2.
The number of samples needed for this portion of the procedure is again twelve, with three compacted
and one uncompacted sample at each of three asphalt binder contents. The mixture properties are again
determined, and the optimum asphalt binder content is selected. The designed GGHMA mixture at
optimum asphalt content selected should have properties meeting the criteria shown in design table. If
those criteria are not met, the mixture must be modified so that all criteria are met.
Step 5: Conduct Performance Testing
Performance testing of GGHMA mixtures consists of three tests: (1) evaluation of moisture
susceptibility; (2) evaluation of draindown sensitivity; and (3) evaluation of rut resistance.
13
2.8 1 Basic Principles
To develop a method for combining aggregates to optimize aggregate interlock and provide the proper
volumetric properties, it is necessary to understand some of the controlling factors that affect the design
and performance of these mixtures. The explanation of coarse and fine aggregates given in the
following section provide a background for understanding the combination of aggregates. The Bailey
Method builds on that understanding and provides more insight into th e combination of aggregates for
use in an asphalt mixture.
The Bailey Method uses two principles that are the basis of the relationship between aggregate
gradation and mixture volumetrics: Aggregate packing, and Definition of coarse and fine aggregate.
With these principles, the primary steps in the Bailey Method are: Combine aggregates by volume,
and analyze the combined blend.
14
presented. Even though an aggregate may have acceptable characteristics, it may not combine well with
the other proposed aggregates for use in the design. The final combination of coarse and fine aggregates,
and their corresponding individual properties, determines the packing characteristics of the overall
blend for a given type and amount of compaction. Therefore, aggregate source selection is an important
part of the asphalt mix design process.
The traditional definition of coarse aggregate is any particle that is retained by the 4.75 -mm sieve. Fine
aggregate is defined as any aggregate that passes the 4.75-mm sieve (sand, silt, and clay size material).
The same sieve is used for 9.5 -mm mixtures as 25.0-mm mixtures. In the Bailey Method, the definition
of coarse and fine is more specific in order to determine the packing and aggregate interlock provided
by the combination of aggregates in various sized mixtures. The Bailey Method definitions are:
i. Coarse Aggregate: Large aggregate particles that when placed in a unit volume create voids.
ii. Fine Aggregate: Aggregate particles that can fill the voids created by the coarse aggregate in
the mixture.
From these definitions, more than a single aggregate size is needed to define coarse or fine. The
definition of coarse and fine depends on the nominal maximum particle size (NMPS) of the mixture.
In a dense-graded blend of aggregate with a NMPS of 37.5 mm, t he 37.5-mm particles come together
to make voids. Those voids are large enough to be filled with 9.5 -mm aggregate particles, making the
9.5-mm particles fine aggregate. Now consider a typical surface mix with a NMPS of 9.5 mm. In this
blend of aggregates, the 9.5-mm particles are considered coarse aggregate. In the Bailey Method, the
sieve which defines coarse and fine aggregate is known as the primary control sieve (PCS), and the
PCS is based on the NMPS of the aggregate blend. The break between coarse and fine aggregate is
shown in Figure A.1. The PCS is defined as the closest sized sieve to the result of the PCS formula in
Equation below: PCS = NMPS x 0.22 where PCS = Primary Control Sieve for the overall blend NMPS
= Nominal Maximum Particle Size for the overall blend, which is one sieve larger than the first sieve
that retains more than 10% (as defined by Superpave terminology). The value of 0.22 used in the control
sieve equation was determined from a two- (2D) and three-dimensional (3-D) analysis of the packing
of different shaped particles. The 2-D analysis of the combination of particles shows that the particle
diameter ratio ranges from 0.155 (all round) to 0.289 (all flat) with an average value of 0.22. The 3 -D
analysis of the combination of particles gives a similar result with the particle diameter ratio ranging
15
from 0.15 (hexagonal close-packed spheres) to 0.42 (cubical packing of spheres). In addition, research
on particle packing distinctly shows that the packing of particles follows different models when the
characteristic diameter is above or below 0.22 ratio.
While 0.22 may not be exactly correct for every asphalt mixture, the analysis of gradation is not affected
if the value ranges from 0.18 to 0.28. The 0.22 factor is the average condition of many different packing
configurations.
2.8.4 Combining Aggregates by Volume
All aggregate blends contain an amount and size of voids, which are a function of the packing
characteristics of the blend. In combining aggregates we must first deter mine mount and size of the
voids created by the coarse aggregates and fill those voids with the appropriate amount of fine
aggregate. Mix design methods generally are based on volumetric analysis, but for simplicity,
aggregates are combined on a weight basis. Most mix design methods correct the percent passing by
weight to percent passing by volume when significant differences exist among the aggregate stockpiles.
To evaluate the degree of aggregate interlock in a mixture the designer needs to evaluate a mixt ure
based on volume. To evaluate the volumetric combination of aggregates, additional information must
be gathered. For each of the coarse aggregate stockpiles, the loose and rodded unit weights must be
determined, and for each fine aggregate stockpile, the rodded unit weight must be determined. These
measurements provide the volumetric data at the specific void structure required to evaluate interlock
properties.
More information relating to the Bailey Method of blending of aggregated are presented in Khalid
Salim Alshamsi paper in 1995.
This method is very important in design of Gap-graded hot mix asphalt to ensure interlock of the
aggregate skeleton so as to obtain high resistant to deformation and durable mix.
2.9 stabilizing additives in bituminous mixes
The additives such as fibers, rubbers, polymers, carbon black, artificial silica or a combination of these
materials are used to stiffen the mastic at high temperature during production and placement and to
obtain even higher binder contents for increased durability (Pierce, 2000). Since Stone Mastic Asphalt
is the focus of the study, the literature pertaining to that has been presented as a separate in the followin g
paragraph.
18
2.9.1 Fibre as an additive
The history of the use of fibers can be traced back to a 4000 year old arch in China constructed with a
clay earth mixed with fibre or the Great Wall built 2000 years ago (Hongu and Philips,1990). However,
the modern developments of fibre reinforcement started in the early 1960s (Mahrez, 2003). Zube (1956)
published the earliest known study on the reinforcement of bituminous mixtures.
19
CHAPTER THREE
GGHMA DESIGN
MATERIAL
SELECTION
STABILIZING
ADDITIVES
MIXING GGHMA
(With other
MIXING GGHMA additives)
(With only Cel.
Fibre)
DRAINDOWN SENSITIVITY
37.5 mm to 26.5mm
26.5 mm to 19.0 mm
19.0 mm to 14.0 mm
14.0 mm to 10.0 mm
10.0 mm to 7.0 mm
7.0 mm to 4.75 mm
4.75 mm to 2.36 mm
2.36 mm to 1.18 mm
1.18 mm to 0.600 mm
0.600mm to 0.300mm
0.300mm to 0.150 mm
21
0.150 mm to 0.075mm
Passing 0.075 mm
Mixing and Compaction Temperatures: This temperature depends on the properties of the modified
asphalt binder stabilized with other additives.
Different recommended methods and materials has been taken into account to make this research reach
its targeted goals. Summaries of the methods and materials requirements are as follows
i. Specification for CA,FA and Mineral filler(AASHTO M17) as per ASTM D692, D1073,D242
respectively
ii. Destructive aggregate tests required for normal design of GGHMA
• LAA (ASTM C131(smaller than 1.5 inch)and C535 for blended aggregates or (CML 2.9),
this assess the hardness of road aggregate
• TFV (as per CML 2.7), this strength for aggregates to qualify for design of SMA.
• Soundness Test (ASTM C 88) or CML 2.10 which objective is to assess the weathering
action of aggregate for use in road pavement.
iii. Nondestructive tests to be done aggregate to comply with GGHMA requirements:
Sand Equivalent test (ref ASTM D2419) It’s important to show the clay content in
aggregates to be used for GGHMA
Specific gravity for CA and FA (ref ASTM C127 & ASTM C128 resp.)
Theoretical Max Specific gravity (ref ASTM D2041) help in determination Effective
specific gravity
Water absorption test(ref AASHTO T84)
Soundness Test
Flakiness Index
22
Material selection and sources to be used in this study are aggregates implying both Coarse Aggregates
(Mafinga Source) and Fine Aggregates and Stabilizing additives selected in this study are Plastic
(Polyvinyl Chloride (PVC)), Reclaimed Rubber (Recycled Tires) and cellulose fibre.
The mineral filler be used is hydrated lime. The selected asphalt binder to be used is 60/70 which will
be tested for compliance according (MoW standard specification 1999) through the following tests:
23
3.3 SM14 Specimens molding Procedure flow Chart
The flow chart below summarizes the specimen molding process in Marshall Method.
BEGIN
#2 Remove aggregates
& asphalt from ovens.
#3 Place proportioned
24
CHAPTER FOUR
PRESENTATION OF RESULTS
4.1 AGGREGATES
Aggregates tests in this study were divided into two categories, namely Consensus properties and
Source properties.
26
Table 2: Flakiness Index Table of results
Aggregate Flakiness Index (%) Check
stockpile
5—10 mm 18.0 ok
10—14mm 19.0 ok
The test results are summarized in the table below whereas the laboratory results of this tests are
attached in the APPENDIX GSA005a and GSA005.
Table 3: Summary results on specific gravities and water absorption for selected aggregates.
27
The required minimum angularity percent for heavy duty roads is minimum 45%. The results are
presented in the table below and the worksheet laboratory results attached to APPENDIX SET014.
The summary of the results are hereby summarized in the following table:
Table 4: % air void in loosely compacted fine aggregate (in SMA design)
28
during the mix design process, they may also used as source acceptance control by the highway
agencies. Those properties are:
Soundness,
Strength, and
Toughness.
29
4.1.2.2 Strength test
Ten Percent Fines Value (TFV) has done in accordance to CML 2.7 method regarding the fact that all
aggregates used in road construction should be strong enough to resist crushing under the traffic wheel
loads. If the aggregates are weak, integrity of pavement structure may adversely affected. The strength
of the aggregates are measured in a crushing test. The ten percent fines value (TFV) gives a relative
measure of resistance of an aggregates to crushing under a gradually applied loads in pavement design.
There specific requirements for the TFV tested both dry and wet condition.
The results presented below in the table are also detailed attached in the APPENDIX TFV009a.
Table 7: TFV results
30
4.1.3 Blending of the aggregates
Aggregates are normally stored in stockpiles as single sized (narrow grading).It is therefore necessary
to mix (blend) different sizes of aggregates from different piles so as to obtain the desired PSD for
specific use as given in the specification. Blending of aggregates is often a trial and error exercise,
although graphical methods may be used to advantage. In this case trial and error method has been used
and the theory of Bailey method employed.
The analysis of aggregate gradations and the combining of aggregates to obtain the desired gradation
are important steps in hot mix design. And the gradation should be made up of the most economical
proper aggregates to be found. The THM 1[ ] specification for SM14 was employed and the results
obtained are as shown in the figure below. The laboratory worksheet are attached in the APP ENDIX
BA001.
BLENDING SM14
100.0
90.0
80.0
70.0
% Passing
60.0
50.0
40.0
30.0
20.0
10.0
0.0
0.0 0.1 1.0 10.0 100.0
Sieve Size - log scale
Min Spec Max Spec 0--3 mm 3--5mm
5--10mm 10--14mm AF BLENDED
32
Table 11: Results of Flash point and Fire point
Test Temperature AASHTO check
in o C M20-70
(1996)
Flash Point 320 Max 232 0 C ok
Fire Point 358 Max 232 o C ok
Test no 1 2
Relative density 1.031 1.032
Density g/cm3 1.0279 1.0289
Average density 1.0284 ≈ 1.03
g/cm3
33
Table 13: Results of the Brookfield dynamic Viscosity
Brookfield dynamic Viscosity Specification Check
viscosity at (cPoise) results (SABS, 1997),
Viscosity in Pa.s
60 0C 168000+ 120--250 ok
0 10378 ok
90 C
135 0C 429 0.22—0.45 ok
34
CHAPTER FIVE
35
the difference between the total weight retained and the original sample weight, expressed as a percent of
the original sample weight:
�(𝑀�– �𝑚)�
𝐸𝑟𝑟𝑜𝑟��% = �𝑥�100% … … … … … … … … … … … … … … … . . (5.1)
𝑀
The % retained is calculated by dividing the weight retained for each sieve by the original sample weight
and, again, expressing the result as a weight percentage. For the 2.36-mm-diameter sieve % retained D
mm sieve.
𝑖𝑛𝑑𝑖𝑣𝑖𝑑𝑢𝑎𝑙�𝑚𝑎𝑠𝑠�𝑟𝑒𝑡𝑎𝑖𝑛𝑒𝑑�𝑖𝑛�𝑎�𝑠𝑖𝑒𝑣𝑒�𝐷�𝑚𝑚
𝑇ℎ𝑒�%�𝑟𝑒𝑡𝑎𝑖𝑛𝑒𝑑 = ��𝑥�100% … … … … … . (5.2)
𝑂𝑟𝑖𝑔𝑖𝑛𝑎𝑙�𝑠𝑎𝑚𝑝𝑙𝑒�𝑤𝑒𝑖𝑔ℎ𝑡�𝑀
The cumulative % retained is calculated by summing all the values for % retained up to the given sieve
size. Also the % passing is calculated as 100%—the cumulative % retained. It should be pointed out
that there are slightly different ways of calculating these values for sieve analyses, and those responsible
for HMA mix design and associated testing should follow the procedures as required by their state
agencies. The results of aggregate sieve analyses was presented graphically, by plotting percent passing
against sieve size in mm. Sieve size is often plotted on a logarithmic scale as per attached appendices
regarding aggregate grading for different stockpiles of aggregates.
5.1.2 Aggregate Specific Gravity and Absorption
When designing HMA, both the mass and volume of the aggregates and asphalt binder going into the
mixture must be known. The mass and volume of a material are related through the values of density or
specific gravity. Density refers to the mass of a material per unit volume. Density values for most
construction materials, including aggregates, are usually reported in units of g/cm3; density values for
HMA and other types of concrete are often reported in units of kg/m3High-density materials feel heavy
for their size.
The term specific gravity is often used interchangeably with density, but has a different meaning. Specific
gravity is defined as the ratio of the mass of a material to the mass of an equal volume of water. It can
also be defined as the ratio of the density of a material to the density of water. Because water has a density
of 1.0 g/cm3 at room temperature, the values of density in units of g/cm are equal to specific gravity
values. However, these terms should be used carefully. It is especially important to make sure that the
units are included when reporting density values. Because specific gravity values are ratios of two
numbers with the same units, specific gravity is dimensionless. The typical density of granite is 2.65
g/cm3 while the typical value for the specific gravity of granite is 2.65.
Aggregate specific gravity is determined using different techniques for coarse and fine aggregate.
Obtaining accurate specific gravity values for aggregates prior to performing an HMA mix design is
36
essential, and engineers and technicians responsible for mix designs must develop proper laboratory
techniques for these procedures. For coarse aggregate, specific gravity is determined using the weight-in-
water method. In this procedure, coarse aggregate is weighed in air, and then in water, in a mesh basket
suspended from a balance. A sketch of a weight-in-water apparatus is shown in figure below. The bulk
specific gravity of a sample of coarse aggregate is calculated using the following equation:
𝐴
𝐵𝑢𝑙𝑘�𝑆𝑝. 𝐺𝑟���� = � ��… … … … … … … … … … … … … … … . (5.3)
(𝐵 − 𝐶)
Where
Bulk Sp. Gr. = bulk specific gravity
A = weight of dry aggregate in air, g
B = weight of saturated, surface-dry aggregate in air, g
C = weight of saturated aggregate in water, g
Figure: Weight-in-water apparatus for determining coarse aggregates specific gravity, reproduced
drawing from NCHRP report no. 673
Because fine aggregate would fall through the wire mesh basket used in determining weight in-water, this
approach cannot be used in specific gravity measurements. Instead, the pycnometer method is used. This
technique requires the use of a pycnometer, which is simply a container that can be repeatedly filled with
the same—or nearly the same—volume of water. Usually, a volumetric flask is used for performing fine
aggregate specific gravity measurements. The flask is partially filled with distilled water and then about
500 g of saturated sand is placed in the flask. The flask is rolled and gently shaken to remove all air
bubbles and then more water is added until the flask is filled just to the calibration mark. The flask is
37
weighed, and the contents carefully poured into a metal pan which is then dried in an oven. The bulk
specific gravity of the fine aggregate is then calculated using the following equation:
𝐴
𝐵𝑢𝑙𝑘�𝑆𝑝. 𝐺𝑟 = � �… … … … … … … … … … … … … … … … . . (5.4)
𝐵+𝑊 −𝐶
Where
Bulk Sp. Gr. = bulk specific gravity
A = weight of oven-dry aggregate in air, g
B = weight of pycnometer filled with water to calibration mark, g
W = weight of saturated, surface-dry aggregate in air, g
C = weight of pycnometer with aggregate and filled with water to calibration mark, g
Figure 1: Pycnometer method of determining fine aggregate specific gravity reproduced from NCHRP
report no 673
5.1.3 Water Absorption
For both coarse aggregate and fine aggregate, absorption is an important property. It is calculated using
the following equation:
𝐴−𝐵
𝑊𝑎𝑡𝑒𝑟�𝑎𝑏𝑠𝑜𝑟𝑝𝑡𝑖𝑜𝑛��% = �𝑥�100%�� … … … … … … … … … … … … … … … … … … … . (5.5)
𝐵
where
Absorption = water absorption in weight, %
A = weight of saturated, surface-dry aggregate in air, g
B = weight of dry (air-dry or oven-dry) aggregate in air, g
38
5.1.4 Bulk specific gravity (G sb) and apparent specific gravity (G sa) of the aggregates
Different specific gravities in mix design practice are useful in making weight-volume conversions and
calculating the void content in compacted HMA.
𝐴
Apparent specific gravity (G sa)=
𝐵+𝐴−𝐶
𝐴
Bulk specific gravity (G sb)=
𝐵+𝐷−𝐶
Where; A=weight of oven-dry sample, B=weight of flask (pyconometer) filled with water, g, C=weight
of flask (pyconometer) filled with specimen and water to the calibration mark, D=saturated dry surface
weight (SSD). The results and calculations involved were reported in the presentation of results chapter
and attached in the APPENDIX SGA005a for both coarse and fine aggregates.
5.1.5 Fine Aggregate Angularity
The angularity of the fine aggregate fraction is as important as the angularity of the coarse aggregate
fraction to the performance of dense-graded HMA. In combination, the coarse and fine aggregates provide
strength to HMA, which helps minimize the potential for permanent deformation. AASHTO T 304,
Method A, Uncompacted Void Content of Fine Aggregate, is used to measure fine aggregate angularity.
A graded sample of fine aggregate (passing the 2.36-mm sieve) is placed within a specially made funnel
which allows the aggregate particles to freely drop into a cylinder of known volume (Figure 4-8). Using
the combined bulk specific gravity of the fine aggregate blend, the percent voids between the aggregate
particles is determined. Results from the fine aggregate angularity test represent this percent of
uncompacted voids in the fine aggregate; higher values of uncompacted voids indicate greater angularity
of the fine aggregate. Requirements for fine aggregate angularity as described in chapter four during
presentation of results. The requirements obtained in this study are nearly identical to those recommended
in the Superpave system.
The fine aggregate angularity % is calculated as follows:
𝑈𝑛𝑐𝑜𝑚𝑝𝑎𝑐𝑡𝑒𝑑�𝑉𝑜𝑖𝑑𝑠�%
𝐷𝑒𝑛𝑠𝑖𝑡𝑦�𝑜𝑓�𝑓𝑖𝑛𝑒�𝑎𝑔𝑔𝑟𝑒𝑔𝑎𝑡𝑒�𝑖𝑛�𝑘𝑛𝑜𝑤𝑛�𝑣𝑜𝑙𝑢𝑚𝑒�𝑐𝑦𝑙𝑖𝑛𝑑𝑒𝑟, 𝑃𝑠
= 100% − �𝑥�100%
𝐵𝑢𝑙𝑘�𝑠𝑝𝑒𝑐𝑖𝑓𝑖𝑐�𝑔𝑟𝑎𝑣𝑖𝑡𝑦�𝑜𝑓�𝑎𝑔𝑔𝑟𝑒𝑔𝑎𝑡𝑒�𝑓𝑖𝑛𝑛𝑒𝑟�𝑡ℎ𝑎𝑛�2.36𝑚𝑚
As per attached processed results in the appendix (APPPENDIX SET014) the uncompacted voids was
calculated on the basis of the above formula. The results show an average of 71% from the two sample
tested which was very higher value of uncompacted voids, this indicates greater angularity of fine
aggregate.
39
5.1.6 Clay Content
The presence of dust or clay coatings on aggregates can prevent the asphalt binder from properly coating
the aggregates within an HMA. This can lead to water penetrating the asphalt binder film and, therefore,
stripping of the asphalt binder from the aggregate. The Sand Equivalent test (AASHTO T 176, Plastic
Fines in Graded Aggregates and Soils by Use of the Sand Equivalent Test) is used to evaluate the
cleanliness of aggregates to identify when harmful clay-sized particles exist in an aggregate blend. The
procedure is conducted on the aggregate fraction of the blend that passes the 4.75-mm sieve. If hydrated
lime is used in the mixture, it should not be included in the fine aggregate used during the sand equivalent
test. The aggregate sample is placed within a graduated, transparent cylinder that is filled with a mixture
of water and flocculating agent. The sand equivalent in % is calculated as follows:
𝐶
𝑆𝑎𝑛𝑑�𝐸𝑞𝑢𝑖𝑣𝑎𝑙𝑒𝑛𝑡�% = �𝑥�100%
(𝐴−(𝐵+𝐶))
Where;
A = Cylinder total suspended reading in mm
B = Flocculating solution height in mm
C = Sedimented aggregate reading in mm
The combination of aggregate, water, and flocculating agent is then agitated for 45±5 seconds. After
agitation, the combination is allowed to sit at room temperature for 20 minutes. After the 20 minutes, the
heights of the sand particles and the sand plus clay particles are measured. The sand equivalent value is
then calculated as the ratio of the height of the sand to the height of sand plus clay, expressed as a
percentage as expressed in the above expression.
As per results obtained and attached in the APPENDIX SET014, the average value of 84% sand
equivalent was reported, this is very high sand equivalent value. High sand equivalent values are
desirable, since this indicates that the aggregate is relatively free of dust and clay particles. Therefore,
minimum values for sand equivalency are specified.
5.1.7 Aggregates Flakiness Index (FI)
Flakiness Index is one of the tests used to classify aggregates and stones. In Pavement design there are
specific requirements regarding the Flakiness Index of the materials. As explained earlier in chapter three
regarding Methodologies of the study. Flakiness Index is found by separating the flaky particles and
expressing their masses as a percent of the mass of the sample. The test is applicable to material passing
a 63mm sieve and retained on a 6.3mm sieve (ref BS 812:105.1:1989).
The value of flakiness index is calculated from the expression below as per CML test no. 2.4
𝑀3
𝐹𝑙𝑎𝑘𝑖𝑛𝑒𝑠𝑠�𝐼𝑛𝑑𝑒𝑥, 𝐹𝐼 = �𝑥�100%
40 𝑀2
Where;
M3 = weight of all the particles passing each groups
M2 = mass remaining after discarding any fraction whose mass iss 5% or less of the individual mass
retained M1 .
Specification for aggregates flakiness index for SMA is maximum 30% the results obtained showed an
average of 19.0% FI, which implies that the aggregate fit for road aggregates as per Tanzania Work
Specification Ministry of Work 1999. See the APPENDIX FI006a analysed results for Flakiness Index
test.
5.2 .1 Ten Percent Fines (TFV)
As explained earlier, the strength of the aggregate may be measured in a crushing test. The TFV gives a
relative measure of resistance of an aggregate to crushing under gradually applied load. In pavement
design there are specific requirements for the TFV of the material tested both in a dry and soaked
condition hereby indicated as TFV dry and TFV wet respectively. The graph below indicates the TFV value
450
400 y = 26.911x + 22.515
350
Gradual Load (kN)
300
250
200
150
100
50
0
0 2 4 6 8
%Fines 10 12 14
From the graph above the TFV wet is calculated by the linear equation:
𝑦 = 26.911𝑥 + 22.515
Where; y from the linear expression is Gradual applied load and x is the corresponding 10% fines. From
this expression the value of TFV wet = 292kN.
TFV dry is as shown in the graph below and the linear expression is as show below the graph.
𝑦 = 30.162𝑥 + 20.455
41
In expression above the load y is equal to the TFV dry=322 kN as x = 10% fines.
Other calculations required was evaluated on the analyzed results as per APPENDIX TFV009a and
TFV009b. The specification report value for TFV value for SMA design as per THM1 is minimum 90%
expressed as ratio of TFV wet to the TFV dry, in this case the calculation is as shown below:
𝑇𝐹𝑉�𝑤𝑒𝑡 292
TFF (wet/dry) = = = 91%
𝑇𝐹𝑉�𝑑𝑟𝑦 322
This ratio show good performance of the selected road aggregate in term of strength as it meet the required
strength as prior mentioned specifications.
Fines calculations
The gradual loads applied F (in kN), to the nearest whole number, required to produce 10% fines for each
test specimen with the percentage of material passing in the range of 7.5% to 12.5% from the following
equation as per CML2.7:
14𝑓
𝐹 =�
𝑚+4
Where; f is the maximum force kN and m = the percentage of material passing 2.36mm sieve at the
respective maximum force.
450
400 y = 30.162x + 20.451
350
300
Load (kN)
250
200
150
100
50
0
0 2 4 6 8 10 12 14
%Fines
5005.0𝑔 − 4324.3𝑔
𝐶𝑎𝑙𝑐𝑢𝑙𝑎𝑡𝑖𝑜𝑛�𝑜𝑓�𝑝𝑒𝑟𝑐𝑒𝑛𝑡�𝑙𝑜𝑠𝑠 = �𝑥�100% = 13.6%
5005.0𝑔
Test 2: Counter set to 500 revolutions
Mass of oven dried CA 16 Retained on #4 Sieve = 4003.8 g
Mass of oven dried CA 16 Retained on 3/8” Sieve = 1001.6 g
Total Mass Retained 5005.4 g
Mass of sample Retained on #8 Sieve after testing = 4369.70 g
5005.4�𝑔−4369.70�𝑔
𝐶𝑎𝑙𝑐𝑢𝑙𝑎𝑡𝑖𝑜𝑛�𝑜𝑓�𝑝𝑒𝑟𝑐𝑒𝑛𝑡�𝑙𝑜𝑠𝑠 = � �𝑥�100% = 12.7%
5005.4�𝑔
From the above calculations the LAA value is reported as the mean of two tests with less variation, the
LAA value is 13.2% which is very low Loss value which implies the high resistance to abrasive force.
5.2.3 Sulfate Soundness Test (AASHTO T104 – 97)
Soundness is the percent loss of materials from an aggregate blend during the sodium or magnesium
sulfate soundness test.
Aggregate Sieve Mass Retained Mass Retained Loss (g)
Before Test After Test
44
In this study the aggregates were fractioned in into five stockpiles including the mineral filler hereby
described as active filler (AF). For the first trial blend the proportions analysis is as shown in the curve
below.
The stockpiles were divided such that 0-3mm, 3-5mm, 5-10mm, 10-14mm and AF (active filler) and the
best trial proportions was found to be 30%, 9%, 15%, 43% and AF is 3%. From these proportions why
do we say Gap-Graded Hot Mix Asphalt? The existence of the large deviations between the value
proportions of the mid-sieves (3-5mm and 5-10mm stockpiles) is the best answer on this question.
BLENDING SM14
100.0
90.0
80.0
70.0
% Passing
60.0
50.0
40.0
30.0
20.0
10.0
0.0
0.0 0.1 1.0 10.0 100.0
Sieve Size - log scale
Min Spec Max Spec 0--3 mm 3--5mm
5--10mm 10--14mm AF BLENDED
Whereas P1, P2, P3, …,Pn are proportions of stockpiles in the blend and G1, G2, G3, …Gn are
individual specific gravity of the respective aggregate stockpile.
30+9+15+43+3
𝐵𝑢𝑙𝑘�𝑠𝑝𝑒𝑐𝑖𝑓𝑖𝑐�𝑔𝑟𝑎𝑣𝑖𝑡𝑦, 𝐺𝑠𝑏 = 30 9 15 43 3 = 2.621
+ + + +
2.578 2.616 2.641 2.658 2.447
45
30+9+15+43+3
𝐴𝑝𝑝𝑎𝑟𝑒𝑛𝑡�𝑠𝑝𝑒𝑐𝑖𝑓𝑖𝑐�𝑔𝑟𝑎𝑣𝑖𝑡𝑦, 𝐺𝑠𝑎 = 30 9 15 43 3 = 2.648
+ + + +
2.63 2.644 2.620 2.688 2.447
5.3.1 Marshall Mix Design of SMA using Cellulose fibres stabilizing additive
The following plots analyzes the Marshall design parameters and the optimum binder content obtained
in the design.
19000
18000
2.35 17000
16000
15000
2.3
14000
13000
2.25 12000
11000
10000
2.2
5.5 6 6.5 7 7.5 8 8.5 5.5 6 6.5 7 7.5 8 8.5
Binder content (%) Binder content (%)
10.0 3.5
8.0 3.0
2.5
6.0
2.0
4.0 1.5
2.0 1.0
5.5 6 6.5 7 7.5 8 8.5 5.5 6 6.5 7 7.5 8 8.5
Binder content (%) Binder content (%)
𝑥1+𝑥2+𝑥3 7.40+7.40+7.50
:𝑂𝑝𝑡𝑖𝑚𝑢𝑚�𝑏𝑖𝑛𝑑𝑒𝑟�𝑐𝑜𝑛𝑡𝑒𝑛𝑡 = = = 7.43%.
3 3
Using the binder content obtained in the equation above the Marshall flow was found to be 3.1 mm as
shown above and the other graph VFB and VMA corresponding to the obtained optimum binder content
was given in the design graph above.
46
VFB v/s Binder content VMA v/s Binder content
25
90 24 5.5 6 6.5 7 7.5 8 8.5
Voids filled with binder (%)
From the above design graphs analyzed the cellulose fibre dossage 0.3% of the mix as an additive results
were its parameters summarized in table given below:
47
5.3.3 Marshall Mix Design of SMA14 using Reclaimed Rubber (8% of the binder) as stabilizing
additive
The following plots analyzes the Marshall design parameters and the optimum binder content obtained in
the design.
2.350 15000
14000
13000
2.300 12000
11000
10000
2.250
9000
8000
2.200 7000
5.5 6 6.5 7 7.5 8 8.5 5.5 6 6.5 7 7.5 8 8.5
Binder content (%) Binder content (%)
8.00 3
7.00 + 7.10 + 7.00
6.00 = = 7.03%
3
4.00
The optimum binder content with Reclaimed
2.00 Rubber was 7.0%.The other design parameters
5.5 6 6.5 7 7.5 8 8.5 was estimated based on the optimum binder
Binder content (%)
content
4.50
80.00
Marshall flow (mm)
4.00
3.50 70.00
3.00
60.00
2.50
2.00 50.00
1.50
40.00
1.00 5.5 6 6.5 7 7.5 8 8.5
5.5 6 6.5 7 7.5 8 8.5
Binder content (%) Binder content (%)
48
VMA v/s Binder content
25.00
24.00 5.5 6 6.5 7 7.5 8 8.5
The SMA14 with Reclaimed Rubber 8% of the binder content mix design parameters summary.
49
5.3.4 Marshall Mix Design of SMA14 usin Polyvinyl Chloride (PVC) (8% of the binder) as stabilizing
additive
The following plots analyzes the Marshall Design parameters and the optimum binder content obtained
in the design.
2.300 7000
5.5 6 6.5 7 7.5 8 8.5 5.5 6 6.5 7 7.5 8 8.5
Binder content (%) Binder content (%)
8.00 𝑂𝑝𝑡𝑖𝑚𝑢𝑚�𝑏𝑖𝑛𝑑𝑒𝑟�𝑐𝑜𝑛𝑡𝑒𝑛𝑡 =
3
6.00 7.20 + 7.20 + 7.20
= = 7.20%
4.00 3
The optimum binder content with Polyvinyl
2.00
5.5 6 6.5 7 7.5 8 8.5 Chloride PVC was 7.2%.The other design
Binder content (%)
parameters was estimated based on the optimum
binder content
Marshall flow v/s Binder content
VFB v/s Binder content
5.00
4.50 90.00
Marshall flow (mm)
4.00
80.00
3.50
3.00 70.00
2.50 60.00
2.00
50.00
1.50
1.00 40.00
5.5 6 6.5 7 7.5 8 8.5 5.5 6 6.5 7 7.5 8 8.5
Binder content (%) Binder content (%)
50
VMA v/s Binder content
20.00
5.5 6 6.5 7 7.5 8 8.5
18.00
17.00
16.00
15.00
From the above analyzed data it can be concluded diffrently in each design parameters as follows:
I. The bulk density of the specimens increased when PVC additive used compared to other
stabilizing additives Cf and Reclaimed rubber as shown in the comparison curve below:
Bulk density v/s Binder content PVC
2.450
Cf
Bulk density (g/cm3)
2.400 Rubber
2.350
2.300
2.250
2.200
5.5 6 6.5 7 7.5 8 8.5
Binder content (%)
II. The Cellulose fibre has shown better performance in case of Marshall stability by achieving higher
stability value trends than the rest which means it has better resistance to rutting and deformations
by the heavy loadings. The PVC has shown lowest marshall stability trends compared to the three
on study stabilizing additives though it has achieved the required design stability of min 6kN.
19000
18000
17000
16000
15000
14000
13000
12000
11000
10000
9000
8000
7000
5.5 6 6.5 7 7.5 8 8.5
Binder content (%)
51
III. The cellulose fibre seems to have higher void content trends compared to the rest stabilizing
additives studied with the Reclamed rubber lagging behind the in void ontent trends.
10.00 Cf
6.00
4.00
2.00
5.5 6 6.5 7 7.5 8 8.5
Binder content (%)
IV. The reclaimed rubber stabilizing additives has shown large marshall flow compared to others this
is due to the absorptive nature of the rubber and its high elastic nature compared to the PVC and
Cf
4.00
3.50
PVC
3.00
Cf
2.50
Rubber
2.00
1.50
1.00
5.5 6 6.5 7 7.5 8 8.5
Binder content (%)
V. The VFB of the ruberized SMA has shown slightly graeter than PVC stabilized SMA while the
cellulose stabilized SMA having low VFB compared to the rest of studied additives. The curve
below analyzes the difference.
90.00
Voids filled with binder (%)
80.00
70.00
PVC
60.00
cf
50.00
Rubber
40.00
5.5 6 6.5 7 7.5 8 8.5
Binder content (%)
52
VI. The VMA smees to be slightly changing in PVC due to high adhessiveness of PVC compared to
the rubber and cellulose fibre which are much affected by rebound property
18.00
17.00 PVC
Cf
16.00
Rubber
15.00
3.00
2.70
2.40
2.10
1.80
1.50
1.20
0.90
0.60
0.30
0.00
CELLULOSE FIBRE RECYCLED TYRES(RUBBER) PLASTIC (PVC)
ADDITIVES
53
CONCLUSION
Based on test results analysed and discussed in the last chapter the following conclusions were made:
The Marshall results has shown the specimens with cellulose fibre has high optimum binder
content than the rest due to the absorptive nature of the fibres.
TheMarshall Stability at the optimum binder content of the cellulose fibre has shown greater
stabilizing additives than are of the three. With only 12.8kN and 16.5kN of PVC and rubber the
celulose fibre has stability of 21.5 kN whih is very high stability only achieved with greater care
in controlling aggregate interlocking factors.
The bulk density of the specimens increased when PVC additive used compared to other
stabilizing additives Cf and Reclaimed rubber.
The cellulose fibre seems to have higher void content trends compared to the rest stabilizing
additives studied with the Reclamed rubber lagging behind the in void ontent trends.
The reclaimed rubber stabilizing additives has shown large marshall flow compared to others this
is due to the absorptive nature of the rubber and its high elastic nature compared to the PVC and
Cf
The VMA smees to be slightly changing in PVC due to high adhessiveness of PVC compared to
the rubber and cellulose fibre which are much affected by rebound property
From the laboratory results, the results of three stabilizing additives were evaluated in their
optimum binder content and the results shown that the cellulose fibre stabilizers were found to be
more effective in reducing the draindown than polynivyl chloride due to absorptive nature of the
cellulose fibre.
Generall cellulose has shown good quality results in both stability and flow as well as draindown
reduction compred to the rest of the studied stabilizing additives. That’s why most of the local
contractors and highway ageny are daily importing cellulose fibres from German for use in SMA
design.
54
RECOMMENDATIONS
I. The Bituminous material Laboratory should be in use very early to erase the problem of students
to search their own placement in conducting their projects.
II. The project time schedule should not be in the same schedule as other modules this reduce
students’ concentrations in either case and sometimes in both case. There should a full semester
for project and research only. This will provide wide understanding to the students.
III. Updating technology in Civil engineering is likely lagging behind the normal world technology,
the institute should help the government and save as an asphalt center in which designers and
technologist are molded.
IV. Our department seems to be like a nice and quality borrow pit for the hig hway labour force
in this country, it should update its teaching system it should invest much in highway material
engineering because it is naked true that the national lack highway material engineering experts
as the result we are helped by expert material engineers from South Africa and Ethiopia. Let
start at DIT.
V. The department also should invest in Instrumentation for highway engineering material
equipment, our people must be ‘hand on eye on’ in equipment instru mentation.
VI. In moving to teaching factory the Institute should invest much in action and ALL people
say ‘lets do’ any good substance start from good laboratory of good knowledgeable people
with good hea d.
VII. The department should buy a full set of SUPERPAVE Equipment (CONTROL) as it will help
the students to understand more practically and shape them to be whom they wish to be.
55
REFERENCES
AASHTO. (1997). “Standard Specification for Plastic Fines in Graded Aggregates and Soils by Use of
the Sand Equivalent Test.” T176-86, Washington D.C.
AASHTO. (1997). “Standard Specification for Soundness of Aggregate by Use of Sodium Sulfate or
Magnesium Sulfate.” T104-97, Washington D.C.
AASHTO. (1994). “Standard Specification for Resistance to Degradation of S mall -size Course
Aggregate by Abrasion and Impact in the Los Angeles Machine.” T96-94, Washington D.C.
AASHTO. (1997). “Standard Specification for Sieve Analysis of Fine and Course Aggregate.” T27 -
97, Washington D.C.
AASHTO. (1991). “Standard Specification for Clay Lumps and Friable Particles in Aggr egate.” T112-
91, Washington D.C.
AASHTO. (1995). “Standard Specification for Sieve Analysis of Mineral Filler for Road and Paving
Materials.” T37-95, Washington D.C.
AASHTO. (1993). “Standard Specification for Bulk Specific Gravity of Compacted Bituminous
Mixtures Using Saturated Surface-Dry Specimens.” T166-93, Washington D.C.
AASHTO. (1995). “Standard Specification for Specific Gravity and Absorption of Fine Aggregate.”
T84-95, Washington D.C.
AASHTO. (1991). “Standard Specification for Specific Gravity and Absorption of Course Aggregate.”
T85-91, Washington D.C.
AASHTO. (1999). “Standard Method of Test for Deter mining the Asphalt Binder Content of Hot Mix
Asphalt (HMA) by the Ignition Method.” T308-99, Washington D.C.
AASHTO. (1995). “Standard Specification for Specific Gravity of Soils.” T100 -95, Washington D.C.
ASTM. (1994). “Standard Test Method for Sieve Analysis of Mineral Filler for Road and Paving
Materials.” D546, West Conshohocken, Pa.
56
ASTM. (1993). “Standard Test Method for Specific Gravity and Absorption of Course Aggregate.”
C127, West Conshohocken, Pa.
ASTM. (1997). “Standard Test Method for Specific Gravity and Absorption of Fine Aggregate.” C128,
West Conshohocken, Pa.
Illinois Department of Transportation. (1997). “Standard Specifications for Road and Bridge
Construction.” State of Illinois.
Illinois Department of Transportation. (2000). “Illinois Modified Test Procedure: Standard Practice for
Superpave Volumetric Design for Hot-Mix Asphalt (HMA).” State of Illinois.
Kandhal, Prithvi S., Parker Jr., Frazier, and Mallick, Rajib B. (1997). “Aggregate Tests for Hot Mix
Asphalt: State of the Practice.” NCAT Report No. 97-6, Auburn University, Al.
NAPA Research and Education Foundation. (1996). “Hot Mix Asphalt Materials, Mixture Design and
Construction.” 2 nd Edition, Lanham, Maryland.
National Center for Asphalt Technology. (1998). “Professor Training Course in Asphalt Technology.”
SHRP. (1994). “Level One Mix Design: Materials Selection, Compaction, and Conditioning.” National
Research Council, Washington D.C.
57
APPENDICES
APPENDIX PSDA001
30.0
20.0
10.0
0.0
0.0 0.1 1.0 10.0 100.0
Sieve Size - log scale
REMARKS:
Date/Signature
30.0
20.0
10.0
0.0
0.0 0.1 1.0 10.0 100.0
Sieve Size - log scale
REMARKS:
Date/Signature
30
20
10
0
0.0 0.1 1.0 10.0 100.0
Sieve Size - log scale
REMARKS:
Date/Signature
30
20
10
0
0.0 0.1 1.0 10.0 100.0
Sieve Size - log scale
REMARKS:
Date/Signature
63 50
50 37.50
37.5 28
28 20
20 14
14 10 193 157.8 35.3 18.28
10 6.3 219.6 180.6 39.0 17.76
REMARKS
MATHIAS, Kulwa
PROJECT DATA COLLECTION
Central Material Laboratory
APPENDIX FI006a
63 50
50 37.50
37.5 28
28 20
20 14 487 435.5 51.0
14 10 292 212.9 79.0 27.06
10 6.3 27 4.0 23.0 85.19
REMARKS
MATHIAS, Kulwa
PROJECT DATA COLLECTION
Central Material Laboratory
APPENDIX TFV009a
PROJECT TITLE : EFFECT OF STABILIZING ADDITIVES AND MINERAL FILLERS MATHIAS, Kulwa
ON THE PERFORMANCE OF GAP- GRADED HOT MIX ASPHALT (GGHMA) ADM NO. 140131452515
450
400 y = 30.162x + 20.455
350
Applied Force kN
300
250
200
150
100
50
0
0 2 4 6 8 10 12
Fines %
TESTED BY: REGISTRATION NUMBER
MATHIAS, Kulwa 140131452515
Date/Signature
450
y = 26.911x + 22.515
400
350
300
250
200
150
100
50
0
0 2 4 6 8 10 12 14
Date/Signature
PROJECT TITLE: EFFECT OF STABILIZING ADDITIVES AND MINERAL MATHIAS, Kulwa ADM
FILLERS ON THE PERFORMANCE OF GAP- GRADED HOT MIX
ASPHALT(GGHMA) No. 140131452515
LAB USED: CML - TANROADS Test Method: ASTM C127 Sampled Date 10.01.2018
Date/Signature
MATHIAS, Kulwa
Central Material Laboratory
APPENDIX SGA005b
LAB USED: CML - TANROADS Test Method: ASTM C127 Sampled Date 10.01.2018
MATHIAS, Kulwa
Central Material Laboratory
APPENDIX SET014
% AIR VOID IN LOOSELY COMPACTED FINE AGGREGATE (in SMA design) AASHTO T304
Bulk specific gravity of fine aggreagate finer than 2.36mm g/cm3 2.578 2.578
Date/Signature `
PROJECT DATA COLLECTION
MATHIAS, Kulwa
Central Material Laboratory
APPENDIX BA001
BLENDING SM14
100.0
90.0
80.0
70.0
60.0
% Passing
50.0
40.0
30.0
20.0
10.0
0.0
0.0 0.1 1.0 10.0 100.0
Sieve Size - log scale
Min Spec Max Spec 0--3 mm 3--5mm
REMARKS:
5--10mm 10--14mm AF BLENDED
Sample
Procedure
1 2
Mass of empty bottle, gm 38.302 40.204
DATE/ SIGNITURE
MATHIAS, Kulwa
Project Data Collection
Central Material laboratory
APPENDIX DT006
Ductility Test
ASTM D 113/ CML 3.7
Sample No
Procedure
1 2 3
Initial Reading, mm 55 53
2405 2511
Ductility in mm
Average Ductility in mm 2458
Remark:
DATE/ SIGNITURE
MATHIAS, Kulwa
Project Data Collection
Central Material laboratory
APPENDIX GSB004
Sample No
Procedure
1 2 3
o
Flash Point C 320 322
o
Fire Point C 358 363
o
Flash Point C Min flash
o o
point value between sample 1 Flash Point C is 320 and Fire point is 358 C
and 2
Remark:
DATE/ SIGNITURE
MATHIAS, Kulwa
Project Data Collection
Central Material laboratory
APPENDIX PT001
Penetration of Bitumen
ASTM D 5 / AASHTO T49
Number of Test
Procedure
1 2 3 1 2 3
Initial Reading 0 0 0
Final Reading 66 67 65
Penetration value (0.10 mm) 66 67 65
* N.B Test Tempreature, load and time shall be 250c, 100 gr. & 5sec. respectively.
Remark:
DATE/ SIGNITURE
MATHIAS, Kulwa
Project Data Collection
Central Material laboratory
APPENDIX PT001
Softening Point
ASTM D 36
Number of Test
Procedure
Sample 1 Sample 2
Ring & Ball 1 2 1 2
o
Softening Point in C 48.45
Remark:
DATE/ SIGNITURE
MATHIAS, Kulwa
Project Data Collection
Central Material laboratory
APPENDIX BVT005
DATE/ SIGNITURE
MATHIAS, Kulwa
Project Data Collection
Central Material laboratory
APPENDIX II-001
TANZANIA NATIONAL ROADS AGENCY
SUMMARY SHEET
10.0 3.5
8.0 3.0
2.5
6.0
2.0
4.0
1.5
2.0 1.0
5.5 6 6.5 7 7.5 8 8.5 5.5 6 6.5 7 7.5 8 8.5
Binder content (%) Binder content (%)
23
80
22
70 21
20
60 19
18
50 17
16
40 15
5.5 6 6.5 7 7.5 8 8.5
Binder content (%) Binder content (%)
MATHIAS, Kulwa
SMA - Mix Design with Cellulose Fibre
Central Material Laboratory
APPENDIX II-003
TANZANIA NATIONAL ROADS AGENCY
SUMMARY SHEET
2.350 10000
9000
8000
2.300 7000
5.5 6 6.5 7 7.5 8 8.5 5.5 6 6.5 7 7.5 8 8.5
Binder content (%) Binder content (%)
4.00
8.00
3.50
6.00 3.00
2.50
4.00 2.00
1.50
2.00 1.00
5.5 6 6.5 7 7.5 8 8.5 5.5 6 6.5 7 7.5 8 8.5
Binder content (%) Binder content (%)
19.00
80.00
70.00 18.00
60.00 17.00
50.00 16.00
40.00 15.00
5.5 6 6.5 7 7.5 8 8.5
Binder content (%) Binder content (%)
MATHIAS, Kulwa
SMA - Mix Design with Pollvinyl Chloride PVC
Central Material Laboratory
APPENDIX II-002
TANZANIA NATIONAL ROADS AGENCY
SUMMARY SHEET
16000
4.00
8.00
3.50
6.00 3.00
2.50
4.00 2.00
1.50
2.00 1.00
5.5 6 6.5 7 7.5 8 8.5 5.5 6 6.5 7 7.5 8 8.5
Binder content (%) Binder content (%)
23.00
80.00
22.00
70.00 21.00
20.00
60.00 19.00
18.00
50.00 17.00
16.00
40.00 15.00
5.5 6 6.5 7 7.5 8 8.5
Binder content (%) Binder content (%)
MATHIAS, Kulwa
SMA - Mix Design with Reclaimed Rubber
Central Material Laboratory
APPENDIX II-004
TANZANIA NATIONAL ROADS AGENCY
SUMMARY SHEET
VIM v/s Binder content PVC Marshall flow v/s Binder content
5.00
10.00 Cf
4.50
Marshall flow (mm)
Void content (%)
Rubber 4.00
8.00
3.50
PVC
6.00 3.00
Cf
2.50
Rubber
4.00 2.00
1.50
2.00 1.00
5.5 6 6.5 7 7.5 8 8.5 5.5 6 6.5 7 7.5 8 8.5
Binder content (%) Binder content (%)
19.00
80.00
70.00 18.00
PVC
60.00 17.00 PVC
cf
50.00 16.00
Cf
Rubber
Rubber
40.00 15.00
5.5 6 6.5 7 7.5 8 8.5
Binder content (%) Binder content (%)
MATHIAS, Kulwa
SMA - Mix Design Parameters variations
Central Material Laboratory
APPENDIX FI006
RECYCLED PLASTIC
CELLULOSE FIBRE
TYRES(RUBBER) (PVC)
BINDER % 7.43 7.0 7.2
3.00
2.70
2.40
2.10
1.80 TESTED: ADMISSION NUMBER
1.50
BY MATHIAS, Kulwa BENG 15 CE 140131452515
1.20
0.90
0.60
0.30
0.00
CELLULOSE FIBRE RECYCLED TYRES(RUBBER) PLASTIC (PVC)
ADDITIVES
MATHIAS, Kulwa
PROJECT DATA COLLECTION
Central Material Laboratory
APPENDIX WORKING PICTURES AND INSTRUMENTS