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To cite this article: Haris Ishaq & Ibrahim Dincer (2019): A new energy efficient single-stage flash
drying system integrated with heat recovery applications in industry, Drying Technology, DOI:
10.1080/07373937.2019.1702557
CONTACT Haris Ishaq haris.ishaq@uoit.net Clean Energy Research Laboratory, Faculty of Engineering and Applied Science, University of Ontario
Institute of Technology, 2000 Simcoe Street North, Oshawa, Ontario, L1H 7K4, Canada
Color versions of one or more of the figures in the article can be found online at www.tandfonline.com/ldrt.
ß 2019 Taylor & Francis Group, LLC
2 H. ISHAQ AND I. DINCER
study investigated the supersonic separator for the balance and modeling assumptions. The drying pro-
purpose of reducing cost for post-combustion capture. cess was also investigated in terms of different param-
The commercial offshore gas processing units nor- eters and numerical methods. Adnan and Hossain[13]
mally ends up with methanol losses which are hydrate published a study considering the biomass drying and
inhibitor during the exportation and processing of gasification for hydrogen production. The wet com-
gas. The energy usage of different industries is position of biomass needs to pass through the drying
described in Figure 1 in past 25 years. Steel, cement process before approaching the gasifier. They investi-
and glass industries occupy a huge part of total energy gated the biomass gasification process accompanied
requirements, and these industries are also providing with drying and chemical looping combustion energy
with the high amount of materials production. supply option using Aspen plus software. The
Currently, the leading industries with respect to the designed configuration consisted of different subsys-
waste heat source temperatures are steel, cement and tem such as drying unit, gasifier, chemical looping
glass industries.[2,4,8,9] combustion section and gas purification process.
Waste heat recovery from cement industry blast Paranuk[14] presented a mathematical model-based
furnace slag usually faces some contradictions by the study to calculate the adsorbers for methanol concen-
requirement of generating amorphous slag to use it tration on zeolites and drying. Their study presented a
for cement production.[10] The Barati et al.[11] pre- mathematical model employing molecular sieve zeolite
sented a study on waste heat recovery from molten properties to describe the methanol concentration and
slag. The high temperature range 1200–1600 C of slag drying processes. They proposed a new approach for
presents some opportunities to recover the waste heat. the adsorption plants calculation for binary system
Presently, the work is being done of three different separation and design.
technologies for recovering slag waste heat. The recov- Dincer and Sahin[15] presented a comprehensive
ery as hot steam is best developed it has the recovery study on the thermodynamic analysis for drying pro-
efficiency of 65%. Ishaq et al.[3] conducted thermal cess model. A new model was presented in this study
management of the cement slag to produce useful out- for thermodynamic analysis of drying process consid-
puts of hydrogen and electricity. The technique ering exergy approach. Exergy efficiencies are derived
employed for hydrogen production was the thermo- as functions of heat and mass transfer parameters. A
chemical CuCl cycle. demonstrative example was taken to validate the dry-
Banooni et al.[12] presented a review paper on the ing model and its applicability comparison with actual
modeling of flash and pneumatic drying. This study drying processes in terms of specific exergies, temper-
focused on different pneumatic drying approaches atures, moisture contents, inlet and outlet exergies
used in literature and conducted an analysis for dis- and humidity ratios. This paper established the drying
similar mathematical models and considered various process in terms of how to optimize the drying pro-
components namely; complementary equations, cess and selectivity of the optimal configuration of
DRYING TECHNOLOGY 3
drying process. Ezzat and Dincer[16] proposed a solar- recovering heat from flue gas and employing that heat
geothermal energy based integrated system for varies for drying process.
application and considered drying as one of the major
subsystems. The useful commodities proposed by the
integrated system were industrial cooling, drying, elec-
tricity, hot water and space heating and results were Flue gas thermal management
justified using energy and exergy analyses. This was The industrial flue gas from the cement kiln reaches
proved to be an innovative solar energy-based integra- to a heater B1 at 650 C of temperature. This heater is
tion with high efficiencies of 69.6% and 42.8% installed to control the flue gas temperature at 450 C
respectively. as per requirement and this additional heat is used to
Fernando and Amarasinghe[17] conducted a study meet the heating requirement for other processes. The
on the mathematical model and kinetics of the hot composition of the flue gas is presented in Table 1.
air-drying process for coconut coir pith. The operat- This flue gas then reaches to a heat exchanger B2. In
ing temperature for the coir pith was considered in this heat exchanger, air is entered via cold stream S1
the range of 100 to 240 C to investigate the com- and flue gas enters to the heat exchanger via hot
pressed coir pith rehydration ability by means of vol- stream S4. Some amount of heat is transferred from
ume expansion. The optimum temperature for hot air the flue gas to the air as this rise in air temperature is
drying was established at 140 C. Stenstrom[18] pub- used for drying purpose. Fresh air is heated from the
lished a review study on the biofuels drying processes. ambient temperature to 300 C which is further
This study considered various types of drying proc- employed to drying process.
esses such as flash drying, rotary drying (requires high
temperature source) and bed dryers. The bed type
dryers offer low temperature requirement, robust
design and controlled capacity in terms of hot air Single-stage flash drying
temperature. The hot air stream reaches the convective dryer via
A unique system utilizing the industrial waste
stream S2 and solid raw material enters through
heat and utilizing it for drying purpose is proposed
stream S6. This convective dryer is set to operate in
in this study. Some gaps have been observed in the
co-current gas flow direction. The heat duty of the
open literature about an efficient recovery of the
convective dryer is found to be 6.17 kW. The compos-
waste heat for useful purposes such as drying. The
ition of the raw material which is taken into consider-
flue gas leaves the cement kiln at very high tem-
ation for drying purpose is tabulated in Table 2. The
perature and offers the room for heat recovery. This
moisture content is removed from the raw material
novel integration is simulated using Aspen Plus
with the help of hot air. The significant results of the
industrial software (9.0). The explicit objective of the
convective dryer are arranged in Table 3. A pipeline
proposed system as (i) to recover the industrial heat
of 12 meters with 0.3 m inner diameter and 90-degree
offered by flue gas via thermal management, (ii)
pipe angle is used which gives a pressure drop of 7.24
simulate and design the drying process required
within the same industry, (iii) to employ the recov- mbar and saltation velocity is 9.77 m/s. The mixture
ered heat from industrial thermal management for then reaches to the cyclone separator B6 which is set
drying process and (iv) separate nitrogen from the to follow the Muschelknautz calculation method with
flue gas for ammonia synthesis. The proposed model diameter of 0.8 meters. The detailed working of the
is investigated in term of energetic and exergetic cycle separator is shown in Figure 4 to display the
approach and efficiencies of the single-stage flash functionality and the separation method of cyclone
drying process are established. separator. This cyclone separates the major moisture
part with hot air through stream S11 and solid stream
is separated out via S12. The moisture and hot air
Methodology and system description streams are then introduced to a solid separator filter
The proposed system is analyzed using thermo- with 6 cells and 1.48 m2 filtering bag area. This filter
dynamic approach. Figure 2 displays the schematic of further removes the remaining solids from the stream
the proposed system while the Aspen Plus simulation and leaves the moisture with hot air via stream S14
model is presented in Figure 3. The cement industry and separated solids are proceeded to the mixer B9
is taken into consideration for both purposes; which separates the solid raw material.
4 H. ISHAQ AND I. DINCER
Figure 2. Schematic layout of the newly designed system for single-stage flash drying.
Figure 3. Aspen Plus flowsheet diagram of the proposed system displaying the thermal management and utilization of recovered
heat for drying.
Table 1. Flue gas composition. industrial software Aspen Plus. The 25 C and of
Composition Wt % 101.3 kPa are assumed to be ambient temperature
H2O 5.6 and pressure.
N2 14.3 Heater B1
CO2 72.1
O2 5.9
Ar 2.1 _ s4 hs4 þ Q_ out
_ s3 hs3 ¼ m
m (1)
T
_ s4 exs4 þ Q_ out 1 _ d
0
chemical exergy calculations, all gases are considered _ s3 exs3 ¼ m
m þ Ex (2)
as real gases. The IDEAL property method is used in T
6 H. ISHAQ AND I. DINCER
Figure 5. The moisturized solid flowrate effect on dryer heat duty and solid residence time.
8 H. ISHAQ AND I. DINCER
pressure of the input stream S9 is kept constant at flowrate in stream S17 and ammonia flowrate in streams
100 kPa but with the rise in moisturized solid flowrate S22 and S22. The nitrogen reacts with hydrogen at
from 0.1 to 1 kg/s, the output pressure of stream S10 350 C and 50 bar to produce ammonia and fractional
drops down from 100 kPa to 97 kPa. As the input pres- conversion of ammonia is 0.25. Two reactors are placed
sure remains steady and output pressure drops down, it in series to achieve high production rate. It can be
causes pressure drop to increase from 0 to 3 kPa. depicted from the figure that both nitrogen and ammo-
nia flowrates increase with the rise in flue gas flow rate.
Figure 8 exhibits the effect of conversion rate on the
Flue gas flow rate and conversion ratio effect on
ammonia flowrate in reactors B13 and B14. The range of
ammonia synthesis capacity
the conversion ratio is considered between 0.15 and
The nitrogen gas is separated from the flue gas which is 0.45. Both of the reactors are set to operate at the nitro-
later used for ammonia synthesis. Although this study gen fractional conversion of 0.25. With the rise in the
has key focus on drying process, it is important to inves- conversion ratio from 0.15 to 0.45, the ammonia produc-
tigate the performance of the ammonia synthesis unit tion flowrate increases from 3.93 to 11.8 mol/s in reactor
and ammonia production capacity. This physical B13 and increases from 7.28 to 18.3 mol/s in reactor B14.
importance of these parametric studies is to explore the As the product of first reactor is set to be fed in the
functionality of the ammonia synthesis system and to second reactor, the ammonia flowrate stream leaving the
investigate how ammonia production will be effected second reactor carrier high flowrate of ammonia.
with the input flowrate of the flue gas and the conversion
ratios of the ammonia synthesis reactors. It is also sig- Effect of the solid and mixed stream flowrates in
nificant to scale-up the design configuration. Figure 7 S10 on the solid and moisturized air flowrates
displays the effect of the flue gas flowrate on the nitrogen
The key focus of this study is on the drying process
which makes it obligatory to investigate the drying
process in deep. This physical importance of these
parametric studies is to investigate the moisture ratio
in the solid stream, to scale-up the current design and
to explore the solid and moisturized air flowrates.
These studies are important to investigate the effect of
the solid and mixed stream flowrates within the same
stream S10 on the solid and moisturized air flowrates.
Figure 9 shows the effect of the solid and mixed flow-
rate of stream S10 on the moisture carrying air flow-
rate in stream S15 and dry solid flowrate in S16. It
can be depicted that the flow rate of moisturized air
Figure 6. Solid input flowrate effect on the inlet and outlet and solid increases with rise in input streams. Figure
pressures and pressure drop in pipe B5.
Figure 7. Flue gas flowrate effect on nitrogen and ammonia Figure 8. Effect of ammonia conversion ratio on the capacity
flowrates. of ammonia synthesis.
DRYING TECHNOLOGY 9
Figure 11. Hot air flowrate effect on the pressure drop in filter B7.
Figure 9. Effect of solid and mixed stream S10 on moisturized through filter B7. This study helps in predicting the
air and solid flowrates. pressure drop in the filter. Figure 11 exhibits the effect
of hot air flowrate on the inlet and outlet pressures of
the filter. The stream S11 is the inlet stream to the fil-
ter while S14 is the outlet stream to the filter. Two
different types of lines are representing the pressures
of the inlet and outlet streams according to the
legends. The upper solid line represents the inlet pres-
sure which is a bit higher while the lower dotted line
represents the outlet pressure of stream S14. The dif-
ference in the pressures of these two streams S11 and
S14 can provide us with the pressure drop values. The
pressure of the stream S11 drops down from 99.1 kPa
to 72.2 kPa while the pressure of the stream S14
decreases from 97.5 kPa to 70.7 kPa.
Model validation
The current study proposes a new approach of recov-
Figure 10. Effect of moisturized air and solid flowrates in ering industrial waste heat and proposes an integra-
stream S10 on solid and moisturized air.
tion to employ the recovered heat for single-stage
flash drying within the same cement plant (Table 4).
10 considers moisturized solid in stream S10 on x-
As of now, additional heat is employed to operate the
axis, moisturized air flowrate in stream S10 on y-axis
drying section and to input the hot air while this pro-
and investigates the effect of these two parameters on
posed configuration recovers the heat from the same
the solid and moisturized air flowrates. The range of
plant and employs it for drying purpose. The study
the moisturized solid is taken between 0.1 to 2 kg/s. It
proposes a new system of this nature. Thus, the sub-
can be depicted that the increase in the inlet flowrate systems can be validated with the literature. The pre-
causes outlet flowrates of dry solid and moisturized sent design of drying is validated with the simulation
air to increase simultaneously. study conducted by Morey et al.[19] using Aspen Plus
industrial software. Dogbe et al.[20] presented a study
on the thermodynamic analysis of a sugar mill using
Hot air flowrate effect on the pressure drop in
waste-heat recovery which can be used for the valid-
filter B7
ation of the present study. An ammonia production
The significance of this study is to investigate the system using Haber Bosch process was published by
pressure drop during the drying process. Some pres- Cinti et al.[21] can be used to the validation of the
sure drop takes place when working stream passes ammonia synthesis subsystem. They used the
10 H. ISHAQ AND I. DINCER
Table 4. Comparative table for the validation of the proposed system with subsystems of heat recovery, industrial drying and
ammonia synthesis.
Reference Analysis type Results
Ross et al.[22] Pressurised flash drying of Reduced coal moisture from 67 wt% to between 30 and 40 wt%,
Yallourn lignite Yallourn lignite feed rate of 725 kg/h.
Entrained flash drying occurred at 10 bar and 800 C.
Gwak et al.[23] Flash drying system and drying Pressure range between 1 to 40 bar.
characteristics low rank coal. Temperature range between 200 to 600 C.
Coal mass rate of 10 g/min.
Coal input temperature of 25 C.
Almost 98% of the moisture was removed.
Adnan and Hossain[13] Integrated drying and biomass Dryer input flowrate of 100 kg/h.
gasification Feed moisture content varied between 0 and 45 wt%.
Simulations were performed with different moisture weights of 15 wt%,
30 wt% and 45 wt%.
Dogbe et al.[20] Thermodynamic assessment of the Aspen Plus waste heat recovery on sugar plant.
sugar mill through waste-heat Integration reduced the irreversibility of sugar-drying unit by 76%.
recovery technologies Cogeneration increased the exergy efficiency by 1.7%.
The flowrate of bagasse was 6447 kJ/kg.
The exergetic efficiency was found to be 23.6%.
Alobaid et al.[24] Numerical and experimental The input flowrate of the flue gas was 587.3 kg/s.
investigation of a heat recovery The inlet temperature of the flue gas was 628.3 C.
steam generator Aspen Plus heat recovery technique was adopted for
thermal management.
Morey et al.[19] Aspen Plus modeling of Energy consumed by the superheated steam drying unit was in the
superheated steam drying at a range of 759-804 kJ kg-1.
corn ethanol plant Almost 1.3 L of water was recovered superheated steam drying unit per
liter of ethanol produced.
Distiller dried grains dryer flowrate was 4.81 kgs-1 and fuel dryer
flowrate was set to be 3.86 kgs-1.
Cinti et al.[21]
Integrated Solid Oxide Electrolyzer Both the solid oxide electrolyzer and Haber Bosch reactor were set to
with ammonia production plant operate at 650 C.
They achieved clean ammonia production with 40% reduction in power
input as compared with the equivalent plants.
The consumption of electricity by solid oxide electrolyzer was dropped
down to 8.30 kWh/kg of NH3.
Present study Single-stage flash drying system The input flowrate of the flue gas was 337 kmol/h.
integrated with industrial The ammonia conversion ratio is 25%.
heat recovery The convective dryer requires 6.17 kW of heat duty to proceed
drying process.
The energetic and exergetic efficiencies of the drying process are found
to be 55.6% and 24.17%.
temperature of 650 C for ammonia synthesis while generates drying process results and numerous sensi-
present study uses a series of two ammonia synthesis tivity studies are also conducted. The convective dryer
reactors operating at 350 C to achieve the effective requires 6.17 kW of heat duty to proceed drying pro-
conversion rate. cess. The energetic and exergetic efficiencies of the
drying process are found to be 55.6% and 24.17%.
This configuration design also results in cost saving
Conclusions
by cutting down the cost of heating the ambient air
This study proposes a unique idea of industrial ther- for drying process.
mal management and utilization of the recovered heat
within the industrial processes to cut down the add-
Disclosure statement
itional cost. In the proposed configuration, the system
is designed to recover the heat from cement slag and No potential conflict of interest was reported by
the authors.
use it for air heating in the drying process. Energy
and exergy analyses for every individual component
Nomenclature
are conducted and every component is investigated to
justify the results. The proposed system mainly com- en specific energy, kW
_ d
Ex exergy destruction (kW)
prises of the thermal management of the flue gas, raw
ex specific exergy (kJ/kg)
materials drying via hot air stream and ammonia syn- h specific enthalpy (kJ/kg)
thesis unit. Aspen plus software tool is not only uti- m_ mass flow rate (kg/s)
lized to simulate the proposed system but it also s specific entropy (kJ/kg K)
DRYING TECHNOLOGY 11
[22] Ross, D.; Doguparthy, S.; Huynh, D.; McIntosh, Chem. 2018, 57, 154–159. DOI: 10.1016/j.jiec.2017.
M. Pressurised Flash Drying of Yallourn Lignite. 08.017.
Fuel 2005, 84, 47–52. DOI: 10.1016/j.fuel.2004.08. [24] Alobaid, F.; Karner, K.; Belz, J.; Epple, B.; Kim,
006. H. G. Numerical and Experimental Study of a Heat
[23] Gwak, I. S.; Gwak, Y. R.; Kim, Y. B.; Lee, S. H. Recovery Steam Generator during Start-up
Drying Characteristics of Low Rank Coals in a Procedure. Energy 2014, 64, 1057–1070. DOI: 10.
Pressurized Flash Drying System. J. Ind. Eng. 1016/j.energy.2013.11.007.