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Abstract
This article follows earlier work on the development of a life-prediction method for carbon-fibre/epoxy laminates. For comparison with the
behaviour of a number of different CFRP laminates already studied, further constant-life fatigue data have now been obtained for a further
CFRP composite and a GRP laminate of similar construction – a 16-ply [(^45,02)2]S lay-up. Fatigue tests have been carried out on these
materials in both the virgin condition and after damage by low-velocity impacts. Following analysis of these new data and a re-examination
of the older data base, the constant-life model has been appropriately modified. It now offers a prediction procedure for the fatigue response
of composite materials in the virgin and impact-damaged conditions which requires, in the first instance, only the tensile and compressive
strengths of the composite in question. The model is equally applicable to both GRP and CFRP, despite the fact that the fatigue response of a
GRP laminate is different from that of an equivalent CFRP material. q 1999 Elsevier Science Ltd. All rights reserved.
Keywords: A. Polymer-matrix composites (PMCs); B. Fatigue; B. Impact behaviour; B. Mechanical properties; Fatigue-life prediction
Table 1
Experimental materials and their sources
HTA/913 ENKA high-strength, standard-modulus Tenax fibre BSL 913 standard epoxy (low-T cure) Ciba-Geigy (UK)
HTA/982 ENKA high-strength, standard-modulus Tenax fibre modified epoxy resin (low-T cure) Fiberite (Europe)
T800/5245 Toray intermediate-modulus, high-failure-strain fibre Narmco epoxy/bis-maleimide BASF (Europe)
T800/924 Toray intermediate-modulus, high-failure-strain fibre Ciba 924 high-strain, toughened epoxy (high-T cure) Ciba-Geigy (UK)
IM7/977 Hercules intermediate-modulus, high-failure-strain fibre 977 modified epoxy Fiberite (Europe)
E-glass/913 Standard E-glass fibre BSL 913 standard epoxy (low-T cure) Ciba-Geigy (UK)
2. Materials and experimental methods 2 mm/min. Compression tests on virgin samples and post-
impact compression tests were carried out in a 100 kN
Although all necessary experimental details have been servo-hydraulic Instron Model 1342 testing machine at a
given in earlier article [7,10,11], a summary is provided fixed loading rate of 20 kN/min, anti-buckling fixtures of
here for the sake of completeness. the kind described by Curtis [21] being used to support
the coupons during compression loading so as to prevent
2.1. Laminates macro-buckling. The monotonic tensile tests on 40 mm
wide samples were carried out under load control in a
The carbon-fibre laminates for which detailed results
200 kN servo-hydraulic Mayes test machine model DH
have already been described in the articles listed include
200, again at a rate of 20 kN/min.
materials containing a variety of different fibres and
Fatigue tests were carried out in 100 kN servo-hydraulic
matrices, but all of the same 16-ply [(^45,02)2]S lay-up.
Instron 1300 series machines under load control at R ratios
They include HTA fibre in 913 and 982 epoxy resins,T800
varying from 10.1 or 10.5 (repeated tension), through the
fibre in 5245 and 924 resins, and IM7 fibre in 977 resin.
fully reversed condition (R 21.0) to repeated compres-
Thus, although we had no control over the nature and extent
sion (R 110). Usually, five or more replicate tests were
of the commercial fibre surface treatments used in the manu-
carried out at several stress levels. Post-impact fatigue tests
facture of the prepregs, these combinations allowed us to
at an R ratio of 10.1 were carried out, also under load
make reasonable comparisons between materials and exam-
control, in the 200 kN Mayes machine, and anti-buckling
ine the effects of materials variables on fatigue performance.
fixtures were again used for compression–compression or
For reference, Table 1 collects details of these materials and
tension–compression fatigue tests. All fatigue tests were
their suppliers, including data from previous articles. The
run at frequencies between 2.5 and 8 Hz with constant-
GRP material was an E-glass/913-epoxy composite of the
amplitude sine-wave loading, under ambient laboratory
same lay-up as the CFRP laminates.
conditions.
The composite prepregs were all notionally zero-bleed
Impact damage was introduced into the test samples by
materials, the laminates being processed according to the
means of a purpose-built, falling-weight test instrument
manufacturers’ recommendations. All materials except for
with a 12.7 mm diameter hemispherical tup, based on BS
the HTA/982 and E-glass/913, which were hot pressed at
2782, part 3, method 353A. The mass of the impacter was
Bath, were autoclaved at DERA Farnborough to a nominal
0.248 kg for 1 J and 2 J impacts, the impact energy being
thickness of 2 mm. Test pieces were cut to dimensions of
varied by changing the drop height. Impact events at 3 J and
200 mm long by 20 or 40 mm wide with a water-cooled
5 J were made from a constant height of 1 m by changing
diamond-wheel saw. The 20 mm wide samples were used
the mass of the impacter. During the impact event the speci-
for establishing the fatigue behaviour of the virgin lami-
men was clamped between two steel rings of internal
nates, while the 40 mm-wide samples were used for impact
diameter 30 mm and the impact head was captured on
tests and for post-impact fatigue tests. The cut edges of the
rebound after impact to prevent secondary strikes.
samples were lightly polished and, after abrasion of the end
surfaces, end tabs of 1.5 mm thick soft aluminium were
glued on with Ciba Geigy Redux 403 epoxy-resin paste,
the adhesive being cured in a dry oven at 408C for 24 h.
3. Experimental results
The central gauge sections of the test samples were 100 mm
long.
3.1. Monotonic mechanical properties
2.2. Experimental techniques
A summary of the monotonic test data for all laminates
Measurements of the monotonic tensile properties were used in this programme is given in Table 2. In anticipation
carried out on the 20 mm-wide samples in a universal of the analysis to be presented later, we draw the reader’s
Instron Model 1195 machine at a cross-head speed of attention to the differences in the values of the ratio of the
M.H. Beheshty et al. / Composites: Part A 30 (1999) 971–987 973
Table 2
Monotonic mechanical properties of experimental laminates (standard deviations in brackets)
HTA/913 a 0.53 72.4 (4.8) 1.27 (0.05) 1.7 (0.1) 0.97 (0.08) 0.77
HTA/982 0.54 80.1 (8.5) 1.20 (0.05) 1.5 (0.1) 0.84 (0.08) 0.76
T800/5245 a 0.69 94.0 (3.1) 1.67 (0.09) 1.7 (0.1) 0.88 (0.10) 0.53
T800/924 a 0.67 92.0 (8.0) 1.42 (0.09) 1.5 (0.1) 0.90 (0.09) 0.63
IM7/977 a 0.67 90.2 (11.3) 1.43 (0.07) 1.5 (0.1) 0.90 (0.07) 0.63
E-glass/913 0.55 34.0 (2.2) 0.77 (0.03) 3.4 (0.3) 0.46 (0.02) 0.60
E-glass/913 b 0.55 34.0 (2.2) 0.86 (0.03) 3.4 (0.3) 0.60 (0.02) 0.70
a
Data for asterisked laminates are from Ref. [10].
b
Strength values obtained at the same loading rate as in fatigue tests.
compression strength to the tensile strength shown in this those of the materials shown in our Fig. 1. They found
table. that increasing the impact energy widened the Weibull
The effect of low-velocity impact damage on the strength distribution and extended the lower limit of the distribution.
of the HTA/982 laminate has already been shown [11], but a An impact event of 0.653 J caused a relatively small change
comparison can now be made of the effects on three of the but the effect increased with increasing impact energy. They
experimental materials under investigation, as shown in Fig. used the median-rank procedure and maximum-likelihood
1. Error bars are shown only for the tensile-strength data: the estimates (MLEs) to obtain the distribution parameters, but
experimental scatter on the residual compression strength although they quote a shape-factor value of l < 40 for the
values was very small, less than the size of the plotting undamaged tensile strength—substantially higher than the
symbol in fact. It can be seen that the tensile strengths of average of about 25 for the tensile strengths of all of our
these materials are largely unaffected by impacts up to 5 J. CFRP materials—they do not give values for the damaged
The line drawn through the residual tensile strength points laminates.
in Fig. 1, a least-squares line through all of the data, has a Fig. 1 shows that the compression strengths, by contrast,
very small slope of 20.007 J 21. The variations from point to are strongly affected by impact events of very low energy, as
point are well within the overall scatter. Tai et al. [22] also is well known. The GRP appears to be much more resistant
recently presented results on the fatigue behaviour of an to impact damage than the CFRP and the material shows the
impact-damaged CFRP laminate. They studied a 2 mm- threshold effect, at about 1 J, which is a familiar aspect of
thick, quasi-isotropic carbon/epoxy laminate, giving no the impact response of laminates [23]. No curves are drawn
indication of fibre or resin type, and they carried out only through the compression data, but it seems likely that the
repeated-tension fatigue tests at R 0.1. For their material, HTA/982 would also show a threshold somewhere between
the residual tensile strength fell more dramatically than 0 and 1 J. The normalized responses of the two CFRP
composites are identical, and it appears, therefore, that
small differences in fibre content, processing conditions
and matrix character do not greatly alter the nature of the
impact damage in materials of this kind. The CFRPs lose
some 65% of their initial compression resistance after
impacts as low as 3 J. By contrast, the GRP composite
loses about 45% of its impact resistance at an energy level
of 5 J.
Fig. 2. s /log Nf data for an E-glass/913 [(^45,02)2]S laminate, together Fig. 4. s /log Nf data for an E-glass/913 [(^45,02)2]S laminate. The lines are
with stress/median-life curves for an HTA/913 carbon-fibre composite of polynomial curves fitted to test data for the undamaged laminate (taken
similar lay-up (dashed lines). The solid curves through the GRP data points
from Fig. 2), and the symbols are actual data for samples with prior damage
are best-fit polynomial curves. from a 2 J low-velocity impact event.
which we refer to as the peak stresses, are the maximum because of the changes in our experimental approach in
values reached in the cycle. Thus, for R ratios between 21 these most recent experiments, and partly in order to
and 10.5, they are the maximum tensile stresses, and are avoid confusion as a result of overlapping of the data.
positive, whereas for the repeated compression stress cycles The difference in the intrinsic load-bearing ability of the
they are the maximum compression stresses and are nega- two species of reinforcing fibre is clearly manifested by the
tive. Other representations could have been used, but this fact that all of the GRP fatigue curves fall inside the general
convention allows uncluttered representations on s /log Nf envelope defined by the s /log Nf curves for the carbon
diagrams. The fatigue data points represent the replicate composite. It can also be seen that whereas most of the
fatigue lives for the GRP composite, and the curves drawn CFRP s /log Nf curves for mainly tensile loading are
through the points are best-fit polynomial curves of order concave downwards, the reverse is true of the GRP curves.
two or three. The dashed lines are stress/median-life curves The responses of the carbon and glass composites in
for the HTA/913 laminate taken from Ref. [10]. The points repeated compression are also different. The s /log Nf curves
on the extreme left of some of these data sets or curves (i.e. for R 110 for most of the CFRP laminates studied in this
at a notional ‘life’ of one-half cycle) represent the mono- work are flatter and straighter, as shown in Fig. 2. The GRP
tonic tensile or compression strength of the material. They curve, however, is curving upwards quite rapidly towards
are shown as positive for tensile strengths and negative for the zero-stress axis, within the experimental window of this
compression strengths. The selection of R ratios represented work, implying a greater sensitivity to fatigue damage in
here is slightly different for the two materials, partly compression than that of the CFRP.
The effects of prior damage on the fatigue behaviour of
the HTA/982 and E-glass/913 laminates are shown, respec-
tively, in Figs. 3 and 4. For the carbon-fibre composite, the
effects of both 1 J and 2 J impacts are shown, and data are
included for three R ratios. For the glass/epoxy laminate,
however, as impacts of only 2 J were studied, fatigue data
are included for four R ratios. It can be seen that impacts of
1 J and 2 J have no effect on the fatigue lives of the CFRP in
repeated-tension cycling (R 0.1). In mixed-mode cycling
at R 20.3, however, the effect of the impact damage on
the compression resistance of the composite can already be
seen, even at 1 J, the data points falling below the s /log Nf
curve for the undamaged material. After a 2 J impact event,
the effect of the damage is very marked. As expected from
the results in Fig. 1, the effects of the impact damage are
Fig. 3. s /log Nf data for an HTA/982 CFRP laminate of [(^45,02)2]S lay-up
after damage by low-velocity impacts of 1 J (solid symbols) and 2 J (open most marked in a repeated compression régime (R 110),
symbols). The lines are polynomial curves fitted to the data for the virgin the stress/life curve being flattened and lowered by both 1 J
laminate [11]. and 2 J impacts. For the glass/epoxy material, the effects of
M.H. Beheshty et al. / Composites: Part A 30 (1999) 971–987 975
the impact damage seem less severe, even for fully reversed normalization with respect to b [10,11], but it gave rise to
cycling (R 21.0), although for repeated-compression some distortion of the distribution because any data set
conditions, the effects appear to be just as marked as for which contains an odd number of data points will yield a
the CFRP laminate. value of unity in the normalized data set and the pooled
In their work on repeated-tension fatigue of a quasi- distribution will then contain a step at an abscissa value of
isotropic carbon/epoxy laminate, Tai et al. [22] showed 1.0. Whether or not this makes a significant difference to the
that the s /log Nf curve for composites damaged at 1.1 J outcome of the analysis then depends on the robustness of
had a reduced data spread, implying a higher value of the the statistical procedure used to estimate the distribution
Weibull shape factor, l , (although they quoted no l values parameters. In our current work with damaged laminates,
for the fatigued materials) in addition to the steeper slopes some difficulty was encountered in obtaining consistent
that we have also observed. They have also noted that the results, and we have therefore re-analyzed all data in our
effect of damage was more marked at lower stress levels and data base by using the mean values of the replicate data sets
was hardly significant at higher stresses. They suggest that instead of the median values. The resulting pooled distribu-
this is because high-stress fatigue is fibre-dominated and, as tion curves were all much smoother as a result, and, as we
impact causes no fibre damage, there is therefore no effect shall show, the degree of consistency obtained by the use of
on high-stress fatigue. At low stresses, however, the link a number of different parameter estimation methods is much
between prior delamination caused by the impact events greater. The mean-rank method was used to obtain the plot-
and fatigue delamination at free edges was apparent after ting position, i=
N 1 1, where i is rank number and N is the
about 10 000 cycles. number of observations in the distribution.
There is disagreement about which of the several possible
3.2.2. Pooling of data methods available for determining the parameters of a
The concept of the pooling of normalized fatigue lives is Weibull distribution is the most appropriate. Freudenthal
of importance in offering the designer a means of assessing and Gumbel [24,25] used the method of moments proposed
the likely reduction in the life of a laminate that has by Weibull [26], but King [27] observes that it is not a very
sustained impact damage. As discussed in earlier articles efficient method and claims that it is not used for composite
[7,10,11], for a wide range of carbon-fibre composites the materials. Whitney [33] used the MLE, whereas Castillo
Weibull shape parameter, l , for such pooled distributions [36] suggests that because of the peculiar behaviour of the
appears to lie in the range 1 , l , 2, with relatively less Weibull distribution for 1 , l , 2, the MLE is not appro-
variation that can be unambiguously ascribed to differences priate for Weibull distributions with l , 2 although it is
in materials characteristics (type of fibre, matrix, etc.). highly recommended elsewhere because it gives the lowest
There are two features of this pooling procedure that are variability. Talreja [28] rejected the MLE approach in
potential sources of difficulty and which may be re-exam- favour of the use of a standardized variable, suggesting a
ined in the light of these latest results: the first is the basis lower limiting value of l of about 10 for the valid use of
of the normalization and the second is the procedure for MLEs. By contrast, in a recent analysis of large single-stress
estimating the Weibull parameters from the pooled data sets for ud and [(^45,02)2]S laminates of HTA/982, Lee
distributions. et al. [29] confirmed that, of a range of estimates obtained by
If the results of a number of replicate experiments in each the use of an expert system developed by Castillo et al. [30],
of which there are, say, ten or more test results, are avail- the MLE gave the lowest level of variability.
able, it is perhaps reasonable to make the assumption that With these uncertainties in mind, we have re-analysed all
the groups of replicate fatigue lives obey a two-parameter of the fatigue-life data sets obtained at the University of
Weibull model and then use a simple least-squares proce- Bath over a period of about ten years in order to provide a
dure to obtain the characteristic values, or scale parameters, good background against which to discuss the most recent
b , of each data set. At this stage, a value for the slope, l (the results on impact-damaged laminates. Two commercial
shape parameter), is not needed, and an indicator of central software packages were used to do this, the more versatile
tendency like b may be obtained to a reasonable degree of of which is Mathcad [31]. A procedure was developed in
accuracy in this way. The values of b for each stress level which five estimates were made, starting with the simplest,
may then be used as the normalizing parameter. We used progressing to the more sophisticated, and feeding the
this procedure in an earlier article dealing with a T800/5245 results from earlier estimates as initiation values for subse-
CFRP laminate [7], and even though some of the data sets quent calculations. This is particularly useful for some MLE
contained only four or five fatigue lives, the result of the calculations which are sensitive to suggested initiation
normalization appeared to be satisfactory. Subsequently, we values, or ‘guesses’, and may fail to converge if these are
revised our approach on the ground that it was more legit- not reasonably close to the actual distribution parameters.
imate to use an experimental normalization parameter rather The estimates made in this way included three which
than the calculated b value, and we used the median values assumed a two-parameter Weibull model (i.e. with the loca-
of the replicate data sets instead. This procedure gave results tion parameter, a , deliberately set to zero), and two where
that were very little different from those obtained by the software was allowed to optimize all three constants, a ,
976
Table 3
Estimates of the Weibull shape parameter, l , for virgin and impact-damaged laminates, obtained by several methods
T800/5245 Virgin 164 1.11 1.20 1.18 1.19 1.19 1.16 1.17 3
T800/924 Virgin 88 1.65 1.42 1.50 1.31 1.56 1.32 1.46 9
IM7/977 Virgin 93 1.14 1.21 1.21 1.20 1.23 1.15 1.19 3
HTA/913 Virgin 88 1.53 1.65 1.63 1.77 1.33 1.48 1.56 10
HTA/982 Virgin 122 0.83 1.14 1.01 1.09 1.04 1.01 1.02 10
E-glass/913 Virgin 47 1.63 1.42 1.60 1.76 1.71 1.65 1.63 7
HTA/913 2 J damage 41 0.71 0.92 0.85 0.88 0.88 0.88 0.85 8
b
HTA/982 1 J damage 62 0.67 0.79 0.70 0.66 0.61 0.69 10
HTA/982 2 J damage 43 0.78 1.09 0.97 1.06 0.95 1.02 0.98 11
M.H. Beheshty et al. / Composites: Part A 30 (1999) 971–987
b and l , in a three-parameter Weibull distribution. For the of the order of only a few tens of cycles. The effect of these
two-parameter model, the methods used were the simple is strongly accentuated by the logarithmic scales. We have
linear least-squares procedure (x on y regression, following sometimes censored these short-life results on the ground
the recommendation of Abernethy [32], rather than the that servo-hydraulic test machines will usually take a
usual y on x), the method of moments, and a MLE. For hundred or so cycles to stabilize so that recorded lives less
the three-parameter model, two estimates were obtained, than 100 cycles may be unreliable. However, such censor-
one by a non-linear error minimization routine and the ing, which risks the exclusion of ‘good’ data, is unnecessary
second by another maximum-likelihood calculation, both when using any estimation method other than the linear
of which used the Mathcad ‘MINERR’ function to obtain least-squares procedure. Despite the higher error, the values
the required solutions. A sixth estimate for the three-para- obtained by this most common of methods for the virgin
meter case was obtained by means of the Levenberg– laminates almost all fell within the range obtained by the
Marquardt (LM) non-linear least-squares routine embodied other techniques except in the case of the undamaged HTA/
in the commercial Origin graphing and analysis package by 982 laminate, where the slope of the regression line is less
Microcal Software Inc. The results from these analyses are than unity. Inspection of the data plot shows that the curve is
summarized in Table 3. non-linear and the estimate of the slope is dominated by the
Experimental data for the first four of the materials given longer lives, which renders it questionable for the determi-
in the table are from Ref. [10], and those for the undamaged nation of minimum extreme-value parameters or low-
HTA/982 laminate were first presented in Ref. [11]. Only quantile life estimates.
the shape parameter values are given here because the Although the estimates shown in Table 3 for the five
values of the scale parameter, b , returned by all procedures undamaged laminates show a reasonably high degree of
for all materials were, as expected, close to unity (about 1.05 consistency, it is difficult to single out a particular estima-
for the undamaged CFRP laminates and 1.13 for the virgin tion method as being universally the most appropriate for all
GRP), and the values of the location parameter, a , returned requirements. For the five undamaged CFRP laminates
for the three-parameter models were always sufficiently almost all estimated values of l fall in the range 1.01–
close to zero to be ignored. The inclusion in this table of a 1.77 apart from the suspect linear least-squares estimate
notional ‘mean’ and ‘coefficient of variation’ for the six for HTA/982. The average values in this table do not appear
separate values is merely to give a feeling for the compar- to correlate in any obvious way with the nature of the lami-
ability of the different estimates. The routine to obtain the nate. The three lowest values are for two of the higher-
three-parameter MLE failed to converge in only one case, performance fibre composites and one lower-performance
that for the HTA/982 composite with 1 J impact damage, fibre. The two highest values are for one high-performance
and converged only with great difficulty in the case of the fibre/resin combination and one conventional combination.
undamaged T800/924 laminate. There seems, therefore, to be no link between the l value
Comparison of the results for the first four materials in and the nature of either the resin or the fibre. The indication
Table 3 with previously published values obtained by the is therefore that this group of values for the CFRP materials
LM routine suggests that the use of the data-set mean values are all more or less at the same level, at an average of about
for normalization has had no marked or consistent effect on 1.3. We note that when using the median as the normalizing
the estimation of the distribution parameters. For the parameter [11], the average value of l for all five
undamaged laminates, for which the largest amounts of undamaged CFRP laminates was 1.39, with a coefficient of
data were available, the degree of consistency between the variation of about 17%. The overall average for the same five
six estimates is unexpectedly high. The three-parameter laminates in Table 3 is 1.28, with a cv of only about 5%.
MLE is close to the average value in almost every case, Thus, it appears that while the use of the mean instead of the
and even the method of moments has provided values median improves the consistency between estimates and the
close to the other estimates, whereas we had previously smoothness of the distribution curves, it does not markedly
found it to be unreliable. No indications of goodness of fit alter the numerical outcome of the calculations.
are given in Table 3, but the root mean-square errors for all Although only one experimental GRP material was
calculations except those involving the simple linear least- tested, the results in Table 3 suggest that the value of the
squares method were between 1 and 4%. By contrast, Weibull shape parameter for this material is higher than the
although the correlation coefficients for all the linear least- highest values for the CFRP materials. One likely reason for
squares fits for the virgin materials were always greater than this class difference is simply that, for the most part, the
0.95, the RMS errors of the fits were usually much higher stress/life curves for CFRP materials are flatter than those
than those for the remaining five estimates, namely between for GRPs, and the spread in any replicate data set is there-
10 and 20%. This higher level of error of the fit for the two- fore usually smaller.
parameter least-squares estimates is frequently found, on We commented in a recent article [11] on some prelimin-
inspection of the plots, to be associated with a large degree ary results for fatigued samples of HTA/982 laminate which
of variability in data points at the extreme left of the distri- had sustained impact damage of 1 J and we were concerned
butions, usually tests showing unreasonably short life times that the damage led to a value of the Weibull shape
978 M.H. Beheshty et al. / Composites: Part A 30 (1999) 971–987
Table 4
Values of the Weibull shape parameter, l , obtained in fatigue and monotonic strength tests on five CFRP laminates and one GRP laminate
structures). As time passes, the failure rate decreases and of stress of the form:
reliability increases. A value of l 1 implies random fail-
ures, independent of time. Such failures may be due to a f
1 2 mu
c 1 mv ;
1
foreign-object damage, lightning strike, human errors, etc.
where a is s alt /s t, the normalized alternating stress; m is
Values of 1 , l , 4 are typical of wear-out which is the
s m/s t, the normalized mean stress; and c is s c/s t, the
origin of many mechanical failures, including low-cycle
normalized compression strength, s t being the monotonic
fatigue, bearing failures, corrosion etc. and there is an
composite tensile strength. By convention, s c is taken as
increasing probability of failure with age (i.e. decreasing
negative, and c is therefore also negative. This is a bell-
reliability). For the most part, then, this categorization
shaped curve which is not necessarily symmetrically
applies reasonably well to the range of results obtained for
disposed relative to the alternating-stress axis (i.e. about
these laminates. The effect of impact events on the CFRP
m 0). The establishment of Eq. (1) has involved a number
laminates is to drive the value of the shape factor below
of modifications to the model, including early consideration
unity, suggesting that the damage caused by the
of a parabolic function (where the parameters u and v were
impacts—mainly matrix cracks and delaminations—
both equal to unity), but the model in the more general form
increases the likelihood of premature failures in addition
shown earlier is more widely applicable to a variety of
to reducing the general fatigue performance of a given lami-
materials.
nate: the two must be seen as distinct effects. The only
The three parameters f, u and v are dependent on the
inconsistency appears to be in the effect of impact damage
logarithm of life, Nf (the number of cycles to failure), but
on the reliability of the GRP laminate, for which the value of
are mutually independent. From early work it was apparent
the shape factor is increased as a result of the impact
that f mainly controlled the height of the curve, u the slope
damage. The variation between the different estimates is
of the contour in the ‘tensile’ mean stress zone and v the
much greater for the damaged GRP than for any other
slope in the ‘compressive’ mean stress zone. These para-
group of estimates. And although the two-parameter linear
meters were not originally thought to have any direct special
least-squares estimates for the virgin and damaged materials
significance in relation to the structure and properties of the
are quite similar, it is clear that all other estimation methods
material, although it did appear [10,11] that there might
give high values for the damaged laminate. It is unclear why
have been some relationship between f and the tensile
there should be such a difference in the responses of the
strength of the laminate. In previous publications we have
carbon and glass composites to impact damage.
illustrated the development of the constant-life model for
The work of Tai et al [22] also suggests that the pooled
use with five CFRP laminates, namely T800/5245 [7], HTA/
Weibull analysis procedure is valid for predicting lives of
913, T800/924 and IM7/977 [10] and HTA/982 [11], all
both damaged and undamaged material, at least insofar as
having the lay-up [(^45,02)2]S, a construction of general
can be judged from their more limited range of results in
interest for aeronautical applications. The procedures that
repeated tension.
have previously been used in the application of this model
may be summarised, as follows.
4.2. A constant-life model for fatigue-life prediction 1. Stress/life data are accumulated at several R ratios (s min/
s max): choice of an appropriate ‘life’ value requires
In the course of our previous work, a wide range of CFRP detailed consideration of statistical models suitable for
composites has been studied with the objective of assessing to the purpose of the analysis, or, more specifically, to the
the potential usefulness of the model and the likely level of design requirements related to safety considerations.
confidence in using it to make preliminary predictions of life 2. Suitable mathematical functions are fitted to the data:
from limited fatigue data sets. There appears to be a general second- or third-order polynomials have been used
relationship between the alternating and mean components hitherto, but more appropriate functions are possible.
980 M.H. Beheshty et al. / Composites: Part A 30 (1999) 971–987
Fig. 6. Constant-life plots for: (a) E-glass/913 and (b) HTA/982 laminates of [(^45,02)2]S lay-up in the virgin condition. The curves, representing equation 1,
are best-fit curves obtained by a non-linear least squares algorithm.
3. Interpolations are made at selected lives (e.g. 10 4, 10 5 generalization of the constant-life (m, a) plot in the form
and 10 6 cycles) and data pairs (m, a) are calculated of a surface representation showing the full variation of (a,
from these interpolations at particular R ratios together m, log Nf). Alternatively, a family of stress/life curves of
with previously measured tension and compression conventional form can be produced for ranges of lives that
strengths. are consistent with the original experimental data window.
4. The data are plotted as an (m, a) diagram (such as those We are interested in offering the designer a conservative
to be discussed in Section. 4.2) and curves of the form of predictive tool-one that will work with a minimum of
Eq. (1) are fitted through the data points by non-linear experimental data but which will allow continuous up-
curve-fitting routines. Values of the parameters f, u and v dating of the predictions as more data become available.
are evaluated, and their variations with log life are estab- For any given new material, an initial experimental
lished. programme would be carried out to determine the mono-
5. It is then possible to predict s /log Nf curves for any tonic tension and compression strengths, together with
desired R ratio by solving the pair of simultaneous stress/life data for stress ratios of 10.1 and perhaps 21.2
equations: in order to locate curves in the left-hand quadrant of the
constant-life diagram. Perhaps three replicate tests might
a f
Nf
1 2 mu
Nf
c 1 mv
Nf ;
2a be done initially at three stress levels for both R ratios. By
pooling the 15–20 fatigue lives so obtained, following the
12R descriptions of Whitney [33] and of Yang and Jones [34], a
am :
2b
11R trial value of the Weibull shape parameter, l , could be
obtained. A crude estimate could then be made of, say,
the characteristic value (Weibull scale parameter) or the
The first of these equations is the constant-life equation, modal value of the distribution of minima for each stress
(Eq. (1)), modified to include information about the life- level. The latter could be obtained on the basis of the
dependence of the two exponents, u(Nf) and v(Nf) and the extreme-value-theory premise [35,36] that the distribution
stress function f(Nf). The second equation is derived from of the minima of a Weibull distribution with shape para-
the conventional definition of the stress ratio. Until recently meter l is also a Weibull distribution with shape parameter
we have used an average value of f in Eqs. (2a) and (2b), l and characteristic value b=n1=l , where n is the size of the
assuming it to be roughly constant. The output of this analy- sample and b is the scale parameter of the replicate test set.
sis can be in one of two forms, depending on the require- The characteristic smallest values (or other appropriate
ments of the user. The first is a three-dimensional quantile values of life) would then be used to derive trial
M.H. Beheshty et al. / Composites: Part A 30 (1999) 971–987 981
Fig. 7. Constant-life plots for damaged [(^45,02)2]S laminates: (a) E-glass/913 glass/epoxy (closed symbols 2 J impact damage); (b) HTA/982 carbon/epoxy
(closed symbols 1 J impact damage; open symbols 2 J). The data points are shown only for the damaged materials in order to avoid confusion: the two sets
of curves without data points are the best-fit curves for the undamaged laminates from Fig. 6.
constant-life curves, with appropriate informed ‘guesses’ because the original s /log Nf curves for repeated tension
being made initially for the parameters f, u and v until suffi- and repeated compression (R 0.1 and 10) for the carbon
cient data were available to permit realistic curve fitting. laminate are much flatter than the corresponding curves for
Initially, the statistical validity of the procedure would be the GRP, the separation of the constant-life curves for the
open to question, and would require careful testing before latter is much greater in both the left and right quadrants of
serious use. However, as further data were acquired, the the plots. It can be seen, nevertheless, that the constant-life
validity would improve, together with the true predictive model works as well for the GRP as for the CFRPs, albeit
capacity of the model. with different values of the fitting parameters, as we shall
see.
4.3. Analysis of new results Some preliminary comments on the effects of impact
damage on the validity of the constant-life model were
Results of the analysis of the fatigue data for the HTA/ made in Refs. [11,19,20]. At the time of writing those arti-
982 and E-glass/913 are shown in Fig. 6. The results shown cles, only results for 1 J impact on the HTA/982 laminate
are for the undamaged laminates, over three decades of life were available, but the more recent results reinforce our
from 10 3 to 10 6 cycles. The curves shown in these and later earlier comments. Thus, the effects of 2 J impact events
plots have all been obtained by the fitting of the three vari- on the behaviour of the E-glass/913 composite and the
able parameters, f, u and v, in Eq. (1), without any effects of both 1 J and 2 J impacts on the behaviour of the
constraints. For the carbon-fibre laminate, Fig. 6(b), the HTA/982 material are all shown in Fig. 7. Both data points
plot shows features more or less identical to those which and fitted curves are shown for the impact-damaged lami-
we have already described for other CFRP materials. In nates, and these may be compared with the behaviour of the
particular, although the position of the peak values of the corresponding undamaged materials, shown only as the sets
normalized alternating stress, a, is shifted in the positive of fitted curves from Fig. 6. An important result is that the
direction along the mean stress (m) axis, the bell-shaped constant-life model is equally as valid for the damaged as
curves for each of the four lives represented are quite for the virgin composites. In both materials, the predomi-
symmetrical about the peak. By contrast, the curves for nant effect of prior impact is to impair the compressive load-
the GRP laminate are much less symmetrically disposed, bearing ability of the laminate, and this is reflected in a
with respect to the extreme values of m (i.e. c and 1), than shifting of the left-hand regions of the curves towards the
any of the CFRPs that we have studied, although the peak origin, accompanied by a squeezing together of the points
values of a occur almost exactly at m 0. Moreover, on the R 10 radius vector, while in the purely tensile
982 M.H. Beheshty et al. / Composites: Part A 30 (1999) 971–987
Table 5
Summary of values of constant-life fitting parameters and errors for undamaged CFRP and GRP laminates. (linked to Excel sheet)
regions the curves are largely unaffected. The overall shape although not very strongly, and, in seeking correlations
of the constant-life plot is apparently unchanged by the prior between the values of f, u and v and the physical character-
damage, and the constant-life equation, Eq. (1), remains a istics of the individual laminates, it seemed reasonable to
valid descriptor of the constant-life surface. recalculate the values of u and v after fixing the value of f as
In order to build up a reasonable constant-life curve, we the mean for the three values of constant life being used at
require, in addition to the end data points representing the the time. This procedure was used in Ref. [10], where it was
monotonic tensile and compressive strengths, at least three noted that for each of the four laminates studied the values
stress/life (s /log Nf) curves to permit the fitting of Eq. (1) by of u and v were all quite close to 2 and increased slightly
allowing the three parameters f, u and v to take any values. with log Nf. In the case of the HTA/913 laminate the
In constructing a life-prediction model, these three s /log Nf observed values of u and v and their dependences on
curves must be appropriately chosen so as to restrict the log Nf were slightly higher than those for the other three
fitting operation in the left and right quadrants and at the higher-performance composites. But apart from these
peak value of the bell-shaped constant-life plots. Our small differences, there appeared to be no particular correla-
experience with various materials now suggests that stress tion between the values of u and v and the characters of the
ratios of 10.5, 20.6 and 110 for undamaged materials and laminates. The observed values of f appeared to be directly
10.5, 20.3 and 110 for damaged materials may be the related to the tensile strengths of the laminates, however,
appropriate curves to determine for fitting purposes, and this caused us puzzlement as the (m, a) data sets on
although the precise choice may be different for other lami- which the analysis is based are already normalized with
nates and other impact energies. respect to laminate tensile strength.
In the light of earlier experience, we have now modified
4.3.1. Values of constant-life parameters our procedures. The accuracy of the fitting of the constant-
life curves (interpolation) and the validity of using them to
Our approach to the evaluation of the parameters f, u and extrapolate, even to a limited extent, beyond the experimen-
v has changed somewhat since we first proposed the use of tal window depends on the validity of the original polyno-
the constant-life model. Initially, we allowed the curve- mial description of the s /log Nf curves. We now therefore fit
fitting algorithm to find the values of all three parameters the polynomials to the complete data sets rather than to the
which gave the best fits, as judged by calculated values of median-life values of a replicate test set, and we establish
the x 2 statistic returned by the programme. In the earlier the constant-life diagrams for four lives, 10 3, 10 4, 10 5 and
work, we found that all three parameters varied with log Nf, 10 6 cycles, instead of the three lives that we used in earlier
M.H. Beheshty et al. / Composites: Part A 30 (1999) 971–987 983
Table 6
Summary of values of constant-life fitting parameters and errors for CFRP and GRP laminates with prior impact damage (linked to Excel sheet)
Table 7
A comparison of the effect of curve-fitting the constant-life data for two of the experimental CFRP materials with fixed values of the parameters u and v
T800/924 4 1.43 0.13 2.14 0.19 2.25 0.17 1.41 0.02 2.15 2.38
6 1.24 0.34 2.65 0.62 2.78 0.54 0.96 0.03 2.15 2.38
HTA/982 4 1.01 0.09 2.05 0.22 2.40 0.25 1.03 0.03 2.15 2.38
6 0.71 0.03 1.85 0.09 2.34 0.11 0.77 0.03 2.15 2.38
including laminates with woven-fibre reinforcement, and a designer if three alternative, physically more meaningful,
wider range of impact energies also needs to be studied. characteristics were used instead of the parameters f, u
Finally, we note that if the reduction in compression andv. For example, the maximum alternating stress allow-
strength following an impact event can be satisfactorily able at any given fatigue life, i.e. the peak alternating stress,
predicted by a model of the kind proposed by Soutis and or the ridge of the envelope shown in Fig. 6, could be used.
Curtis [12] or Papanicolaou and Stavropoulos [37], for This maximum is readily obtained by differentiating Eq. (1)
example, then the likely effects of impact damage on the with respect to the mean component of stress, m. The
fatigue response of a ‘new’ laminate could be reasonably normalised mean stress for this condition is:
well predicted even before any impact and fatigue-after-
uc 2 v
impact experiments had been carried out [20]. m2 ;
4
u 1 v
4.5. Design parameters resulting in an explicit expression for the peak alternating
stress:
The constant-life model could be more attractive to the
u1v
u v 11c
amax fu v :
5
u1v
Two other characteristics may now be defined from the
original parameters to describe the curve:
1. The mean of u and v, or (u1v)/2, describes the narrow-
ness of the ‘bell’ of the bell-shaped constant-life curve,
and could be referred to as a fatigue sensitivity. Thus, if
(u1v)/2 is large the value of alternating stress decreases
rapidly as the mean stress moves away from the optimum
position, whereas if (u1v)/2 is small the material is more
robust, with alternating stress reducing only slowly as the
mean stress moves away from the optimum position.
2. The ratio u/v represents the tensile bias or asymmetry of
the curve with respect the mean ordinate between the
tensile and compressive limits, in itself a mark of bias
in the fatigue behaviour. For u v the curve is
symmetric. The peak alternating stress is located at m
(1 2 c)/2 and has a value of f[(1 1 c)/2] 2u. For u/v , 1,
the material behaves better with tensile mean stress and
poor with compressive mean stress, and vice versa.
An illustration of the differences in the variations of these
three parameters with life for three of the experimental
laminates is shown in Fig. 11. The relatively small differ-
ences between the two CFRP laminates and the much
greater difference between these and the GRP composite
are clearly shown by these plots. The final illustration in
this article, Fig. 12, presents a wider comparison, on a
Fig. 11. Variation of the three fatigue design parameters, amax, (u 1 v)/2, more sensitive scale, of the variation of the parameter
and u/v, with life for two CFRP and one GRP laminate of [(^45,02)2]S amax with life for all undamaged laminates used in this
construction. study. It is clearly seen in this figure that of the six
986 M.H. Beheshty et al. / Composites: Part A 30 (1999) 971–987
[2] Fernando G, Dickson RF, Adam T, Reiter H, Harris B. J Mater Sci [20] Beheshty MH, Harris B. In: Crivelli-Visconti I, editor. Science, tech-
1988;23:3732–3743. nologies and applications. Proceedings of the Eighth European
[3] Adam T, Fernando G, Dickson RF, Reiter H, Harris B. Int J Fatigue Conference on Composites, ECCM8, Naples, Italy, 1. Abingdon,
1989;11:233–237. UK: Woodhead, 1998:143.
[4] Dickson RF, Fernando G, Adam T, Reiter H, Harris B. J Mater Sci [21] Curtis PT, editor. CRAG test methods for the measurement of engi-
1989;24:227–233. neering properties of fibre-reinforced plastics composites. RAE,
[5] Harris B, Reiter H, Adam T, Dickson RF, Fernando G. Composites (Farnborough), Technical report TR 88012, (Procurement Executive,
1990;21:232–242. Ministry of Defence, Farnborough, Hants, UK), 1988.
[6] Adam T, Gathercole N, Reiter H, Harris B. Advd Compos Lett 1992; [22] Tai NH, Yip NC, Lin JL. Compos Sci Technol 1998;58:1–8.
1:23–26. [23] Dorey G. Fracture of composites and damage tolerance, in practical
[7] Gathercole N, Reiter H, Adam T, Harris B. Int J Fatigue 1994; considerations of design, fabrication and tests for composite materi-
16:523–532. als, article 6. AGARD Lecture Series No. 124, (AGARD (NATO),
[8] Harris B, Gathercole N, Reiter H, Adam T. In: Balkema AA, editors. Neuilly-sur-Seine, France), 1982.
Constant-stress fatigue response and life-prediction for carbon-fibre [24] Freudenthal AM, Gumbel EJ. Proc. Roy. Soc. (London)
composites, Proc. Duracosys ’95, a research conference on The 1953;A216:309–332.
Durability of Composite Systems, Free University of Brussels. Rotter- [25] Freudenthal AM, Gumbel EJ. J Am Stat Assoc 1954;49:575–597.
dam: Netherlands, 1995:63–73. [26] Weibull W. A statistical report of fatigue failure in solids. Royal
[9] Harris B, Gathercole N, Lee JA, Almond DP, Adam T, Reiter. Institute of Technology of Sweden Stockholm, Transactions no 27.
Fatigue-life prediction for fibre-reinforced plastics. In Proceedings of 1949.
the Seventh European Conference on Composite Materials ECCM7, [27] King RL. Polymers in a marine environment: 1987. (Marine Manage-
London. Abingdon, UK: Woodhead Publishing, 1996:69-74. ment (Holdings) Ltd, London), article 4, 1989.
[10] Harris B, Gathercole N, Lee JA, Reiter H, Adam T. Phil Trans Roy [28] Talreja R. Proc Roy Soc (London) 1981;A378:461–475.
Soc (London) 1997;A355:1259–1294. [29] Lee JA, Harris B, Almond DP, Hammett F. Composites 1997;28A:5–15.
[11] Beheshty MH, Harris B. Compos Sci Technol 1998;58:9–18. [30] Castillo E, Alvarez E, Cobo A, Herrero T. An expert system for the
[12] Soutis C, Curtis PT. Compos Sci Technol 1996;56:677–684. analysis of extreme value problems. University of Cantabria, Spain,
[13] Cantwell WJ, Morton J. The impact resistance of composite materials 1993.
- a review. Composites 1991;22:347–362. [31] Mathcad, now in version 8, is available from MathSoft Inc., 101,
[14] Richardson MOW, Wisheart MJ. Composites 1996;27A:1123–1131. Main St, Cambridge, MA 02142, USA.
[15] Stellbrink KKU. Influence of low-velocity impact on the fatigue beha- [32] Abernethy RB. In: Abernethy RB, editor. The new Weibull handbook,
viour of CFRP laminates. Fatigue and Creep of Compos Mat 2nd ed. Florida, USA. 1996.
1982;319–327 Ch 36. [33] Whitney JM. Fatigue of fibrous composite materials STP 723. Phila-
[16] Cantwell W, Curtis P, Morton J. Composites 1983;14:301–305. delphia, PA: American Society for Testing and Materials, 1981:133–
[17] Ramkumar RL. The long-term behaviour of composites, ASTM STP 151.
813. In: O’Brien TK, editor. The long-term behaviour of composites, [34] Yang JN, Jones DL. Fatigue of fibrous composite materials, ASTM
ASTM STP 813, Philadelphia, PA: American Society for Testing and STP 723. Philadelphia, PA: American Society for Testing and Mate-
Materials, 1983:116. rials, 1981:213–232.
[18] Clark G, Saunders DS. Mat Forum 1991;15:333–342. [35] Bury KV. Statistical models in applied science. London: Wiley, 1975.
[19] Beheshty MH, Harris B. Proceedings of the International Conference [36] Castillo E. Extreme value theory in engineering. Boston/London:
on Fatigue of Composites (ICFC), Paris. Paris: Société Française de Academic Press, 1988.
Métallurgie et de Matériaux, 1997:355–362. [37] Papanicolaou GC, Stavropoulos D. Composites 1995;26:517–523.