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1. INTRODUCTION TO CRYOGENICS
2. CRYOGENICS IN SPACE
The first clue to the existence of absolute zero came from the
expansion and contraction of gasses. We know that hot air rises and cold air
falls. Air rises when it’s heated because it expands, so it’s less dense than the
cooler air around it. It has buoyancy, just like a piece of wood in a pond,
which floats because it’s less dense than the water. Air sinks when it cools
because it contracts, so it’s denser than the warmer air around it.
Although nothing can be colder than absolute zero, there are a few
physical systems that can have what are called negative absolute temperatures.
Oddly enough, such systems are hotter than some with positive temperatures!
Here’s a bit more detail. Certain physical systems have small set of
energy levels that they can be in. For example, a laser uses this principle. The
atoms (or molecules) that produce the lasing effect can be in one of a number
of energy states. Normally, only a small percentage of the atoms are in the
highest energy states; many more are in the low energy states. Scientists have
found equations that describe how many of the atoms are in which energy
state. As you might imagine, these equations depend on temperature. The
hotter the system, the more atoms are in the higher energy state. In fact, if you
know what fraction of the atoms are in each energy state, you can plug that
into the equation and solve for the temperature. A laser operates by pumping
energy into the atoms, pushing many of them into the high energy states.
When the atoms drop back into the lower energy states, they give off the
energy as a beam of laser light. But between the time they get pumped up and
the time they drop back, they’re in an abnormal state, with lots more atoms
than normal in the high energy state. If you plug this abnormal distribution
into the equation and solve for temperature, you may get a negative number.
4. CRYOGENIC LIQUIDS
Liquid air sounds like a contradiction in terms. In fact, it's not: air,
when cooled enough, condenses into a liquid and even freezes solid. We're
familiar with this phenomenon in the case of water: steam condenses to liquid
water which freezes to ice. Or, to put it the other way, ice melts to form water
at 0 Centigrade and boils to produce steam at 100 Centigrade. (These
temperatures change as the pressure changes. At high altitudes, for example,
water boils at a lower temperature because of the lower air pressure.) Carbon
dioxide is another familiar example of a gas that freezes: it can be cooled and
frozen as "dry ice".
All gases, when cooled, condense. Two gases often used in their
liquid forms are nitrogen and helium. These are the commonly used cryogenic
liquids. Nitrogen gas, when cooled, condenses at -195.8 Celsius (77.36
Kelvin) and freezes at -209.86 Celsius (63.17 Kelvin.) Or, to reverse the order,
solid nitrogen melts to form liquid nitrogen at 63.17 Kelvin, which boils at
77.36 Kelvin. Liquid nitrogen is used in many cryogenic cooling systems.
weight of 4.Helium 3, the rarer isotope, has a nucleus of two protons and one
neutron. Helium 3 boils at 3.2 Kelvin. This boiling point is one degree colder
than that of helium 4. Both helium 4 and helium 3 can be cooled to below
their boiling temperatures by reducing the pressure to below atmospheric
pressure. Liquid helium, like water, boils at a lower temperature when the
pressure is lower. In fact, when liquid helium is kept in containers that are at
atmospheric pressure, the helium temperature changes as atmospheric high
and low pressure areas pass. These temperature changes are small, but
measurable. With vacuum pumps, we can reduce the pressure in a helium
container much more than happens with normal atmospheric pressure changes.
As a practical matter, a pumped bath of liquid helium 4 can be used to cool
down to about 1 Kelvin. A pumped bath of liquid helium 3 can be used to cool
down to about 0.3 Kelvin
5. ADIABATIC DEMAGNETIZATION
REFRIGERATOR(ADR)
Calorimeters
Calorimeters are sensors which measure heat input. This ADR was
designed to cool calorimeters for the X-Ray Spectrometer (XRS) instrument.
These calorimeters measure the energy of x-ray photons by measuring the heat
energy deposited when the photons are absorbed. The instrument will be used
to measure x-rays coming from distant astronomical objects.
Heat Switch
The heat switch is used to allow heat to be dumped periodically to the
helium bath (not shown.) The main components are: external shell (the brown
cutaway part); getter chamber and connecting tube (off the left end); and the
interleaved copper end pieces (the yellowish, reddish pieces that almost
touch.)
Thermal Bus
The thermal busses (shown here in yellow) are copper rods that
connect the calorimeters (which need to be cooled) with the salt pill (where
the cooling action takes place.)
Salt Pill
The salt pill is where the cooling action takes place. The pill (actually
a cylinder) is made of ferric ammonium alum (FAA), also called ferric
ammonium sulfate. FAA was chosen to give good cooling power in the
temperature range where this ADR wil operate. (Other ADR's use other
materials.) When in use, the salt pill end of the ADR is slid into a
superconducting magnet. Changing the applied magnetic field causes the salt
pill to cool or heat. The horizontal lines running through the salt pill represent
the wires that provide good thermal contact from the salt pill material to the
heat switch and thermal busses.
Suspension
The outer structure of the ADR consists of metal rings and tubes,
which allow the ADR to fit securely within the superconducting magnet. (The
magnet is not shown in this drawing.) The salt pill is suspended within this
rigid outer structure by means of Kevlar cords. (Kevlar is a DuPont
trademark.) Kevlar is strong enough to hold the salt pill in place during the
stress of launch, but has low thermal conductivity so that not much heat leaks
into the salt pill through the suspension. The ends of the Kevlar lines are
attached to bolts (shown in blue.) By turning the bolts, technicians can tighten
or loosen the cords.
The ADR must warm up periodically to dump stored heat into the
"warm" end temperature sink. During the warm part of the cycle, the whole
ADR, including whatever sensors it may be cooling, is warm. One reason that
the XRS ADR can have such a long cold part of the cycle (over a day) is that
the "warm" heat sink is at a low temperature -- only 1.3 Kelvin. If the
temperature of the "warm" heat sink were raised, then the cold part of the
ADR's cycle would shrink, and the warm part would lengthen.
Schematic
magnetic shielding, to prevent the magnetic fields from interfering with other
equipment.
Working
The purpose of the cold end salt pill is to absorb this heat, so that the
astronomers' sensors can stay at their best operating temperature. To hold the
cold end temperature steady while the heat is flowing in, the ADR operators
must slowly reduce the magnetic field produced by the magnet at the cold end
pill. The operators must remove the stored energy from the cold end salt pill
before they ramp the magnetic field all the way down to zero. For that step,
they send the heat:
From the Cold End Salt Pill to the Middle Salt Pill
The middle salt pill is designed so that it can be cooled to a
temperature slightly colder than that of the cold end salt pill. That's just what
the operators do when they're ready to dump the heat from the cold end to
middle pill. (They cool the middle salt pill down by reducing the magnetic
field produced by the magnet that surrounds it.) Then they activate the heat
switch that connects the middle and cold end salt pills. This allows heat to
flow from the cold end pill to the (now slightly colder) middle pill.
As heat flows from the cold end salt pill, operators must increase the
magnetic field produced by the magnet that surrounds the cold end pill. If they
left the field constant, the temperature of the salt pill would drop as the heat
flowed out. When they have transferred as much heat, and ramped up the cold
end magnetic field, as much as they want, the operators stop ramping up the
magnetic field. They then turn the heat switch off, to block any flow of heat
back from the middle pill to the cold end pill.
The operators must also start slowly decreasing the field of the cold
end salt pill's magnet, to keep the temperature in the cold end pill constant.
From the Middle Salt Pill to the Hot End Salt Pill
Before they can transfer heat from the middle pill to the hot end pill,
operators must bring the middle pill up to the top of its temperature range and
bring the hot end pill to the bottom of its temperature range. They do this by
ramping up the magnetic field of the middle salt pill magnet and ramping
down the field of the hot end salt pill magnet. When the middle salt pill's
temperature is higher than the hot end pill's, operators turn on the heat switch
that connects the 2 pills. Heat now flows from the middle pill to the slightly
colder hot end pill.
When the heat has been transferred, the operators turn off the mid to hot end
heat switch.
All the time that the middle and hot end salt pills have been
transferring the heat out, the cold end salt pill has been absorbing heat,
preparing to start the cycle over again
ADVANTAGES
stage XRS ADR had such a low high-end temperature, 1.3 Kelvin, that the
only heat sink it could use was a bath of liquid helium -- a bath that evaporates
away as it cools.
Continuous Cooling
A single-stage ADR must shut down periodically to warm up and
dump its load of stored heat into the heat sink. In an Advanced ADR, the end
stage could be cooled periodically by a slightly colder stage. Thus, the end
stage of an Advanced ADR could provide continuous cooling.
Lower Weight
The Advanced ADR could be lower in weight than a long hold time
one-stage ADR. The salt pill of a long hold time one-stage ADR needs to be
large enough to absorb a large amount of heat energy. The salt pills of
a continuous ADR can be much smaller, since they can be cycled frequently
without interrupting the cooling.
XRS shows how liquid helium cooling and an ADR can work
together as part of a satellite cooling system. XRS is also interesting for
another reason. Because the volume of liquid helium was so small, the system
included some unusual design features. These features were intended to
lengthen the lifetime of the liquid helium coolant supply by reducing the need
for cooling.
All the really low temperature cooling systems have one thing in
common. Unlike the refrigerator in your kitchen, none of these systems will
work at room temperature. They all must be cooled to low temperatures in
order to produce the even lower temperatures that we are aiming for. The XRS
ADR was cooled by a tank of liquid helium at 1.3 Kelvin (1.3 degrees above
absolute zero. Surrounding the liquid helium tank was a tank of solid neon at
17 Kelvin (17 degrees above absolute zero.). At Goddard the helium tank, the
ADR, the x-ray sensors, were all built and all the equipment attached directly
to them.
You might imagine that measuring the temperature rise from a single
photon is fairly difficult, and you'd be right! Briefly, here is how it is done:
First, the X-rays must be focused onto the detectors. This is done with
a set of conical mirrors made of hundreds of layers of very thin foil.
The detectors need to be kept extremely cold (60 milli Kelvin). This
requires a complex cryogenic system, including liquid helium and
solid neon. It also requires the use of several filters to keep out stray
light, radio waves, and any other radiation other than X-rays.
The signals from the detectors are amplified and shaped by a package
of analog electronics and then processed digitally to determine the
energy of each photon.
In addition to the need to keep the heat capacity of the absorber to the
minimum, the XRS must operate at a low temperature to minimize the phonon
noise and maximize the sensitivity of the resistive thermometer. To achieve
the required energy resolution, with the required detector size implies that the
operating temperature must be below 0.1 K. For the XRS, there are four stages
of cooling.
The primary source of cooling is a 130 liter solid neon dewar. The
life of the neon is extended by the use of a mechanical cooler which cools the
outer radiation shield of the dewar. The solid neon maintains a temperature of
17 K, and surrounds a 32 liter tank filled with liquid helium. The liquid
helium is vented to space, and maintains a temperature of K. The final
stage of cooling is accomplished via the use of an adiabatic demagnetization
refrigerator (ADR). This allows operation down to 50 mK; for the XRS, the
nominal operating temperature will be 60 mK. Accurate temperature
regulation is crucial, as the detector response depends directly on its
lasting hour, can be done partially while the observed astrophysical target
is behind the Earth.
8. REFERENCES
1. www.nasa.gov.
2. “Cryogenics and Refrigeration” by Barrom.