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Original Article
a r t i c l e i n f o a b s t r a c t
Article history: The present work investigates the effect of material geometry in terms of material thickness
Received 25 May 2019 on the mechanical properties of glass fiber reinforced isophthalic polyesters. The tensile
Accepted 1 June 2019 strength, flexural strength, and Barcol hardness quantify the mechanical properties in this
Available online xxx article. The experimental tests as per the ASTM standards show that the tensile strength
and hardness increase with the increase in the thickness of laminates. The flexural strength
Keywords: is determined to decrease with the increasing thickness of laminates. The statistical anal-
Glass fiber ysis through ANOVA test shows that material thickness is a significant factor affecting the
Isophthalic polyesters mechanical properties with 83.88, 70.37, 97.63 and 62.19% contribution toward the vari-
Mechanical testing ance in the tensile strength, Young’s modulus, flexural strength, and hardness respectively
Microstructure characterization within the selected range of values for glass fiber reinforced isophthalic polyesters. The ten-
Tensile failure modes sile failure mode analysis indicates that the increase in the thickness of laminates increases
ANOVA delamination failure. It is also found that the anisotropic behavior of the composites leads
to an angular failure of the specimen in the tensile test. The random orientation of fibers
leading to anisotropic behavior and increasing voids/decreasing interfacial bonding with
the increasing laminate thickness is visualized in the microstructural studies through SEM
images.
© 2019 The Authors. Published by Elsevier B.V. This is an open access article under the
CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
Abbreviations: FRP, fiber reinforced polymer; GFRP, glass fiber reinforced polymer; SEM, scanning electron microscope; ANOVA, analysis
of variance.
∗
Corresponding author.
E-mail: ns.mohan@manipal.edu (N. Mohan).
https://doi.org/10.1016/j.jmrt.2019.06.003
2238-7854/© 2019 The Authors. Published by Elsevier B.V. This is an open access article under the CC BY-NC-ND license
(http://creativecommons.org/licenses/by-nc-nd/4.0/).
Please cite this article in press as: Bhat R, et al. Mechanical testing and microstructure characterization of glass fiber reinforced isophthalic
polyester composites. J Mater Res Technol. 2019. https://doi.org/10.1016/j.jmrt.2019.06.003
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1. 6 36 12
2. 8 48 16
3. 10 60 20
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Fig. 7 – Fractured specimen of 6 mm thickness after the of the specimen [19]. Table 7 also indicates that three out of
tensile test. five specimens had an angular type of failure instead of lateral
failure. The reason for the angular failure is the anisotropic
characteristic of the composites [20]. The orientation of the
fibers has a significant influence on the mechanical property
[21]. The anisotropic behavior is highly induced in the com-
posites having randomly oriented fibers [22] as is the case
of the composite specimens prepared for the current study.
Specimens 3 and 4 faced delamination type of failure, wherein
the damage primarily occurred due to the separation of layers
from each other [23]. The delamination failure is developed
generally due to excessive inter-laminar stresses generated at
the interfaced between adjacent piles. The delamination fail-
ure in the specimen during mechanical testing can also be
known as premature failure.
The same is evident from Table 3, wherein specimens 3 and
4 demonstrate a lower tensile strength compared to the other
three for the 6 mm thick laminate. Table 8 indicates that all the
specimens bearing 8 mm thickness demonstrate the angular
type of failure at the top end. As discussed earlier, the angular
failure indicates the anisotropic behavior due to randomly ori-
Fig. 8 – Fractured specimen of 8 mm thickness after the ented fibers, and the top end failure represents the formation
tensile test. of the main chap at the top location [19–21]. Also, it is observed
from Table 8 that the majority of specimens failed at the grip.
group is lesser than the variance between the group. Thick- The reason for this being the local damage caused resulting in
ness is proved to contribute 70.37% toward the variance in excessive stress concentration due to a high clamping force
Young’s modulus, corresponding to a high degree of correla- and the absence of tabs, the presence of which provides a
tion (83.88%). cushion effect to the applied grip force [24]. Table 9 indicates
that four out of five specimens bearing 10 mm thickness fails
3.2. Tensile failure mode analysis at the top, which is an indication of high-stress concentra-
tion resulting from the high clamping force and absence of
Figs. 7–9 represent the pictures of the fractured specimens of the tab [24]. It also indicates that the majority of failures are of
6, 8, and 10 mm thickness respectively after the tensile test. delamination type because of the combined effect of increased
From Fig. 7, it is evident that the mode of fracture varies in the thickness of laminates and the high clamping force at the grips
6 mm thick laminates. The variety of fracture modes observed [25,26].
in comparison to the standard codes as per the ASTM stan-
dards is given in Table 7 for 6 mm thick samples. Table 7 shows 3.3. Flexural test experimental and statistical results
that all the specimen fail at the top location. The reason being
the formation of the main chap causing the stress concentra- The results obtained for the conducted flexural strength test
tion at the top end portion. Though multiple chap formation is as per the ASTM D7264 standard is given in Table 10. The
the actual phenomenon, the formed main chap at the top por- results indicate that the thickness has a significant effect
tion inhibits the further development of chaps at other portion on the flexural strength in case of glass fiber reinforced
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polyester composites. J Mater Res Technol. 2019. https://doi.org/10.1016/j.jmrt.2019.06.003
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Table 7 – Mode of failures in 6 mm thick specimen as per the ASTM D3039 standards.
Specimen number (left to Mode of failure as per the First character (Failure type) Second character Third character
right in Fig. 6) ASTM standards (Failure area) (Failure location)
Table 8 – Mode of failures in 8 mm thick specimen as per the ASTM D3039 standards.
Specimen number (left to Mode of failure as per the First character (Failure type) Second character Third character
right in Fig. 6) ASTM standards (Failure area) (Failure location)
Table 9 – Mode of failures in 10 mm thick specimen as per the ASTM D3039 standards.
Specimen number (left to Mode of failure as per the First character (Failure type) Second character Third character
right in Fig. 6) ASTM standards (Failure area) (Failure location)
6 mm 8 mm 10 mm
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6 mm 8 mm 10 mm
Factor 2 103.79 51.896 9.87 0.003 Fig. 11 – SEM image for the 6 mm thick glass fiber
Error 12 63.10 5.259 reinforced polyester composites.
Total 14 166.90
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Availability of data
4. Conclusions
All the data are available with the authors and can be provided
In the present work, the contingency of mechanical prop- on request.
erty over the material thickness is investigated on the glass
fiber reinforced isophthalic polyester composite material. The
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