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Plant Design (CH3042)

Reference : Chemical Engineering Design


by Gavin Towler, Ray Sinnott
Evaluation


Assignments (I,II) : 30 Marks

Project : 40 Marks

Exam : 30 Marks
Introduction

For designing new/improved processes, knowledge of
the fundamental science alone is not sufficient (e.g.
thermodynamics, reaction kinetics, heat/mass transfer
etc.).

Economic, environmental, and ethical implications
– e.g. reaction rate may be high at elevated temperatures,
however, the cost of utilities may be high, the stresses on the
material increase, safety considerations may limit.
Design Process
Design Process

Set Design Basis :
– Precise statement of the problem, e.g. production rate and purity specifications
– Location of the plant site
– Conditions, Availability of raw materials, utilities etc

Design Concepts
– Rarely these are completely new. Mostly based on previous (established)
designs using well-understood equipment.
– Develop a process flowsheet containing the unit operations and type of
equipment
Fitness Testing

Multiple designs may exist. It is too costly to build
several designs.

Instead build mathematical models of the process
and use computer simulations to predict the
performance.

Data for the kinetics, thermodynamics is required.
Economic Evaluation

Many different designs may exist

Primary criterion for design selection is economic
performance, safety and environmental impact

Economic evaluation involves analyzing capital and operating
costs to determine return of investment (process economics),
e.g. heat exchangers

Several designs may have very close economic performance,
the safest or a standard design may be chosen.
Equipment Selection

After the flow sheet is made, detailed design is done

Detailed specifications of vessels, heat exchangers,
pumps and instruments are made

Mostly the focus is on equipment selection rather than
flowsheet modifications, e.g.
– choosing between different types of heat exchangers
– Using trays or packed columns in a distillation column etc
Design Constraints
Chemical Manufacturing Process
Continuous and Batch Processes

Batch Process :-
– Designed to operate intermittently
– Frequently shut down or in start up mode

Continuous Processes :-
– Operates 24/7, throughout the year
Continuous and Batch Processes

Batch processing
– allows production of multiple different products or different product grades in the
same equipment
– low capital for small production volumes
– scale of production is limited
– Usually used for small volume high value products

Food products

Pharma

Continuous processing
– Large production volumes
Optimization


Economic objective functions are sensitive to uncertainties in
prices for feeds, raw materials, energy etc.

Optimization under uncertainty
Optimization

External constrains : Often give rise to
inequality constraints

Optimization

Techniques
– Search Based methods, Newton method
– Linear Programming
– Convex Programming
– Non-linear programming
Optimization in Practice

Optimization of process operations : Planning,
scheduling, supply chain management
(LP,MILP)

Optimization of batch processes
Optimization in Practice

For many batch processes, the production rate
decreases during the production period. Hence, there
exists an optimum batch size for minimum production
cost.

For continuous processes, operation is limited by
gradual changes in process conditions, e.g. deactivation
of catalysts or fouling of heat exchangers. Simlilar to
above, there is an optimum cycle time.

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