Professional Documents
Culture Documents
Note: The source of the technical material in this volume is the Professional
Engineering Development Program (PEDP) of Engineering Services.
Warning: The material contained in this document was developed for Saudi
Aramco and is intended for the exclusive use of Saudi Aramco’s employees.
Any material contained in this document which is not already in the public
domain may not be copied, reproduced, sold, given, or disclosed to third
parties, or otherwise used in whole, or in part, without the written permission
of the Vice President, Engineering Services, Saudi Aramco.
Contents Pages
INTRODUCTION................................................................................................................ 1
REFERENCE......................................................................................................................49
APPENDICES.....................................................................................................................50
Appendix A Refractory Wall Thickness - Calculation Sheet ......................................50
Appendix B Refractory Heat Loss - Calculation Sheet ..............................................51
INTRODUCTION
Refractory and insulation systems are essential components in Saudi Aramco boilers and furnaces.
The primary purposes of refractory and insulation systems are to protect the steel structure and
tubes from overheating, and to reduce heat loss.
MEX 105.08 will introduce the participant to the types, components, installation procedures and
criteria used to select refractory and insulation materials for Saudi Aramco boilers and furnaces.
This module will also present the procedure for calculating the heat transfer through refractory
and insulation materials. This procedure is used in determining the required thickness of the
refractory and insulation materials.
Saudi Aramco requirements for furnace refractories are covered by Standard AES-F-001, which
includes API Standard 560. Requirements for boiler refractories are covered by Standard 32-
AMSS-021. There is no industry boiler standard covering refractories. These specifications
provide some basic requirements, but generally permit manufacturers' standard designs to be used.
Some of the requirements in these standards need explanation or additions, and these are
discussed below.
Service Temperature
The service temperature of a refractory material is the temperature at which the material begins to
deteriorate, and therefore operating temperatures should never approach this limit. Refractory
materials in each component layer should have a service temperature of at least 300°F greater than
the calculated hot face temperature of that layer. This applies to both the hot face and backup
layers. In the case of the backup layer, the hot temperature occurs where the backup layer meets
the hot face layer. The minimum service temperature of all refractory materials used in furnace
radiant and shield sections should be at least 1800°F (Standard 560, par. 7.1.3.). The minimum
service temperature of burner refractories should be at least 3000°F.
The design temperature of metallic anchors is considered to be the same as the calculated
refractory temperature at the tip of the anchor. The following guide can be used for selecting
metallic components:
Note (1): Austenitic materials shall be supplied and installed in the fully solution-annealed
condition. After annealing, anchors should not be bent except where the bend
point on the anchor will be below 1000°F.
Casing Temperature
Reduction of heat loss is a primary consideration in selection and design of refractory lining
systems. The lining system for furnaces should be designed to achieve a casing temperature of
180°F in 80°F ambient still air (Standard 560, par. 7.1.1.). This corresponds to a heat loss of 218
Btu/hr-ft2 of surface area. Although this ambient temperature is unrealistic for Saudi Aramco, it
is a standard basis for setting casing heat losses and determining lining thicknesses. This basis is
equivalent to a casing temperature of about 200°F in 100°F ambient still air.
Saudi Aramco AES-F-001 adds one requirement to this design basis: that the casing
temperature, where the casing is easily accessible by operating personnel, shall not exceed 150°F
in 100°F ambient air. This is for personnel protection. Since it is impractical to design a furnace
refractory wall to meet this requirement, other means of protection must be provided. One
solution used on the Ras Tanura 493-F-301/2/3/4 Rheniformer Furnace was to provide wire mesh
fencing several inches away from the hot casing, so that it could not easily be touched.
For boilers, the thickness of the external insulation should be designed to give a cold-faced
surface temperature of 150°F, with a surface wind velocity of 5 mph and an ambient temperature
of 115°F (32-AMSS-021, Par. 5.7.1). This corresponds to a heat loss of
140 Btu/hr-ft2.
Refractory and insulation materials are used in boilers and furnaces primarily for the following
purposes:
• To reduce heat loss through the boiler or furnace enclosure to the atmosphere.
• To protect portions of the tube surface from excessive heat transfer rates.
Refractory lining systems generally consist of high-temperature refractory materials that are
supported or reinforced by metallic components. Commonly used refractories are refractory
bricks, castable refractories, and ceramic fibers. In most high-temperature applications, it is
not practical to meet the heat loss requirements with a single-layer lining, so a dual-layer lining
system is used. A lower grade, better insulating material is used for the backup layer. These
refractory lining systems are discussed in this module.
Typical refractory components in process furnaces are shown in Figure 1 and are summarized
below. An internal refractory lining is used throughout the furnace to protect the enclosure and
structure, and to reduce heat losses.
Stack
Breeching
Header Box
Convection
Section
Sidewalls End Tube
Support
Arch
Dividing Wall
Radiant
Section
Floor
Burners Unshielded
Endwalls
Radiant Section:
• Walls and arches. The major lining systems used in furnaces consist of three types of
refractory linings:
• Floor. Brick and castable linings that are strong enough to withstand maintenance
turnaround traffic and scaffolding.
Convection Section:
• Endwalls. Single-layer castable refractory lining is used on the flue gas side of the end tube
supports.
• Header boxes. Single-layer castable refractory or ceramic fiber lining is used on the inside
surface.
Refractory Properties. The chart in Figure 2 presents the characteristics of typical refractories.
Lightweight insulating firebrick offers the low heat conductivity of efficient insulation plus the
ability to withstand direct exposure to furnace heat.
Four grades of heavy-duty brick including two special refractory compositions offer marked resistance
to spalling, exceptional load carrying capacity at high temperatures and negligible reheat shrinkage.
Insulating Castables
Castable series Kaolite Kaolite Kaolite Kaolite Kaolite Kaolite Kaolite
2200 2200-HS 2300-LI 2500-LI 2500-HS 2800 3300
(as cast) (as gunned) (as cast) (as gunned) (as cast)(as gunned) (as cast)(as gunned)
Recommended methods of application (X)
Cast or rammed X X X X X X X X X X X
Trowled X X X X X X X X X X -
Gunned X X X X X X X X X X -
Lb req'd to place one cu ft 56 71 82* 54 74 60* 78 85* 84 86* 68
**Required water, U.S. qt per bag
Vibrating 11.5-12 11.5-12 - 11.5-12 12-13 - 13.14 - 9.5-10 - 4-4.5
Casting and rodding 11.5-12 11.5-12 - 11.5-12 12-13 - 13-14 - 9.5-10 - 4.5-5
Recommended use limit, F 2200 2200 2200 2300 2500 2500 2500 2500 2800 2800 3300
Melting point, F 2670 2495 2495 2670 2740 2740 2700 2700 3300 3300 3530
Density, lb/cu ft Fired 58 74 82 58 67 60 77 84 85 88 68
Modulus of rupture, psi (ASTM C 268-70)
Dried 18 to 24 hr @ 220F 130 475 540 150 210 210 280 390 370 300 250
Fired 5 hr @1000F 120 200 - 140 130 100 220 370 290 190 240
@1500F 100 200 160 110 110 - 180 360 260 200 180
@2000F 150 200 - 190 130 100 140 310 350 250 180
@2200F 200 250 130 190 - - 240 430 400 270 300
@2300F - - - 240 - - - - - - -
@2400F - - - - - - 570 700 - - 350
@2500F - - - - 370 230 570 750 410 490 -
@2600F - - - - - - - - - -- 350
@2800F - - - - - - - - 1400 610 550
@3000F -- - - - - - - - - - 750
@3200F - - - - - - - - - - 850
Cold crushing strength, psi (Per ASTM C 133-72)
Dried 18 to 24 hr @ 220F 700 1600 1850 500 740 530 740 1240 1180 480 900
Fired 5 hr @1000F 600 1400 - 450 590 300 670 1150 950 550 850
@1500F 500 1200 950 450 610 - 600 1120 900 460 700
@2000F 550 1000 - 400 490 350 490 770 1070 860 700
@2200F 600 1250 1000 500 - - 440 1110 1390 1150 800
@2300F - - - 500 - - - - - - -
@2400F - - - - - - 990 1150 - - 1200
@2500F - - - - 950 680 1170 1210 2030 1480 -
@2600F - - - - - - - - - - 1300
@2800F - - - - - - - - 4150 1900 1400
@3000F - - - - - - - - - - 1500
@3200F - - - - - - - - - - 2200
Permanent linear change, % (ASTM C 269-70)
Dried 24 hr @ 220F -0.1 -0.1 - 0.0 - 0.0 0.0 0.0 0.0 0.0 -0.1
Fired 5 hr @1000F -0.2 - - -0.2 -0.2 -0.2 -0.3 -0.3 -0.1 -0.3 -0.1
@1500F -0.3 -0.2 -0.2 -0.4 -0.2 - -0.2 -0.3 -0.1 -0.2 -0.2
@2000F -0.5 - - -0.6 -0.2 -0.2 -0.3 -0.3 -0.4 -0.4 -0.1
@2200F -1.1 -0.7 -0.7 -0.9 - - -0.4 -0.4 -0.6 -0.5 -0.1
@2300F - - - -1.8 - - - - - - -
@2400F - - - - - - -0.5 -0.5 - - -0.1
@2500F - - - - -0.1 +1.0 +0.6 +0.6 +0.5 +0.5 -
@2600F - - - - - - - - - - +0.2
@2800F - - - - - - - - -0.5 -0.3 -0.2
@3000F - - - - - - - - - - -0.5
@3200F - - - - - - - - - - -1.0
Chemical analysis, % fired basis (ASTM C 573-70)
Alumina Al2O3 35 42 42 41 44 44 41 41 60 60 94
Silica SIO2 36 26 26 37 35 35 37 37 33 33 0.5
Ferric oxide Fe2O 5.6 6.9 6.9 0.9 0.9 0.9 3.2 3.2 0.4 0.4 0.2
Titanium oxide TiO2 1.2 1.0 1.0 1.7 1.8 1.8 2.2 2.2 0.7 0.7 -
Calcium oxide CaO 21.1 22.6 22.6 18.6 17 17 16.3 16.3 5.0 5.0 4.6
Magnesium oxide MgO 0.2 0.6 0.6 0.4 0.2 0.2 0.3 0.3 0.1 0.1 0.1
Alkalies, as Na2O 0.8 0.6 0.6 0.3 1.3 1.3 Trace Trace 0.8 0.8 0.5
Thermal conductivity, (ASTM C 417-60)
BTU•in./h•ft2•F 1.6 1.9 2.1 1.6 1.9 1.6 2.5 2.9 3.4 3.5 4.5
Pounds per bag 40 50 50 40 50 50 75 75 75 75 50
• Without rebound loss. **Water requirements indicated are offered as a guide. Actual water required may be subject to field conditions. Data are
average results of tests conducted under standard procedures with cast samples, except as otherwise noted ,and are subject to variation. Results
should not be used for specification purposes.
Typical refractory components in boilers are shown in Figure 3, which is an illustration of Ras
Tanura HP Boiler No. 8.
Castable Refractory
External
Insulation
Flue Gas
Burner Throat
Baffles
Castable
Refractory Castable
Refractory
Refractory
Floor Brick
Refractory
Brick
Because of the membrane water wall construction used in most boilers, very little internal
refractory is needed to protect the outer casing and structure. However, to reduce heat losses,
most of the boiler is covered with an external layer of insulation.
Castable refractory is used to seal the enclosure in areas where the tube arrangement does not
permit a membrane water wall. Castable refractory is also used in the boiler section for flue gas
baffles.
Refractory firebricks are used for removable sections of flue gas baffles.
A layer of refractory bricks, or comparable castable refractory, covers the floor tubes to reduce
heat transfer to these tubes.
High-temperature castable refractory is used to form the burner throats and to protect the
surrounding tubes.
Flue gas ducts and stacks are often covered with an external layer of insulation.
Brick Construction
Two types of refractory bricks are widely used in boilers and furnaces: refractory firebrick and
insulating firebrick. Commonly used firebricks of both types are composed mainly of alumina
(Al2O3) and silica (SiO2), most having a composition of about 45% alumina and 50% or more
silica. For special applications, particularly when very high service temperatures are required, the
alumina content can be increased to over 99%.
Refractory firebricks are used for hot face applications in boilers, furnaces, and combustors where
high strength and temperature resistance are of primary concern. Refractory firebricks also have a
generally high resistance to spalling. The physical characteristics of refractory firebrick are
dependent upon the refractory and binder components used, the forming method, and the
temperature at which the firing is done. These bricks have a high density (about 180 lb/ft3) and
service temperatures of 3000°F or higher.
Insulating firebrick is used in applications, such as furnace linings, where a high insulating value is
more important than strength. Insulating firebrick is a type of porous refractory brick material. It is
manufactured by firing mixtures of high-quality clay, sawdust, and other constituents. Density of
the bricks is about 30-50 lb/ft3, and service temperatures are 2000-3000°F.
Firebricks can be purchased in many standard sizes and shapes. The most common standard brick
size is 9 in. x 4-1/2 in. x 2-1/2 in. Mortar is used to bond the bricks together. Expansion joints
must be provided in all brick linings to allow for thermal expansion of the bricks.
This lining system consists of a wall of bricks at the inside hot face of the lining and a backup
layer of lightweight insulating block material next to the furnace casing. The IFB wall is usually
4-1/2 in. thick, although 9 in. thick walls are often used in very high-temperature furnaces. A
typical IFB wall is shown in Figure 4.
Although "brick and block" linings have been used successfully for many years, more recent
practice has been to use castable or ceramic fiber linings for process furnaces. These linings are
less costly than IFB walls and are more suitable for shop preassembly of furnace sections.
Backup Material
The backup material used in most IFB walls is a layer of mineral wool block insulation, typically
1-3 in. thick. Mineral wool is usually a low-melting-point glass material. Materials are available
with service temperatures of up to about 1900°F.
Because of its superior properties and competitive cost, some recent IFB systems have used a
backup layer of ceramic fiber material instead of the mineral wool. Ceramic fiber can withstand
higher temperatures than can mineral wool, so it offers a better safety factor should the IFB wall
develop cracks.
Support System
IFB walls are supported by shelf angles that are attached to the furnace structure. Due to the
thermal expansion of the wall, it is necessary to support the wall vertically about every 6-10 ft.
Horizontal expansion joints are provided at each shelf angle.
Vertical expansion joints are also provided about every 10 ft. The expansion joints are typically
packed with ceramic fiber material.
Tiebacks are used to stabilize the wall and hold it in place. Each tieback must be designed to
permit some horizontal and vertical movement of the brick wall caused by thermal expansion. In
vertical walls, not all bricks need to be tied back. A common practice is to tie back half the bricks
in every fourth row of bricks, which is 12.5% of the wall. Other tieback patterns are also used.
Standard 560 requires a minimum of 10% of the bricks to be tied back (Par. 7.2.1). Typical
tieback details are illustrated in Figure 5.
Casing
CS Pipe
Staple Type
Tieback
Block
Insulation
Shelf Angle
IFB
Elevation
Elevation
Plan View -
Staple-Type
Tieback
Plan View - V-Clip
Tieback
In some furnaces, sloping walls or flat IFB arches are provided. In these cases, all bricks must be
tied back.
In vertical cylindrical furnaces, the arch effect of the bricks acts to hold the vertical wall in place.
Tiebacks are not usually required, unless the furnace diameter is extremely large (over about 25 ft
in diameter).
Floor Refractory
The floor tubes in boilers are covered with a layer of refractory firebricks to reduce heat transfer
to these tubes. The floor insulation in furnaces is also covered with a layer of refractory firebricks
to provide for wear during maintenance turnarounds. The bricks in both applications are laid in
place dry, and are not mortared. Castable refractory of equivalent density and service
temperature is sometimes used in place of bricks.
Dividing Walls
Dividing walls are used between the radiant section zones of multi celled furnaces, such as the Ras
Tanura 493-F-3-1/2/3/4 Rheniformer Furnace. These are gravity walls constructed of high-duty
refractory firebrick. The maximum height of the wall is about 24 ft. The base width is
approximately 2 ft (2-1/2 to 3 bricks wide). The width decreases in 2-3 steps, so that the top few
feet is 9 in. wide (equivalent to 1 brick).
Vertical expansion joints are provided at the ends of the gravity wall. Intermediate expansion
joints are also provided, and these are usually lapped joints. Mortar is not used in lapped joints
(dry joints).
Sulfur Furnaces
High-duty refractory firebricks are used as the front layer in sulfur furnace refractory linings.
These layers are typically 9 in. thick. Castable insulation is used in the backup layer.
Thermal Expansion
Refractory firebricks experience thermal expansion when heated, and this must be considered in
the design of refractory lining systems. Expansion joints are required in all types of brick
construction.
For IFB walls, the size of the expansion joint should be approximately twice the thermal
expansion calculated, using the manufacturer's thermal expansion data, and based on the
refractory design temperature. The expansion joint is filled with ceramic fiber material.
For refractory brick used as the top layer of the floor in boilers and furnaces, the allowance for
thermal expansion should be about 3/32 in./ft (unless the manufacturer's data indicate that a
greater allowance should be used). Expansion joints should be covered with refractory bricks to
keep debris out.
In cases where expansion joints are provided in more than one layer of refractory, the joints
should be staggered so that there is no direct line of sight back to the casing.
Expansion joints should also be provided around burner blocks and tube supports.
Castable Refractory
Castables are concrete-like mixtures of "refractory" aggregates and cement that are formulated to
be mixed with water. The water allows the mixture to be formed into the desired shape and
structure. Most castables contain a hydraulic-setting calcium aluminate cement. A variety of
materials are used for the aggregate.
Several types of castable refractories are available. These are listed in Figure 6, according to
density. Strength, thermal conductivity, and service temperature generally increase with density.
Lightweight castables are used for their insulating properties. Heavyweight castables are used for
their high strength and high service temperature properties. Dense castables have properties
similar to those of refractory firebricks.
Notes:
(1) In the installed condition after drying at 220°F for 18 hours.
(2) As determined by standard test procedures.
(3) Certified by manufacturer.
Castable refractory lining systems consist of single- or dual-layer castable refractories held in
place by metallic anchors that are welded to the casing. Typical castable linings are shown in
Figure 7.
To avoid problems with field mixing, all castable materials (including "L-H-V") should be factory
premixed and packaged by the manufacturer.
It is also essential that refractory materials used in the field be properly stored. Exposure to any
amount of water will damage castable materials. These materials should be shipped and stored in
moisture proof containers. The storage area should be protected from the weather. Material
from broken bags, or any material showing signs of having been exposed to moisture (containing
lumps or hard throughout), should not be used.
Anchors
Castable linings are supported by the boiler or furnace casing, or shell, using metallic anchors.
Many anchor designs are used, with the most common consisting of "V" clips welded to the steel
casing. For dual-layer linings, separate anchors should be provided for each layer of castable.
Typical anchors are shown in Figure 8. Anchor patterns are shown in Figure 9.
Note (2)
Note (1)
Notes:
Installation
Castable refractory systems can be installed by either pouring or gunning. Gunning is a technique
that involves shooting the cement mixture into place with a pneumatic gun. The material that falls
to the ground is called rebound and is waste material. Gunning is a very economical method of
application. However, gunning is a skilled craft, and the techniques of the applicator can make
the difference between the success and failure of the installation.
Castable refractory linings can also be installed as panels. The castable is poured at grade, and
then the panel is lifted into place. The panels are bolted together, and the metal backing becomes
the furnace casing.
Almost all refractory problems are the result of irregularities in the installation process. The
quality of castable refractory applications is highly dependent upon the use of proper installation
and curing procedures. This is particularly important for gunned refractories. Experienced
refractory workers should be used for all castable refractory jobs. The water used in mixing
castables should be clean and potable.
Because of the possible variations in the quality of castable refractory installations, the installation
process should be carefully monitored with a series of tests and inspections.
• Before installation. Samples of each batch of castable should be tested to ensure that the
material properties meet the specifications and have not deteriorated during storage.
Compressive strength, density, and permanent linear change should be tested in accordance
with standard ASTM testing procedures.
For gunned linings, the skill of each operator should be determined by having the operator
gun a test panel of each refractory to be used. The panels should be tested for soundness,
using a hammer test, and for density.
• During installation. For each castable being applied, random samples should be taken during
each shift. These should be tested for strength, density and linear change to ensure that the
materials, as applied, have the required properties. Test panels should also be taken for each
operator to ensure proper operation of the equipment.
• After installation. A hammer test should be used to determine the soundness of refractory
linings. When defective areas in the lining are encountered, such as voids or dry-filled areas,
a dull sound will be heard. Any unsound areas should be cut out and replaced.
After the installation is completed, castable refractory linings must be cured and dried out before
they are ready for service. These steps should be carried out in accordance with the refractory
manufacturer's instructions.
• Curing is a process in which the calcium aluminate cement binder in the castable sets up, and
achieves a satisfactory strength. During this period of time, which is usually 24 hours,
moisture is required to complete the hydration reaction.
• After the curing step is completed, castable refractories must be dried out to remove any
free water remaining in the lining. This is accomplished by gradually heating the furnace or
boiler, over a period of 2 to 3 days, to near operating temperatures. If the lining is not
properly dried out, excessive quantities of steam can form inside the refractory, causing
sections of the lining to spall.
Thermal Expansion
Hydraulic-setting castable refractories can be used to form a monolithic structure without expansion
joints. This is made possible by the shrinkage that takes place in most castable refractories during
initial heating (dry-out). With few exceptions, shrinkage cracking is large enough to accommodate
thermal expansion that occurs upon subsequent heating of the material. However, expansion joints
should be provided around burner blocks and tube supports.
Other Applications
Single-layer castable linings are used in many places with moderate temperatures to protect the
steel structure and to limit heat losses. These applications include header boxes, flue gas ducts,
and stacks. The lining should be a mediumweight castable, at least 2 in. thick. A commonly used
material in this service is a 1:4 mixture of lumnite and haydite (L:H).
Thin single-layer linings are usually supported by chain link fencing or wire mesh that is anchored to
the steel casing. Carbon steel or stainless steel material is used, depending on the temperatures.
Ceramic Fiber
Ceramic fiber construction is the most recent development for furnace insulation systems.
Ceramic fiber is manufactured by a blowing or spinning process in which a molten alumina-silica
raw material is transformed into very small-diameter fibers. These ceramic fibers are then formed
into blankets, 1-2 in. thick, about 2 ft wide, and several ft long.
Ceramic fiber blankets are available in densities of 4-12 lb/ft3, and with 2000-2600°F service
temperatures. Using special materials, service temperatures can be increased to 3000°F. In
contrast with other refractory materials, thermal conductivity decreases with increasing density,
up to a density of about 16 lb/ft3.
Ceramic fiber is also available in the form of rope, cloth, paper, board, vacuum-formed shapes,
and bulk material.
A ceramic fiber lining system consists of several layers of blanket, with a higher-density layer
(typically 8 lb/ft3) on the hot face and lower-density layers (typically 4 lb/ft3) as backup. Mineral
wool block insulation is sometimes used for the layers closest to the casing. The lining is held in
place by metallic anchors that are welded to the casing. Typical ceramic fiber lining details are
shown in Figures 10 and 11.
Ceramic fiber blanket linings have advantages over conventional brick or castable lining systems:
Ceramic fiber blankets are subject to shrinkage in service, and this shrinkage must be provided for
in the lining system design. The hot face blanket layers should be constructed with overlapped
joints, as shown in Figure 10. The overlapped joints should be in the direction of gas flow.
Gas Flow
Alloy Stud and Washer
Lapped Joints
Stainless Steel Foil
Steel Shell Over Studs. Edges
Overlapped 8-12 in.
Seal Punctures with
Viscous Ceramic Ceramic Fiber Putty
Fiber Cement to Protect Stud End
and Washer (or Wrap
with Wet Blanket)
In the backup layers, butt joints can be used, with the blankets compressed at least 1 in. to allow
for shrinkage. Joints in successive layers should be staggered. This reduces the possibility of
direct heat flow back to the casing.
Corners/edges should be wrapped around to accommodate fiber shrinkage during service and to
ensure a continuous lining. Typical details are shown in Figure 11.
Joint
Joint
External Corners
Shell Shell
Coating
Cement
Burner Block
Burner Seams
Unprotected ceramic fiber blankets should be restricted to velocities of 40 ft/s across the surface.
At higher velocities, the blanket may shred. For velocities up to 100 ft/s, "rigidized" ceramic
fiber, ceramic fiberboard, or ceramic fiber modules may be used.
Ceramic fiber linings can be easily damaged, and are not suitable for use on floors or in any
location where mechanical abuse is likely. However, when damage occurs, the lining is easily
repairable.
Ceramic fiber lining systems have been in use for about 20 years. Improvements are constantly
being made, so experienced manufacturers should be consulted before developing the final
specifications for or approving a ceramic fiber system design.
Some concerns have been expressed recently about potential health hazards to lining installers,
from breathing in tiny ceramic fibers. Installers should be provided with protective equipment to
avoid this problem.
Anchors
Typical ceramic fiber anchors are shown in Figure 12. Anchors consist of the following
components:
• Intermediate retaining clips to hold the first blanket layers in place during installation,
particularly on overhead sections.
• An anchor at the hot face. These are usually metal washers that twist and lock in place.
These washers are covered with a wet blanket patch for protection against direct radiation,
as shown in Figure 7. Alternatively, ceramic retainer cups, filled with moldable ceramic, can
be used. Typical anchor patterns are shown in Figure 13.
38
25
67
Rapid-Fix
Washer
38
A 6x3 Section
Cup-Lock
For 24 in.
Wide
Blanket
Lap Joint for Hot
Face Layer
Thermal Expansion
External Insulation
Blanket insulation (at least 2 in. thick) and weatherproofing is used on external boiler surfaces
(including tube waterwalls, drums, and headers) to reduce heat losses.
External blanket insulation is also used on flue gas ducts. This can keep the inside steel
temperature above the flue gas dewpoint. Sometimes, external insulation is also used on steel
stacks.
Guidelines for selecting refractory lining systems are contained in Figure 14. These can be used
to select appropriate linings for various sections of process furnaces and comparable sections of
boilers.
Selection of refractory lining systems and materials for their components is highly dependent upon
the fuels to be used in the boiler or furnace. Serious corrosion and refractory degradation
problems can be caused by high levels of sulfur and metals in the fuel.
Hot Air and Hot Flue Gas Ducting Single- or multilayer lining or ceramic fiber
lining.
When fuels that contain sulfur are fired, most of the sulfur is converted to SO2, with a small
percentage converted to SO3. The SO3 combines with water vapor to form sulfuric acid, which
can attack some refractory materials. Below the water dewpoint (about 300°F), liquid sulfuric
acid is formed, which is highly corrosive to the metallic components in the lining system.
The type of lining system and materials chosen must reflect the quantity of sulfur in the fuel. The
chart in Figure 15 can be used to select refractory lining systems based on fuel sulfur content.
These systems and materials are discussed below.
Low-Sulfur Fuels
If the fuel contains less than 0.5 wt% sulfur, the potential for corrosion is small, and no special
materials considerations are required. Any combination of refractory lining materials should be
satisfactory.
High-Sulfur Fuels
If the fuel contains more than about 0.5 wt% sulfur, sufficient SO2/SO3 is produced that it can
easily penetrate any fiber structure. Provisions should be made in the design of refractory systems
to protect against potential casing corrosion and insulation damage.
• Block insulation should not be used in refractory lining systems where the hot face layer is
permeable (IFB, lightweight castable, ceramic fiber). This insulation can be severely
damaged by the acid condensate.
• Ceramic fiber materials have good resistance to sulfuric acid attack. However, fiber
insulation is easily permeated and offers no protection against casing corrosion. Stainless
steel foil can be used as a vapor barrier between layers of the ceramic fiber. This vapor
barrier should be located at a point in the lining where the temperature is above the
dewpoint. This is usually between the first and second layers of blanket from the casing.
• In lining systems that do not provide an effective barrier, a glass-filled polyester protective
coating should be applied to the inside casing surface.
• Castable refractory lining systems generally offer satisfactory service. Although castable
refractories are not completely impermeable, experience has shown that they offer good
protection against acid corrosion. Lightweight castable material can be used as a backup
layer in insulating firebrick and ceramic fiber lining systems.
• Insulating firebrick should contain less than 2.0 wt% CaO. This generally requires the IFB
to have a service temperature of 2600°F or greater. Sulfuric acid can react with the CaO,
causing refractory failure.
When the fuel fired contains significant quantities of metals (more than about 100 ppm vanadium
and sodium), the resulting metals in the fuel ash can cause some deterioration of the hot face
refractory. Higher concentrations of vanadium plus sodium (over 400 ppm) can severly attack the
refractory. In these cases, dense-type refractories should be provided for the hot face layer.
Since current Saudi Aramco fuels contain relatively low quantities of metals (vanadium and
sodium), these considerations do not apply to Saudi Aramco furnaces and boilers.
Design fuels for Saudi Aramco boilers and furnaces have various sulfur levels, which requires
using different types of refractory linings. For example, the following are the design fuels for two
Ras Tanura furnaces:
Design Fuels:
Waste Gas
H2S = 7.6-8.1 vol%
Heat transfer calculations are required for the design of refractory lining systems. The following
calculation procedures can be used to determine the rate of heat loss through the lining and the
resulting casing temperature, the required thicknesses of the component layers, and the design
temperatures of tiebacks and supports. These calculation procedures can also be used to
determine the adequacy of existing or proposed refractory linings.
Appendix A contains a calculation sheet for determining the required thickness for a refractory
lining. Appendix B contains a calculation sheet for determining the heat loss through a refractory
lining and the resulting casing temperature. These two appendices can be duplicated and used for
work assignments.
The following general equation for conductive heat transfer is used to calculate the heat flow
through the refractory lining:
Thermal Resistance
The thermal resistance of the refractory lining is the sum of the resistances of the individual
component layers:
R = r1 + r2 + ... (Eqn. 2)
t
r1 = 1 (Eqn. 3)
k1
where: r1 = Thermal resistance of first lining component, hr-ft2-°F/Btu.
t1 = Thickness of first lining component, in.
k1 = Thermal conductivity of first lining component, Btu-in./hr-ft2-°F.
This temperature is the most important factor in determining the design of the refractory lining.
Hot face operating temperatures should be realistic estimates of the actual temperatures
experienced in operation.
If not specified, the following can be used to estimate hot face operating temperatures in furnaces:
• Radiant section unshielded walls: use the temperature of the flue gas leaving the radiant
section (bridgewall temperature, Tbw).
• Radiant section shielded walls (walls located behind tube rows): average of Tbw and the
average radiant section tube metal temperature, + 100°F.
• Convection section walls: divide convection section into upper and lower sections. For
each section, use the entering flue gas temperature, less 200°F.
• Hot air and flue gas ducts: use the design air or flue gas temperature in the section of
ducting being considered.
The heat loss through the refractory lining is in equilibrium with the heat loss from the casing to
the atmosphere. Heat loss to the atmosphere can be determined from the following equations,
based on the temperature of the casing.
For standard design conditions (vertical wall, casing temperature of 180°F in 80°F ambient still
air), this corresponds to a heat loss of 218 Btu/hr-ft2 of surface area. For standard ambient air
conditions, Work Aid 2 can be used.
r
Ti = T1 - 1 T1 - T 2
R
Note that in these procedures, it has been assumed that the refractory lining consists of two
layers, as is the usual case. However, similar procedures can be used for any number of layers.
Thermal conductivities of refractory materials are temperature dependent, so that a trial and error
procedure is required in these heat transfer calculations. The thermal conductivities are first
estimated and then revised, based on the calculated refractory temperatures. Since the rate at
which thermal conductivities change with temperature is not great, repeated iterations are not
usually required.
For the first estimate of thermal conductivity, the interface temperature (Ti) between the two
layers can be estimated as follows:
Ti = T1 - X(T1 - T2) (Eqn. 8a)
This procedure can be used to determine the required wall thickness to meet specified conditions,
such as a heat loss rate, or a casing plate temperature. The sample problem in Figure 16
demonstrates this procedure.
1. For the specified conditions, determine the refractory hot face temperature. Calculate the heat
loss rate (or the corresponding casing plate temperature) using Eqns. 4-7.
2. Determine the thickness of the hot face layer. Unless otherwise specified, the following can
be assumed for standard furnace conditions:
3. Estimate the refractory interface temperature, using Eqn. 8a. Calculate the average temperature
of the component layers, and determine the thermal conductivity of each layer.
4. Calculate required thermal resistance (R), using Eqn. 1a. Then, using Eqns. 2-3, calculate the
required thickness of the cold face layer (rounded up to the next 1/2 in.).
6. Using the calculated interface temperature as the new estimated interface temperature,
recalculate the average temperatures of the refractory layers, thermal conductivities, heat
loss, etc.
7. Determine if the resulting temperatures and heat loss meet the specified requirements.
FIGURE 16
This procedure can be used to determine the heat loss rate through a refractory lining and the
resulting casing plate temperature. The sample problem in Figure 17 demonstrates this procedure.
1. Determine the refractory hot face temperature. Estimate the casing temperature. Calculate
the heat loss based on these conditions, using steps 3-6 above.
2 Locate the casing temperature/heat loss point on the chart in Work Aid 2.
3. Select another casing temperature, recalculate the heat loss, and plot a second point.
4. The actual heat loss should be located very close to the intersection of a line drawn between
these two points and the appropriate ambient air condition curve shown on Work Aid 2. If
the appropriate ambient air conditions are not shown, it may be necessary to develop a new
curve, using Eqns. 4-7.
With practice, it should be possible to locate the second casing temperature point very close
to the final solution point.
5. Determine if the resulting temperatures and heat loss meet the specified conditions. If not,
some revisions to the design may be required.
The following sample problem illustrates the procedure for calculating the heat loss through a
refractory wall. The data are found on the fired heater data sheet for Ras Tanura 015-F-100A
Atmospheric Furnace.
* This was estimated form the first trial. Any reasonable estimate can be used.
FIGURE 17 (CONT'D)
2000
1500
Temp at tip of Anchor:
500
0.5"
3" 7"
FIGURE 17 (CONT'D)
Using the hot face, cold face, and interface temperatures calculated above, the temperatures of the
tiebacks and supports can be calculated. The temperature profile through each refractory layer is
assumed to be linear. As stated earlier, the design temperatures of tiebacks and supports are
considered to be the same as the calculated refractory temperatures at the tip of the metallic
component. (The actual temperatures may be somewhat lower, due to the much higher thermal
conductivities and resulting heat flow through metallic components.) The diagram in Figure 17
illustrates the calculation of tieback temperatures.
Work Aid 1: Procedure for Calculating Heat Loss Through a Refractory Wall
This Work Aid is designed to assist the participant in The Calculating Heat Loss Exercise.
An engineer may have to calculate the heat loss through a refractory wall to determine the design
requirements for refractory materials, tiebacks, and supports. Since several of the terms are
dependent on each other, calculating heat loss is an iterative process consisting of making an
initial estimate and refining the estimate based on the calculations.
2. In the 1st Trial Column calculate the interface temperature, using the data provided.
3. Use the interface temperature, Ti, calculated in the 1st Trial and substitute it into the
formula at the top of the 2nd Trial column. Repeat the calculations in step 2.
4. Compare Ti in the two trials. They should be about the same. If they are not, repeat for a
3rd Trial.
5. Locate the casing temperature/heat loss point on the chart in Work Aid 2.
6. Select another casing temperature, recalculate the heat loss, and plot a second point.
7. The actual heat loss should be located very close to the intersection of a line drawn between
these two points and the appropriate ambient air condition curve shown on Work Aid 2. If
the appropriate ambient air conditions are not shown, it may be necessary to develop a new
curve, using Eqns. 4-7.
With practice, it should be possible to locate the second casing temperature point very close
to the final solution point.
8. Determine if the resulting temperatures and heat loss meet the specified conditions. If not,
some revisions to the design may be required.
Work Aid 2: Data Bases for Calculating Heat Loss--Heat Loss Versus Casing Temperature
This Work Aid is used in determining the corresponding Ambient Air Temperature in Exercise 1.
Work Aid 3: Data Bases for Calculating Heat Loss--Thermal Conductivities of Typical
Refractories
Mean Temperature, °F
GLOSSARY
REFERENCE
API Publications
ASTM Publications
Materials Specifications
APPENDICES
Appendix A Refractory Wall Thickness - Calculation Sheet
The following procedure can be used to calculate the required refractory wall thickness:
Plant Location Boiler/Furnace
Service Location
Hot Face Temperature, T1, °F = Ambient Temperature, Ta, °F =
Casing Temperature, T2, °F = Wind Velocity, V, m/h =
Corresponding Heat Loss Rate, q Btu/hr-ft2 =
Required Resistance
T1 - T 2 ______ - ______
R= =
q ______ hr - ft2 - °F/Btu =
Estimated Interface Temperature:
Ti = T1 - X(T1 - T2) = (_____) - (____) (____ - ____) °F =
Hot Face Layer:
Material =
Thickness, t1 in. =
1st Trial 2nd Trial
T + T2 ______ + ______
Avg. Hot Face Temp., Th = 1 =
2 2 °F =
Thermal Conductivity, k1 (Work Aid 2) 2
Btu-in./hr-ft - °F =
t
Thermal Resistance, r1 = 1 =
k1 hr - ft2 - °F/Btu =
Cold Face Layer:
Material =
Required Thermal Resistance:
r2 = R - r1 = (_______) - (______) hr-ft2 - °F/Btu =
T + T2 ______ + ______
Avg. Cold Face Temp., Tc = i =
2 2 °F =
Thermal Conductivity, k2 (Work Aid 2) Btu-in./hr-ft2 - °F =
Calculated Cold Face Thickness,
t2 = r2 k2 = (______) (______) in. =
Use Cold Face Thickness, t2: in. =
t
Thermal Resistance, r2 = 2 =
k2 hr-ft2 - °F/Btu =
Total Thermal Resistance, R = r1 + r2 hr - ft2 - °F/Btu =
Calculated Interface Temperature:
r _____
T i = T 1 - 1 T 1 - T 2 = _____ - _____ - _____
R _____ °F =
Calculated Heat Loss:
T1 - T2 ______ - ______
q= = Btu/hr-ft2 =
R ______
Corresponding Casing Temperature, T2 °F =
The following procedure can be used to calculate the heat loss through a refractory wall:
Ambient Temperature, Ta °F =
Wind Velocity, V m/h =
Calculated Hot Face Temperature, T1 °F =
Calculated Cold Face Temperature, T2 °F =
Hot Face Layer: Material, =
Thickness, t1 in. =
Cold Face Layer: Material, =
Thickness, t2 in. =
Final Conditions
Heat Loss, q: Btu/hr-ft2 =
Casing Temperature, T2 °F =